A.

Tabel Perhitungan Hasil Standarisasi Larutan Na2EDTA

No Jenis Larutan Konsentrasi (M) Vol. Larutan (mL)
1 CaCO3 0.0100 10
2 CaCO3 0.0100 10
Rata-rata

B. Tabel Perhitungan Hasil Analisis Sampel

No No. Sampel Vol. Sampel Faktor Pengenceran
1 2278 25 1
2 2487 25 1
3 2488 25 1
4 2503 25 1
5 5395 25 1
6 5416 25 1
7 5417 25 1
8 5418 25 1
9 5419 25 1
10 5420 25 1
11 5421 25 1
12 5422 25 1
13 5423 25 1
14 5424 25 1
15 5409 25 1
16 5410 25 1
17 5441 25 1
18 5444 25 1
19 5445 25 1
20 5446 25 1
21 5410 S 25 1
22 5417 S 25 1
23 5420 D 25 1
24 5441 D 25 1

C. Tabel Perhitungan Relative Percent Difference (RPD)

No No. Sampel (mL) Vol. Sampel (mL) Simplo (mg/L)
1 5420 25 8
2 5441 25 68
Ket. Memenuhi syarat jika perbedaan persen relatif (Relative Percent Different atau RPD) ≤ 5%

D. Tabel Perhitungan Recovery

1. Perhitungan Kadar Standar CaCO3
No Jenis Larutan Vol. Larutan (mL) Faktor Pengenceran
1 CaCO3 10 1
2. Perhitungan Kadar C Target Value
No Vol. Spike (mL) Vol. Sampel (mL) Vol. Sampel (mL)
1 Spike 10 15

3. Perhitungan %R
No No. Sampel C Sesudah Spike ( Mg/L) C Sebelum Spike (mg/L)
1 5417 460 76
2 5410 448 96
 Vol. Titrasi (mL) Konsentrasi Na2EDTA (M)
10 0.0100
10 0.0100
0.0100

Vol. Titrasi (mL) Kadar CaCO3 (mg/L)

2.8 112
4.7 188
1.4 56
7.1 284
1 40
7.7 308
2.4 96
7.8 312
5.2 208
0.2 8
5 200
4.8 192
0.3 12
0.2 8
2 80
1.9 76
1.7 68
3.5 140
3.5 140
1.7 68
11.2 460
11.5 448
0.2 8
1.7 68

Duplo (mg/L) RPD

8 0
68 0
Different atau RPD) ≤ 5%

Vol. Titrasi (mL) Kadar CaCO3 (mg/L)

10 1000
 Total Vol. (mL) C Target Value
25 400

C Target Value (mg/L) %R

400 96.00%
400 88.00%