No.
SL
ITPreliminaxs 4FlameTest I
Lmateh
stiak
ing
|aiotzodued 3. 2.|
diHL
l A paatih Preliminoy
A SolubilibyExornihion
e Solubikhy Colot
Hk 1:Heof
a
ofteh phinum into in in
the the dil. cold EXPERIMENT
acanc
salt foy Bwnsen Selt HcL water
oian oiYe HLI
is
is oY madiint end
treated flame LYSIS
ANA
Sall-1 SALT
a the
bist
poste
ith out
by a
is (soa),Al,
aloualessgad NoLsmell effenescence olbua No soluble less
Colour
NobziskNo
Na Coapletely
soluble ompletely
smell calaugless chotatexishie OBSERVATION
of to
of often the
zning gas fleme
eqgs -flogaeAbsence
cail h
Sughu theAbsence
Acetate.
absence oY
presence
Sulphite
Absencaaf AbsanceLojof Cult Absence
INFERENCE
of of
of of of
SulghideSud Ba group NHH, Cult
2 Sca N;
I Nityate
2+
No saddish bown WaporAbs ence ef Niite
ifh pumqent small
2A iHle of tho salt is xubbed toite dil Hso Np smel of vineqax Absence of Acetate
and the s mel is noted
3 No byisk efsemvesconce |Absence of Oxalate
Al. H, so. to expe al he iss wing geses
and a pinch of MnO, is added.
Alitle of tha salt i beated itt cenc h.so, No chaackerishi yeoehionAbsewce of cÍBí end r
sA RHle of ha salt i heated sith No yeldish byawn fume Absene of Nibate
cone Hh so, and a papen hall
6A Hle of the salA heated wih Nocharecteyishie zeashioa AbsemLe of CI, B omd
con H, sl. and a pinch af Mn,
2
SL
No. EXPERIMENT OBSERVATION NFERENCE
Systemohe Tests For Anions
PAEPEARA TION OE SopIuY CAR BoNAT ExTAALT
Lpust oi the solt ismied with 2 pohfpe sobd sodim
corbogateia a lo0 al beakay 20 mlde Hlled soateN is odbhit oaditis bailed
tiat._extrat
Aite. of the exfvat is idi fed Athick white ppt presene of Suphate
ith dil HeL hested A H zffunvsCuAL
effeVEA insoluble in conle HcL onfsmel
Lecases and coaled.Ihan Bala Saln ik
ANALYS1s OF CATIDN
Test Foy Ammenhiw) lon
A1Hle of the salt is treatl ita white et Absence of NH
Prepoohion Of Driqinal Solutos
Ahout I qm of the salt is dsolued in
10 of watey in a boling tube.
salt is toeplately saluble group T ahsent
in HcL
2
No ppt Absemce af qzoup 1
3Boil off Hys from the aove so lution presene of
Ctatbd coith lead aatate pagpr)ada drge
of Cane HND, bail ool, add solid NHacL
aad axcesc of NHyoH Soluhion.
Csaßsmaary Teut of Cahihui
Dsolue th qoup IIppt in dil. H4
A jon is onsimel.
bwhich dissalves in enAs.
|AL ioni confimes
obtainod.
3
SALT- 2 SALT ANALYSI5
OBSERVATION INFERENCE
SL EXPERIMENT
No.
ANNDN ANAL YSIS
I Prelimin ary Examination
less
Colouy absence of Cuzt N;2+
1Colout LPYesence of NHt
2 Solubility in cold watez Completely Soluble
Nitale oy Acetate.
3| Solubilty in dil HCI Completely Soluble |absence of qyoup I
4Flame fest:
AlHle af the salt is made inb Nachaacterishie calauAbsenco of Btstc24
Cut
a paste with con HCL and the paste isb flame
kod odueadiat a bumsen flamie by,uing
plaiauan wise 07 a buant maleh shick.
TBeliminary Tesk for Anions
2
A tle of the salt is teated with No byis k efexvascanseAbsence of Co
HCL
Vinagar Snzall esene of acetot Aekal
3 A :Htle of the Salt is ad med aitH No bzisk effervescence Absence of exalote
LH.So to espel allLke issuing gaea
and a pinch of Mnl is added.
4Altle of the salt is hantesith No chaaacferishe xeacho Absene of cLBy
Gonc. HsOn
sA Hle of Hho salf is heated with cone.tA Yaddish bro On fumaAbsence of Nitrate
ond a poper ball
6A :He ofsf the salt is heafod aith n0 chaxacferis fie zeachionAbscoce of cLBy
conc Has0h and a pinch of Mn0z
fSysfemaie Tests Foy Anions Prapeyatiof Na, Coy Extract
iLfort
Aont of Be salt is mìxed aikh lpayt afof puye solid Ssan Canbanate ina lo0ànk.
Boaker. 29 mL dis klla wator i added o it amd bailad for akyat lo minutea t is aaled
and Altexal. The Altexate is allad Ssodfum Catbo nake Eatyact
Red calou tuaning Aatate ik con firmed
. HANO,, heated till sffey vascene ceaseszown on bailing
oole and Hun neit akzed wif6 NHa0 .
The exeess of d Ammonia is boiled off
SL OBSERVATION INFERENCE
EXPERIMENT
No.
this neubal solahas, nautra FeC
soluhon is addid
|Aoalssis of Cahion
est Foy Anmoniwnm lon
LAlHle of the salt s traotod ith No precipifakaa Presencp of NH
Na, cO, salahon
Conimaoy Tas fos Ammonius) lern
Nessley Test
Rronpre cipitate or Precence ef Anmonium
Broun colouy onfrmel.
kddedt anl Neslex Rea4ent
test tube
Resalt
Aniba- CHe coo
Cahioo-NH
Ca Cla SALT |ANALYSI S - 3
ANON ANALYSIS
2Prelininavs Examinaion
Colour Coloyles oy wite absence of Cuzt N; 2t
2 Sdubhy in old Wotey
2
Gmpealy So luble |Presene of NH Nitvate
Acetate
3Sletlty in dil HCI Completely Soluble alosence of qYoup I
4Elen2.Test
btick ved lame pxesene of Ca2t
Ereliminany Tut for Ariord.
No briskeffeyvesee Abance of co'
H
24 HHie of the solt i yubhel oth smeof vinegar Absense of Acetal
5
SL OBSERVATION INFERENCE
No. EXPERIMENT
No btisk effesvsene
Ma,isadld
A H af koa salt i baates hconH So, Aolaurles punzst Presene of hbzil
sodling
noist
ga funing ia
aizdunse wkite fus The qas isic HCL
tet tube
5A le f the salt is heated with con. H, s0,n veddish bzoan fuames Abanco of itrate
and a papearball
4A H of tha salt hented with con Hso, ayeeash
odapinch of Mal, qxeaidh yelle
yellow gaalaningPesene of
blue
Ptegasahen f Sadeum Catbonate Estuat
solid SodiaCasbonale in a loDnl beakar
The fltsate is call Sodiua Caabota Extract
LATION ANALYSLS
Test Foy Amoasiwato las
Absenca of NH
solation
Pyepeyohon of Original Soluhon
Abaut Lam cf Hoa satk dissolvedia Omlof tey iaa boiinatube
gYoup I bsant
salf isconglehely soluble in H
6
INFERENCE
OBSERVATION
EXPERIMENT
2 Hs is added bth Oviginal Solution
No ppt
3Goil off H,s from the above soluhion Ctestl No pot Albsence of qraup TIL
Anth lend acakaka pagasladd adrap of
con HN, baiceol. Add salid NHac
and exceAs of NH 0H soluthon
4T the sbove solahion H,sis pased absence of qyoup L
white ppt
LAngex). AAd salid Nhcl exces of NHeoH
Conhvmalory Test of Cahons
Test Fos atoup
The bite _ppt is dsolved hotdloehe
Lacid ond diwided into 3pashians.
|Absence of Bazt
Na yellaupt
LAbsege ofs2t
2T fhe seond port Caso,soluboois No ppt
addud ol boilel
ite csystallik-ppt Ca2t ooofismed
3 T the thid puat ammoniwm hycdaaxide
Bvick Red Floma Ca2t coakcmed
hcoa HCI in asatah gbss foym a paah
a bugat match Stizk
ReAult
Anion chloride
Cahon - Cot
