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The strength of the gel formed is a function of the amount and type of solids in suspension, time, temperature and chemical
treatment.
So measuring the strength of gel structure over a period of time (10 sec/10 min/30 min) will give readings that are near in values.
Progressive gels
When there is a wide range (difference) between the initial (10 sec) and 10- or 30-min gel readings it is called progressive gels,
and is an indication of solids buildup. If the initial and 10-min gel readings are both high with little difference between the two, it
is called flash gels and may indicate that flocculation has occurred (in muds with clays added or drilled).
Depending on the mud type used progressive gels can be caused by solids build up in the system or contamination from calcium
source, salt or carbonate and bicarbonate.
N.B: Some fluid systems like FLO PRO are operated in the flash gels range for hole cleaning in deviated and horizontal drilling, in
this case the polymer network breaks easily applying shear so you have to differentiate based on mud system used.
ECD (EQUIVALENT CIRCULATING DENSITY): The pressure on a formation while circulating is equal to the total
annular circulating pressure losses from the point of measurement to the bell nipple, plus the hydrostatic pressure of
the mud. This force is expressed as the density of mud that would exert a hydrostatic pressure equivalent to this
pressure.
ECD (lb/gal) = ρ (lb/gal) + Pa (psi)
0.052 x TVD (ft)
Relation between ECD and flow rate: ECD is directly proportional to annular pressure loss. And annular pressure loss is directly
proportional to square of annular velocity which also increases by increasing flow rate as per the below equations, when flow
rate increases, annular velocity and annular pressure loss increase and ECD increase.
Relation between ECD & PV: Plastic viscosity is described as that part of resistance to flow caused by mechanical friction.
Primarily, it is affected by:
Solids concentration.
Size and shape of solids.
Viscosity of the fluid phase.
The presence of some long chain polymers (POLY-PLUS)
The Oil-to-Water (O/W)
Pv as a physical property by itself only will not affect the ECD as seen in the above equations, Pv does not have a direct relation to
ECD in the equation.
Pv will reflect an increased pressure loss especially inside the drill string as if the Pv increased, this means that the 600 rpm reading
increased (it will increase the friction coefficient inside string and the eventually the pressure loss).
However an increase in plastic viscosity can mean an increase in the percent by volume of solids, a reduction in the size of the
solid particles leading to increased surface area of cuttings which will be reflected in increased plastic viscosity, if not controlled it
will eventually cause undesired overall viscosity of the mud system and result in significant changes in pump pressure in the field
this is very obvious in the ERD wells.
In the above figure in the rheograph it is clear that the extrapolation of the 600 and 300 rpm reading to the y axis is giving higher
values than the LSYP.
40
Micron
30
20
10
0
d10 d25 d50 d75 d90
120
Volume % Less Than
100
80
Volume (%)
60
40
4.2 SG
20 4.1 SG
0
1 10 100 1000
Patricle Diameter (μm)
The net negative charge is compensated by the adsorption of cations (positive ions) on the
unit layer surfaces. The cations that are adsorbed on the unit-layer surfaces may be
exchanged for other cations and are called the exchangeable cations of the clay.
The quantity of cations per unit weight of the clay is measured and reported as the CEC. The
cation may be a single charge ion such as sodium (Na+) or a double-charge ion such as
calcium (Ca2+) or magnesium (Mg2+).
When dry clays come into contact with water the interlayer Spacing expands, and the clay adsorbs a large “envelope” of water.
The water makes hydrogen bonding with clay surfaces and as a result the clay swells and well bore instability starts.
The thickness of the adsorbed-water film is controlled by the type and amount of cations associated with the clay. Water adsorbed
to the large, flat, planar surfaces comprises the major part of the total water retained by hydratable clays.
Divalent cations such as Ca2+ and Mg2+ increase the attractive force between platelets, thus decreasing the amount of water that
can be adsorbed (in formation clays), one cation will attract two negative ions. Monovalent cations such as Na+ give rise to a lesser
attractive force and allow more water to Penetrate between the platelets. That’s why smectites are always the most swellable
shales.
Illites have the same basic structure as montmorillonites (smectites), but they do not show interlayer swelling. The compensating
cations are primarily the potassium ion (K+). The spacing between unit layers is 2.8 Å. The ionic diameter of the K+ is2.66 Å.
This allows the K+ to fit snugly between unit layers forming a bond that prevents swelling in the presence of water. Since the unit
layers do not swell and separate when exposed to water, the potassium ions (K+) between
The unit layers are not available for exchange.
Increasing the concentration of any given cation will increase the probability that it will displace another cation , this is why using
high potassium ion concentration in drilling fluids makes potassium more exchangeable with other clay ions like sodium , thus
reducing the clay hydration effect (like transforming smectites to illites) .
Two ways that potassium can become associated with clay minerals (Eberl concept):
The ion exchange reaction is governed by the law of mass action; that is the rate of exchange depends on the concentration of
the ions (i.e. the higher the ratio of K ion to Na ion, the faster the rate of exchange of K+ for Na+). In addition to ion exchange, ion
The fixation of potassium is a unique property for potassium only that once its fixed , its very difficult to become exchanged again
unless the other cations are significantly increased.
The CEC of montmorillonites is within the range of 80 to 150 meq/100 g of dry clay.
The CEC of illites and chlorites is about 10 to 40 meq/100 g, and for kaolinites it is about 3 to 10 meq/100 g of clay.
The Methylene Blue Test (MBT) is an indicator of the apparent CEC of a clay.
9. What are the types of stuck pipe and what is the difference between them?
What causes stuck pipe?
Types of stuck pipes
Mechanically stuck pipe can be grouped into two major categories:
1. Hole packoff and bridges.
2. Wellbore geometry interferences.
Packoffs and bridges are caused by:
Settled cuttings
Shale instability
Unconsolidated formations
Wellbore geometry interferences are
Caused by:
Key seats
Under gauge hole
Stiff drilling assembly
Mobile formations (like plastic salt)
Ledges and dogleg
Mechanical sticking is caused by physical obstruction or restriction. Mechanical sticking usually occurs when the drill string is
moving. It also is indicated by obstructed circulation.
Occasionally, however, a limited amount of up/down mobility or rotary freedom is evident, even when the pipe is mechanically
stuck.
Differential sticking is defined as stuck pipe caused by the differential pressure forces from an overbalanced mud column acting
on the drill string against a filter cake deposited on a permeable formation.
When a filter cake builds up on the formation, it increases the contact area between the wellbore and the drill pipe. Excessive
drill solids and high fluid loss increase filter-cake thickness increasing differential sticking probabilities.
It usually occurs while the pipe is stationary during a connection or when taking a survey, and is indicated by full circulation and
no up/down mobility or rotary freedom, other than pipe stretch and torque.
It is a Standard API test done in HTHP wells to simulate the filtration and fluid invasion under HT HP conditions usually 300 F and
500 psi differential.
PPT test
The Permeability Plugging test or Apparatus (PPA) is designed to provide accurate simulation and measurement of down-hole
static filtration. PPT is ideal for predicting how a drilling fluid can form a permeable filter cake to seal off depleted/under pressure
intervals.
The PPT utilizes a conventional HTHP Heating Jacket to simulate reservoir temperature. The fluid cell is inverted, with pressure
applied from the bottom of the cell and filtrate collected out the top. Pressure is transferred to the mud by a small hydraulic hand
pump through a small floating piston within the cell.
The pressure applied can be simulating the same over balance applied on a depleted formation (ex: 3000 psi), also The PPT employs
a ceramic filter disc, which is available in varying porosities.
The disc offers a more authentic representation of the formation as it can be selected based on the formation porosity thus testing
the efficiency of selected bridging materials and it size combination in well bore strengthening.
Sag is most often associated with well angles of 50 to 80° , low annular velocities and low
viscosity clean muds. Possible consequences include lost circulation, stuck pipe, packoffs,
wellbore instability and well-control problems.
Barite sag can happen on static or dynamic conditions, static sagging is usually noticed after
long trips typically, bed growth under static conditions (pumps off) is minimal, although
slumping is most likely to occur during Static periods.
For these reasons, drilling practices prior to and after trips can often prevent static sag-related problems, One of the practices is
tripping in stages and circulating BTMs up.
12. Define dynamic barite sag and it's relation with flow rate & temperature?
Dynamic barite sag is barite settling under dynamic conditions (while drilling or circulation), many factors contribute to dynamic
settling like fluid rheology, hole angle , interval length , flow rates ,pipe eccentricity, and rotation, and annular velocities.
From drilling fluids perspective maintaining adequate low shear rate viscosities minimize sagging the same concept of hole
cleaning in deviated and ERD wells applies.
High temperatures cause mud thinning and increased settling. HTHP testing is necessary To ensure that rheological properties are
adequate under well conditions, in crtical ERD wells, Fann Model 50 and 70 for WBM and oil/ synthetic-base muds is recommended
for LSRYP measurements at actual wellbore conditions (pressure and temperature).
Large annular clearances or low circulation rates promote sag due to low annular velocities. Higher flow rates will reduce sag
tendencies, but pressure limits and downhole tools can limit this as an option.
Long intervals sliding without rotation also promotes barite sagging, usually if high rpm is used in ERD wells sagging is greatly
minimized.
Well design may require compromises in order to minimize and control sag. Sag tendency generally increases with hole angle and
probably is most critical in extended-reach drilling under High Temperatures and High Pressures (HTHP).
These chemicals include emulsifiers, soaps and wetting agents. They act by
reducing the interfacial tension between two liquids or between a liquid and a
solid. Surfactants have a hydrophilic (water-loving) polar head and an organophilic
(oil-loving or lipophilic) non-polar tail.
The balance between the strength and character of the hydrophilic end and lipophilic end can be measured using The Hydrophilic-
Lipophilic Balance (HLB) range. The HLB number can characterize the functionality of a surfactant. As shown in below Figure, oil-
in water emulsifiers have higher HLB values and water-in-oil emulsifiers have lower HLB numbers, with wetting agents in the
middle.
Primary emulsifier: Primary emulsifier us used to primarily emulsify water in oil, it exhibits low wetting properties such as
VERSAMUL (refer to the above HLB range).
In tight emulsion systems usually the primary emulsifiers are soaps that are formed by the reaction of a fatty acid ester with an
alkali (such as lime) where the hydrogen on the fatty acid is replaced by a metal, such as calcium from lime.
Secondary Emulsifiers: Exhibits more wetting characteristics for solids and also emulsifier for water in oil.
In tight emulsion systems 2ndry emulsifiers are used to supplement water in oil emulsion and change the wettability of solids to
oil wet (VERSACOAT).
A wetting agent is a surface-active agent that reduces the interfacial tension and contact angle between a liquid and
a solid. This causes the liquid to spread over the surface of the solid.
Wetting agents have one end that is soluble in the continuous-phase liquid and the other that has a strong affinity for
solid surfaces thus causing the solids to be oil wet and kept in solution, if the solids become water wet they will
aggregate and settle of the solution.
Activity can also be estimated based on the chemical composition of the brine (salinity). Pure water has an AW of 1.0. Calcium
chloride brines used in most non-aqueous emulsion muds have an AW between 0.8 (22% wt) and 0.55(34% wt.), Lower values for
activity are more inhibitive.
The transfer of water between an emulsified brine and a shale is often compared to osmosis.
Shale control using this controlled (or balanced) activity is limited mainly to oil- and synthetic-emulsion muds.
Water-base muds containing additives (such as glycols and silicates) exhibit only weak semi-permeable membrane characteristics.
Consequently not only we can inhibit the shales by having lower activity of the water phase, theoretically the shales can be dried
under osmosis by using a high water phase salinity fluid with lower activity than formation water.
Calcium chloride (CaCl2) is normally used to obtain activities from 1.0 to 0.40 , due to the high salinity of calcium chloride
solution it can be used to give the least activity compared to other salts like sodium chloride .
Also using water in oil emulsion enhances the performance of organophilic clays thus giving better viscosities and higher carrying
capacity for oil base muds.
16. In spud mud, you add soda ash in the beginning to precipitate calcium then
you add lime, lime contain calcium?
Calcium is precipitated at the beginning to allow proper prehydration of bentonite and water intake , if calcium is present it will
not allow proper hydration of clay platelets as discussed above in previous questions , then lime is added if desired to flocculate
the gel mud to give the highest rheology for hole cleaning.
POROSEAL: polysaccharide/latex copolymer technology, developed and used to seal shales and low permeability formations. This
product works through a plastering effect thus minimizing pressure transmission and for instance stabilizing the micro-fractures.
It provides supplemental fluid loss control in high temperature applications.
IDCAP D: Low molecular weight dry acrylic acid copolymer, designed for clay encapsulation and clay dispersion inhibition.
Its action is similar to PHPA but the low molecular weight makes it unique as it have minimal effect in viscosity with higher
concentrations that aid in clay encapsulation.
Its mechanism is that it adsorbs a water envelop around the polymer chain aby hydrogen bonding thus reducing the free water.