gia Tp. Hé Chi Minh ‘ai hoe Bch Khoa p6 AN MON HOC Qué Trinh & Thiét Bi THIET KE THAP CHUNG CAT HON HOP ACETONE - NUGC LOAI THAP DEM NANG SUAT : 1500 (Kg/h) GVHD : V6 Thj Ngoc Tudi SVTH : V6 Ngoc Tiép MSSV : 69902203 Lép : HC99HL, Nganh : Céng Nghé Hoa Ly Nem hoc 2002 ~ 2003MON HOC GVHD : V6 Thi Ngge Tusi MUC LUC LOI MG BAU CHUONGI : GIGI THIEU CHUNG CHUONG2 : CAN BANG VAT CHAT 1. CAN BANG VAT CHAT: 1. Bé thi can bing acetone- nuéc 2. Xée dinh chi sO hdi hvu a) Chi s6 di hvu t6i thiéu b) Chi so héi mu thich hgp I. CAN BANG NANG LUGNG: 1, Can bing nang higng cho thap chung cat: 2, Can bing nhiét ludng cho thiét bi ngung w 3. CAn bing nhiét lugng cho thiét bj am ngudi 4, Cn bing nhiét higng cho thiét bj gia mhiét, CHUGNG 3 : TINH TOAN THIET BI CHINH I. DUONG KINH THAP: 1. Butdng kinh doan cit: 2. Bung kinh doan chung: Il. CHIRU CAO THAP: IM. TRO LUC CUA THA’ CHUONG 4 : TINH TOAN CO KH I. TINH CHIEU DAY THAN THAP Il. TINH DAY, NAP THIET BI 1.Nap 2. Bay Il. TINH DUONG KINH VA BULON ONG DAN 1. Ong din hoi 2. Ong nhap ligu: 3. Ong din léng: 4, Ong hoan lu: CHUONG 5 : TINH TOAN THIET BI PHU I. THIET B] NGUNG TY SAN PHAM BINH I, THIET BI GIA NHIET NHAP LIEU II, NOIDUN IV. BOM CHUONG 6 : TINH GIA THANH THIET BI TAI LIEU THAM KHAO SVTH: Vo Ngoc Tiép - Trang 2- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus LOI GIGI THIEU Trong thy té, chiing ta str dung rat nhiéu dang hod cht khée nhau: hén hgp nhiéu chit hay dan chat tinh khiét, Nhu cu vé mot loai hod chat tinh khiét cting rat lén, Qué tinh 6 thé dap ting phan ndo dé tinh khiét theo yéu cdu lA chung eft: 18 qua tinh tach ede cu tit trong hdn hgp ling ~ Ing, hay hén hgp ling — khi thnh ede cau tit riéng biét diva vao 46 bay hoi khéc nhau cita chiing. Va adi vdi hé acetone ~ nude, do khéng c6 diém ding phi nén c6 thé dat duge bat ky 6 tinh khiét theo yéu cdu nbd qué tinh chung eft Nhiém vy thiét ké: tinh toan hé thng chung luyén lién tue dé téch hn hgp hai cu tit: acetone — nude vdi cde sé ligu sau day: Jing suat sin phdim dinh : 1500 Kg/h ‘ng 46 sin phi'm dinh : 95% theo khdi lvgng Néng d6 nhap liéu : 30% Ap suat lam viée : 4p sudt thudng. SVTH: Vo Ngoc Tiép - Trang 3- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus CHUONG 1 :G1I61 THIEU CHUNG 1. Gigi thigu so b6 = Acetone oé cOng thife phan tit : CH;COCH, .Khéi lugng phan tit bang 58 ave Acetone li chit I6ng s6i 56.1°C, tan v6 han trong nuée, né 14 dung mdi cho nhiéu chat hitu co... N6 hod tan tt td axetat, nitro xenluloz, nhifa phenol focmandehyt, chat béo, dung méi pha son, mye in &ng déng. Acetone la nguyén liéu dé téng hop thily tinh hitu cd. Ti Acetone cé thé téng hgp xeten, sumfonal (thud ngii), cdc halofom.... Tinh chat hod hoe Cong hgp véi natri bisuntit: on (CH,COCH, + NaHSO;-» CH,- C - SO,Na CH, (1-metyl-1-hydroxi etan sunfonat natri ) C6ng hop axit HCN OH CH;COCH, + HCN > CH; -C -CN i cH, (pH 4-8) Phan ting ngung w on 0 CH,-CO-CH, + HCH,C=0 — CH,-C-CH-C-CHy CH, CH, (4-oxy-4-métyll-2-pentanon) Acetone khé bj oxi héa bdi thud thit Pheling, Toluen, HNOses, KMnO« Chi bj oxi héa bai hn hgp KMnO, + H2SO,, Sunfécrémic K,Cr0; + H,SO,. Bj gay mach cacbon, Phan ttng khit hod: CH,COCH, + Hy > CH;CHOH-CHs, Digu ché: Oxy héa nugu bac hai: CH,CHOH-CH; ~> CH,COCH; + H,0 Theo phuong phap Piria : nhiét phan mudi canxi cilia axit cacboxylic: (CHCOO),Ca > CH;COCH; + CaCO; Tit din xudt co magie: SVTH: Vo Ngoc Tiép - Trang 4- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus Br CHsC-Cl_ + CHy-MgBr-> CHs-C-CHs + Mg ° ° a Phan tng Kucherév CHs-CaCH + HO —#8°H, CH;-C-CHs ° 2. Cong nghé chung cat hén hgp Acetone —Nuée : Ta ¢6 Acetone 13 mOt chit lng tan vO han trong nude va nhiét d6 sdi cila Acetone (56.1 0C 4 760 mmHg) va Nude (100 0C 4 760 mmHg) : 1a kha cach xa nhau nén phuong phdp hiéu qua nhdt dé thu dite Acetone tinh khiét 1a chung eft phan doan dya vao dQ bay hoi khéc nhau cia cdc cu tit trong hin hgp. Chon logi thép chung cat va phuong phdp chung cat : Chung c&t1a qué tinh phan tach ede hn hgp léng thanh ede cfu tit riéng bigt dya vao sy khée nhau vé d6 bay hoi cia chting ( hay nhiét d6 s6i)), bing céch ap di lap tai nhiéu Min qué winh bay hoi — ngung tu, trong dé vat chat di tit pha ling vao pha hoi hode nguge lai D6i vei chung eft ta c6 hai phung phap thyte hién Chung eft don gidn (ding thiét bj hoat ddng theo chu ky): Phung phép nay sit dung trong 4c triting hyp sau : Khi nhiét d6 s6i cla cdc edu tir kh. Khi khong d0i héi sin phim c6 a6 tinh khiét cao Tach hén hop léng ra khéi tap chat khong bay hoi. au vit. Tach so b6 hn hep nhiéu Chung eft lién tue hdn hgp hai cfu ti (ding thiét bj hogt dng lién (uc): 1a qua trinh dude thie hién lién tue, nghich dong, nhiéu doan, Ngodi ra cdn c6 thiét bj hoat dong ban lién tue. Trong truding hgp nay, do sin phdm 1a Acetone — vai yéu cu cé 46 tinh Khiét cao khi sit dung , cOng vdi hdn hgp Acetone — Nude lA hn hyp khong c6 diém ding phi nén chon phung phap chung cft lién tuc 14 hiéu qua nit. Chon loai thép chung cat : C6 rt nhigu loai thip dude sit dung, nhung du c6 chung mot yéu cdu ed ban 1 dign tich bé mat tiép xvie pha phai ln, diéu nay phy thude vo dé phan tan cla mt liu chit nay vao hu chat kia Ta khdo s4thai loai thap chumng ct thuting ding Ia thap mam va thép chém Thap mam gém than thép hinh try, thing ding, phia trong 6 gin cdc mam cé cu tao khdc nhau, trén d6 pha léng va pha hai dude cho tiép xtic véi nhau. Gém c6 : mim chép, mam xuyén 15 , mdm van. Thudng sit dung mam chép . Thap chém 14 mO¢ thép binh tru, gém nhiéu doan n6i vdi nhau bing mat bich hay han . Vat chém duge a6 dy wong thép theo mot hay hai phutsng phdp : x€p ngdu mhién hay xép th ur SVTH: Vo Ngoc Tiép - Trang 5- MSSV:69902203pO AN MON Hoe GVHD : Vo Thi Ngoe Tus Chon loai thap dém dé thye hién qué trinh chung eft vi nhiing wu diém sau Cau tgo don gidn Trd lye thifp Tuy nhién thép dém cing 6 nhude diém 1a Hiéu sudt thap 6 én dinh kém, ‘Thuyét minh quy trinh edng nghé: Hén hgp Aceton — nutéc 6 néng a6 Aceton 30% (theo s& mol), nhiét 46 khoang 27°C tai bén chifa nguyén liéu (1), dude bom qua thiét bi gia nhiét ( trao 446i nhit vai sin phdm déy)(5). Sau d6 duige dita dén thi€t bj dun néng nhap Tiéu(6) bing hoi nude bao hda, @ day nhp ligu dude dita d€n nhiét d6 soi va duge dita va0 thap chung c4t(11). Trong thép, hoi di tir dudi lén gap chit ling tit én xuGng. 6 day c6 suf tiép xiic va trao déi nhiét gitta hai pha vdi nhau, Pha lng chuyén dong trong phdn chung cing xu6ng dudi cng gidm ndng 46 cfu tit d& bay hoi vi da bj néi dun 16i cudin ede edu tit. Nhi€t d6 cng lén én cang thd'p , nén khi hoi dit dudi lén thi cfu ti c6 nhigt dd si cao 18 nude sé ngung tu lai, cud eng trén dink thap ta thu dutge hén hdp e6 edu ti Aceton chiém nhiéu nhdt (95% theo phn mol ), Hai nay di vao thiét bi ngung tu(14 ). Mot phn léng ngung dutge héi luru vé thap, mt phan chat lng ngung di qua thiét bj Kim ngudi sén phém dinh (17 ). Mot phan cfu tit c6 nhiét 46 s6i thap duge b6c hai, cn lai cu tit e6 nhiét 46 s6i cao trong chat léng ngay cdng tang. Cuéi cing, d day thap ta thu dude hén hgp léng gém hau hét cu tit khé bay hoi (nude). Hn hdp léng 4 day c6 ndng dd Aceton 1a 3% theo phan mol, cdn Igi i nude, Dung dich ling diy thép dude dun tai ndi dun (12) bic hai cung ep lai cho thap dé ti€p tye Lm viée, phan cdn Igi trao d6i nhiét vai nh§p ligu. Hé théng lam viéc lién tuc cho ra sin phdm dinh la Aceton, sin phdm day sau khi trao déi nhiét vdi nhap liéu dugc thai bé. SVTH: Vo Ngoc Tiép - Trang 6- MSSV:69902203pb} AN MON HOC GVHD: V6 Thi Noe Ts S046 guy trinh cong ngh@ chung eft hbu hgp Aceton — nude: os SVTH: Vo Neoe Tig Trang 7 MsSv68902203MON Hoe GVHD : Vo Thi Ngoe Tus G_2: CAN BANG VAT CH. I. Can bing vat chat: S6 ligu ban dau: Nang sudt 1500kg/n Néng d6 dung dich ddu: xp= 30% mol Néng 46 dinh: Xp = 95% mol Nong dé dung dich day: xw = 3% mol Céc ky higu: FP lwgng nhap liéu ban dau (kmol/h), (kg/h) D,D: hugng sin phdm dinh (kmol/h), (kg/h) W,.W: lugng sin phdm diy (kmol/h), kg/h) xp néng d} mol acetone trong nh4p liéu Xp, néng d6 mol acetone trong sin phdm dinh xy. ndng 49 mol ciia acetone trong sin phim day Phuong trinh cin bing vat chit: F=D+W ay F xp= D xp + W xw Q) Tinh kh6i hvgng trung binh: Mor =Xe Mi + (I-Xe) Mz =0,3x58+(1-0,3)18=30kg/kmol Man =Xp Mi + (1-Xp) Ma =0,95x584(1-0,95)18=56kg/kmol Maw =Xw Met (1-xy) Mz =0,03x58+(1-0,03)18=19,2kg/kmol Sudt lugng sin phim inh: D_ = 1500 96.786 (kmol/h) D 0 F = 26,786 + W F*0,3 = 26,786 * 0,95 + W * 0,03 F=91,27kmol/h Gidi hé phuong tinh trén ta duge:{ |" ” LW = 64,485kmol/h Tir (1) va (2) ta of hay [PF =2738.13¢Ke/4) W = 1238.12(Kg/h) 1. Dé thi cn bang acetone- nude: Thanh phan c4n bing léng (x)- hai (y) tinh bang phan % mol va nhigt d sOi ctia hén hgp 2 cu tit ¢ 760 mmHg x jo [s [10 [20 [30 [40 [so [eo [70 [80 [90 | 100 SVTH: Vo Ngoc Tiép - Trang 8 MSSV:69902203pé AN MON HOC GVED : V6 Thi Ngoc Tusi y |o [60.3] 72 | 80.3 | 82.7] 84,2] 85,5 | 86.9 | 88,2 | 90.4 | 94,3 | 100 t_| 100 | 77,9 | 69,6 64,5 | 62.6 | 61.6 | 60,7 |59.8 59 | 58.2 | 57.5 | 56,9 ‘Vé dé thi y-x: Dé thi cn bing aceyone- muée 100 | | 80 z (| 4 60 4 # 4 a 20 ° ° 2 © 4080100 ‘Thanh phan pha ling Dé thi Tay * 400 RY Dé 80 \ thi T- xy 80 SS 70 AA 60 40 30 20 10 ° 0 10 20 30 40 50 60 70 80 9 100 SVTH: V6 Ngo '$V:69902203pO AN MON Hoe GVHD : Vo Thi Ngoe Tus 2, Xe dinh chi sé hdi lu thich hop: a) Chi 6 hdi lau 16% thidu: Dudng cin bang vé theo sé liéu thyc nghiém cé khodng 16m nén dé xdc dinh Ruy, ti A(0,95;0,95) ve AB tiép xiic duting can bing cit true tung tai diém 6 tung 6 géc 18 0,65. Ta co’: Re: qo 865 > Rn = 0,462 Rm : oe “ b) Chi sé hdi lu thich hop: Cho ede gid tri Rx; > Rxpin d€ tim ede gid ti tung dQ Bi tong ting va ve ede dung néng 46 Him viée cia doan luyén tng véi cdc gid trj Bids : Bi= Rx, +1 Tim cde diém a ( y= x= xp ), b( y= x= xw ) VA dung x = xp ( song song voi true tung ). Cit mdi gid tri Bi ta vé duge duting néng d6 lm vige cia doan luyén va doan chung . Nhu vay tng vdi mdi gid tri Ry ta 06 s6 don vi chuyén khdi chung twong tng la my. Ta c6 bang sau : Ry Bi my m,(Rgt1) 0.600 [0.594 [11.139 | 7.2834 0.785 |0.532__|8.595__| 7.5321 0878 [0.506 [5.934 | 6.0881 0970 [0.482 |5.94 | 6.7318 1.063 |o460 | 6.313 | 7.7737 SVTH: Vo Ngoc Tiép - Trang 10- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus 1.155, 5.928 | 8.0018 ‘Thé tich thap A V=f*H fit dién thap, H : chiéu cao lim viée oda thp, m Ta biét tiét dién cila thép ti 18 thudn vdi Iugng hoi di trong thap, ma Iwgng hoi lai tf 16 thudn véi higng I6ng héi hfu trong thap, nh vay ti€t dién thép tilé vai hugng hdi luu . Tela f~(R,+1)* GD Trong mét diéu kién lim viée nhat dinh th) Gp 1a khong déi, nén f~(R,+ 1). Can chiéu cao thép ti 1é véi sO don vj chuyén khéi H ~ m, , nén cui cing ta 6 thé viet PH ~ m, (Ry +1) Tit d6 ta sé lip dude su phu thude gitta Ry _m, * (R, +1). M6i quan hé ny s cho ta tim duge mét gid trj Rx mA thé tich eila thigt bj chung edt ting vai nd 1a ti Ry. Ve dé thi quan hé gitta (m,,*(Rx; + 1) _ Rx) dé Om Rey : TZ Duidng lam vige : Phuong trinh dung lam viée eta phn edt : D 26.786 2.267x -0.038 IL. Can bang nang hidng: 1. Can bling nhigt lugng cho thép chung cat: Phuong tinh cin bing nang lygng QW Qp2+Qn=Qy+ Qt Qxq2+ Qnee * Nhiét lugng do hén hgp ddu mang vio Qe(I/n) SVTH: Vo Ngoc Tiép - Trang 11- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus QF Cote Trong a6: F= 2783.13(Kg/h) ty = 62.5°C (Nhiét 46 Cp: Nhiét dung rién, te = 62.5°C + Cyyse = 4188.265(1/Kg.06) Caccune = 2313.125(U/K 2.46) Ces XEX Cacctone + (1X F) x Cre 0.58 x 2313.125 + (I ~ 0.58) x 4188.265 = 3100.684 (/Ke.d6) => Qp = 2738.13 x 3100.684 x 62.5 = 0.53 x 10” (ih) ao cia hén hgp dau : 8 trang th = 147.395(kW) ‘* Nhiét lugng do hai at mang vao thap Qns(J/h) Qh2 = Dako = Dot + C262) Dang hoi nue 6 As 2at, r) = 2208 (kI/Kg) , t° = 119.6°C TC; : t° va Nhiét dung riéng cia muéc ngung (J/Kg.d6) * Nhiét dng do liu litdng Iéng héi htu mang vé Qn=QexCRx te Trong Ca = Cp : Nhiét dung riéng ca sin phdm dinh ty? = 57.5°C + Caceion = 2296.875 (1/Kg.dd) Crete = 4188.125 (W/Ke.d6) Cp = CR = Xp X Caccton + (1 =X p) X Crass |.984 x 2296.875 + (1 - 0.984) x 41 88,125 327.135 (KG) = 1350 (Ke/h) Gp=DxR=1500x 0, te=tp = 57.5°C, => Qa = 1.806 x 108 (Ih) = 50.18(KW) lugng do hoi mang ra d dinh thap Q, Q)= DUR) x20 Trong dé: A : Nhiét Iudng riéng ciia hai é dinh thap © Nhi p= Rasctone Xp + ArseaeX (> Yn) Pp = 0.984 Aacetone = Tacetone + th X Cacetone Arsuse = Trade + to X Cruse sc Taccine = 523.35 (KI/Kg) Tyas = 2426.77 (KJ/Kg) => Anus = 2667.59 x 10° (Ke) SVTH: Vo Ngoc Tiép - Trang 12- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus Ancctone = 655.42 x 10° (I/Kg) => Ap = 687.614 (kI/Kg) => Q, = 1.96 x 10° (ih) = 544,361 (kW) © Nhiét lugng do sin phém day mang ra Qw: Trong dé: W = 1238.12 (Kg/h), xw=0.091 ty = 85°C = Cacctone = 2386.25 (I/Kg.d6) Cruse 4200 (J/Kg.d6) 034.054 (I/Kg.d0) 0.424 x 10° (J/Kg) = 117.93 (kW) © Nhigt lugng tn that ta ra mOi truing xung quanh Qxq2! Qxer = 5% x Qn2 Vay: Luong hoi dét can thiét dé dun s6i dung dich 6 day thap: Qh2- Qxq2= Qy + Qw — Qr- Qe + Qy~ Qe Qa. 0.95% rp = 197.51 (Kghh) 2. Can bang nhigt lugng cho thiét bj ngung tu: Negumng ty hodn toan : D(L+R)x m=Gy x C,x(%— th) Trong a6 vto: Nhit 6 vao va ra eta mude Lim lanh Chon nhiét d6 vao va ra eila nude lam lanh Ia: t = 27°C th =40°C = 335°C = Tacetone = 521.46 (KI/Kg) =D > ti2= True = 2425.60 (KI/Kg) => ty = DX acetone + (I -¥p) X Crass = 551.93 x 10° W/Kg) Sudt lvgng nude edn tiéu wn: DxR+Dxey _ 1500x(0.9 +1)x551,963x1000 Coxe) 4180.94x(40—27) 3. Can bang nhigt lugng cia thiét bj lam Ignh: Phung trinh cén bing nang lvgng : D (tp + Cp x (ty’=t2’)) = Gys x Cy X (-t) =G, = 28940.87 (Kg/h) t7=57.5°C + Nhiét d9 vao eta sin phim dinh '=30°C + Nhiét dé ra ciia sin phdm dinh, t}=27°C + Nhiét dé vao ciia mféc 1am lanh. 40°C = Nhiét d6 ra ca nuéc Lim lanh. ty = 33.5°C + Nhiét dé trung binh cia nue lam lanh. SVTH: Vo Ngoc Tiép - Trang 13- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus = 4176,625 (I/Kg.dd) 5 33.5°C Crccone =2252.190/Kg.d0) 8 t = 32 = 30 Cy = 4177.625 (WK g.dd) 3 =43,75°C {oo = 2284J/Kg.do) th = 563168(J/Kg.do) Lugng nude cin ding Du “1 Gy = LEG o* Coltte) _ 17999. 684(K em) Catt) Can bing ning lwgng cho thiét bi gia nhiét (tn dyng nhiét sin phdim 4: Dang nhiét sin phim day dé gia nhiét cho nhap ligu, cI 3 3.75°C on nhigt 46 ra eda sin phém day a 45°C Qu = Gy.Cu.(85-45) = 0.344x4034.05x(85-45) = 55508.825(W) Gif sit nhigt 46 mat mat ra méi truting 1A 40% => Qu’ = 95%.Qw = 46131 (W) Nhiét 46 ra ea nhp ligu 12 $5508,528 = 2 27 = 41.13°C 0.76x3100.684 SVTH: Vo Ngoc Tiép -Trang 14- MSSV:69902203DO AN MON HOC GVHD : Vo Thi Ngoe Tuoi CHUONG 3: TINH TOAN THIET BI CHiNH I. Dung kinh thap: ay \113600.0, Trong d6: Vy, Iugng hoi trung binh di trong thap(m’/h) 6c dO hoi trung binh di trong thap(an/s) Vi luigng hoi va lugng léng thay Adi theo chiéu cao thép va kh4c nhau trong mdi doan nén ta phai tinh dutng kinh trung binh riéng cho tiing doan: chung va cat. 1, Dudng kinh doan eft: Duong kinh thap dude xc dinh theo cOng thie: D= Xptky 0.34095 2 2 Né&ng 6 trung binh cila pha hoi theo phutong trinh duting lim viée Y m70.474x 40,5=0.796 Nhigt 9 trung binh cia pha Ing, pha hoi theo gidn dé T-x 625» 559°C ¥ n=0.796 > t=65°C Khi higng mol trung binh, khéi lugng riéng cia pha hoi M a=Y oe Myt(1-Y ia)-Mu=49.84(kg/kmol) = 0.625 Néng 46 trung binh cila pha léng: x’p: 797(kg/m°) Khdi lugng riéng cla pha Ing x'y=0.625-> x,' = 0.843 phan khoi lving 9% [Pe = 747. kg/m? Pq =983.45kg/m? Lugng hoi trung binh di trong doan edt: a+: 2 * go: lugng hoi ra ca sin phdm dinh g0=GatGp= D (Ret 1)=2850kg/h * gy: Iugng hoi di vao doan eat: £:-G,+Gp=G,+Gp=Gi+1500 Lugng hai g:, hiim Ivong yi, lung lng G, duge xéc dinh theo: a SVTH: Vo Ngoc Tiép - Trang 15- MSSV:69902203MON HOC GVHD : V5 Thi Ngoc Tus 8:=6,+D BY, =Gx+Dx, (=x, Bit = Bale nstayrt(1-¥iTa te 1 Yot (I Yo My Tai 625°C 2 516.285(Ki/ ke) 1, = 2249,882(Ki/ kg) = 521.257(kj/ kg) r, = 2425.466(kj/ kg) 'g) = 2107.83¢kg/h) y, = 0.867 1 = 745.99(Kj/ kg) G, ~ 607.83¢k8/h) Tai ty=57.5°C > { Gidi hé trén ta duge: Do dé: gen Se = 2478.915(kg/h) Van t6c hoi di trong thap: a \ox6 Ly oa Pot Be =A-L7: [2Va Paw Ho) yoas ous Py ) | iy) Paw J @, :T6c dO bit d4u tao oho tueng(m/s); o,:BE mat riéng cia dém(m*/m*):VcThé tich ty do céa dém(m'/m'); g: Gia tc trong trudng(m/s’); G,,G,: Litgng ling va ligng hai trung binh(kg/h); 2,4.P,9Kh6i htgng trung binh cia ling va cia hoi(kg/m’); 4,,1,:B9 nhdt cia pha Ing d nhiét 46 trung binh va 6 nhdt ciia nude 6 20°C(Ns/m’) A= 0.125 Pye» = 1.797 (Kgim’) Su» = 776.39 (Kg/m') Chon dém vong Raschig bing sit, kich thudc 25 x 25 x 3 (mm) 81=195(m?/m') Cae thong sO dém: | yg = 0.75(m3/m°) py = 600K gf m°) 59 > 1, = 0.2316 x 10° (Ns/m’) 607.83 (Kg/h) = 0.169 (Kg/s) Gy = 2478.915 (Kg/h) = 0.689 (Kg/s) Pr = 1000 (Kg/m*) wi'x165x1.797_ (0.2316x109 *) 9.8150.764776.39 of 7000 (0.689) °\776.39 Jpoms-aas 69) { 1 or) J => wy = 6.11 (m/s) SVTH: Vo Ngoc Tiép - Trang 16- MSSV:69902203pO AN MON Hoe GVHD : Vo Thi Ngoe Tus Chon te a} Lim viée w = 0.85.w.=5.19 (m/s) Dudng kinh doan eft _ Ve © \ 5x3600KW y Lugng hoi tung binh di trong thép: Vey (m'/h) = ga, (Ke/h) x pyy (Ke/en') = 2478.915 x 1.797 = 1379.47 (m'/h) 4137947 Vx3600%5.76 2. Duiing kinh doan chung: Néng 46 trung binh pha léng: no kethw _ 03 a) 2 ng dQ trung binh pha hoi theo phung trinh duting 1am viée: Yau" = 2.267 X Xn.” = 0,038 = 0.336 8t dO trung binh cila pha lng, pha hoi tir gidn d6 Txy: Xm” = 0165 + t= 65°C Yn” = 0.336 + t,"= 88°C Khéi lugng mol trung binh va khéi lydng riéng pha hoi: Ma.” = Yin” X Maccione + (I = Yon") X Mau = 0.336 x 58 + (I - 0.336) x 18 = 31.44 (Kg/mol) "XT, _ 3144x273 24xT,” 224x(88+273) Dew => Da= 0.3m). = 0.165 1.061 (Kg/m') Kh6i lugng rigng pha ling: Xm” = 0.165 > Xn" = 0.389 65°C + freer 139.25(Kg/m*) Pewse’ =980.25(Kg/ m*) ) a-x Px Pacstone Pause Lutgng hai tung binh di trong doan chung: ae’ = SEL Kei) > px” = 869.93 (Kg/m') Trong dé: 1°: higng hoi di vao doan chung gn’: lung hoi ra khdi doan chung Vi higng hoi ra khdi doan ching bing ludng hoi di vao doan luyén nén. Be = 21 Hay Lugng hoi di vio doan chung g1” .Iudng hai ling G1” va ham Iwgng lng x1” dude xdc dinh theo phwong trinh can SVTH: Vo Ngoc Tiép - Trang 17- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus W =1238.12(Kg /h) Xy = 0.03 + xy = 0.091 Yw= 0.4 (phan mol) dyfa vao dudng cn bing J, = 0.754 (phan khdi long) gun = 1572413.4 ty Yow (= yw dty Tai day thap: 01.893(KI/ Kg) 2361.355(KJ/ Kg) 1y'= $01,893 x 0.754 + (1 ~ 0.754) x 2361.3: 15724134 gi = ————= 1639.09 (Kj ay = Spo 1639.09 (Kem) Gy’ = 1639.69 + 1238.12 = 2877.21 (Kg/h) ve 1639.6930.754+1238.120.091 ty =85°C > 959.32 (KJ/Kg) = 0.469 2877.21 => Litgng hoi trung binh di trong doan chung: iy? = 1039.09 2107 83 1975 seep hy 2 Van t6e hoi di trong thip: 195x1.061 9,810.75" x869.93 t." = 65 + pie” = 0.2225 x 103 (Ns/m’) G, = 2877.21 (Kghh) = 0.799 (Kg/s) 3, = 1837.46 (Kghh) = .052 (Kg/s) ’ 22 Wy’ = 0.85 x w.’ = 5.29 (m/s) 0.2225x109 1000 16 93)" | ~o1s saa 222)" Lael | Vo. \ 869.93 TRV, aR T6S75- 3600.0, Vn3600x5.29 Vib = 1873.46 x 1.061 = 1765.75 (m’sh) => Chon duving kinh : D = 400 (mm). IL. Chiéu cao thap: * Chiéu cao ciia thép dém (toan thép): H=N; x hg +8 +1) (m) 0.344 (m) SVTH: Vo Ngoc Tiép - Trang 18- MSSV:69902203pO AN MON HOC GVHD : V5 Thi Ngoc Tus Trong dé: Ny: $6 dia ly thuyét 0.8 + 1: Khong céch cho phép 4 dinh va day thap (m) hu: Chiu cao tueng dviing ciia bac thay déi néng a6, c6 thé tinh, theo ede cng thife sau: ook Trong a6: K :hé 5 a,b.c,d,e.f: cdc s& mai,tim bing thy nghiém Puy : Kh6i lang riéng trung binh cita pha Ing va pha hoi (Kgim’) Holly | DO nhdt trung binh ciia pha Idng va pha hdi (Ns/m’*) (kh6i lugng riéng, d nhét ly theo mhiét d6 trung binh) G,,G,: Lutgng ling va ligng hoi trung binh di trong thép m :hé s6 géc can bing y= f(x) véi mat phing ngang (Kg/h) Tacé: K =1764 d=0.342 © =0.19 f= 0.038 Gy= LAG _ 607834287721 _ 1749 59 (Kei) 2 2 eat 28502 169.09 = 244.545 (Ke/) p, = PetPs T6539 86898 = 823.16 (Ke/m’) ot . py boy - 1797 +8998 = 1.429 (Kgim') 84 = 195 ("Im") Vq = 0.75 (m'/m') we'+w," _ (6.11+6.22)x0.85 w 5.24 (ais) 2 2 Cy tgg= EAS = BS = 62°C 2 2 ‘at Cong e BEE _ 85488 a6 506 2 2 Je pn = 1 x Ig os +2 x Ie pe Trong 46: jy,}i:06 nhdt dOng hfe eila ede eu tit thanh phan x1.Xo: néng d6 phdn mol eda cde effu tit trong hén hop = 62°C pieacetone) = 0.227.103 (Ns/m*), x = 0.03 Hagsuae) = 0.4578. 103 (Ns/m*), x2 = 0.97 olg py = 0.03 lg 0.227.10° + 0.97 lg 0.4578.10° = -3.348, => pH, = 0.4483,10-3 (Ns/m?) SVTH: Vo Ngoc Tiép - Trang 19- MSSV:69902203MON HOC GVHD : V6 Thi Ngoc Tusi 1°, = 76.5°C — 1; = 0.2053.10% (Ns/m?), x1 = 0.95 Ho = 0.3766.10" (Ns/m’), x2 = 0.05 .95 x 1g 0.2053.10" + 0.05 Ig 0.3766.10" = -3.6744 2116.10" (Ns/m*) Shea 16x [HES 24) x 195"? x 0.75! x \0.2116.10 us ow soe tp 212.52 (2244585) 823.16 {2 2116.10 x 3.83x2244.545 1996 (m) lias.) “a9 (oaa83.10 3.83 224 1742.52 SS H=Ni x hy + 08 +1) = 8 (m) * Chiéu cao lam vige cia thdp: H’ = hy, x m, (m) hyy : chiéu cao ca mot don vj chuyén khdi (m) mg: s don vj chuyén khdi xc djnh theo néng d6 pha Ing 2 dx mee Lyoaa mG. hy =h; + +h, G, Trong 6: hy : chiéu cao ila 1 don vj chuyén kh6i d6i vdi pha hoi hy: chidu cao cha 1 ddn vj chuyén kh6i d6i vai pha Ing aya Re Ps) 256. (#=} Rey” .PreS(m) pad a: hé sO phu thugc vao dang dém : dém vong a = 0.123 Hi, : 46 nhét pha léng (Ns/m’) (1, = 0.4483.10° (Ns/m’*) Ve: thé tich ty do cila dém (Vg = 0.75 (m’/m’)) px: Khdi lugng riéng pha léng (p, = 823.16 Kg/m') vy :hé sO thm wat cia dém .né phy thude vao tf s6 gidta mat ad tudi thye tf lén tiét dién ngang cia thép va mat dd wdi thich hgp, x4e dinh bing dé thi (HIX 16,{5]) Us E mat d6 tdi thy té (m’/m7h) Uy, = B.8,; mat d6 twéi thich hgp (m'/m*h) B = 0.065 (m'/m.h) ( Bang IX.6,[5]) G day : V, :Iuu ludng thé tich chat Iéng (m’/h) Gy _ 1742.52(Kg/h) ve = = 2.1176 (m'/h) Px 823.16(kg/m) dién tich mat edt thap (m’) F,= 2p? = 2x04? = 0.125 (m4) ; 4x04? = 0.125 (m’y 8a: dién tich bé mat ring cda dém (m’/m’) SVTH: Vo Ngoc Tiép - Trang 20- MSSV:69902203MON HOC GVHD : V6 Thi Ngge Tusi 04 = 195 (m*/m’) Rey : Chuan sé Re pha hoi Row OPM OL A2955.24 Hy 5, 0.2116x107x195 Re, : Chudn s6 Re pha léng = 72.59 1742.52 0.04.6, 3600 FBym, — 6126x195x0.4483.107 D, : hé sO khuéch tan trong pha hoi (m*/s) 0.04x Ry 1,758 aq ¢ ye p,= 130° (1, 1) POVKS+ VHA Ma Mp) Trong dé: 73 + 76.5 = 349.5°K 8 (g/mol) 18 (g/mol) Va.Vp :thé tich mol cia khi A.B Va = Vacctone =3 X 14.8 + 6 x 3.7 + 7.4 = 74 (cm’/mol) 8.9 (cm‘/mol) 4.3.10%349.5'9 (1 ITE F189 PSE =0.161(em? /s) =1.61.10-°(m? /s) D, :hé s6 khuéch tin trong pha ling: 7.4.10 °(@M,).T ve D, Trong dé: Mg :Kh6i lugng mol ciia dung m6i, Mg = 18 (g/mol) T: 273 + 62 =335°K n’ sd nhdt ciia dung dich (ep) Hnuae” = 0.4578.10° (Ns/m”) 6: hé sO két hgp cho dung méi Va: thé tich mol cla dung chat Vacetone = 74(em*/mol) 0.4578 (ep) 2.6 = D, = ARO C-6x18)" 1535 _ 9 9 x 10°(em"/s) =2.8 x 10° (in"/s) O.AS78x74 Pr, : Chudn s6 Pran ta pha hdi Hy __0.2116x10% Pr 9.197 (N) 5D, 1429x1.61x10 Pr, : Chudn si Pran cia pha ling 4 0.4483x10 * © B,D, 823.16x2.8x10" Xée dinh hé sO thé wat = 194.59(N) SVTH: Vo Ngoc Tiép - Trang 21- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus 170m* Phy F, 0.126") Un = B.8y = 0.065(m°/m.h) x 195(m7/m*) = 12.675(m'/m?.h) Us 168 1 39 U,, 12.675 Tir bang 1X.6,[5] >o=1 0.75 0.123x1x195 =16.8(m° J m*.h) en Pry! (m) Jn ps x72,59°* x9.1977" = 0.4(m) OAAS3K10™ ) 1 75882 x194.5°5 = 0.274) 823.1 he thy = 04 2822545 6 974 217524) 1742.52 Igy X my = 1.752 x 5.9 = 10.34 (m) TL. Phan tinh trd luc cia tha) Buting kinh twong dung: 015 3, 195) Chudn s6 Renoy: od, Rey = 24e?, Vay * Phan cat: Re, = Sela _ $:1920.0159.797 _ grgi9g Veaty, 0.75x0.228.10 My _ mM, , mM, me He hy = Hy = 0.22.10" (Ns/m*) thy = 65° du, =H, = 0.44.10" (Ns/m*) My =49.8 49.8 _ 0.79658 | (1=0.796)x18 We 0.44.10" => H,, = 0,228.10 (Ns/m*) Bye = 56X75 19! *9,797*H1951 (022.109 _ yy 554 OB AP ac = (14K.)-APe (6 \""/, SVTH: Vo Ngoc Tiép - Trang 22- MSSV:69902203GVHD : V6 Thi Ngge Tusi MON HOC you yon 5 yea sag. sre (7) { 0.3.10 : \2478.915) (776.39) (0228.10 } 1° = 59 => Ig = 0.625120.23.10°*+(1-0.625)1g0.469.10° = x= 0.3.10 (Ns/m?)) = AP ye = 34269.92(N/m") * Phan chung: ~ 5.29x0.015x1.061 _g654.9 #4) 0.75x0.13.10 (yer) = 0.13.10 (Ns/m?)) _ 1,56x3,5x5.29' 81.061 X195"? x(0.13.104)° _ = 052 305.4(Ns/m?) AP en) = me oe (ety =5.154{ 287721)" ,( 1.061 nt 29.107) 01 1873.46) “(869.93) “\0.13.107 J => AP yey =18703.85(N/m’) = Téng trd lye: AP = APy. + AP yay = 52973.77(N/m). SVTH: Vo Ngoc Tiép - Trang 23- MSSV:69902203I kinh cd DO AN MON HOC GVHD : Vo Thi Ngoe Tuoi CHUONG 4 : TINH TOAN CO KHi Tinh chiéu day than thap: Chon thigt ké'than try b&ng phuéang php hé quang. Thin thip duge ghép vai nhau bing nhiéu méi ghép bich, Chiu cao dém doan chung :1.752 x 2 =3.5 (m) Chiéu cao dogn eft: 10.5 3.5 = 7.0(m) Chia thép lam 3 dogn * Phan chung:3.5(m) * Phin efi chia fim 2 doan méi doan [2 : 3.5(m) Khodng cach giita 2 ting 4ém la :0.35 (m) Chiéu cao todn than thap : H’ = 0.4+ 3.5+0.3543.5 +0.6 + 3.54= 11.85 (m) Chon vat ligu im than thap 1A thép khéng gi XISHIOT dé thigt ké than, day va Cée thang s6 dc trung eda thép khdng gi la Gigi han bén kéo : 64 = 550 x 10° (N/m?) Gidi han bén chay ; oa = 220 x 10° (Nim’) Hi $6 gin khi kéo 16.6 x 10° (1/°C) Kh6i higng ring ciia thép : p= 7.9 x 10° (Kg/m') nbigt : 2 = 16.3 (Wim°C) n toan bén kéo : ny = 2.6 Yan toan bén chy : ny = 1.5 Médun dan héi: E,..., = 2.01875 x 105 (N/mm*) Nhiét 6 néng chay :t°,¢ = 1400°C He s6Poatxong : w= 0.33 G gida méi doan dém c6 hai ctta dé nhap dém, théo dém va lam vé sinh. Dudng 100 (mm), cae etka nay phan bs doc theo hai dung sinh cia thép. Digu kién kam viée cba thip: Ap sudt bén trong thép tinh (tai dy thap ): P=Pj, + Pat APey PUt= pane tT 1 Pan = 937.84 (=x) _ 0.091 | @-0.091) + O94 A= 0.090) _, 725" 9685 Pav Places PHO => P=9.81 x10" + 937.84 x 9,81 X11,85 + $2973.77 261476.3(Nim)= 0.261(N/mm*) Tinh hg s6'bén cla thin hinh tru = 0.95 (han tay howe bing hé quang dién, giip méi hai ben) H=Zd _ 11.85-0.35 HLS Ed : Téing s6 In nhdt ciia cde duting kinh cdc 16 trén mot dung sinh => Ed =0,1x340.05 = 0.35 (m) Ung sudt cho phép x0.95 = 0.92 =x SVTH: Vo Ngoc Tiép - Trang 24- MSSV:69902203MON HOC GVHD : V6 Thi Ngge Tusi 211,54x10°(N/m?) 220x108 x1 =146.67x105(N/m?) min ({ox}, [64]) = 146.47 x10°N/m?) Kiém tra Lg, = 88570 99 516997 »25 0 dyin dah theo sng thie sau DuP___400x wP___40080261 = 9 s9¢mm) 2fol, 2x146.67x0.92 Bé day thye té ca than thép: Pec C : Hé 86 bé sung CHC, HCat Co Co SHG s6'bé sung do din mon hod hee eda moi tudng Co: He s6'b8 sung do tn man eo hoc eda moi trvBag Cc : Hé s6°é sung do sai Ich khi ché tao, lp rép Cy: Hé 86 bé sung 4€ quy trdn kich thuse 10 (nim) x 0.1 (mm/nim) + 0.22 + C, $ = 0.3941.22 +Co=3 (mm) Kigm tra bé day eta thin S-Ca_3-1 224C, = 5x10 * <0.1(thda) D, 400 Kiém tra dp sudt tinh todn cho phép bén trong thiét bi [py = 2AobPaS=C,) _ 2x146.6720.92K8-1) _ 34(N/ mm?) > P(théa) D, +(S-C,) 400+ (3 Kiém tra ting suai theo ép suit thi: [p, +(s-c, JP. AS-C.)9 Py = PytP=0.261x1.5+937.84x9.81x1 1.85x10 =0.5 N/mm? [400 + (3-1)Jo.5 23-092 = 54,62 <2 = 222 _193,33(tho’) 12 IL. Tinh day, nap thiét bi: Chon ndp Ellipese tiéu chudin loai e6 g3. Chiéu day $ duge tinh sie De D 3.8 [o].k, —P 2h, hy : Chidu cao phan I8i cia dy (np) hy = 0.25.D, = 0.25 x 400 =100 (mm) 2h s6 bén méi han SVTH: Vo Ngoc Tiép - Trang 25- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus k :hé s& khong th aguyén, k= 1-4. = 1-202 < 9.75 Di 400 . 400x0.262 400 c_oasec 3.8x211,54x0.75x0.874 — 0.261 2x10 CHC. 4Ch+ Cet Comm) = 1 4040.44 1C,42= 3.44 + Cy => $=038+3.44+C, =4(mm) Kigm tra bé day = 75x10 < 0.14thda) Kiém tra Gp sual tinh toxin cho phép: ppp 2lolelS=C.) _ 2x146.67x092x4-D D, +(S-€,) 400+ (4=1) Kiém tra ting suit cho phép theo 4p suat thi thuy lye: IN / mm? > P(thod) fb? +2h,S-C)P, [4007 + 2x10004-yh.s 4669 < Bee Ga OF, 83.33(thoa) 7.6kg hy (S—C) — 7.6x0.75x0.92x100(4 1) 12 2, Tinh diy Twang tu: Q: Iu hugng thé (m'/s) v: vin te (m/s) 1. Ong din hoi ra khéi dink: Lau long khi di qua 6g: (4R).D= (1+ 0.9)x1500 Chon v = 20 (mm/s) ae 42850, V3600xzx20x1.797 => Chon d= 150 (mm) 2. Ong nhap ligu Tinh twong ty G 850(Kg/h) 0.167 (mm) =2738.13(Kg/h) p= 869,.93(Kg/m*)} — 4 = 50 (mm) Chon v=0.45(m/s) 3. Ong din léng ra é day thap : d= 50 (mm) 4, Ong hoan twa d= 50 (mm) Bich lién bing kim loai den: SVTH: Vo Ngoc Tiép - Trang 26- MSSV:69902203GVHD : V6 Thi Ngge Tusi Dy D, | D Dp Di | Ds Z 50. 37 140 110 90 M12 4 150 159 | 260 225) 202 | Mi6 8 IV. Tinh bich ni Chon bi khong e6. Tinh ton theo phung phép tdi trong gisi han. Vat ligu am bich cing loai v4t ligu vai vat ligu Fim than, Bulon Iam bing thép CTs T’=8s'C Ung suit cho phép cila v4tligu Lim bulon, bfeh: 86.75 (Nimm’) [o}* = 108.94 (N/mm) Cae thong s6 cia bich tra & bang XIIL.27,{5] Dung kinh trung binh : D, = 400 (mm) Duting kinh bich : D = 515 (mm) Bung kinh tam bulon : Dy = 475 (mm) Bung kinh mép vat : Dy = 450 (mm) Bulon : M16 Chidu cao bich : = (= 20 (mm) 1, ‘Tinh bulon Xie dinh lye nén chigu trye : Qi = Qu + Qk Qe: Iue do sip suat trong thiét bj Q= p= Fx400°x0 262 = 32907.2(N) nén, Qk : lye cn thigt dé gitt duge kin trong dém 1. Dip.bo.t.P D+ 2.bi + 2.b/2 = 400 + 2x1.5 + 2x23. 5 (mm) 450-400 = 426.5 (mm) -15=23.5 bo = 4b = 11.75 (mm) m:hé s& p suat riéng. Chon dem Ia amiaing day 8 = 3 (mm) qo = 10 (N/mm’), m = 2 Qu = Wx426,5x11.75x2x.062 = 8245.5 => Qi = Q + Qk =41152.75 N) Lye cdin thigt 48 ép chat d&m ban ddu: Qo = nDa.bo.qo = 3.14x426.5x1 1.75x10 = 157357.18 (N) Lye tée dung Ién 1 con bulon: gg = B= AM) _ 15735718 _ ag67 g6¢N) Zz Z 20 Bung kinh chan ren = 1.13.97, x TROT REZ = 15. 2mm: d= 1.13.)9(,] 21.13 6/15 475 = 152mm) {6} = ko [o]' = 0.5x86.75 => Chon dy = 16 hay M16, Kiém tra lai vige chon Z ‘Chu vi vong bulon : C= x.Db = mx475 = 1491.5 3.375 (Nimm2) SVTH: Vo Ngoc Tiép - Trang 27- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus X= ClZaton = 1491,5/20 = 74.575 74, Kiém tra 4.66 ¢ (4.3 + 5) tht P<0.3 (thda) 2. Tinh bieh : Xée dinh: = 475-450 «19 sm) _ 475 ~ 404 36(mm) te= 0.61x16, —43575_| 12.5 99 4 0.741.246x 222 (2) ( = 14.5 (mm) | 1638x108.94 | 36 43.375 \ 20 => Chon t= 20 (mm) * Bulon Kich thuéc bulon sinh dau 6 canh theo tiéu chudin:der = 16 (mm) Chiéu r6ng déu bulon : D = 25 (mm) Chiéu cao du bulon ; h = 9 (mm) Chiéu dai bulon : 1= 70 (mm) Chiéu dai ren : 38(mm) V. Dia phan phéi long: Bung kinh thép : D, = 400 (mm) Dung kinh dia : Dg = 250 (mm) Ong din chat I6ng : 19 Sng loai 25 x 2 (mm) Buse 6ng din léng trén dia : 48 (mm) Dia dude Lam bling thép CTs c6 bé day 1a 5 (mm) VI. Lui aa d¢m Busing kinh lui : D, = 369 (mm) Chiéu réng bude : b = 23 (mm) Bé réng thanh d3 dém : 5 (mm) Xie dinh bé day luéi 43 4ém_ SVTH: Vo Ngoc Tiép - Trang 28- MSSV:69902203DO AN MON HOC GVHD : Vo Thi Ngoe Tuoi Kh6i Iugng trén lvdi : m= Meta ayo + Mouse mem ita = VePs == Hea = p= Hee. 0.4 x3.5x600 = 263.76({Kg) 7.0.4 Mute = py Vyy-Ve = 968.5% x3.5x0.75 = 319.314 (Kg) => m= 583.07 (Kg) TAi trong trén lui mg xD? 4 = 45541(N/m?) = 0.0455(N/ mm’) Chigu day tinh ton ti thigu ea li Sng >9, = P Vole, 2d S=D.K. (mm) D. % K=0.45 0.6 ,Chon K=0.6 Za : tng s6 dutdng kinh cdc 16 trong v6 Sng P: Ap suat tinh toan v6 Sng, D, : Dudng kinh vé éng D, = 369 (mm) Goi x Ri s6 thanh trén lu6i nén c6 (x + 1) khe => Sx + 18041 169 =>x=15 =a 6x 18=288 369-288 369) = 0.22 0.0455 0015S _ 9.03 \ 0220146 iam => $=400x 0.45 x Chon s = 10 (mm) VIL. Tinh tai treo, chan dé: 1. Tinh s¢ b9 khdi higng thap: Thin Bay Nap Bich bem: Ludi G = Gihan +Gaiy + Gasp + Grich + Gas + Grate + Gring + Gate phan psi +6 4e 406* ~ 0.4? \11.85%7900 = 355.4(Kg) Gass = =(D3 - Di). 7 pi) Ge = 64.2 (Kg) = Gasy = 1.01x64.2 = 64.842 (Kg) 6 (Kg) => Goi = 1.01x6.6 = 6.67 (Kg) Gbich = $6 bich Fl A: Dung kinh ngoai cia bich D, : Duting kinh ngoai cia than thap 3 Gaay= 5020.55" 0.406" )2420 10 77850 = 125.72 (Ke) 2 x0.4?x10.5x600 = 791.3 (Kg) Gdem = =p, Zi Haha a SVTH: Vo Ngoc Tiép - Trang 29- MSSV:69902203bd AN MON HOC Khéi Ivgng mét thanh : tpi Depa i DP Khéi lugng mét lydi : 15 x + => Gis GVHD : V6 Thi Ngge Tusi 3x15 4x0. 005?x0.4x7850 = 2.79 (Kg) Eeo.4PxI1854115:10°+25.5.10 Jlon0 } x7850 = 56.23(Kg) Ling = 1754.86 (Ke) Néi dun Ges = Gate + Giing + ang stn + Gren Gis = (206% —1.2° 1 7.7900 =152.2 (Ke) Ging = 781-281. 441000 = 1318.8 (Ks) Ging sofa = 46 025? — 0,019" \135x8500 = 237.8 (kg) Gren = a0 340° ~ 1.206? x2x25.10°°x7850 =105.5. (Kg) => Gps = 1813.8 (Kg) Dia: x x =2x|2p?.8-n.2.pi,3 |p, al fois-04 oi 253,10 -19x% 0.025? x0.4°x3.10-" ~19x20,025*x2.10 LG = 4,969.612 (Kg) Tai trong cia thép : Gex = UG x 9.81 = 48752 (N) 2, Tinh tai treo: Chon vat Tiéu Lim Chon 86 tai treo Ia 4 => TAi trong cho phép lén | tai treo 1a G? = Gryae/4 = 48752/4 = 12188 (N) Céc thong sé cita tai treo Tai trong |Bé mat | Tdi trong cho LB cho php | 43 phep Trén mét | F.104m’ | Lén bé mat 43 tai treo q-10°%(Nim’) G.10* (N) 28 173 1.45 150120 Tam I6t: Cao: H= 260 (mm) Bé rng: B= 140 (mm) Day: $=6 (mm) 3. Chan di $6 chan a3: 4 SVTH: Vo Ngoe Tiép = Trang 30- By 1302158 i treo Ld thép CTs, tim 16t Ia vat ligu lam than thidt bi. 60 20 30 MSSV:69902203bO AN MON HOC GVHD : V6 Thi Ngge Tusi Céc thong s6’cita chan do Téi trong cho | Bé mat do | Tdi tong Lo BOB BH hS I d phép trén 1 F.10*(m*) | cho phép chan dé: Trén bé mat da G10 4.10 “(Nim’) 25 444 0.56 250180 215 290 350 185 16 90 27 SVTH: Vo Ngoc Tiép - Trang 31- MSSV:69902203DO AN MON HOC GVHD : Vo Thi Ngoe Tuoi CHUONG 5: TINH TOAN THIET BI PHU I. Thiét bi ngung tu san phdm dinh: Dang nuéc lanh di trong Sng, ding sin phim dinh di ngo’ Diéu kién ahiét 46 ciia qué tinh: Al, =57.5-27=30.5"°C Nhigt lugng edn trao 4éi vai thiét bj ngung tu: 5 1500(0.9 + 1)$51930 Que D (R41 rps FASS ES = 436944.6W) Lyng nude lanh clin gidi nhiét: Qui 69. eaktg =) 4180.94(40 = 27) 1g chiim, At nim ngang, vat ligu bling dng thau, hé so = &(kg/m*) Chon thiét bi loai dinohiet: 2 =93 WimK p =8500kg/m* Thigt bi gm 187 Sng, xép thinh 7 hinh 6 canh, sé Sng d ving ngoai cing 1a 43 Sng. Chon éing e6 duting kinh fa 25x2mm. Bung kinh trong thiét bi Dypat(b-1)+4dy=35(15-1)+4x25=625mm ts bude Sng; chon br s6 ng trén duting chéo cia hinh 6 canh. a: sf Sng trén mot canh cia hinh 6 canh ngoai cing be2a-1=2x8- He s6 cp ahigt tir sda phim dinh dén thank thiét bj: ape PE ON at Ti t1=57.5°C tra duge p=748.75(kg/m') 1 =0.23.10° (Nei?) '23350(0/kg) : dn nhigt ngumg ty acetone. (C=2296.875(I/kg.do) : nhiét dung rigng ciia acetone. 2. =0.165Wim.d8: hé s6 ef'p nhigt ciia acetone D?—nd? _ 0.625: 0.082 De+nd 0.6254 Chon Ar=3°C = Trang 32- MSSV:69902203 SVTH: Vo Ngoc TiépDO AN MON HOC GVHD : Vo Thi Ngoe Tuoi Tir d6 ta tinh dude a, = 3151(W/m? 46). He 86 eéfp nhit trung binh eda chim Sng: .,= 60g, =0.6x3151=1890(W/m’.46) He 86 e@ip ahigt ti thanh dn nuse: Tit tgp = 0227 = 33,5°C tra dug Spy = 993.95kg/ m> Ht, = 0.759.107 Ns/m? deg = 0.625 Wim.d6 Van te nutée di trong 6ng: =—4Gn 2 Bg gems) Pandy? 993.95x187x7x0.021 Rea 282 4199.25 ——Nu__ . y peel Pr Pre Chon At, =9°C DPtw= tart AL=48.5"C Tra chudin s6 Prsss=5.2 Prias=4.8 Tinh duge Nu=24.87 = Nth 601.86 d Nhigt tdi rigng: qu=a.,At, =5596.74 6718 on = 4a en He s6 truyén nhiét K: = 1.3% <54e(tho’) 8 =0.002 a, = 1890W/m? a4, = 621.86 4, =1/11600 r= 1/5800 Q > Bé mat truyén nig = 4513 KAU, . F Chigu dai ging truyén nhigt: L=—— ein dn |. Thiét bi gia nhiét nh4p ligu: Sau hi tn dung ahiét ca sin phdm day d€ gia nhigt cho nhdp ligu thi nhiét 46 cia nh§p ligu 46.5°C, chia dén nhiét 46 s6i. Vi vay, tig tuc gia nhiét cho nhap liu bing hdi nude bio ha 4 dp suat 2at, T°C = 119.6°C. SVTH: Vo Ngoc Tiép - Trang 33- MSSV:69902203DO AN MON HOC GVHD : Vo Thi Ngoe Tuoi Dang néng : 119.6°C -* 119.6°C. Dong lanh : 41.13°C 7 62.5°C. Chon thiét bi 18 éng xodn, bing dng thau, dung kinh 25x3¢mm) Dang ahép ligu di trong Sng, dong néng di ngoai dng At, = 119.6 — 41. Aiy = 119.6 62.5 At, —Aty Nhigt Iugng hoi aude cin cung ep: Qe = Cp.Gp.(62.5 — 41.13) = 3100.68x0.76x(62.5 — 41.13) mat Ia 5% => Qr’ = 1.05.Qr = 52876.7 (W) Hoi ngung ty ngodi Sng xo‘n: =0725.a(-) wim? (=) 8 > tag = 119.6°C + r= 470984 (IK) Chon Aa = 5°C + tar= fap = Au = 119.6 $= 114.6 °C 17.1°C > A =186,7(W/m? 46) .725,186,7 470984 \ 5x0.025, Ging Aty = 29817.85(Wim’."C) Chit lng s6i sti bot! os= 69.10°{ Ps | (2) A007 canny \p-p.) Vo) cr r: dn ahiét hod hai (Keal/m.h."C) T, : Nhiét 6 s8i (°K) o: Sie cing bé mat trén_ mat gidi han phan chia gitfa ling va hoi (Kg/m) Cy : Nhiét dung riéng ciia cht lang (Keal/Kg."C) pr: Khdi lugng riéng ca hoi (Kg/m") pr: Khéi lugng riéng cia ling (Kg/m*) by :D6 nhét déng lye hoc ciia chit ling (Kg.s/m*) q: Nhiét téi (Keam’sh) Ay: D6 din nhiét cla chat long (Keal/m.h."C) 1241 (Keal/Kg) ) = 5963.57(W/m?.49) => = 470.984 (KI/Kg) 943.4 (Ke/m’) Mh = 0.232.10-3 (Ns/m2) = 2.35.10-5 (Kg.s/m?) 62.50 = 335.5°K 3100.68 (W/Kg.d6) = 0.74 (KealKg.d6) 827.22 (Kg/m') zl x) 0.58 (1-058) 742.625 * 981.625 =827.27(Kg/m*) SVTH: Vo Ngoc Tiép - Trang 34- MSSV:69902203MON Hoe GVHD : Vo Thi Ngoe Tus d= ACpp. \arow ao = 3.58.10°%x3100.68x827.22x3 82722 | ag = 22 774eW.80) = 0.2385(Keal/ mb. C) 1 2 :18.3.10% 65.75.10" => hy = 4152.2 (Keal/m?h."C) = 4828.99 (Wim?.’c) = 14.32.10 *(N/m) = 1.46.10 *(Kg/m) Nhiét trd cua dp cin fa va ban than thi Eran, +24 1,(m" 467 W) ét bi: au hai pi 11 = 1/5800 n= 1/11600 = Yr=291.10" 3 _ 0.003 x8 Nhigt tdi rigng : qog= 4) ug = 29817.85 At yr dr Iq, = o,-At, qe= Chon Aty = 5 tw = thy - An = 114.6°C 6 > bap = ts - Alp = 685°C T 502.03 +2.91.10-* 4828.99 52876.7, 524m’) “Ag 1502,03x67.22 F 0524 Chidu dai toan bé eiia Sng : L, = 6.67(m) ed, 314K. 005 Chon duting kinh vong xon : D = 0.25(m) = 250 (mm) + Chidu di mot vong xo8n : ly = 0.25.n = 0.785 (m) S6 vong xodn : n= L/be= 8.5 (ving) ~8 (vong) Khoding cach gitta 2 vong xodn : hy = 1.5.dx = 1.5 x 0.025 = 0.0375 (m) Chidu dai mot bude xoxn : hyx = hy + dx = 0.0625 (m) Chigu dai ton bd vongxogn : H = ng . hb, = 8.5x0,0625 = 0.53(m) SVTH: Vo Ngoc Tiép - Trang 35- MSSV:69902203DO AN MON HOC GVHD : Vo Thi Ngoe Tuoi TIL. N6i dun Diing hai nuide bio hoa c6 4p sudt tuyét Adi 18 2 at, T = 119.6°C 48 céip nhigt cho dung dich. Dang néng : 119.6°C (hai) + 119.6°C (hai) Dong lanh : 85°C (ling) —> 99°C Atl = 119.60€ ~ 850C 12 = 119.60C => At, Nhigt lung hoi ause edn cung effp: Qn = 1.05.(Qy + Qu ~ Qr~ Qu) =488 (KW) Chon thigt bj 18 Sng xodn, duting kinh d= 25 x 3 (mm) Hoi ngung tu trong Sng xodn 725. (] (Wim?."C) Md f tng= Chon Atl = 50C + twi = tnq- Atl = 114.60C 19.60C + r = 470984 (J/Kg) Gath 119.6 4114.6 17.1 C= A =186.7(W/m? 4d) 2 2 = a, = 0.725x186.74{ 470984)" _ 5963.57 " \5x0.025 } Chil ling s6i ( 3% mol Ia Aceton, 97% mol nutée) avnesi0%{ 2)" (2) ane pi Pa) Pl eS (Kealim’h.C) oJ wc Te 1 = 471.984 (KI/Kg) = 112.41 (Keal/Kg) pn = 943.4 (Kg/m') Hy = 2.35.10" (Kg.s/m*) T,= 99°C =372°K Cr= 4034.05 (J/Kg.48) pr= 937.84 (Kg/m3) 0.091. (1-0.091) 5 968.5 3.98.10" x4043.05x937. Sax] 57.84 = 0.95(W/ m.46) = 0.871(Keal/ m.h."C) toto 1 1,1 GG; 15.6.10° 61.675.107 => 6 =12.451.10°(N/m) = 1.27.10 (Kg/m) = a, = 4437.02 (Keam’h."C) SVTH: Vo Ngoc Tiép - Trang 36- MSSV:69902203DO AN MON HOC GVHD : Vo Thi Ngoe Tuoi 5160.25 (Wim?."C) Nhiét trd cba ldp cin edu 2 phia va ban than thiét bi f, +S rem" a6/W) =2.91,10% Nhiét tdi riéng: nq = w= Go = Gog-Aty = 29817.85 at ar Chon Atl 114.600 A 99 + 5.5 = 104.50C At =twl ~tw2 = 10.10€ 3 q8= Oude = 5160.2545.5 = 28381.375 = 4.8% <5% (thda) 7 = 1532.63 r, +2.91.104 + a, a, 5963.57 5160.25 Q 488000 Katy, — 1532.63x30 10.61 (m*) F _ 10.61 _ nd 0.025 Vi ding xodn dai qua thi tré lye In, khi ngung ty hoi bén trong Sng thi nude ngung 48 tich Iai Lam gidm bé mat ruyén ohiét. Vi vay, ta e6 thé chia ng xodn ra 3 doan bE tri theo dang 3 try dng tam. Chon ving ngoai cing e6 duting kinh: Dy = 1100 (mm) Chiéu dai mdi vong : le) = #.D) = 3.454 (m) Svang xodn: ny = 20 (vong) Chiéu dai 20 6ng: Lar = beam Khodng cach giita 2 vong xofn: Chigu dai mét buiée xogn: hye Chiéu dai toin bo Sng try vong xodn: H Chon vong thi 2 ¢6 duéing kinh : D2 = 700 (mm) Chiéu dai mdi vong : ly = x.D2 = 2.198 (m) S6 vong xodn: nz = 19 (vang) Chigu dai 20 Sng: Lez = ke.m2 = 41.726 (mm) Chon ving thi 3 ¢6 dung kinh : Ds = 380 (mm) Chigu dai mi vong : les = x.Ds = 24.158 (m) Chidu dai 20 Sng: Lys = Ly — Le: “Lao = 24.158 (m) Chiéu dai toan bd eda Sag : L, 9.08 (m) i= 1.5.d, = 37.5 (mm) 1s + dy = 62.5 (mm) hig = 1.25 (m) SVTH: Vo Ngoc Tiép - Trang 37- MSSV:69902203DO AN MON HOC GVHD : Vo Thi Ngoe Tuoi 5 vong xoft 24.158 86 vong xodn: Tose = 20 (one) IV. Bom Ap dung phung trinh Bernoulli cho 2 mit eft 1-1 va 2-2 Vi 2,2 2g Ye =Pr= lat > Hy=Z2 +¥hr = 7000 + Dhy Zhe: tng ted Iye bao gbm t8n thet doc duiing trong ng din thing tén 16a that trong dng xon Chon chiéw dai Sng din It :L = 11 (m), dung kinh D = 25 (mm) 1738.13 (Kghh), p = 869.3 (Kg/m') 75.104 (m*/s) cuc bd 5 (mm) => v= 1.8 (as) Q= 8.75.10 (m/s) 2 = 50 (mm) = v2= 0.45 (mis) Ta e6 vi a a+3.sa4 298) 0158 (TeiogRe-.sy (8 10g175813.5— & = & =0: 0158x0.075 0.050 0. 2x9.81 voas+1} => Hb =7.0 + 3.8 = 10.8 (m) QH, pg _ 8.75.10 *x10.81869.3%9.8 1000. 1000x0.75 Noll TM 09x09 yy shigu sudt truyén dong ne shigu sudt dong ea Bé phong qué tdi, chon bem e6 cOng suf: N = 2.N, = 2x0.11 = 0.22 (KW). => Céng sudt bom ly tam: N= =0.11Kw) Céng sudt dng co dién : Nec 136 SVTH: Vo Ngoc Tiép - Trang 38- MSSV:69902203bO AN MON HOC GVHD : V6 Thi Ngge Tusi CHUONG 6 : TINH GIA THANH THIET BI Chi it Khéi Iugng vat ligu (kg) ‘Thép X18HLOT CTs Béng thau V6 thép 355.4 Nips day 5 Néi dun 152.2 Ong xodin 237.8 Bich néi than 123.72 Lu@i 43 dem Ludi phan phéi lng 2.79 36.23 Cie Sng din = ‘S811 182.74 273.8 vatligu Gid(ddng/ kg) ‘Thanh én ‘Thép X18HI0T. 50000 29055000 cr: 10000) 1827400 dng thau 15000 3567000 Bulon S6 lun; Gia (déng/ con) | Thanh tién M8 5000 MIO MI2 12 MIG 88 M20 32 740000 Chi tit khée dngidsn vi ‘Thanh tién Lutu lugng ke 500000 1000000 Nhigt ké 200000 200000 Bom 2000000 880000 Téng tién vat ula: 37269400 déng Tidn cong ché tgo tinh bling 100% tién v4t ut. Do 6 tng s6 tién 1a 74538800 déng. SVTH: Vo Ngoc Tiép = Trang 39- MSSV:69902203DO AN MON HOC GVHD : Vo Thi Ngoe Tuoi TAI LIEU THAM KHAO [1]. Vo Van Ban, Vi Ba Minh,” Gido trinh Qud trinh va thiét bi cong nghé héa hoc Tép 3”, BHBK Tp.HCM. [2]. Pham Van Bén, “Gido trink Qud trinh va thiét bi cdng nghé héa hoc Tép 5”, DHBK Tp.HCM. [3]. Pham Van Bon.Va Ba Minh, Hoang Minh Nam, "Gido trinh Qué trinh va thiét bi cng nghé hda hoc Tap 10 Vidu va Bai tap"’, BHBK Tp.HCM. [4]. °Sé tay Qué trinh va thiét bi cong nghé héa hoc Tap 1’', DHBK Ha NOi. LS]. “Sd tay Qué trinh va thiét bj céng nghé héa hoc Tép 2'’, BHBK Ha Noi [6]. Gs,Ts Nguén Bin, ‘’Thiét bj trong céng nghé hod chat va thc phém, Tap 1 va Tap 2” [7], Phan Van Thom,” Sd tay thigt ke thiét bj hod chét va ché ign thuc phdém da dung’’,1992, [8].Hé Lé Vien, “Thiét ké va tinh todn cdc chi tiét thiét bj hod chdt”, Nha x KT-Ha N6i, 1978. [9]-Trin Van Thanh,"'Hod higc hitu co", DHKT Tp. HCM, B6 mén hifu 4,198, bin KH va SVTH: Vo Ngoc Tiép - Trang 40- MSSV:69902203