MESSRS. PETROBRAS GLOBAL TRADING B.V / ENI TRADING & SHIPPING S.P.

CERTIFICATE OF QUALITY JOB MA 007/16

VESSEL: MT TORM GUNHILD

VOY. : 006 CT TERMINAL: TA SÃO LUIS
CARGO : DIESEL S-10 DATE: April 24th to 27th, 2016
Samples drawn from the ship's cargo tanks 1P/S; 2P/S; 3P/S; 4P/S; 5P/S; 6P/S from M/T TORM GUNHILD, at TA-SÃO LUIS facilities after
transhipment operation

TANK: Vessel's composite

HOUR: 02:12
DATE: 27/04/2016

ANALYSIS METHODS SPECIFICATION RESULTS

Apperance Visual (1) PASS

95% v/v Recovered, °C EN ISO 3405 360 max 343.3
Recovered at 250°C, %vol EN ISO 3405 65 max 35.5
Recovered at 350°C, %vol EN ISO 3405 85 min 97.1
Total Sulfur, mg/kg EN ISO 20846 10 max 7.2
Viscosity at 40°C, mm²/s EN ISO 3104 2.0 to 4.5 2.721
Cu Strip 3h 50°C, EN ISO 2160 1 max 1
Ash Content, % mass EN ISO 6245 0,01 max 0.002
Flash Point, °C EN 2719A 55.0 min 73.0
Density 15°C, kg/m³ EN ISO 12185 820.0 to 845.0 839.1
EN ISO 12937 200 max 65.1
Water,mg/kg(2)
EN ISO 10370 0.30 max 0.01
Micro Carbon on 10% Residue, %mass
EN 116 0 max -18.0
Cold Filter Plugging Point ,°C
EN ISO 5165 51.0 min 53.0
Cetane Number(2)
EN ISO 4264 46 min 51.1
Cetane Index
Polycyclic Aromatic Hydrocarbons, %mass(2) EN 12916 8 max 1.05
Lubricity, μm(2)(3) EN ISO 12156-1 460 max 402
Oxidation Stability, g/m³(2) EN ISO 12205 25 max 2.0
Total Contamination, mg/kg (2) EN 12662 24 max <6.0
FAME Content, %vol.(4) EN 14078 7.0 max 0.0
Cloud Point, °C(4) EN 23015 report -9.0
Electrical Conductivity, ps/m EN ISO 3170 report 208
Manganese, mg/L(4) EN 16576 report (*)

Remark
All the analysis above were performed in TRANSPETRO's Laboratory and witness by Saybolt Concremat chemister.
( 1 ): Clear and Bright
( 2 ): Analysis were performed in the RNEST-PE laboratory, as per Petrobras's request.
( 3 ): Analysis has been performed without addition of biodiesel
( 4 ): Analysis were performed in the Saybolt laboratory in Aratu-BA.

Valber Reis de Silva

CRQ 015383

São Luis ( MA ) April 27th, 2016

SAYBOLT CONCREMAT
Inspeções Tecnicas Ltda
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