Professional Documents
Culture Documents
for example, whole sections of core have been removed, logging will not be
possible over the affected intervals, and the log must be marked accordingly
(Fig. 4.14).
If good practice has been followed, a note in the core box should give precise
depth details of the samples removed (and perhaps even a brief lithological
description). Sometimes it will be possible to examine these samples at a later
date, and fill in the missing sections of the log.
90
Core logging
Fig. 4.14 On a large-scale log, the precise location of samples taken can be marked on
the graphic lithological column. This is often more informative than a simple depth.
weathering zone at the top. These may be evident to the logger, but the record
of the slight colour change would be buried amongst the text of the log, and
may not be noticed by subsequent users of the log. Suitably labelled trend
arrows would clarify the position, and emphasize an important but subtle
feature of the succession.
Trend arrows and the like can be used wherever the geologist wishes to
highlight some depth-dependent variable of the rock. In addition to grain-size
variation and volcanic cycles, they can indicate changes in the degree of
fracturing, mineralogical composition, angularity of clasts, colour, or anything
else that the geologist thinks may help in the interpretation of the core. The
arrows may be drawn in a column especially reserved for ‘trends’ (Fig. 4.15), or
may be situated in any other convenient position on the log, such as beside the
lithology column, or the written descriptions. It is, of course, important to ensure
that the arrows are properly labelled, so that it is quite clear to what they refer.
91
Cores and Core Logging for Geoscientists
92
Core logging
Fig. 4.15 The use of trend arrows to highlight grain-size variations at different scales.
93
5 Core analysis and testing
94
Core analysis and testing
95
Cores and Core Logging for Geoscientists
Formation
w Pressure Pf
MUD
Pressure
m Pf+δP
Pf+δP
MUD
Pressure Mud cake
Formation Pf+δP
Pressure Pf
FORMATION
Inner core barrel
FORMATION
Mud cake
Pf+δP
Mud cake
Pressure Pf Pressure Pf
Mud
Mud
M
M
n
io
io
ud
ud
at
at
in in
m
va r va r
ding fo ding fo
Pressure
gradient
Pressure Pf
Fig. 5.1 Simplified representation of pressure gradients and the movement of formation
and drilling fluids in a permeable formation being penetrated by a coring bit and
barrel. Pf is the original formation pressure, whereas the mud is (or should be) at a
slightly higher pressure, Pf + dP. The pressure differential δP is responsible for fluid
movements.
become misplaced in the core boxes, owing to their rattling around during
transport. This danger may be averted if the fragment sampled can be clearly
96
Core analysis and testing
identified as a chip off a larger and better labelled core piece. Otherwise, if
sampling accuracy is important, loose chips are best avoided.
The use of a hammer to remove samples from larger sections of core is the
commonest sampling method for indurated lithologies. It is usually easy to
remove samples only from the outside margin of a core, especially if it has not
been slabbed. A chisel may be helpful in sampling from the centre of a length of
core, although it takes practice before this can be done without risking significant
damage to the remaining core.
The simplest method of sampling the interior of a core while minimizing
damage is to use a core plug drill (Section 3.3.2; Fig. 5.2). This is a heavy-duty
bench drill fitted with a hollow cylindrical diamond bit that cuts out a small core
or ‘plug’ from the rock sample. Plug diameters vary, but 25 mm is common (Fig.
5.3). Portable plug drills also exist, but they are rather unwieldy and need a
source of water. Plug samples have the advantage of being accurately positioned
and oriented in the core, and are of uniform size. Damage both to the sample
plug and to the remaining core is minimized.
The preservation of friable or soft core by freezing has been described in
Section 3.2.6. Frozen friable core is not usually easy to sample by hammering, as
it tends to shatter rather than break cleanly. Drilling out core plugs is the simplest
method of removing spot samples, although water, which is the most common
coolant used with the core plug drill, is unsuitable for use with frozen core. The
solution, as with slabbing of frozen core, is to use liquid nitrogen instead of
water: this allows good-quality plugs to be taken, and the additional cooling of
the sample, to a point well below 0°C, allows it to be handled briefly without
thawing. In order for the plug to remain intact once it is thawed, it can be
encased in a tightly fitting sleeve. Lead sleeves were once used, but Teflon or
other plastic is now more common. This plugging of frozen core can be
undertaken on either the unslabbed or the slabbed core. However, frozen core
will often have been recovered and preserved within a sleeve of fibreglass,
aluminium or similar material, and gaining access through this by slabbing or
otherwise, even while frozen, may cause disturbance. An alternative is to use the
core plug drill to cut plugs right through the sleeving, thereby causing the
minimum of sample disturbance.
Problems are caused in a heterogeneous sleeved core where a particular
lithology is required, as one is sampling ‘blind’. The obvious solution is to keep
plugging the core until a sample of the required lithology is obtained. A more
elegant method is to use X-radiography or X-ray tomography (Section 5.2.3) to
‘see’ through the core sleeve and locate the required sampling points.
Sampling of preserved core pieces for the analysis of reservoir fluids can pose
problems, since every effort must be made to prevent the fluids from being
displaced or evaporating. As explained above, samples for reliable fluid analysis
are more likely to be derived from the centre of the core. However, the use of a
97
Cores and Core Logging for Geoscientists
Fig. 5.3 Various types of core sample. The bag contains a core chip, and on the left is a
piece of full-diameter core. Full-diameter samples should be taken only where
absolutely necessary, as they remove a complete section of core. The two cylinders are
25-mm plugs cut from a consolidated core, and on the right is a plug cut with a liquid
nitrogen lubricant from frozen unconsolidated core, and encased in a plastic sleeve.
Discs of wire mesh at each end allow porosity and permeability analysis to be
undertaken.
slabbing saw or core plug drill with associated drilling fluid is likely to
contaminate the original reservoir fluid. Depending on the state of the core, a
suitable piece may be removed from the centre with a hammer and, if necessary,
a chisel, with every effort being made to minimize damage to the remaining core.
It is important to take a single large sample rather than a handful of small
fragments, since fluid will very rapidly evaporate from the latter. If the core has
been frozen at wellsite so that the contained fluids are immobilized, the use of a
core plug drill and liquid nitrogen coolant should allow undisturbed samples for
fluid analysis to be taken from the centre of the core.
Even if the samples were not frozen at the wellsite, they may still be frozen
later and plugged with liquid nitrogen. If, for example, a whole-core sample has
been preserved in wax (Section 3.2.6), it can be frozen and a core plug cut
through the wax coating. The same process can of course be applied to a core
piece on which no preservation technique has been attempted, although the
98
Core analysis and testing
closeness with which the remaining core fluids correspond to the original
formation fluids must in this case be held in considerable doubt.
The samples discussed so far, whether small or large, are all essentially ‘spot’
samples, used to analyse for a certain parameter at some point within the cored
section. However, one of the advantages of a core is that it is not just a series of
spot samples, but a single continuous piece of rock, and some types of analysis
seek to take advantage of this fact. An example is given by permeability analysis.
Permeability is often measured by taking small plugs at specific depths, and the
result is usually quoted as a permeability value at that depth in either a horizontal
or vertical direction (Section 5.2.5). However, it is possible to measure perme-
ability in a whole section of unslabbed core. If an intact length of core is chosen
that is, say, 25 cm long, then the permeability value obtained will not be a spot
analysis, but will be valid over that length of core. In theory, permeability could
be measured over any length of core, but in practice such long sections of intact
core are rarely recovered.
At the other extreme, it can be argued that a standard permeability plug
analysis is not a true ‘spot’ sample, as it is measured on a plug perhaps 25 mm
long. Within this plug, laminae may exist with greatly varying permeability. To
measure at this scale, ‘micropermeameters’ or ‘probe permeameters’ have been
developed (Fig. 5.4). They are mostly variants of flowmeters that measure the
gas, at a set pressure, that enters the rock from a fine-tipped hollow probe
pressed against it. By taking numerous measurements on an inhomogeneous
core, it is possible to determine the lithological features—such as low-
permeability laminae—that control the gross permeability over a greater length
of core.
Suppose an exercise is carried out to calibrate an electric wireline log against
a core taken over a certain interval of a well, and that the wireline log purports to
give an elemental analysis of the formation. It would be possible to take spot
samples of core every 25 cm, say, and to analyse them by X-ray fluorescence
spectrometry (XRF) to obtain an elemental analysis. The XRF results could then
be compared with the wireline log interpretation. However, this would not be a
strictly valid comparison, as no wireline logs analyse a particular point (spot
sample) on the borehole wall. Wireline logs record an integrated result from a
certain depth interval in the well, which is dictated principally by the inherent
resolution of the tool used (Section 2.8).
If the wireline log being calibrated in this instance had a resolution of
50 cm, a better comparison would be achieved by carrying out XRF analyses
on a series of samples, each of which had been obtained continuously over a
50 cm section of core. The analytical results could then be compared with the
electric log value obtained from the point halfway through the sampled
interval (Fig. 5.5). This should give a closer comparison than with the spot
samples taken every 25 cm.
99