Professional Documents
Culture Documents
net/publication/237725065
CITATIONS READS
33 345
3 authors:
Zahia Toutou
Saint-Gobain Weber
15 PUBLICATIONS 176 CITATIONS
SEE PROFILE
Some of the authors of this publication are also working on these related projects:
All content following this page was uploaded by Zahia Toutou on 13 November 2019.
Abstract
Squeeze flow of a Bingham fluid between two parallel plates is studied by means of a variational approach [K.J. Zwick, P.S. Ayyaswamy, I.M.
Cohen, Variational analysis of the squeezing flow of a yield stress fluid, J. Non-Newtonian Fluid Mech., 63 (1996) 179–199.]. The trial velocity
field consists of a central region of pure extensional flow, mid-way between the plates, and sheared regions adjacent to the plates. The width of the
region of extensional flow is chosen to minimise an energy dissipation functional. The analysis assumes that the separation of the plates is small
compared to the plate radius, and the predictions are compared with those of previously published analyses.
© 2005 Elsevier B.V. All rights reserved.
Keywords: Squeeze test; Bingham fluid; Squeezing flow paradox; Variational approach; Extensional flow
1. Introduction plates, without any rotation. The upper disc can be displaced at
controlled constant velocity, while the lower one remains sta-
Squeeze tests are often used in practice as a straightforward tionary. The squeezing of the sample between the two plates
technique to determine the flow properties of highly concen- induces a radial and axial flow. R is the radius of the plates,
trated suspensions such as concrete, molten polymers, ceramic h the height of the sample, F the compression load applied on
pastes, etc. Most of those materials behave as highly viscous or the plates and c is the compression speed (Fig. 1). The tested
quasi-plastic fluids and can be described as Bingham fluids as a material fills permanently the area between the plates. In the
first approximation. The maximum particle size and the sliding following, we will speak of large and small h/R ratios. However,
behaviour at the interface of such materials prevent the use of it has to be noted that both small and large h/R ratios are smaller
any traditional viscometric tests (coaxial cylinders or cone-plate than 1. The assumption that the thickness of the sample is small
apparatus for instance). compared to its radius is always assumed to be fulfilled.
In this work, several assumptions on the flow pattern allows The roughness of the plates can be also a test parameter. Use
the generation of a kinematically admissible velocity field in of rough plates imposes a sticking flow; the no-slip boundary
terms of a parameter β, in respect to which a functional is min- condition is assumed to be fulfilled. On the other hand, in the case
imised, using the fact that the upper and lower bounds of this of smooth plates, the material can slip along the solid surface.
functional are converging for small disc separation. The com- Only rough plates and sticking flows are considered in this work.
pression load is calculated from the dissipation inside the sample
and the obtained solution is compared with the literature.
3. Behaviour law
2. Description of the squeeze test
The yield criterion used in the Bingham behaviour law in
this study is the von Mises yield criterion [1]. It writes in three
The squeeze test is a simple compression test (plastometer
dimensions and in the case of an axi-symmetric flow:
test) carried out on cylindrical samples with reduced slender-
When
ness. This apparatus consists in two coaxial circular parallel
1 (d) 2 (d) 2 2
2 (σrr ) + 21 (σθθ ) + 21 (σzz
(d) ) + (σ )2 < K 2
rz i (1)
∗ Corresponding author.
E-mail address: nicolas.roussel@lcpc.fr (N. Roussel). there is no velocity gradient in the sample.
0377-0257/$ – see front matter © 2005 Elsevier B.V. All rights reserved.
doi:10.1016/j.jnnfm.2005.12.001
2 N. Roussel et al. / J. Non-Newtonian Fluid Mech. 135 (2006) 1–7
part. ∂Vr
|σrz | < Ki → =0 (5b)
If (2) is true, the following general form of the behaviour law ∂z
is then used, under the assumption of an incompressible body.
where Vr is the radial flow velocity.
It links the stress tensor deviatoric part and the strain rate tensor
This simplification eases the analytic treatment of the flow
via a scalar function of the second invariant of the rate of strain
but, as a direct consequence, a paradox appears on the mid-plane.
tensor:
By symmetry, the shear stress falls to zero at z = 0. According to
(d)
σij = 2f (I2 )Dij (3) the previous behaviour law, the plastic criterion is not fulfilled
and the fluid must move as a rigid plug. But, at the same time,
the gap between the plates is being narrowed and the fluid has to
yield even on the mid-plane. The plug must therefore deform and
the solution is inconsistent. It should be noted that, even if the
obtained flow field is kinematically inconsistent, the expression
for the compression force in terms of the geometric configura-
tion of the test agrees well with the experimental values on a
variety of yield stress fluids. In fact, while integrating the com-
pression force, any error in the calculated flow field is averaged
and the overall energy dissipation stays in reasonable bounds. As
an alternative, Wilson [5] approximates the behaviour law by a
biviscosity equation. The Bingham model is then approached as
a limit of the biviscosity model. However, this alternative method
is only a way to avoid the paradox in the particular case of the
Bingham fluid. In the more general case, the inconsistency in the
calculated velocity fields is explained by the fact that the lubri-
Fig. 1. Squeeze test geometry. cation analysis only allows a one-dimensional yield criterion to
N. Roussel et al. / J. Non-Newtonian Fluid Mech. 135 (2006) 1–7 3
be specified. Adams et al. [9] can be quoted: “A comprehensive where Γ is an energy function defined by the following relation:
yield criterion is one which is based upon a combination of all
(d) ∂Γ
of the acting components of the stress”. Let us come back now σij = (8)
to the squeeze flow paradox but, this time, let us use the three- ∂Dij
dimensional expression of the von Mises yield criterion (2). The In the squeeze flow geometry studied here, St is the free surface
symmetry imposes that there is a zone around the mid-plane at the periphery of the squeezing test. Boundary conditions are
where the shear stress falls to zero. Eq. (2) then becomes: t = 0 on St . For a Bingham fluid, the Γ function can be written
If using the behaviour laws (3) and (4) in terms of the second
1 (d) 2 (d) 2 2 invariant of the strain rates tensor:
2 (σrr ) + 21 (σθθ ) + 21 (σzz
(d) ) ≥ K 2
i √
Γ = 2ηI2 + 2Ki I2 (9)
there is a velocity gradient.
The previously neglected stress tensor components σrr (d) , σ (d) Zwick et al. [14] found that the lower and upper bounds of the
θθ
and σzz allow the criterion to be fulfilled even on the axis. There
(d) functional Jv associated with the flow of an Herschel–Bulkley
is no rigid plug. The fluid is yielding everywhere in the sample fluid converge (minimum principle for strain and maximum prin-
as assumed in the present study. More recently, Sherwood and ciple for stress) for large values of a non-dimensional parameter
Durban [10] have carried out a rigorous three-dimensional stress that reduces in the case of a Bingham fluid to:
analysis for generalised non-Newtonian fluids, including a Bing- 3Fh
ham fluid, under slip wall boundary conditions. The present work ĥ = (10)
2πKi R3
also follows a three-dimensional approach to a Bingham fluid
squeeze flow but under no-slip wall boundary conditions. A vari- At the end of the test, for small h/R, the strain rate increases.
ational principle is used to obtain an appropriate approximated The viscous stress terms dominate the yield stress terms and the
solution. magnitude of Eq. (10) becomes increasingly great. As the two
bounds of the functional converge for small h/R, it is not of any
interest from a practical point of view to determine both of them
5. Variational analysis
in order to analyse the flow when the film thickness is small
compared to the radius of the plates. Knowing the difficulty of
Using a variational principle which focuses on the rate of
finding a stress field that satisfies both the stress boundaries and
energy dissipation within the control volume bounds a func-
the equilibrium equations, only the upper bound of the func-
tional, which is related to the energy of the flow. This principle
tional is calculated in the present study. The minimum principle
was initially applied by Prager [11] to slow Bingham fluids flow
for strain is used to obtain an appropriate approximation of the
and was then extended by Johnson [12] to creeping flows of
problem solution. A necessary step is then to find a velocity
non-Newtonian fluids. Yoshioka and Adachi [13] showed that
field that satisfies the boundary conditions and the equation of
this principle was applicable for fully yielded flow of yield stress
incompressibility.
fluids.
Let us consider a control volume V, with a surface S divided
6. Bingham fluid flow
into a velocity boundary Sv and a traction boundary St . A bound-
ary value problem for the steady, inertialess flow of an incom-
The volume between the plates can be divided in two zones:
pressible non-Newtonian fluid can be written [14]:
On Sv , U = Vsv (6a) • Zone 1: the plastic criterion is reached and overcome. Shear
flow occurs in this zone.
(d)
On St , n · (σij − pI) = t (6b) • Zone 2: the plastic criterion is reached and the shear stress
equals zero. This zone must include the mid-plane. The flow
(d)
In V, ∇ · (σij − pI) − f = 0 (6c) in this zone is extensional.
β = 2 (3g + 2)sin
⎛ ⎛ √ ⎞⎞
g
1 2 2(3g + 2) 3/2
(3g+2) 3
× ⎝ tan−1 ⎝
⎠⎠ (24)
3 3g (3g + 6g + 4)
2
The perfect plastic fluid is a particular case of the Bingham fluid Fig. 3. Fractures in the outcoming sample (clay paste).
with η → 0. In this case, the Bingham number g → 0 and β → 1.
The shearing flow zone disappears and the flow in the sample or, using Eq. (23) and the definition of the Bingham number:
is entirely extensional and sliding at the interface with a shear √
stress equal to the yield stress. On the other hand, the Newtonian 2πKi R2 (3 3β2 h + βR + 2R)
F =− (27)
viscous fluid is another particular case of the Bingham fluid 3βh(β + 2)
with Ki → 0. In this case, the Bingham number g → +∝ and
The load also depends on the yield stress and on the plastic
β → 0. The extensional flow zone disappears and the velocity
viscosity via the β parameter.
field calculated from (19a) and (19b) equals the theoretical flow
In the case of a perfect plastic fluid, β = 1 and η = 0, the force
field originally given by Stefan [17] for a Newtonian viscous
expression then becomes:
fluid.
2πKi R2 2πKi R3
F =− √ − (28)
8. Compression load 3 3h
Once the flow field is obtained, the constitutive law allows The first term is linked to the dissipation due to the extensional
the identification of the deviatoric part of the stress tensor. The flow whereas the second term is linked to the dissipation associ-
momentum equation gives the pressure gradient at the plate ated with the shear at the plate surface. The first term is generally
interface. The compression load can then be integrated from ignored by previous authors (Covey [18] or Lanos [19]) but is
the pressure on the plates which is itself integrated from the taken in account by Adams et al. [9]. For perfect plastic fluid
flow, this term corresponds to p(r = R, z) = 0 and σrr (d) = 3−1/2 K
pressure gradient. But, as it will be shown in Section 9, there i
has been disagreement about the stress boundary conditions at (effect of the traction in the outcoming sample). The load does
the edge of sample (r = R). As a consequence, the integration of not depend on the compression speed. This was expected from
the pressure gradient is not obvious. Most of the time, p(r = R, an analysis based upon plasticity theory. In the case of a plastic
z = h/2) = 0 is assumed but the pressure for r = R and z ≤ h/2 is fluid, Eq. (28) can be compared to the one obtained by Sher-
unknown. The stress in the outcoming sample that generates wood and Durban [10]. This expression is obtained imposing an
the fractures shown in Fig. 3 is not taken into account in the average boundary condition:
calculation. h/2
In order to avoid any additional assumptions on the stress σrr dz = 0 at r = R (29)
boundary conditions, the value of the force acting on the plates −h/2
boundary condition, which is what “sticking” is usually taken term includes a correction due to the traction effect at r = R dur-
to mean. ing plastic
√ flow. With p(r = R) = 0, the correction term must be
On the other hand, using Eq. (26), in the case of a Newtonian 2Ki h/ 3R.
viscous fluid, β = 0 and Ki = 0 Pa, the load expression is equal to Starting from the fixed plates case, Petrov [20] derived a solu-
the exact solution originally found by Stefan [17] with p(r = R, tion suitable for Bingham number values g 1 (larger h/R):
z = h/2) = 0.
4 4Rηc
3πηcR4 F = Fplast 1 + (34)
F =− (30 ) 5 Ki h 2
2h3
where Fplast is the compression force if the plastic viscosity
9. Comparison with previous solutions equals zero. This can be calculated using (27).
The solution obtained herein can be compared to these solu-
The following reduced parameters are more convenient to tions. As the compression force is calculated from the dissipation
represent the test results [19]; the reduced force F* = −Fh/πR3 and not from the pressure integration on the plates, there is no
and the geometrical ratio h/R. Using this representation, the need for a pressure boundary correction for the largest h/R (but
result for a perfect plastic fluid (Eq. (28) is a linear function still smaller than 1). The proposed solution is in good agreement
of the geometrical ratio h/R: with the corrected lubrication theory (Fig. 4) in the larger h/R
range.
∗ 2Ki h 2Ki
F = √ + (31) The numerical simulations done by Matsoukas and Mitsoulis
3 R 3 [4] taking into account the unyielded regions confined near the
The lubrication theory, in the case of a Bingham fluid flow with center of the disks are also plotted. In the [0.01;0.1] h/R range,
a no-slip condition, gives for the compression force (Sherwood they gave the following approximation of their results:
and Durban [10]): 1.981 1.026
ηcR2 h h
F= 1.282 1 + 1.238g (35)
2πKi R3 4πKi R3 h R R
F= + (2g)1/2 + O(g) (32)
3h 7h
For small h/R, when the viscous effects become predominant,
and the reduced force is a suitable solution should converge towards the purely viscous
solution. This is the case for the solution obtained in this work
2Ki 4Ki ηcR 1/2
F∗ = + 2 for g 1 (33) and for Covey’s solution and the numerical results of Matsoukas
3 7h Ki
and Mitsoulis but not for the lubrication theory, Adams solution
Some corrections were made by Adams et al. [9] in order and Petrov solution. Among the three solutions that tend towards
to take into account the pressure boundary conditions at the the viscous theoretical solution, it can be noted that the numerical
edge. An additive term of order 31/2 Ki h/R appears in F* . This results obtained by Matsoukas and Mitsoulis give the lowest
Fig. 4. Comparison of various theoretical predictions of the reduced force F* = −Fh/πR3 . Compression speed = 2 mm/s, R = 0.05 m, Ki = 6.5 kPa, initial g value = 0.17
for h/R = 0.3.
N. Roussel et al. / J. Non-Newtonian Fluid Mech. 135 (2006) 1–7 7
value of the compression force. As the compression speed is [3] D.N. Smyrnaios, J.A. Tsamopoulos, Squeeze flow of Bingham plastics,
constant, this means that this solution corresponds to the lowest J. Non-Newton. Fluid Mech. 100 (2001) 165–190.
dissipation rate (Eq. (25)). We believe that this means that their [4] A. Matsoukas, E. Mitsoulis, Geometry effects in squeeze flow of Bing-
ham Plastics, J. Non-Newton. Fluid Mech. 109 (2003) 231–240.
solution is the closest to the real velocity field. [5] S.D.R. Wilson, Squeezing flow of a Bingham material, J. Non-Newton.
Fluid Mech. 47 (1993) 211–219.
10. Conclusion [6] J.R. Scott, Theory and application of the parallel-plate plastimeter, Trans.
Inst. Rubber Ind. 7 (1931) 169.
An analytical solution of a Bingham fluid flow between two [7] G.H. Covey, B.R. Stanmore, Use of the parallel plate plastometer for
the characterisation of viscous fluids with a yield stress, J. Non-Newton.
parallel moving plates was determined. The solution obtained Fluid Mech. 8 (1981) 249–260.
is expressed in terms of compression load and plate separation [8] J.D. Sherwood, G.H. Meeten, C.A. Farrow, N.J. Alderman, Squeeze-film
and is suitable for rapid identification of Bingham parameters rheometry of non-uniform mudcakes, J. Non-Newton. Fluid Mech. 39
using the standard assumptions: the studied flow zone is limited (1991) 311–334.
to the volume between the plates and the height of the sample is [9] M.J. Adams, I. Aydin, B.J. Briscoe, S.K. Sinha, A finite element analysis
of the squeeze flow of an elasto-viscoplastic paste material, J. Non-
assumed to be small compared to the plate radius. Newton. Fluid Mech. 71 (1997) 41.
This solution avoids the squeezing flow paradox by using [10] J.D. Sherwood, D. Durban, Squeeze flow of a power-law viscoplastic
a three-dimensional approach and a three-dimensional formu- fluid, J. Non-Newton. Fluid Mech. 62 (1996) 35.
lation of the yield criterion. This demonstrates the need to [11] W. Prager, Studies in Mathematics and Mechanics, R. von Mises Pre-
study this type of flow using three-dimensional criteria even sentation Volume, Academic Press, New York, 1954, pp. 208–216.
[12] M.W.J.R. Johnson, On variational principles for non-Newtonians fluids,
if the problem symmetry and geometry tend to suggest a one- Trans. Soc. Rheologie V (1961).
dimensional approach. The final proposed flow field is a com- [13] N. Yoshioka, K. Adachi, On variational principles for a non Newtonian
bination of an extensional flow zone and a shear flow zone. The fluids, J. Chem. Eng. Jpn. 4 (1971) 217.
thickness of the region of extensional flow is chosen to minimise [14] K.J. Zwick, P.S. Ayyaswamy, I.M. Cohen, Variational analysis of the
an energy dissipation functional. squeezing flow of a yield stress fluid, J. Non-Newton. Fluid Mech. 63
(1996) 179–199.
Finally, the solution obtained was compared to the literature [15] C. Lanos, Reverse identification method associate to compression test,
and seems to be suitable to small and higher h/R ratios. It fulfils in: Proceedings of the XIIIth Int. Cong. on Rheol., vol. 2, Cambridge,
two requirements: it tends towards the perfect plastic solution 2000, pp. 312–314.
for large h/R ratios and towards the Newtonian viscous solution [16] N. Roussel, Analyse des écoulements de fluides homogènes complexes
for small h/R ratios. et plastiques diphasiques: application à l’essai de compression simple,
PhD Thesis, I.N.S.A Rennes, France, 2001.
[17] M.J. Stefan, Akad. Wiss. Wien. Math-Natur. Klassa Abt. 2, 69, 1874.
References [18] G.H. Covey, Application of the parallel plate plastometer to brown coal
rheometry, PhD Thesis, Melbourne University, 1977.
[1] R. von Mises, Mechanik der Plastichen Formänderung von Kristallen, [19] C. Lanos, Méthode d’identification non-viscosimétrique de comporte-
Z. Angew Math. Mech. 6 (1928). ments de fluides, Thesis, I.N.S.A. Rennes France, 1993.
[2] G.G. Lipscomb, M.M. Denn, Flow of Bingham fluids in complex geome- [20] A.G. Petrov, The plane problem of the extrusion of a viscoplastic
tries, J. Non-Newton. Fluid Mech. 14 (1984) 337–346. medium by parallel plates, J. Appl. Math. Mech. 62 (4) (1998) 565–573.