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CommentsReference Material CRM AR-1539 Certificate Number
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CERTIFIED WEIGHT REPORT

Part Number: 93126 Solvent: Lot#
Lot Number: 062921 Ethyl acetate 253613
Description: EPA Method 622 / 8140 - Analytes 062921
19 components Formulated By: Prashant Chauhan DATE
Expiration Date: 062924
Recommended Storage: Freezer (0 ºC)
Nominal Concentration (µg/mL): 200 062921
NIST Test ID#: 6UTB 5E-05 Balance Uncertainty Reviewed By: Pedro L. Rentas DATE
Weight(s) shown below were combined and diluted to (mL): 100.0 0.057 Flask Uncertainty
Expanded SDS Information
Lot Nominal Purity Uncertainty Target Actual Actual Uncertainty (Solvent Safety Info. On Attached pg.)
Compound RM# Number Conc (µg/mL) (%) Purity (%) Weight(g) Weight(g) Conc (µg/mL) (+/-) (µg/mL) CAS# OSHA PEL (TWA) LD50

1. Azinphosmethyl (Guthion) 954 6247400 200 99.5 0.5 0.02010 0.02020 201.0 2.3 86-50-0 0.2mg/m3 (skin) orl-rat 4.4mg/kg
2. Bolstar (Sulprofos) 840 SZBD086XV 200 94.1 0.2 0.02126 0.02136 201.0 1.3 35400-43-2 1 mg/m3 orl-rat 65mg/kg
3. Chlorpyrifos (Dursban) 90 9894900 200 99.6 0.5 0.02008 0.02018 201.0 2.3 2921-88-2 0.2mg/m3 (skin) orl-rat 82mg/kg
4. Coumaphos 596 8447100 200 99 0.5 0.02020 0.02030 201.0 2.3 56-72-4 N/A orl-rat 41mg/kg
5. Demeton, (Mix of Isomers O:S [25%:75%]) 957 11069800 200 94 0.5 0.02128 0.02132 200.4 2.3 8065-48-3 0.1mg/m3 (skin) orl-rat 4mg/kg
6. Diazinon 108 10179800 200 98.1 0.5 0.02039 0.02045 200.6 2.3 333-41-5 0.1mg/m3 (skin) orl-rat 66mg/kg
7. Dichlorvos (Vapona) 151 7670500 200 98.2 0.5 0.02037 0.02047 201.0 2.3 62-73-7 1 mg/m3 (skin) orl-rat 17mg/kg
8. Disulfoton 165 11264900 200 97.9 0.5 0.02043 0.02051 200.8 2.3 298-04-4 0.1mg/m3 (skin) orl-rat 2mg/kg
9. Ethoprop 175 8110700 200 98.8 0.5 0.02024 0.02034 200.9 2.3 13194-48-4 N/A orl-rat 33mg/kg
10. Fensulfothion 510 7562100 200 98 0.5 0.02041 0.02051 201.0 2.3 115-90-2 0.1 mg/m3 orl-rat 1.8mg/kg
11. Fenthion 686 7577600 200 98.4 0.5 0.02033 0.02037 200.4 2.3 55-38-9 0.2mg/m3 (skin) orl-rat 190mg/kg
12. Mevinphos 219 11872800 200 96.3 0.5 0.02077 0.02081 200.4 2.3 7786-34-7 0.1mg/m3 (skin) orl-mus 4.3mg/kg
13. Naled (Dibrom) 953 11902300 200 96.9 0.5 0.02064 0.02074 201.0 2.3 300-76-5 3mg/m3 orl-rat 250mg/kg
14. Parathion methyl 406 10582700 200 98.6 0.5 0.02029 0.02038 200.9 2.3 298-00-0 0.2 mg/m3 orl-rat 14mg/kg
15. Phorate 492 10104200 200 97.5 0.5 0.02051 0.02056 200.4 2.3 298-02-2 0.05mg/m3 orl-rat 1.1mg/kg
16. Fenchlorphos (Ronnel) 951 9402700 200 98.8 0.5 0.02024 0.02034 200.9 2.3 299-84-3 10mg/m3 orl-rat 1250mg/kg
17. Tetrachlorvinphos (Stirophos) 265 7619600 200 99.5 0.5 0.02010 0.02020 201.0 2.3 961-11-5 N/A other-rat 1160mg/kg
18. Tokuthion (Prothiophos) 956 10984900 200 97 0.5 0.02058 0.02068 201.0 2.3 34643-46-4 N/A orl-rat(male) 1569mg/kg
19. Trichloronate 930 CH30415 200 98 0.2 0.02041 0.02051 201.0 1.3 327-98-0 N/A orl-rat 16-37.5mg/kg

• The certified value is the concentration calculated from gravimetric and volumetric measurements unless otherwise stated.
• Standards are prepared gravimetrically using balances that are calibrated with weights traceable to NIST (see above).
• Standards are certifed (+/-) 0.5% of the stated value, unless otherwise stated.
• All Standards, after opening ampule, should be stored with caps tight and under appropriate laboratory conditions.
• Uncertainty Reference: Taylor, B.N. and Kuyat, C.E., "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Result,"
NIST Technical Note 1297, U.S. Government Printing Office, Washington, DC, (1994).

Part # 93126 Lot # 062921 1 of 2 Printed: 7/23/2021, 11:15:04 PM


Absolute Standards, Inc.
800-368-1131
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• The certified value is the concentration calculated from gravimetric and volumetric measurements unless otherwise stated.
• Standards are prepared gravimetrically using balances that are calibrated with weights traceable to NIST (see above).
• Standards are certifed (+/-) 0.5% of the stated value, unless otherwise stated.
• All Standards, after opening ampule, should be stored with caps tight and under appropriate laboratory conditions. ANAB ISO 17034 Accredited
• Uncertainty Reference: Taylor, B.N. and Kuyat, Certified
Comments
C.E., Reference
"Guidelines Material
for Evaluating and ExpressingCRM
the Uncertainty of NIST Measurement Result," AR-1539 Certificate Number
NIST Technical Note 1297, U.S. Government Printing Office, Washington, DC, (1994).
https://Absolutestandards.com

Peak FID RT
No. Analyte (min.)

1 Dichlorvos 7.47
2 Mevinphos 10.73
3 B-Mevinphos impurity 11.07
4 Demeton-O 13.15
5 Ethoprop 13.71
6 Phorate/Naled 14.64
7 Demeton-S 14.74
8 Diazinon 15.29
9 Disulfoton 15.65
10 Fenchlorphos 16.23
11 Parathion methyl 17.76
12 Trichloronate 17.97
13 Chlorpyrifos 18.50
14 Fenthion 19.11
15 Tokuthion 20.54
16 Tetrachlorvinphos 20.65
17 Bolstar 22.60
18 Fensulfothion 22.72
19 Azinphosmethyl 28.62
20 Coumaphos 30.10

Part # 93126 Lot # 062921 2 of 2 Printed: 7/23/2021, 11:15:04 PM