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DEFINITION OF COATING TYPES
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Wood thecnology
coating finishing guide .
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FINISHING SYSTEM GUIDE
3.cost analysis
4.Surface preparation
5.Method of application
7.Performance tests
9.Solvent Selection
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4.Surface preparation
Coatings performance is directly related to proper surface preparation.
Coating integrity and service life will be reduced if surfaces are improperly
prepared. As high as 80% or more of all coating adhesion failures can be
directly attributed to inadequate surface preparation.
This Surface Preparation Guide will help you in writing the coating
specification for your particular coating project by allowing you to copy and
paste the required information into your Coating Specification Template. You
can page through this guide in a linear fashion or link directly to the
following sections:
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7 8) surface smoothness, surface stability and resistance to cracking because
joints are eliminated.
Edge phenomena :
The porosity of edges and routed surfaces of MDF presents some unique
finishing problems with pigmented systems.Loss of adhesion, racking or peeling
of the finishing system may occur in the routed areas or edges. This failure is
more prone to occur with catalyzed finishes such as : Primer, Surfacer and
Pigmented Conversion Varnish, but may occur with other highly pigmented
systems. This phenomena occurs only in the routed areas and edges and does
not occur on the smooth MDF face.When the first coat of primer or primer
surfacer is applied to these porous routed areas, the resin tends to soak into the
wood leaving behind a very highly pigmented surfacer layer. The stress from
subsequent topcoats can cause adhesion loss and peeling in these areas over
time.
Reduce the sealer from 50 to 100% with lacquer thinner, depending on the
porosity of the MDF. This is a penetrating application rather than a build
coat. This treatment controls penetration of subsequent coats into the wood.
It functions much like a washcoat when used with a wood filler. If the
subsequent primers and topcoats are catalyzed, the Vinyl Sealers would be
catalyzed too.
,
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5.Method of application
The following are the most commonly used application methods in industry
today. If you have any questions about these methods, or others, contact
your local representative for help.
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5.1 Sample of :Two Component Spray:Good spray painting is accomplished by
means of proper procedures and motions.
Start to spray in exactly the same place each and every time.
Always lap the same distance
Always move the gun at the same rate of speed.
Keep the gun perpendicular to and at the same distance from the surface to
be sprayed at all times to 10 inch distance
The spray gun stroke is made by moving the gun parallel to the work and at a
right angle to the surface. The distance from the gun to the work should be
from six to ten inches for most coatings.
Overlap 50%
Work with straight uniform strokes moving the gun across the surface in
such that the spray pattern overlaps the previous stroke by 50%.
Too close -- The closer the gun is held to the work, the more paint is
deposited on the surface and the faster the gun must be moved to prevent
sags.
Too far -- Holding the gun too far from the work causes dry spray and
excessive spray dust.
The relation between gun distance and stroke speed is quickly understood
and the average operator will move the gun in or out as needed to permit a
comfortable speed while depositing a full coating of material.
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CAUSE Dried material in side port “A” restricts passage of air through
port on one side. Results in full pressure of air from clean side of
port in fan pattern in direction of clogged side.
REMEDY Dissolve material inside port with thinner. Do not use metal
devices to probe into air nozzle openings.
CAUSE Dried material around the outside of the fluid nozzle tip at
position “B” restricts the passage of atomizing air at one point
through the center ring opening of the air nozzle. This faulty
pattern can also be caused by loose air nozzle or a bent fluid
nozzle or needle tip.
REMEDY If dried material is causing the trouble remove air nozzle and wipe
off fluid tip using rag saturated with thinner.
Tighten air nozzle.
Replace fluid nozzle or needle if bent.
CAUSE A split spray pattern (heavy on each end of a fan pattern and
weak in the middle) is usually caused by:
2
has an unatomized “salt and pepper” effect indicates that the
atomizing air pressure is not sufficiently high or there is too
much material being fed to gun.
REMEDY Increase pressure from air supply.
Correct air pressures as discussed elsewhere
7.Performance tests:
7.1 pencil hardness test
The microtomic pencil scale hardness test has been established as a rapid
and dependable means of determining the film hardness of a given coating.
In using this system, pencils of the standard high-density graphite, drawing-
pencil type are used. These pencils come in various degrees of hardness,
following the scale given below, and are generally supplied by any leading
pencil manufacturer.
Softer 5B 4B 3B B HB F H 2H 3H 4H 5H Harder
Since hardness in this test is determined by the lead cutting into the paint
film, hardness as determined by this method is expressed as F Pencil, 2H
Pencil, etc.
HOW IT WORKS
1. Pencils for use in this test should not be sharpened in a pencil sharpener,
but should instead be sharpened by a knife so that the exposed lead has not
been marred or pared away.
2. The exposed lead is then sanded flat so that an equal cutting surface
is provided around the circumference of the lead.
3. The panel to be tested is placed flat on the table and the pencil is
held firmly in the hand and the same position as when writing
4. The pencil is moved forward on the film surface at an angle
approximately 45 degrees.
5. This procedure is followed with pencils of increasing hardness until
the first pencil which cuts into the film is found.
6. The hardness rating on the previous pencil is the rated hardness of
the film.
INTERPRETATION
Pencil Hardness is a measure of film hardness. The adhesion and flexibility
or mar resistance cannot be calibrated accurately from the use of the Pencil
Hardness test.
8.Solvent Selection
ALLPHATIC SOLVENT:
These thinners are used to reduce medium and long oil alkyd enamels such
as XXX and architectural/industrial maintenance alkyds. They are also used
as dilutents in lacquers and enamels but are not strong enough to be true
solvents in any resin quality other than alkyds. Aliphatic solvents are non-
photochemically reactive, HAPS compliant and non-polar.
Aromatic solvents :
are economical solvents that are widely used in alkyds, polyesters, acrylics,
vinyls, lacquers, epoxies either alone or in combination with other solvent
types. All aromatics are photochemically reactive.
Toluol (Toluene) XX1 is fast evaporating, strongest aromatic and not HAPS
compliant.
Alcohols :
are widely used as part of a solvent blend for lacquers and lacquer thinners.
Alcohols, especially Butyl Cellosolve and Butyl Carbitol are water miscible
and are used as cosolvents in water-based coatings. Cosolvents are critical
in maintaining solubility and stability as well as film formation of water-
based coatings. They are polar and non-photochemically reactive.Alcohols
must never be used with two-component polyurethanes because the OH
group of the alcohol reacts with the NCO group of the polyurethane and
neutralizes the chemical reaction. Alcohols include:
"
Methanol R6K1 is extremely fast evaporating. Poisonous. Primary use is for
dye stains. It is not HAPS compliant.
&
Ketone solvents offer very strong solvency to reduce viscosity rapidly and
to increase conductivity. Ketones are widely used in lacquers, alkyds,
polyurethanes, polyesters and epoxies and also as part of a solvent blend in
many other coating qualities.
Acetates are strong solvents used widely for nitrocellulose lacquers and
polyurethanes and in blended solvents. They range from fast evaporating
(Methyl Acetate) to extremely slow (Butyl Carbitol Acetate). Acetates are non-
photochemically reactive and HAPS compliant.
(
Never use lacquer thinners or solvents containing alcohols because it will
react with the catalyst and neutralize the reactive groups and change the
cure mechanism.
Never use any solvent that has been improperly stored or could have
absorbed moisture.
Xylene and other aromatics may be used to reduce conductivity.
Ketones are very efficient in reducing viscosity. MAK is often required for
the High Solids Polanes because of its high solvency and slow evaporation
rate.
MAK or cyclohexanone are often used as retarder solvents or as part of
solvent blends to optimize application properties
There are many volatile hazardous air pollutants (HAPS) listed in the
regulation, but the major solvents impacting the coatings industry are:
Toluene
Methanol
Xylene
Aromatic-Naphtha-100-Flash
Aromatic-Naphtha-150-Flash
Ethylene-Glycol
/
Butyl-Cellosolve®
MEK
Butyl-Carbitol®
MIBK
Butyl-Carbitol®Acetate
Isophorone-
At the present time it affects only wood finishing operations but is likely to
affect all market areas in the future. In the miscellaneous metal category,
HAPS regulations are anticipated in 2003. Title V operating permits, which
will be required for all major sources, does affect users that coat metal and
plastic. Contact your State Air Pollution Agency to determine the compliance
schedule for your area.The HAPS regulation for wood finishing is applicable
to all major sources - wood finishers with a potential to emit 10 tons per year
of a single HAP or 25 tons of combined HAPS based on 24 hours/day, 365
days/year production. For major source wood finishers, the regulation
requires less than 1.0 pound HAPS emission per pound of solids for existing
sources. For new sources, the requirement is less than 0.8 pound HAPS per
pound of solids. Currently application only to wood furniture
manufacturing operations.
The compliance date for largest users (>50 tons/year emissions based on
1996 emissions)was November 21. 1997. Compliance date for users emitting
10 to 50 ton/year was December 7, 1998.
The term is HAPS compliant, not HAPS free.
The regulations do not require HAPS free.
HAPS data for any product can be obtained through your Sherwin-Williams
representative.
The regulations also restrict manual conventional spray equipment.
Nearly all water reducible coatings contain HAPS - i.e., Butyl Cellosolve,
Butyl Carbitol, other glycol ethers or amine solubilizers - but generally these
coatings are still HAPS complying.
.
Many of our customers will not be affected by HAPS regulations because
they are small and emit less than the threshold level. Another exception
exists for small users who use no more than 250 gallons/month of coating,
gluing and cleaning, wash-off, dilutent and reducing solvents.
,
increasing
temperature.
)
separator of spray line. least once every
shift, or every
eight hours.
A.
8 BUBBLES APPEAR IN Excessive moisture A. Reduce moisture
OPEN GRAIN WHEN content. content to 6 to 8%.
APPLYING B. B. Utilize slower
SEALER/TOPCOAT
evaporating
solvent blend or
flow additive to
reduce surface
tension.
A.
11 COLOR DOES NOT Color system was not A. Check wet retain
MATCH STANDARD followed. for color as well as
1
B. verify approved
step panel color
standard.
B. Standard should
be same as
substrate.
C. Check sanding
procedure.
D. Check solvent
blend.
E. Check application
0
of stain as well as
method of flash-off
time.
F. Topcoat. Make
sure same product
is used for gloss
and clarity.
"2
B. Using slow drying resin sealer and topcoat
type stains. in catalyzed
C. Not using recommended system.
system and exceeding B. Use only
recommended film recommended
thickness. stains. Refer to
D. Stain or sealer not Product Data
completely flashed off. Page.
C. Refer to Product
Data Page.
D. Allow for longer
dry time. Check
oven temperature
and dwell time.
"
example, check
waterborne
systems for tannin
bleed as well as
acid-cured
systems. Avoid
self sealing – use
sealer.
A.
18 END GRAIN DARKER End grain more A. Wash coat before
WHEN STAINED absorbent than top grain. staining.
1
B. B. Use faster solvent
blend.
""
Data Page for
shelf life
information.
"&
recommendations.
F. Cool substrate
before stacking.
"(
necessary, to
diaphragm pump.
"/
coupling nut on cup lid tube and clean.
(suction feed). F. Thin material.
I. Fluid pipe not tightened G. Clean.
to pressure tank lid or H. Clean or replace.
pressure cup cover. I. Tighten; check for
defective threads.
".
film. weather
E. Roughness of substrate conditions, choose
or underline coat and a slower
variations in porosity. evaporating
F. Draft condition. solvent than
G. Temperature of material. originally
recommended.
C. Adjust spray
equipment.
D. Apply more
material to
surface.
E. May require a
primer surfacer
with filling
properties versus
a sealer.
F. Find reducing
solvent or blend to
provide proper
flow in a draft OR
eliminate the draft.
G. Material should be
applied at
temperature
recommended on
Product Data
Page.
",
soften packing
with a few drops of
light oil.
")
coalesce below
50º-60ºF. Film that
has not coalesced
properly will be
powdery or exhibit
very poor film
integrity.
E. Refer to Product
Data Page.
A.
43 ODOR (Latex Coatings) Bacteria growth. A. Keep lids tightly
1
B. sealed.
B. Avoid extreme
high temperature
changes.
C. To correct
problem, add
small amounts of
formaldehyde.
"0
I. Gun should be
worked 6 to 10
inches from
surface.
J. Mix material
thoroughly.
K. Eliminate
excessive drafts.
L. Raise humidity of
room.
&2
cloth before
application of the
next coat.
M. Moisture content
should be 6 to 8%
level.
A.
48 POOR/ INADEQUATE Excessive stain pigment A. A cleaner wipe.
ADHESION OVER DARK not penetrating. B. Multi-step system:
COLOR STAINS B.
1
dye stain, then
wipe stain.
&
stroke does not go redesign
beyond object.) equipment.
J. Gun held at wrong angle G. Remove cap and
to surface. fluid tip and clean
K. Fluid pressure too high. or replace, if
L. Operation too slow. necessary.
M. Improper atomization. H. Hold the gun 6 to
N. Reducer added too fast 10 inches from
without sufficient stirring. surface.
O. Natural oxidation of the I. Release trigger
material if allowed to after every stroke.
remain open to the air J. Work gun at right
over a period of time. angles to surface.
K. Reduce fluid
pressure.
L. Speed up
movement of gun
across surface.
M. Use larger air cap
(internal mix);
increase volume of
air through horns
(external mix).
Check line and
tank settings.
N. Add reducer
slowly, stirring
constantly.
O. Addition of proper
amounts of
solvent, plus
infusion of fresh
material will put
batch into con-
dition if oxidation
has not proceeded
too far.
2
52 SKINNING OF LIQUID A. While it is possible to A. Make sure that
minimize skinning, it is containers in
something which will which the material
occur to a varied degree is stored are air
whenever any air-drying tight. Dipping
material is exposed to tanks should
air. preferably have an
oil or water-sealer
NOTE: If the break is too cover, and cover
pronounced, it may not should be in place
be possible to put the whenever tank is
material back into not in use.
condition satisfactorily B. Cover remaining
for use. Prepare new contents of
batch for use. partially filled
container with
B. Oil-type materials. small amount of
appropriate
&"
C. Synthetic type. solvent before
D. Waterborne. sealing.
C. Cover remaining
contents of
partially filled
container with
small amount of
synthetic reducer
before sealing.
D. Float water and
appropriate co-
solvent blend.
Cover remaining
before sealing.
A.
55 SPOTTY DRYING Unclean surface. A. Clean carefully
1
B. with solvent.
B. Check sanding
procedures.
&&
HEAVY AT CENTER valve set too low. of air by opening
B. Atomizing pressure too spreader
low. adjustment valve.
C. Material of too great B. Increase pressure.
viscosity. C. Thin material with
D. Fluid pressure too high suitable thinner.
for air cap’s normal D. Reduce fluid
capacity, pressure feed. pressure.
E. Fluid tip too large for E. Use smaller fluid
material used. tip.
63 STREAKS A. Dirty air cap and fluid tip. A. Remove cap and
B. Not overlapping strokes fluid tip and clean
correctly or sufficiently. or replace, if
C. Gun moved too fast necessary.
across surface. B. Follow previous
D. Gun held at wrong angle stroke.
to surface. C. Take deliberate,
E. Gun held at wrong slow strokes.
distance from surface. D. Work gun at right
F. Air pressure too high. angles to surface.
&(
G. Split spray. E. Hold gun 6 to 10
H. Tipping gun. inches from
I. Streaks telegraphing surface.
through from primer coat F. Use least air
or under coat. pressure
J. Variation in porosity of necessary. Refer
substrate such as to Product Data
fiberboard or Page.
particleboard due to G. Reduce air
manufacturing process adjustment or
or uneven belt sanding. change air cap.
H. Spray pattern
should strike
surface at right
angles.
I. Make certain
primer coat or
underline coat is
properly, evenly
applied and
uniformly sanded.
J. May require
double filling of
primer application
to remedy
problem.
Substrate supplier
should be made
aware of the
problem. New
batch of substrate
may be required.
&/
moisture content
to 4-10% to avoid
telegraphing.
D. Use hot press
operation
wherever possible
but avoid
excessive drying.
Keep closed
assembly time to a
minimum.
E. Apply glues
uniformly and
avoid excess. Use
hot press
operation
whenever possible
but avoid
excessive drying.
F. Adjust depth of
sanding according
to the side of the
face veneer which
is exposed.
G. Condition and
maintain moisture
of the pressed
panel to 5-8%.
&.
pigmented finishes into
proper suspension
before application.
Failure to stir properly
unbalances formula of
applied material and
often will cause poor
drying.
E. Improper ventilation.
67 WHITE SPOTS A. Water mixing with the A. Clean air line and
lacquer either through separator. Be sure
the separator or by not surface to be
having the surface dry. finished is dry.
Bleed the line at
least once every
shift, or every
eight hours.
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<<
Carefully clean the surface of the wood, which is to be well dried (12-14%
humidity) and free from grease, wax or resin traces.
Waterborne products tend to raise the wood fibre and produce rough
surfaces.A thorough sanding is particularly important: 150 grit sanding is
recommended for softwood while 180 grit sanding is recommended for
hardwood.It is not advisable to use steel wool to prepare the bare timber
because this gives rise to the formation of bluish stains.
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.All stains can exhibit some degree of light sedimentation over time, which is usually
easy to re-disperse. During the winter there is a greater risk of sedimentation
because the solubility of pigments in water increases with temperature. The product
should therefore be stored, for the shortest time possible, in a warm place, preferably
at a temperature of no lower than 10°C. Stir well before use.
4 3
Once the can has been left open, the waterborne coating may decay as a result of the
attack by bacteria, moulds and fungi commonly present in the air. This phenomenon
is easily detectable because of bad smells, viscosity increase, moulds in the surface
and change of colour.
Avoid any attempt to recover used old product whose good preservation is not sure
as well as avoid to keep open the cans containing waterborne products during
summertime or in tropical areas.
The addition of "thor acticide hf+hd biocide (0.1-0.3%), increases preservation and
service life of products left in open containers such as dipping tanks
To clean items coated with waterborne products, considering their general poor
chemical resistance (ie. to alcohol, ammonia and abrasives), we suggest the use of
blends of neutral detergents with lukewarm water.
Sanding of the basecoat must be performed by means of 240-320 grit papers, paying
attention - especially when using orbital sander - not to apply too high pressure since
it may cause a significant temperature increase. This heating is detrimental to
waterborne coatings films since, being thermoplastic, they melt for excessive
heating.
The best results are achieved when using stearate sanding papers, which enable the
optimal sanding and provide much higher yields than conventional papers.
Automatic sanding must be performed with the machine perfectly calibrated and
working at low rotation speed of the belt and little pressure on roller/pad. Seek advice
from your abrasives supplier on the specific paper to be used with waterborne
coatings.
(&
6 4=
Drying of waterborne products must take place at temperatures not below 15°C and
at a relative humidity preferably not exceeding 80%. Out of these limits, there is a
slowing down of the drying and/or formation of a less hard and resistant film. It is
always advisable for drying to be forced, with air previously de-humidified and warm
(25-35°C).Use trolleys with well spaced holders enabling an optimal air circulation
also on panels surface, particularly when panels are of big size such as doors,
cabinet doors and side, etc.In case of drying with automatic equipment such as
simple or multi-stage ovens, provided with heating systems, always let the coated
items cool before stacking to avoid sticking marks.
4 3
Because of the hydrophilic nature of cellulose, waterbased products tend to raise the
wood grain thus resulting into a rough surface.A thorough sanding of the surface is
extremely important: the best results are achievable by sanding the substrate with
progressively finer papers up to 180-220 grit.
4 +
Veneers are to be glued very carefully and with waterproof glues, since waterborne
coatings tend to stress any gluing mistakes with the detachment and/or swelling of
the veneer, particularly in non-contact areas. B3/D3 class glues are suggested,
thanks to their good water resistance.Considering the wide variety of materials
existing on the market, a preliminary test is always recommended.
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G-450 :Is a one-pack clear waterborne self-priming topcoat for use on parquet
flooring, an application that requir es special characteristics of elasticity, hardness,
abrasion resistance, ease of application by roller and brush, and ease of touching-up
and maintenance.
On untreated surfaces fill any cracks using binder :FILLER B with the sawdust
obtained by wood floor smoothing. To this purpose, also FILLER A Tinned at 10%
with water can be used.
When the filler has dried, sand the floor carefully using 80-120 grit sandpaper.
Remove the sanding dust with a vacuum cleaner before applying the coating.
Apply the first coat of G450 thinned 10% with drinking water using a roller or a brush.
Make sure that the product is well spread and there are no areas of build-up.
After 3-4 hours, when drying is complete, the product is ready for sanding. It is
preferable to sand manually using 150-180 grit paper or with mechanical systems
using 220-240 grit paper. Then apply a second coat, followed by a third coat after 1-2
hours without sanding.
Some resinous timbers (such as iroko, merbau, etc.) contain colored substances that
tend to be dissolved by the product during application. To avoid this problem when
coating these timbers, apply the waterborne basecoat W28 as an initial barrier coat.
Do not allow the product to build up in any areas and make sure that it is spread
uniformly and with the recommended application weight of about 70-80 g/m² for each
coat. This can easily be achieved using normal brush application. Higher application
weights require much longer drying times.
For maintenance of parquet floors already coated with G450 or other types of clear
coating (including solvent-based coatings), sand well using 150 grit sandpaper, clean
the substrate, then apply one or two coats of G450 as described above. Make sure
that the surfaces are free of grease and/or synthetic wax.
Spray application of G450is not recommended. Actually, with this application method
it is easy to exceed in quantity with the consequent possibility of several
inconveniences such as detachment of the coating film from the wood substrate.
Accidental application of thick layers of product may cause spots and cissing and
slow down drying to such an extent that the film lifts from the wood.
Keep from freezing: store in areas where temperatures do not fall below 5°C.
During application and drying, the ambient temperature and the temperature of the
coating must be no lower than 10°C.
Use only drinking water for thinning.
Mix the product using a stick or a spatula. Avoid stirring too vigorously not to
incorporate air in the product which may lead to the formation of bubbles during
application.
Ventilate the room during and after application to improve drying.
The coated floor is ready for foot traffic the next day.
After application wait 48-72 hours before placing furniture or carpets on the floor.
For the first 2-3 weeks the coating is not perfectly dry and remains slightly sensitive
to water. If the floor is washed and/or water deposits in some areas after treatment,
this may give rise to reversible blooming on the film of coating.
Wash working tools immediately with water. Dried coating can be removed by
washing with acetone.
Coating residues must be disposed of in accordance with current legislation. Do not
pour residues down drains.
Due to the great number of exotic timbers available on the market, it is advisable to
perform a preliminary test to verify that the product does not undergo cissing,
blushing or lifting caused by substances contained in the wood.
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When drying of CW3 complete, all normal sanding systems, both manual and
automatic, can be used, paying attention not to exert excessive pressure as this
could lead to a considerable increase in temperature. This temperature increase,
which is particularly evident in case of use of scotch brite or belt sanders would be
detrimental to the film of waterborne coating as it is thermoplastic and liable to melt
on heating.
For best results, use stearate sandpaper, which provide excellent dedusting with
much higher efficiency than conventional sandpaper.
Consult your abrasives supplier for information on specific papers for waterborne
products.
Store the product in rooms where the temperature does not fall below 5°C.
During application, keep the product, the substrate and the room at a temperature of
at least 15°C.
Coating residues (washing water, booth water, used coating) must be disposed of in
accordance with current legislation. Do not pour residues down drains.
In view of the wide variety of materials used for manufacturing wooden products,
when switching from a solvent-based to a waterborne coating system it is always
advisable to contact your suppliers’ technical departments to check whether your
equipment and components are appropriate or whether more suitable types exist. In
particular, check: electrostatic guns, pumps, seals, silicones, glues, booth treatment
water products, packaging materials, fillers, sandpaper, etc.
(.
10 Basic Finishing Rules for Avoiding Common Wood Finishing Problems
1. Make sure all finishing personnel are familiar with application of the products.
Refer to Product Data Pages as well as consult with Sherwin-Williams
Sales/Service Representative for proper handling.
2. Have complete system pre-tested and documented detailing each
operation from white wood sanding to final inspection. Follow written
procedures daily.
3. Inspect all application equipment on a daily basis – ensure it is clean and
in working order.
4. The curing schedule should be routinely monitored. Oven temperatures
as well as plant environmental conditions should be noted. Variations
may require solvent additions. Refer to Product Data Pages.
5. Always thoroughly mix materials before application.
6. Reduce finishing materials in accordance with Sherwin-Williams Product
Data Page.
7. Use good housekeeping measures – a clean finishing area produces
clean work, reduces loss time caused by rejects, accidents, fire, etc.
8. Check stock rotation. Note batch date (Julian calendar) and rex number
when material is received. Use oldest date first.
9. Finish standards should be utilized at each finishing operation to ensure
consistent quality and color.
10. In refilling leftover material, strain into clean containers, fill containers to
the top, and close tightly so that there will be no air leakage into the
package. Label and date. Refer to Product Data Page for proper handling
of catalyzed materials.
(,
Facts in Formulating Water Based Industrial Wood Coatings
The practice of formulating water based industrial wood coatings is different
to that of
formulating industrial wood coatings using solvents as the thinner.
Different,but not difficult.
As with many changes in technology,a certain period of time is needed to
obtain the
necessary experience to properly formulate and apply high quality coatings
based on water.
When using solvent based systems the solvents are used to dissolve
binders and to adjust the
final application viscosity of the paint.With water borne technology,in
general acrylic emulsion
and/or polyurethane dispersions,we prefer to consider water as the carrier of
the binder since
it is not used to dissolve the polymer particles.Water is furthermore used to
adjust the final
viscosity.
A wide variety of other polymer types may be used in industrial wood
coatings.They can range
from the extremes of water insoluble polymers to the highly soluble together
as well as the
many types of intermediate developments such as alkali soluble
emulsions,micro gels,water
reducible polymers,etc.
Commonly used water based technology can be listed as follows:
-Acrylic (co)-polymer emulsions
-Polyurethane dispersions
-Urethane-acrylic hybrids (blends)
-Urethane-acrylic co-polymer dispersions
-Alkali soluble acrylic emulsions
-Modified urethane dispersions
-Modified urethane-acrylic co-polymer dispersions
To enable the coating formulator to make the right choice out of the
impressive range of water
based binders available,he/she needs to know some details of polymer
technology.
Emulsion Polymerisation.
Of the range of procedures available for the production of polymers in the
presence of water:-
-Emulsion polymerisation
-Aqueous solution polymerisation
-Dispersion polymerisation
-Polymerisation in mini-emulsions
-Mi-cellar polymerisation
emulsion polymerisation is the most commonly used technique.
()
Emulsion polymerisation is characterized by the fact that a water-soluble
free radical initiator is
used to polymerise the radically polymerisable monomers to produce a
water insoluble
polymer.It is common practice to also incorporate some water-soluble acid
co-monomers.
This method of polymerisation offers the advantage of high polymerisation
rate and high
molecular weight.The viscosity of the emulsion is however not molecular
weight dependent.
The particle size of these emulsions can range from 50-500 nm,the stability
of the emulsion is
obtained through the use of surfactants in conjunction with the effect of
charged polymer end-groups:
sulphate groups from per-sulphate initiators and ionic groups from the use
of ionic co-monomer,
e.g.carboxylate groups from acrylic acid.
EMULSION POLYMERISATION
Reaction system
•water
•monomers
•emulsifiers
•initiator
•(modifier)
•(salts)
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Triethanolamine (TEA)is the ideal amine for neutralisation since it will not
react with
isocyanate.A disadvantage of TEA is its high evaporation rate and toxicity at
low
concentration.N,N-dimethylethanolamine (DMEA)is an alternative
neutralising agent but is,
however,reactive with isocyanate.
C Dispersion
The dispersion process depends on the pre-polymer viscosity and the
presence of acid.
Sometimes small quantities of an emulsifying agent or a temperature
increase of the water are
used to improve the dispersion process.
D Extension
During the extension step,for which hydrazine or ethylenediamine (EDA)are
well known
agents,the molecular weight increases from 1,000-10,000 to over 100,000.In
comparison to
solvent-based urethanes the higher molecular weight of polyurethane
dispersions is an
advantage towards solvent resistance.
Of importance for the physical behaviour of a polyurethane dispersion is the:
-Type of isocyanate
-Type of diol or polyol
-Presence of co-solvents as NMP
-Hardness and flexibility
-Presence of cross-linking
A comparison of the advantages of the use of acrylic emulsions and
polyurethane dispersions
is summarised in the table below:
Formulating
Formulating in the right way depends on a range of important matters:
Which type of wood has to be coated,what is the final use of the coated
wood,is the shape
flat or 3-dimensional,what is the method of application,what is the allowed
total film weight,
what are the curing conditions,is cross linking allowed,is the material
stacked after cure,etc?
What is the coating type?
-Stain
-Sealer
-Sand able primer
-Top coat
-One-coat system
/2
What is the application method?
-Conventional air spray
-Airless spray
-Air mix spray
-Electrostatic spray
-Roller coating application
-Curtain coating application
-Vacuum application
-Dipping
Application lines often differ from factory to factory.Line dimensions
and speeds are different and the same is noticed for drying
conditions.
When exporting formulations,the formulator must have an eye for the
specific safety and environmental rules in the country where the
coating is finally applied.Regulations can differ from country to
country or even within a country.This will restrict the formulator in the
choice : of e.g.film forming agents or cross linkers.
Last but not least there is the consideration towards the coating
quality:
Coating quality demands can differ per:
-Style of finishing (open/closed pore)
-Circumstances of final use
-Specific film quality demands:DIN 68 861/Moebelfakta/Fira,etc
-Economics
All in all:many questions arise when the coating chemist is asked to
present the right formulation.It is of vital importance to supply the
paint chemist with all the necessary information on
substrate,application method,quality demands and on maximum
allowed price.
Good communications between sales staff,client and coating chemist
is important.
1.Emulsion (45%)75,0
2.Water,demineralised 8,0
3.Coalescent premix,pH 8 6,0
4.Surface wetting agent 0,3
5.Anti foam agent 0,7
6.Flatting agent 2,0
7.Wax emulsion 6,0
8.Thickening agent 2,0
TOTAL: 100,0
/
In this clear coating formulation example,the binder content is 75 %of the
total weight by volume.The binder plays an utmost important role in the
performance of the film during and after application.
Film quality and price are dominated by the choice of binder.
With respect to the other ingredients of this,and other,coating formulations
many are added to either compensate for a weakness in the quality of the
binder or they are added to obtain a certain performance change,such as
viscosity or gloss level.
Water is not renowned for having the best wetting properties on many
substrates.Its surface tension,of approximately 72 mN/m,needs to be
reduced to obtain good surface wetting and even flowing films on the
substrate.
The surface tension of acrylic emulsions,supplied in water,is lower because
the surface tension of the water present is reduced through the use of
emulsifier.
The use of wetting and anti-foam agents,which all influence surface tension
and can affect foam stabilization and film defects,such as cratering,should
preferably be kept to a minimum.
wide choice of additives such as:anti-foam agents,wetting agents,film
forming agents, thickeners,waxes and matting agents.
1:Gloss reduction
The selection of the right matting agent normally means the formulator
having to choose from
what the coating factory stocks.
Often one has to make a selection out of the available raw material or
additive list.
In many cases this results in making compromises.Many matting
agents,offered by various
suppliers in Europe,are available but only a few are normally in stock.For our
comparison
tests we have chosen from standard universally used types.Yet differences
can still be found
with respect to:
-The matting effect
-Alcohol resistance
-Water resistance
-Compatibility with the binder system
-Film appearance
-Detergent resistance
-Touch
-Glossing-up at scratching the surface
"
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1.Gloss reducing Polyurethane dispersions:
2.Scratch resistance
Again a selection has been made out of a range of well-known and
commonly used wax dispersions and water dispersible powder waxes.
In general water dispersible powder waxes have more influence on the final
gloss level of the applied coating.
The particle size and the form of the wax particles floating to the top of the
liquid coating surface causes light scattering,which reduces gloss.In this
case the quantity of matting agent has to be adjusted to the correct level.
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3:Wetting
Van der Waals forces and high polarity,as described by many of my
colleagues serving the additive industry,force water to form a droplet.Strong
polar liquids have a high surface tension,non-polar liquids do not have the
desire to form a droplet.Water,as an important component of emulsions and
dispersions,therefore has an influence on the performance of the liquid
coating and can be the cause of serious headaches to the
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A selection of wetting agents added to a standard test
formulation based on binder(above)gave the following results:
Test result 2 :
Wetting agents
A B C D E F G
Binder 100 100 100 100 100 100 100
Demi water 11 11 11 11 11 11 11
Wetting agent 0.45 0.45 0.45 0.45 0.45 0.45 0.45
DPM 2.7 2.7 2.7 2.7 2.7 2.7 2.7
DPnB 2.7 2.7 2.7 2.7 2.7 2.7 2.7
NMP 2.3 2.3 2.3 2.3 2.3 2.3 2.3
Demi water 0.4 0.4 0.4 0.4 0.4 0.4 0.4
Byk 024 1 1 1 1 1 1 1
PH 7.8 7.8 7.8 7.8 7.8 7.8 7.8
Gloss (20°/60° ) 64/87 64/87 64/87 65/86 76/89 65/86 65/86
König hardness (sec.)147 164 188 168 130 148 174
viscosity Din#4 (sec.) 15 14 16 14 15 15 15
Film appearance ok ok ok ok ok ok not ok
Stain resistance Leneta 2C
Demi water 16 h 5 4-5 4-5 5 4-5 5 4-5
Ethanol (48%)16 h 3 3 3 3 3-4 3 3-4
Detergent 16 h 4-5 4-5 4-5 4-5 4 4 4
Coffee 16 h 5 5 5 5 5 5 4-5
Hot pan 1 h 4-5 5 4-5 5 4 5 4-5
Ethanol (48%)1 h 3-4 3-4 3-4 3-4 4 3-4 4
Remarks: not
compatible
_____________________________________________________________________
//
4:Anti Foam Agents
A wide variety of anti-foam agents are now available for water borne systems
from many ,sources.This is a far cry from the early days of the introduction
period of water borne systems ,when binder suppliers often had to develop
their own range of anti-foam agents.
tego family
byk family
The presence of foam in the coating can be caused by different ways:
-Air entrapment during the production process.
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5:Viscosity Adjustment:
In general,water based industrial wood coatings need a viscosity adjustment
when finalizing,the paint formulation.The final viscosity adjustment of the
lacquer takes place after a certain ,period of aging,preferably at least 15
hours.This is necessary due to the influence of the film-forming
agent on the swelling of the polymer particle.
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6:Film forming
Good film formation is an absolute requirement when we expect the final
dried paint film to ,have the required resistance properties.Proper film
formation will give the right performance .towards solvent,chemical and
water resistance.Although not directly detectable by the human
eye,or even by using a microscope,the poorly coalesced coating may have
voids or micro,pores that will enable fluids to attack the substrate or to
weaken the coating film.Spot tests on the cured film,preferably applied on an
absorbing substrate,will indicate the ,optimum level of solvent addition to
obtain maximum film build.Selection of the film-forming agent will depend
upon the allowed solvent technology (regulation depending)and the required
speed of drying.Normally a range of several glycol ethers are used or,when
allowed,a combination of fast and slower evaporating glycols.
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7:The Binder
Careful choice of the right water borne binder system is of high importance
to the paint,formulator.During the last 10 years they have seen many water
based technologies added to the list of water borne binders to choose
from.All binder types have their own specific advantages.
We can now choose a product that will fit into the range of demands set by
the final ,application.
-Self cross-linking acrylic emulsions will stepwise improve the resistance to
water,chemicals and solvents.
-The use of Surfactant free self cross-linking emulsion chemistry will
decrease,foaming during production and will increase wood
wetting,transparency and flow.
-Urethane-Acrylic co-polymers will offer increased resistance to chemicals
and solvents,hand cream resistance and abrasion resistance.UA copolymers
are often used to formulate one component coatings used for tabletops or
office furniture,where resistance demands are very high.
-Hydroxyl acrylic emulsions are used to formulate coatings that cure with
melamine or urea formaldehyde and some acid,or by means of isocyanate
addition.They provide highly resistant coatings used for wood imitation
paper and for kitchen and office furniture.
-Fatty acid modified polyurethane dispersions and Fatty acid modified
Urethane-Acrylic dispersions are needed when demands with respect to
wood wetting,filling and transparency are strong.Fatty acid modification
furthermore features high resistance to solvents and chemicals.
-Water based UV curing dispersion chemistry will provide a high resistance
level and immediate block resistance after cure.
-Alkali soluble acrylic emulsions containing sufficient carboxylic acid are
soluble in amine or ammonia and provide solutions with high pigment
wetting power and,due to the rheology,the required coating transfer
properties.Colloidal acrylic emulsions are used for highly filled primers
and,because of their small particle size,for impregnating
agents and stains.
/,
Wood &Grain Raising:
-Wood Type
-Co solvent use,type and quantity
-pH level
-Solids content
-Coating thickness
-Surface tension
-Solubility of the polymer
-Emulsifier type used for polymerisation (cationic/anionic)
-Tg,MFT
-Drying speed and method
-Surface preparation
-Particle size
-Viscosity
-Application method
On study on grain raising clearly showed that the choice of wood type had a
major effect on the grain raising seen.The grain raising of oak pine, beech
etc,are not equal.There are no known standard test surfaces nor special
laboratory equipment that can be used to quantify grain raising.The wood
quality and type of grain raising differs too much in wood panels to make
use of equipment which measures the roughness of the coated wood by
means of,for example,a laser technique/digital surf,interferometry or
con-vocal microscopy.The composition of wood is simply not consistent
enough and can differ across the surface of the sample.
Therefore a subjective method,based upon the views of a panel of 5
technicians,was used to judge the roughness of the tested wood types.
The following table indicates our conclusions:
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Classification of the different factors
influencing the Grain Raising
Nature of
polymer/pH* Latex 3 Application Spray 1
method gun
Hydrophobicity high 3
pH Low 4
/high
Low 3
Cationic/anionic /high
Wood depends -
Conclusion:
/0
WOOD COATING
DEFINITION OF COATING TYPES
CLEAR TOPCOAT: A final coating which contains binders, but not opaque
pigments, and is specifically formulated to form a transparent or translucent
solid protective film.
INK: A fluid that contains dyes and/or colorants and is used to make
markings, but not to protect surfaces.
SEALER: A coating, containing binders, which seals the wood prior to the
application of subsequent coatings.
STRIPPER: A liquid used to remove cured coatings, cured inks, and/or cured
adhesives.
TONER: A wash coat which contains binders and dyes or pigments to add
tint to a coated surface.
.2
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