You are on page 1of 15

j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2

Available online at www.sciencedirect.com

journal homepage: www.elsevier.com/locate/jmrt

Original Article

Process optimization of A356 aluminum alloy


wheel hub fabricated by low-pressure die casting
with simulation and experimental coupling
methods

Guojiang Dong a, Shide Li a,b, Shaozhong Ma a, Dongsheng Zhang c,


Jiang Bi a, Ji Wang b,d, Mikhail Dmitrievich Starostenkov e, Zuo Xu b,*
a
Key Laboratory of Advanced Forging & Stamping Technology and Science of Ministry of Education, Yanshan
University, Qinhuangdao, 066004, China
b
CITIC Dicastal Co., Ltd., Qinhuangdao, 066004, China
c
Hebei Key Laboratory of Special Delivery Equipment, Yanshan University, Qinhuangdao, 066004, China
d
State Key Laboratory of Metastable Materials Science and Technology, Yanshan University, Qinhuangdao, 066004,
China
e
General Physics Department, Altai State Technical University, Leninist. 46, Barnaul, 656099, Russia

article info abstract

Article history: The aluminum alloy wheel hub is mainly produced by low-pressure die casting process
Received 18 February 2023 (LPDC), in which casting quality is closely related to the process parameters. In this paper,
Accepted 29 March 2023 the LPDC process of the A356 alloy wheel hub was numerically simulated by ProCAST
Available online 1 April 2023 software, and the forming quality of the wheel hub under different cooling processes has
been studied. The result indicated that the liquid aluminum exhibited different solidifi-
Keywords: cation characteristics under three cooling processes of 300 L/h for 150 s, 400 L/h for 140 s
A356 aluminum alloy and 500 L/h for 130 s. A sequential solidification state was obtained under the condition of
Low-pressure die casting 400 L/h for 140 s. By comparing the tensile properties of the rim under different cooling
Numerical simulation processes, it was found that the wheel hub casted under 400 L/h for 140 s had higher tensile
Microstructure strength and elongation, which were 178.9 MPa and 6.6%, respectively. The reduction of
Mechanical properties casting defects, microstructure refinement, and uniform distribution of eutectic Si particles
in the wheel hub are the main reasons for the improvement of mechanical properties.
© 2023 The Author(s). Published by Elsevier B.V. This is an open access article under the CC
BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

accidents are caused by the safety problem of wheel hub


1. Introduction structures [1,2]. In addition, under the background of “carbon
neutralization”, energy saving and emission reduction have
According to statistics, about 1.3 million people die in car ac- become one of the development trends [3,4]. Therefore, the
cidents every year worldwide, and 10%e15% of traffic

* Corresponding author.
E-mail address: zxtc@dicastal.com (Z. Xu).
https://doi.org/10.1016/j.jmrt.2023.03.214
2238-7854/© 2023 The Author(s). Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://
creativecommons.org/licenses/by-nc-nd/4.0/).
j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2 3119

structure safety and weight reduction of wheel hubs are rate may lead to pore condensation. In low temperature and
increasingly important in automobile manufacturing field [5]. high filling rate condition, a higher cooling rate was generated
The material types of wheel hubs mainly include steel, and it had a greater effect on the peak pressure flow stress.
aluminum alloy, and magnesium alloy. Due to its advantages According to the above research, the LPDC defects of wheel
of lightweight, good heat dissipation, high safety factor and hub under different process parameters can be predicted by
flexible design, aluminum alloy wheel hub accounts for about numerical simulation method, and the parameters of forming
54% of the global wheel hub market [6,7], and about 80% of process window can be optimized to improve the casting
aluminum alloy wheels are produced by LPDC [8]. As a rapid quality, so as to promote the application and development of
near-net shape-forming process, LPDC process has high pre- LPDC technology in the industry [31].
cision, good surface quality and high production efficiency A review of the work carried out so far shows that the re-
[9e11]. Although the process has been applied widely, it is searchers have carried out a series of studies on LPDC simu-
easy to appear defects such as shrinkage porosity, shrinkage lation and process parameter optimization, the influence of
hole, and oxidation slag inside the product because of the different key parameters of the process on the forming quality
complex manufacturing process [12,13]. These defects have a and microstructure of wheel hub casting is still not clearly
great influence on the selection and adjustment of techno- defined. Therefore, this paper optimized the process param-
logical parameters in the process of LPDC. Hence, selecting eters of the LPDC wheel hub by the combination of numerical
appropriate process parameters is a major area of interest simulation and process production test method. Also, the in-
within the field of achieving stable and high-quality die- fluence of process parameters on the mechanical properties
casting wheel production. and microstructure of wheel hub was studies. Firstly, the
For the selection of process parameters in LPDC, the pre- filling and solidification process under different process pa-
vious research is mainly based on numerical simulation, then rameters were simulated by ProCAST software, and the defect
experimental verification to optimize the process parameters. distribution and the optimized process parameters were ob-
Ou et al. [14,15] presented a modeling methodology to simu- tained. According to the process parameters, the A356 alloy
late the temperature field evolution in the production of A356 wheel hubs were trial-produced, and the overall shrinkage
automotive wheels, and the model was able to predict clusters porosity and shrinkage hole of the wheel hub were examined
of porosity associated with encapsulated liquid with an by X-ray detection. Then the mechanical properties and
equivalent radius of ~27 mm. Numerical simulation can pro- microstructure of different parts were tested and compared in
vide a general direction for process optimization, to reduce the detail. Based on the previous research, the process parameters
number of experiments and achieve the purpose of improving of the LPDC A356 alloy wheel hub were optimized by numer-
the efficiency and success rate of experiments [16e18]. ical simulation, and more comprehensive mechanical prop-
Combining production experience with theoretical studies of erties tests were conducted to verify the accuracy of the
casting, the LPDC process can be divided into the filling pro- simulation. The influence of different cooling process pa-
cess and the solidification process [19]. The filling stage mainly rameters on the mechanical properties and microstructure of
requires the simulation and experiment of the flow state of the wheel hub was further analyzed. The research result in
molten metal. Using other liquids with similar viscosity to this paper will provide a meaningful guidance for the pro-
replace liquid metal can be more convenient to observe the duction of high-quality wheel hubs.
filling process of liquid metal under pressure. Viswanath et al.
[20] investigated the free surface flow characteristics during
mold filling through water model experiments and numerical 2. Experimental
simulations. The effect of flow condition was analyzed by
adjusting the filling pressure and the shape of the gate, and 2.1. Numerical simulation
then a numerical flow model coupled to heat transfer was
developed. According to the model, the filling pressure can be The LPDC process of the aluminum alloy wheel hub is as
adjusted appropriately to ensure a smooth filling process, to follows: to begin this process, the molten aluminum alloy in
obtain a product with better performance [21]. In actual pro- the holding furnace is injected into the mold cavity through a
duction, because of the diversity and complexity of the mold riser pipe at a certain pressure. After mold filling, pressure
structure, the research of the filling process is commonly holding, cooling solidification, pressure relief and other
complicated [22,23]. The solidification process is mainly technological steps, the wheel hub casting is formed, as
affected by temperature and pressure of molten aluminum, shown in Fig. 1.
the process parameters can be optimized by experiments with
production equipment [24,25]. Therefore, a large number of 2.1.1. 3D modeling
researchers choose to optimize the process parameters in the To verify the effect of different process parameters on the
solidification process [26,27]. quality of the LPDC aluminum alloy wheel hub, finite element
Previous studies have compared and analyzed the me- simulation is one of the most common procedures. When
chanical properties and microstructure of products under modeling the wheel hub model with UG software, the model
different cooling processes. The results show that aluminum was appropriately simplified to improve simulation efficiency.
alloy castings with finer grain size can be obtained by properly LPDC aluminum alloy wheel hub mold mainly consists of a top
increasing the die cooling rate [28,29]. Azqadan et al. [30] die, side dies, a bottom die, a split cone, a gate cup and a gate
determined the influence of cooling rate on the mechanical sleeve. The riser tube, heat insulation furnace, top rod and top
properties of LPDC AZ80 alloy and found that a lower cooling plate mechanism were simplified in the simulation modeling.
3120 j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2

Fig. 1 e Diagram of LPDC wheel hub, 3D model, and real object.

In addition, to make the simulation results more accurate, the 2.1.2. Finite element modeling
insulating device was set at the corresponding positions of the ProCAST software was used for finite element modeling of
side and top mold. Fig. 2 displays the die casting mold and its wheel hub mold models. Due to the complex structure of this
3D model. The reference direction of the wheel hub region model, tetrahedron mesh with good geometric adaptability
described later is consistent with the hub in Fig. 1. was selected to mesh the mold when dividing the finite

Fig. 2 e 3D models of LPDC aluminum alloy wheel hub mold: (a) 3D assembly model; (b) Mold physical drawing; (c) Side die;
(d) Top die; (e) Bottom die; (f) Steam distribution cone: pouring bushing, sprue cup.
j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2 3121

Fig. 3 e Finite element model and mesh division: (a) casting mold; (b) Section A-A; (c) Side die; (d) Top die; (e) Bottom die;
(f) Other components; (g) Wheel hub.

element mesh. The mold cavity is the main calculation posi- of the alloy were measured by X-ray diffractometer (XRD) and
tion in the simulation, where surface mesh size needed to be differential scanning calorimeter (DSC). The material of the
set to 5 mm. There are more detailed features in the spoke top die, bottom die and split cone is H13 steel, the material of
area inside the cavity, and the mesh size was set as 3 mm. The the side die is 35CrMo, and the material of the gate cup and
surface mesh of some small-sized parts and the location of the gate sleeve is ceramic. The physical parameters (density,
cooling boundary were set to 2 mm for detail features like the specific heat and material parameters) of the above materials
spoke edge and wheel center position. The grid ruler of the are listed in Table 2. Fig. 4 shows the DSC and XRD curves of
position surface of the top die, bottom die, side die and heat A356 aluminum alloy.
preservation device was set to 10 mm to improve the calcu-
lation efficiency. After the global grid check, the minimum 2.1.4. Process parameters and experimental design
side length of the surface grid quality is less than 0.25, the According to production experience with theoretical studies
maximum aspect ratio is greater than 6, the minimum tria of casting, casting pressure and time play a direct role in the
internal angle is less than 6 , the tetra ratio of volume mesh molding process. To provide data necessary for numerical
mass was less than 0.001, the simulation accuracy is satisfied simulation, the data source for simulation was extracted from
and the convergence is good. Finally, the finite element model a commercial LPDC wheel casting machine which was
of the mold was obtained by generating the volume mesh completed at CITIC Dicastal's plant located in Qinhuangdao,
from the surface mesh with good quality. Fig. 3 presents the Hebei, China. The data included the activation time of pres-
finite element model of the wheel hub mold. sure system and the activation time of cooling system.
The time in the pressure holding stage plays a key role in
2.1.3. Material parameters the forming quality and overall production efficiency of the
In the process of numerical simulation, the material physical LPDC wheel hub. Pressure holding times of 130 s, 140 s and
parameters of mold and molten aluminum have a great in- 150 s were set in different finite element simulations, to study
fluence on the simulation result. Table 1 shows the material the influence of different pressure holding time on the form-
composition obtained by fluorescence spectrum analysis. To ing quality of the LPDC wheel hub [14]. Fig. 5 displays the
obtain phase types and solidus/liquidus temperatures of A356 experimental scheme and pressure setting. During the solid-
aluminum alloy, phase curves and thermogravimetric curves ification process of liquid aluminum, the flow rate and

Table 1 e The chemical composition of A356, H13 and 35CrMo alloys.


Elements Si Mg C V Cr Ti Mo Mn Al Fe
A356 6.74 0.35 e e e 0.09 e e Bal 0.08
H13 1.0 e 0.405 1.0 5.125 e 1.425 0.35 e Bal
35CrMo 0.225 e 0.425 e 0.95 e 0.2 0.875 e Bal
3122 j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2

Table 2 e Physical parameters of die and casting.


Materials Density/ Specific heat/ Conductivity/ Solid- Viscosity/ Young's Poisson's
(kg$m3) (kJ$kg1$K1) (W$m1$K1) liquidus/( C) (centipoise) modulus/(MPa) ratio
A356 2.7  103 0.963 151 548e613 1.17e1.83 e e
35CrMo 7.7  103 0.517 37.7 1425e1494 3.41e4.73 55e23.5  104 0.27
H13 7.8  103 0.422 28.7 1355e1473 3.46e5.45 106e20.9  104 0.36
Ceramic 3.97  103 1.13 1.32 e e e e

duration of cooling water influence the solidification process. properties and microstructure test analysis. The size and
The solidification process of LPDC affects the forming and location of the samples are shown in Fig. 6.
distribution of defects, microstructure morphology and phase The unidirectional tensile test was carried out by WDW-100
uniformity of wheel hub forming. In the cooling process, the electronic universal testing machine. The tensile test was
cooling system at the side dies position plays a leading role in carried out according to GB/T 228-2002. The tensile test tem-
the overall cooling. To study the influence of different cooling perature was room temperature, and the tensile speed was
water processes on the solidification process and the influ- 2 mm/min. Each tensile result was averaged by 5 samples. The
ence on the final wheel hub performance and structure, the samples were cut from the 1e5 positions of the hub casting,
cooling water process is 300 L/h for 150 s, 400 L/h for 140 s, and and the samples were first coarsely and finely ground with 800
500 L/h for 130 s. Cw, 1000 Cw, 1500 Cw and 2000 Cw sandpaper impregnated
The parameters of the simulation model were set in detail with water in turn. Then particle size of 1 mm diamond abrasive
as follows: the surface heat transfer coefficient was 1000 W/ spray and gold velvet polishing cloth was used to mechanically
(m2$K) between the mold, 2000 W/(m2$K) between the mold polish the sample in the MPD-1 polishing machine until the
and the aluminum alloy casting, 20 W/(m2$K), 5000 W/(m2$K) mirror surface had no trace. Used the Sigma 500 scanning
between the mold and the air cooling and the cooling water electron microscope (SEM) on the microstructure observation.
[15]. Since the initial temperature will only affect the number The A356 aluminum alloy was chemically corroded with Kel-
of cycles in which the simulation reaches the steady state and ler's reagent (V(HF): V(HCl): V(HNO3): V(H2O) ¼ 1: 1.5: 2.5: 95) for
has little effect on the final steady state temperature, the 15 s. Finally, the microstructures were observed by Zeiss Axio
initial temperature of the mold was selected as 500  C, and the Scope A1 optical microscope. The hardness test was performed
initial temperature of the molten aluminum was 700  C [32]. by QATM automatic microhardness tester, the test load was
2 N, and the pressure holding time was 10 s. After grinding and
2.2. Experimental procedure polishing, the samples from 1 to 5 positions met the hardness
test conditions, and the average value was taken from 10 po-
The BQ-C-6 type low-pressure casting experiment machine sitions measured for each position. And its hardness standard
was used to trial the production of A356 aluminum alloy error is 4%.
wheel hubs and analyzed the forming quality of wheel key
position and organization performance.
Firstly, the SRE90 CNC type X-ray detector was conducted 3. Results and discussion
for the wheel hub internal inspection and analyzed the trial
production wheel hub under different process parameters 3.1. Mold filling and solidification
distribution of internal defects. Then, tensile samples, hard-
ness test samples, and microstructure analysis samples were Fig. 7 presents simulation results of the mold filling at
cut at different locations of the wheel hub for mechanical different stages of the LPDC aluminum alloy wheel hub.

Fig. 4 e Material parameters of A356 aluminum alloy: (a) DSC curve; (b) XRD diffraction pattern.
j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2 3123

After filling the cavity, the holding-pressure was raised to


the maximum value (0.95 bar) and maintained to start the
feeding and solidification process. An appropriate solidifica-
tion range can effectively increase the production efficiency
and integrated performance of LPDC wheel hubs. To demon-
strate the solidification effect of molten A356 alloy under
different cooling processes, three process parameters with
similar cooling efficiency were chosen: 300 L/h for 150 s, 400 L/
h for 140 s, and 500 L/h for 130 s, as shown in Fig. 8.
It can be seen that when the water flow was 300 L/h (Fig. 8
(a)), the outer rim solidified firstly due to the thin thickness of
this zone. What's more, the water-cooling channel locates in
the lower part of the side die, which is close to the outer rim.
The wheel hub solidification result was better when the
Fig. 5 e LPDC process pressure curves of the A356
duration of cooling water increased at a lower water flow rate.
aluminum alloy wheel hub.
The molten A356 alloy at the junction of the spokes and the
center of the wheel hub solidified at the end. Two factors are
the main reasons for the slow solidification of this position:
the structure of this area is complex and the wall thickness of
the part is large. The final stage of solidification tended to
Firstly, the molten A356 aluminum alloy entered the mold cause shrinkage porosity, shrinkage cavity defected, and
cavity through the riser pipe and the gate cup under pressure, affect the microstructure growth of this part and the me-
then fills the bottom of the cavity through the spokes. The flow chanical properties of the wheel hub.
process was relatively smooth and there was no uneven When the water flow was 400 L/h and the duration was
diversion as shown in Fig. 7 (a). The result indicated that the 140 s (Fig. 8 (b)), the wheel hub started to solidify at the outer
pressure selection of the molten as it entered the mold was rim, but the overall solidification sequence was basically from
appropriate. When the molten aluminum flowed to the outer top to bottom and from outside to inside. It can be seen that
rim, the molten in the middle section of the spokes formed the final solidification result of the wheel hub was good during
closed areas and appeared air entrainment. When molten this cooling process. Under the condition of this process, there
aluminum flowed through the outer rim, it diverted and is also an isolated solidification region at the junction of the
merged. Turbulent flow is likely to occur after the impact and spoke and the hub, leading to an increase in defects in this
collision of two liquid aluminum streams at the confluence, region.
which resulted in defects. In order to reduce the defects in When the water flow rate was 500 L/h and the duration was
Fig. 7 (b), the filling pressure required to be controlled at this 130 s, the wheel hub solidified can be seen in Fig. 8 (c). Due to
stage to ensure a smooth flow of the molten aluminum. After the excessive cooling rate of the outer rim and the inner rim,
the molten aluminum was filled through the outer rim, the there was an isolated solidification area in the rim. The
flow velocity began to slow down. At this stage, the filling probability of casting defects such as shrinkage porosity and
pressure could be properly increased to improve the feeding porosity in this area was greatly increased, and it was easy to
capacity of the fluid. The contact pressure between the molten generate hot joints, which lead to thermal stress and hub
aluminum and the mold will also be increased to improve the deformation after the completion of hub molding. After the
heat exchange efficiency, speed up the production rate and wheel hub had been formed, thermal stress was generated,
improve the efficiency of production. When t ¼ 22.08 s, the which lead to the deformation [33]. In conclusion, when the
molten aluminum was filled into the inner rim, and the filling water-cooling process is 400 L/h for 140 s, the wheel hub will
process was completed, as shown in Fig. 7(c)e(f). be solidified sequentially and the casting quality of the hub

Fig. 6 e Schematic diagram of mechanical properties testing of A356 aluminum alloy wheel hub.
3124 j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2

Fig. 7 e Mold filling simulation of the LPDC fabricated A356 aluminum alloy wheel hub at different times: (a) t ¼ 15.52s;
(b) t ¼ 16.94s; (c) t ¼ 18.09s; (d) t ¼ 20.01s; (e) t ¼ 21.11s; (f) t ¼ 22.08s.

will be better, while the shrinkage defects will be more under From an overall point of view, with the increase in the pres-
the other cooling process. sure holding time, the defects of the wheel hub showed a
decreasing trend, and the maximum shrinkage porosity of the
3.2. Simulation result analysis parts with shrinkage porosity decreased. When the pressure-
holding time was 130 s, the feeding ability of the molten was
Fig. 9 provides simulation results of wheel hub internal de- poor during solidification. Because of the shorter pressure
fects at different pressure-holding times (130 s, 140 s, 150 s). holding time, the probability of shrinkage defect was higher

Fig. 8 e Solidification process of the LPDC aluminum alloy wheel hub under different cooling processes: (a) 300 L/h for 150 s;
(b) 400 L/h for 140 s; (c) 500 L/h for 130 s.
j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2 3125

Fig. 9 e Shrinkage defects of the LPDC A356 alloy wheel hub fabricated at different holding times and different cooling
processes: (a) 130 s; (b) 140 s; (c) 150 s; (d) 140 s, 300 L/h for 150 s; (e) 140 s, 400 L/h for 140 s; (f) 140 s, 500 L/h for 130 s.

and the degree of shrinkage was more serious. In addition, the distribution is 90 clockwise. The reason is that the defect is
gap between the wheel hub casting and the mold increased located at the junction of four side dies, and the junction is
because of the failure of timely filling, which affected the heat affected by two cooling water pipes. So, the cooling rate at this
transfer and cooling of the mold and was also part of the location is relatively high, and shrinkage defects are easy to
reason for the increase in shrinkage and porosity. When the occur. However, cooling flow and time control change gently,
holding time was 140 s, the inhibition effect on defects was and the cooling coupling effect of the two cooling pipes is
much higher than that at 130 s. Because of the location of the small, so defects are not easy to appear at the rim position
die and its thinner thickness, the cooling rate was faster and when the cooling flow rate is 400 L/h and the time is 140 s, as
there was a greater probability of small-size shrinkage. Under shown in Fig. 9 (e). Due to the influence of cooling efficiency
this condition, the maximum shrinkage rate of the shrinkage and undercooling degree at the hub center flange position,
area was 1.4%, and it was concentrated in the outer rim area. there are some defects in the center hub edge of the simula-
The prediction results are similar to those obtained in the tion. To verify whether the simulation defect conforms to the
study of Dhisale [19], which has a lower shrinkage porosity. real production condition, the following X-ray observation
The wheel hub solidification result was better under the will be carried out for verification.
140 s holding time process, which was within the solidifica-
tion window period. With the pressure holding time 3.3. X-ray observation analysis
increasing to 150 s, the shrinkage area reduced, and the
shrinkage rate decreased by 0.2% compared with 140 s. How- According to the simulation, it is known that when the cooling
ever, the reduction of shrinkage porosity was slight, which flow rate is 400 L/h and the time is 140 s, the simulated
indicated that the solidification result in this area was close to shrinkage defects are more than the other two process pa-
the optimal value and was conducive to the growth of crystal rameters, so the test die casting of this process is not carried
nucleus and grain refinement. The production rate of the out in this manuscript. Based on the simulation results, the
wheel hub will decrease with the increase in pressure holding BQ-C-6 low pressure casting machine was used for trial pro-
time, resulting in the reduction of economic benefits. There- duction with two sets of process parameters: 1. Pressure-
fore, the process is relatively appropriate when the pressure is holding time of 140 s, side mold water flow of 300 L/h, dura-
maintained for 140 s. tion of 150 s, and 2. Pressure-holding time of 140 s, side mold
Through numerical simulation, it is concluded that the water flow of 400 L/h, duration of 140 s. It can be seen from
reasonable pressure holding time is 140 s, Fig. 9 (d), (e), and (f) Fig. 10 that preliminary observation of shrinkage porosity and
show the simulation of defects under different cooling pro- cavity defects was carried out through X-ray.
cesses at 140 s. In the lower or higher cooling flow rates, the It can be seen from Fig. 10 (a) that there is no obvious
defects are increased, as shown in Fig. 9 (d) and (f). And there shrinkage cavity defect at the spoke position under the two
is a shrinkage defect at the rim position, the defect process parameters, indicating that the solidification result at
3126 j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2

Fig. 10 e X-ray inspection of wheel hub fabricated at different processes: (aec) Process 1; (b) Process 2.

this position is good and consistent with the simulation re- 3.4%. This is because this process parameter is located at the
sults of Fig. 9 shrinkage defect. In the spokes center area, boundary of the forming process window, resulting in poor
shrinkage and loosening traces appeared. The results as mechanical properties. The average yield strength and tensile
shown in Fig. 10 (b), indicate that the unreasonable design of strength of the samples in process 2 are 100.9 MPa and
the cooling process in this position may lead to the failure of 178.9 MPa, respectively, which are 2.0% and 11.3% higher than
timely feeding of molten A356 alloy. The large difference in those in process 1. The average fracture elongation is 6.6%,
thickness between the wheel center and spoke is also one of which is 94.1% higher than process 1. Besides, the average
the reasons leading to more defects so the simulation accu- tensile strength and the average yield stress of process 2 was
racy in Fig. 9 (e) is partially verified. What stands out in Fig. 10 higher than those of the grain-refined process [35].
(c) is the crack defect that appears at the inner rim position of The hardness of the spoke, the outer edge, the lower edge,
the rim in process 1. It indicates that the uneven shrinkage the upper edge, and the inner edge of the hub specimens were
caused by thermal stress leads to defects at this position, measured and compared with that of the cube specimen with
while there are few similar defects at the corresponding po- a side length of 10 mm under two different processes. It is
sition in process 2, which is consistent with the shrinkage considered that the hardness error is consistent with the
defect at the simulated rim position in Fig. 9 (d). By analyzing hardness value of this point within 4%. The hardness of the
the X-ray observation results, it can be shown that the simu- two sets of specimens does not change significantly at
lation is accurate which is similar to the prediction results different locations. The spoke area is the hardest part with an
proposed in the study of Fan [34]. average hardness of 71 HV and 69.8 HV, followed by the lower
edge with an average hardness of 67.5 HV and 68.4 HV. The
3.4. Mechanical property analysis main reason is that these two parts have high density or a few
defects. The difference in hardness between the outer rim and
Fig. 11 shows the comparison of mechanical properties tests the upper part of the rim is larger, the difference is 8.9% and
results in five regions of the wheel hub under the two sets of 7.7% respectively. As for the rest of parts, the difference in
process parameters in Section 3.3. The mechanical experi- hardness is less than 3.3%. This is owing that the aluminum
ments in each area were repeated five times and the average matrix distribution at the outer rim position is more uniform,
of the results was taken. The average yield strength of the and there are fewer shrinkage defects. In the upper part of the
samples from five regions in process 1 is 98.9 MPa, the average rim, the difference in microstructure density between the two
tensile strength is 160.7 MPa, and the average elongation is processes is small. In addition, the uniform distribution of
j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2 3127

Fig. 11 e Mechanical properties of LPDC processed aluminum alloy wheel hub: (a), (b) Mechanical tensile property; (c),
(d) Hardness testing; (e), (f) Craft contrast; (g) The corresponding position of the samples.

eutectic Si particles is also one of the reasons for its high 3.5. Metallographic structure analysis
hardness. The results of the mechanical properties test meet
the requirements of the aluminum alloy hub proposed in In the process of wheel hub casting, the differences in wheel
Kaba's [35] research. hub configurations lead to different wall thicknesses of
3128 j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2

Fig. 12 e The metallographic microstructure at different regions of the wheel hub: (a) Spoke; (b) Outer rim; (c) Under the rim;
(d) On the rim; (e) Inner rim.

spokes, upper rims, and lower rims. Moreover, the solidifica- fabricated by LPDC with local squeeze [36]. By comparing and
tion sequence and the cooling processes at different locations analyzing the distance between the secondary dendrite arms
are also different. In this section, the metallographic micro- of the two groups of processes in 3.3, it was found that the
structure of five characteristic positions of the wheel hub secondary dendrite arm spacing and grain size of the hub
(spoke, outer rim, lower rim, upper rim, and inner rim) under obtained by process 2 were smaller than those obtained by
different casting processes have been observed, as shown in process 1. Because a large water flow can produce greater
Fig. 12. The range of SDASs is similar to that of the same alloy cooling speed, which is beneficial to grain refinement.

Fig. 13 e Metallographic structure at tensile fracture: (aec) Process 1; (d-f) Process 2.


j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2 3129

Fig. 14 e The SEM morphologies and EDS mappings of different regions of the wheel hub: (a) Spoke; (b) Outer rim; (c) Under
the rim; (d) On the rim; (e) Inner rim; (f) EDS mapping of Al, Mg and Si.

The microstructure of the wheel hub is dominated by a-Al the secondary dendrite arm spacing is 38.7 mm and 34.5 mm,
and eutectic Si, and eutectic Si is distributed around a-Al in respectively (Fig. 13 (a)).
granular form. Therefore, the microstructure morphology at From the comparison of tensile properties, it can be seen
different positions of the LPDC aluminum alloy wheel hub is that the tensile strength and elongation of process 2 are higher
not the same. By comparing the spacing of secondary dendrite than those of process 1. By enlarging the fracture position
arms at five locations, it can be found that the spacing di- (Fig. 13 (b) and Fig. 13 (c)), it can be found that the sample
mensions between the outer and inner rims are the smallest. microstructure uniformity obtained by process 1 is signifi-
Because these two zones are located on the edge of the wheel cantly lower than that obtained by process 2. And there are
hub during molten aluminum filling and solidification, with more Si particle segregation and small-size shrinkage defects
thin wall thickness and proximity to the water-cooling chan- in the sample of process 1. In process 2, the number of
nel, a fine grain structure is formed at higher cooling rates. The shrinkage defects in the sample is reduced, and the distribu-
grain size at the spoke is significantly larger than that at the tion of a-Al and eutectic Si is more uniform. The main reasons
other four positions. The secondary dendrite arm spacing at for the improvement of tensile properties are the refinement
the hub obtained by process 1 and process 2 is 55.9 mm and and uniformity of grain structure and the reduction of
48.2 mm, respectively. The solidification sequence of the hub is shrinkage defects. Under the tensile load, the crack tip was
from the top to the bottom inner rim, rim, outer rim, spoke, and first initiated at the tip of the hole defect of the sample and
center. The solidification rate of the spoke is relatively slow and then expanded along the area where eutectic Si accumulates.
the grains have enough time to grow, resulting in the spacing of The microcrack gradually developed into a macroscopic crack,
secondary dendrite arms in this position being significantly which eventually lead to the fracture of the sample. In addi-
larger than that of the outer rim, rim, and inner rim. tion to the pores inside the sample, the segregation of eutectic
Fig. 13 displays the metallographic observation of the Si particles is also the main reason for the decrease in tensile
fracture location of the tensile specimens cut at the rim. At properties. The area where eutectic Si is concentrated is hard,
low multiple observation, the microstructure morphologies brittle, and poor toughness, so the sample tends to fracture in
obtained under the two processes are almost the same, and the area where there are many shrinkage defects and Si
3130 j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2

Fig. 15 e The fracture morphologies of tensile specimens in the rim region under different LPDC processes: (a) Process 1;
(b) Process 2.

particles are biased. The non-uniform distribution of Si par- matrix. While the Mg element was distributed uniformly in
ticles and shrinkage defects are the main causes of the the matrix.
decrease in tensile properties of the alloys. Fig. 15 compares the fracture morphologies of the tensile
specimens in the rim region under different LPDC processes. It
3.6. Microstructure analysis can be seen from Fig. 15 (a) that there are a few cleavage steps
and dimples in the fracture morphology, and the size of the
Fig. 14 compares the SEM microstructure at different positions dimples is small, which illustrated the fracture mode of the
of the hub. As can be seen from the picture, the aggregation tensile specimen was the mixed tough-brittle fracture. The
area of eutectic Si at the spoke has a wide size, and the morphology of dimples and cleavage is similar to that
morphology of Si particles is irregular and long, with a size mentioned in Kong's [36] study. The result indicates that the
distribution of 3e8 mm. The size change of the secondary toughness of the sample is poor. Enlarging the cleavage step
dendrite arm at different positions is almost the same. area, as shown in Fig. 15 (b). Some small-size shrinkage de-
In the outer rim area, there are a few small shrinkage fects and Si particles can be seen on the surface of tensile
holes, and the shape of the shrinkage holes is an approxi- fracture. The above characteristics further confirm that
mately circular or irregular strip (Fig. 14 (b)). In addition, the shrinkage cavity and eutectic Si particle aggregation are the
size of the eutectic Si particle segregation region is main reasons for the reduction of toughness during the tensile
decreasing. In the rim region, the microstructure is similar to process. Under the water-cooling process of 400 L/h for 140 s,
that of spokes and outer rim, but the size of a-Al cell crystal the tensile fracture morphology of the sample is displayed in
decreases, which is related to the solidification conditions in Fig. 15 (b). The number of dimples on the specimen surface
this region. Fig. 14 (e) shows the microstructure at the inner increased significantly. The area in the red dashed box is
rim which has the smallest secondary dendrite arm size. The enlarged, and Si particles and small dissociation steps can be
size of a-Al cell crystal ranges from 10 to 30 mm. Under the seen. The change in fracture morphology indicates that the
three processes of mold-filling, solidification, and cooling, the fracture toughness of the sample is improved under the pro-
microstructure of each part of the hub has great differences. cess parameters. At a larger water-cooling flow rate, the so-
During the mold-filling process, the molten A356 alloy at the lidification rate of molten aluminum is accelerated, the
inner rim has the longest flow distance in the mold, and the spacing of secondary dendrite arms is reduced, and the dis-
temperature of the molten is lower than the other parts. The tribution of a-Al and eutectic Si particles is relatively more
solidification rate of this part is faster than that of other areas uniform, resulting in the simultaneous increase in strength
because the inner rim of the wheel is thinner and the effect of and toughness at this position of the hub.
cooling water during the pressure-holding solidification
process. The energy dispersive spectroscopy (EDS) mapping
of Al, Mg, and Si was added in Fig. 14. As shown in Fig. 14(f), 4. Conclusions
the element distributions of Al, Mg, and Si at the inner rim
were exhibited. The size of cellular dendritic crystals ranged The LPDC of the A356 aluminum alloy wheel hub was simu-
from 20e50 mm. The Si particles distributed surround the a-Al lated by ProCAST, and the influence of pressure holding time
j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2 3131

and cooling processes on the quality of the wheel hub was references
compared. With the casting parameter optimization, two
group LPDC parameters were chosen for the trial-
manufacturing of the wheel hub, namely process 1 (pressure [1] Zhao YQ, Zhu MM, Lin F, Xiao Z, Li HQ, Deng YJ. Thermal
hold time: 140 s and water cooling: 300 L/h for 150 s), process 2 modal analysis of novel non-pneumatic mechanical elastic
(pressure hold time: 140 s and water cooling: 300 L/h for 150 s). wheel based on FEM and EMA. AIP Adv 2018;8(1):015229.
The mechanical properties and microstructure of wheel hubs [2] Duan YC, Zhang FF, Yao D, Hu JH, Dong R, Zhao X, et al.
Multiscale fatigue-prediction method to assess life of A356-
were analyzed in detail.
T6 alloy wheel under biaxial loads. Eng Fail Anal
2021;130:105752.
(1) The pressure holding time has a great effect on the [3] Gu GT, Zheng HR, Tong LY, Dai YX. Does carbon financial
casting quality of the wheel hub. From the simulation market as an environmental regulation policy tool promote
result, the overall defects of the hub are decreased at a regional energy conservation and emission reduction?
pressure hold time of 140 s. When the water-cooling Empirical evidence from China. Energy Pol 2022;163:112826.
[4] Tian SS, Dai Z, Dai M, Chen WQ, Zhang Q. Comprehensive
process was 400 L/h for 140 s, the wheel hub first
assessment of energy conservation and CO2 emission
starts to solidify at the outer rim, and then the wheel
reduction in future aluminium supply chain. Appl Energy
hub solidified in sequence. At this time, the casting 2022;305:117796.
quality of the wheel hub was better, whereas other [5] Sun X, Meng FR, Liu JR, Mckechnie J, Yang JX. Life cycle
processes were prone to shrinkage cavities and porosity energy use and greenhouse gas emission of lightweight
defects. vehicle-A body-in-white design. J Clean Prod 2019;220:1e8.
(2) Under the cooling process of 300 L/h for 150 s, the yield [6] Kumar S, Tewari SP, Rajak U, Dasore A, Verma TN. Properties
evaluation of A356 and A319 aluminium alloys under
strength and tensile strength of the rim were 98.9 MPa
different casting conditions. Mater Today Proc
and 160.7 MPa, respectively. As for the cooling condition 2022;49(2):523e8.
of 400 L/h for 140 s, the yield strength and tensile [7] Jiang WM, Fan ZT, Liu DJ, Liao DF, Dong XP, Zong XM.
strength of the rim increased to 100.9 MPa and Correlation of microstructure with mechanical properties
178.9 MPa, which is 2.0% and 11.3% higher than those of and fracture behavior of A356-T6 aluminium alloy fabricated
process 1. The fracture elongation also increased from by expendable pattern shell casting with vacuum and low-
3.4% to 6.6% when the wheel hub was fabricated by pressure, gravity casting and lost foam casting. Mat Sci Eng A
2013;560(10):396e403.
process 2.
[8] Shahane S, Aluru N, Ferreira P, Kapoor SG, Vanka SP.
(3) The secondary dendrite arm spacing at the rim and Optimization of solidification in die casting using numerical
spoke were 38.7 mm and 34.5 mm under the cooling simulations and machine learning. J Manuf Process
parameter of 300 L/h for 150 s and 400 L/h for 140 s, 2020;51:130e41.
respectively, which indicates that the microstructure of [9] Liu WP, Peng T, Kishita Y, Umeda Y, Tang RZ, Tang WCJ, et al.
the wheel hub was more refined under the condition of Critical life cycle inventory for aluminium die casting: a
lightweight-vehicle manufacturing enabling technology.
process 2. Due to the larger cooling water flow of pro-
Appl Energy 2021;304(15):117814.
cess 2, the solidification rate of liquid aluminum
[10] Luo AA, Sachdev AK, Apellian D. Alloy development and
increased and the solidification time shortened, which process innovations for light metals casting. J Mater Process
was conducive to the reduction of secondary dendrite Technol 2022;306:117606.
arm size. [11] Mattia M, Timelli G, Bonollo F, Garagnani GL. Impact
behaviour of A356 alloy for low-pressure die casting
automotive wheels. J Mater Process Technol
2009;209(2):1060e73.
[12] Sun JY, Le QC, Fu L, Bai J, Tretter J, Herbold K, et al. Gas
Fund projects Entrainment behavior of aluminium alloy engine crankcases
during the low-pressure-die-casting process. J Mater Process
Supported by Natural Science Foundation of Hebei Province of Technol 2019;266:274e82.
China (E2021203138). [13] Wang RJ, Wu SP, Chen W. Mechanism of burst feeding in
ZL205A casting under mechanical vibration and low pressure.
Trans Nonferrous Metals Soc China 2018;28(8):1514e20.
[14] Ou J, Wei CY, Cockcroft S, Maijer D, Zhu L, Lateng A, et al.
Declaration of competing interest Advanced process simulation of low pressure die cast A356
aluminum automotive wheels-Part I process
The authors declare that they have no known competing characterization. Metals 2020;10(5):563.
financial interests or personal relationships that could have [15] Ou J, Wei CY, Cockcroft S, Maijer D, Zhu L, Lateng A, et al.
Advanced process simulation of low pressure die cast A356
appeared to influence the work reported in this paper.
aluminum automotive wheels-Part II modeling methodology
and validation. Metals 2020;10(11):1418.
[16] Jiang JF, Zhang Y, Wang Y, Xiao GF, Liu YZ, Zeng L.
Microstructure and mechanical properties of thixoforged
Acknowledgements
complex box-type component of 2A12 aluminum alloy.
Mater Des 2020;193:108859.
This work is financially supported by the Hebei Natural Sci- [17] Jiang JF, Yan J, Liu YZ, Hu GQ, Wang Y, Ding CJ, et al.
ence Foundation (No. E2021203138). Investigation on heat treatment of large-sized and complex
3132 j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 3 ; 2 4 : 3 1 1 8 e3 1 3 2

AlSi9Mg aluminum alloy components formed by squeeze [27] Erzi E, Gursoy O, Yuksel C, Colak M, Dispinar D.
casting. J Alloys Compd 2022;924:166504. Determination of acceptable quality limit for casting of A356
[18] Duan YC, Zhang FF, Yao D, Tian L, Yang L, Guan YP, et al. aluminium alloy: supplier's quality index (SQI). Metals
Numerical prediction of fatigue life of an A356-T6 alloy 2019;9(9):957.
wheel considering the influence of casting defect and mean [28] Wang LD, Li XS, Wang C, Wang LM, Cao ZY. Effects of cooling
stress. Eng Fail Anal 2022;118:104903. rate on bio-corrosion resistance and mechanical properties
[19] Dhisale M, Vasavada J, Tewari A. An approach to optimize of Mg-Zn-0.5Ca casting alloy. Trans Nonferrous Met Soc
cooling channel parameters of Low pressure Die casting China 2016;26:704e11.
process for reducing shrinkage porosity in Aluminium alloy [29] Agrahari S, Panda I, Patel FM, Gupta M, Mohanty P. Effect of
wheels. Mater Today Proc 2022;62(6):3189e96. cooling rate on microstructures and mechanical property of
[20] Viswanta A, Manu MV, Savithri S, Pillai UTS. Numerical Al 1230 alloy in a sand casting process[J]. Mater Today Proc
simulation and experimental validation of free surface flows 2020;26(2):1771e5.
during low pressure casting process. J Mater Process Technol [30] Azqadan E, Uramowski J, Roostaei AA, Behravesh BS,
2017;244:320e30. Javaid A, Williams B W, et al. The effect of cooling rate and
[21] Jadhav AR, Hujare DP, Hujare PP. Design and optimization of degassing on microstructure and mechanical properties of
gating system, modification of cooling system position and cast AZ80 magnesium alloy. Mater Sci Eng A Struct Mater
flow simulation for cold chamber high pressure die casting 2022;844:143176.
machine. J Mater Process Technol 2021;46:7175e81. [31] Yavuz H, Ertugrul O. Numerical analysis of the cooling
[22] Li Y, Liu JX, Zhang Q, Huang WQ. Casting defects and system performance and effectiveness in aluminum low-
microstructure distribution characteristics of Aluminium pressure die casting. Int J Metalcast 2021;15(1):216e28.
alloy cylinder head with complex structure. Mater Today [32] Fan P, Cockcroft S, Maijer D, Yao L, Reilly C, Phillion A.
Commun 2021;27:102416. Examination and simulation of silicon macrosegregation in
[23] Zhang C, Fu Y, Wang H, Hao H. Multi-objective optimization A356 wheel casting. Metals 2018;8(7):503.
of process parameters during low-pressure die casting of [33] Huang JM, Zhao HD, Chen ZM. Microstructure and properties
AZ91D magnesium alloy wheel castings. China Foundry of A356 alloy wheels fabricated by low-pressure die
2018;15(5):327e32. casting with local squeeze. J Mater Eng Perform
[24] Christy JV, Arunachalm R, Mourad AHI, Krishnan PK, Piya S 2019;28(4):2137e46.
Al-Maharbi M. Processing, properties, and microstructure of [34] Fan P, Cockcroft S, Maijer D, Yao L, Reilly C, Phillion A.
recycled aluminium alloy composites produced through an Porosity prediction in A356 wheel casting. Metall Mater
optimized stir and squeeze casting processes. J Manuf Trans B 2019;50(5):2421e35.
Process 2020;59:287e301. [35] Kaba M, Donmez A, Cukur A, Kurban AF, Cubuklusu HE,
[25] Hamasaiid A, Dargusch MS, Dour G. The impact of the Birol Y. AlSi5Mg0.3 alloy for the manufacture of automotive
casting thickness on the interfacial heat transfer and wheels. Int J Metalcast 2018;12(3):614e24.
solidification of the casting during permanent mold casting [36] Kong DC, Sun DZ, Yang BC, Qiao HB, Wei CY, Lang YL, et al.
of an A356 alloy. J Manuf Process 2019;47:229e37. Characterization and modeling of damage behavior of a
[26] Koziel T, Pajor K, Gondek L. Cooling rate evaluation during casting aluminum wheel considering inhomogeneity of
solidification in the suction casting process. J Mater Res microstructure and microdefects. Eng Fail Anal
Technol 2020;9(6):13502e8. 2023;145:107018.

You might also like