Professional Documents
Culture Documents
Ect Test
Ect Test
The Institute of Paper Chemistry (IPC) has provided a high standard of professional service and has exerted its best efforts
within the time and funds available for this project. The information and conclusions are advisory and are intended only for
the internal use by any company who may receive this report. Each company rpust decide for itself the best approach to solv-
ing any problems it may have and how, or whether, this reported information should be considered in its approach.
IPC does not recommend particular products, procedures, materials, or services. These are included only in the interest of
completeness within a laboratory context and budgetary constraint. Actual products, procedures, materials, and services used
may differ and are peculiar to the operations of each company.
In no event shall IPC or its employees and agents have any obligation or liability for damages, including, but not limited to,
consequential damages, arising out of or in connection with any company's use of, or inability to use, the reported informa-
tion. IPC provides no warranty or guaranty of results.
.- -k
TO
MEMBERS OF THE FOURDRINIER KRAFT BOARD GROUP
OF THE
AMERICAN PAPER INSTITUTE
This study was directed toward improving Edge Crush Test (ECT) measurement
technology by developing a safer, simpler, and more efficient method of
sample preparation and testing. The specific objective was to compare ECT
results obtained with unwaxed specimens prepared using newer ECT sample
cutting and supporting procedures with results obtained using the current
TAPPI method.
The 2-inch height dimension of the specimen is cut using a two bladed pneuma-
tic Billerud ECT cutter. The cutter is made by Lorentzen and Wettre, Sweden.
The specimens may be cut to width with the same or some other convenient
cutter. The 2 x 2 inch specimens are tested using a modified Japanese ECT
test fixture (Model 105) marketed by the Sumitomo Corporation, Chicago, IL.
They modified the fixture for us to provide a controlled spring pressure of
up to 11.4 psi for double-wall boards. The fixture fits between the platens
of H&D and rigid platen testers. An easy-to-use design has been recommended
to the Sumitomo Corporation.
Box compression predictions were made using the McKee box compression
equations and each set of ECT data. Predictions made with both the TAPPI and
Japanese test fixture/Billerud cutter ECT values correlated well with actual
box compression results; however, the predictions were generally on the low
side. Slight adjustments of the McKee equation's constants corrected this.
Double-wall predictions were generally low, but the McKee equations were
derived using only single-wall data.
After you have had an opportunity to review the report we will appreciate any
comments you may have.
William J. Whitsitt
Group Leader
Containers Group
Paper Materials Division
WJW/sb
Enclosure
Page
SUMMARY 1
INTRODUCTION 3
Sample Cutters 5
DISCUSSION OF RESULTS 12
Sample Height 12
McKee Formulas 40
Modified Formulas 44
CONCLUSIONS 50
ACKNOWLEDGEMENTS 52
LITERATURE CITED 53
APPENDIX 54
THE INSTITUTE OF PAPER CHEMISTRY
Appleton, Wisconsin
SUMMARY
This study was directed toward improving Edge Crush Test (ECT)
of sample preparation and testing. The specific objective was to compare ECT
results obtained with newer ECT sample cutting and supporting procedures using
unwaxed specimens with results obtained using the current TAPPI method. Three
alternate ECT procedures involving several types of sample cutters and holders
were compared to the standard TAPPI ECT procedure. Approximately 200 lots
ranging from 150 lb. single-wall (SW) to 500 lb. double-wall (DW) boards were
in combination with the 2-inch Billerud cutter, was found to compare the most
favorably with the TAPPI method. Results obtained with the original hand-
tightened version of the fixture showed excellent agreement with TAPPI results,
wall board and high series single-wall board required a higher clamping pressure
to achieve good comparison with TAPPI results. A single set of springs (with
spring constant K = 20.4 lb/inch) which applied pressures of 7.1 psi (on 150-mil
caliper board) and 11.6 psi (on 300-mil caliper board) appeared to work well for
all board series, although a lower pressure could be used for lightweight
boards. An easy-to-use design involving the original fixture fitted with the
Box compression predictions were made using the McKee box compression
equations and each set of ECT data. Predictions made with both the TAPPI and
Japanese test fixture/Billerud cutter ECT values correlated well with actual box
compression results; however, the predictions were generally on the low side.
wall predictions were generally low, but the McKee equations were derived using
bination. ECT results were considerably lower than TAPPI values using these
was also investigated and found to have no effect on ECT in the range of 1.5-2.0
inches. Wedge spacing in the Weyerhaeuser test fixture was not a factor in the
INTRODUCTION
compressive strength (ECT). ECT test results are used to predict top-load box
compression strength.
TAPPI method T811 describes the ECT test. Specimens are cut on a cir-
cular saw into two-inch widths (machine direction) and, depending on flute and
The top and bottom 1/4 inch of the specimen is dipped in wax to provide support
The TAPPI ECT test requires operator care and is very time consuming.
For these reasons we investigated other methods of cutting and supporting speci-
mens to make the test quicker and safer. Other cutting methods investigated
to support the specimen during testing included the SCAN-method support blocks
(see SCAN-P33:71)*, the Weyerhaeuser test fixture (see TAPPI method UM-814), and
platen machines. The original TAPPI method (T811) mandates the use of a
testers have been introduced which utilize fixed platens equipped with a load
cell. TAPPI has revised method T811 to permit use of these machines. (See
blade Billerud knife-cutter, and the Japanese knife-cutter. Each has the advan-
tage of being safer and quicker than saw-cutting; we tested to see which, if
any, works as well. Alternate ways to support the specimen during testing have
also been developed in order to avoid waxing. We studied the Weyerhaeuser test
fixture and the Japanese test fixture, along with the SCAN-method support
SAMPLE CUTTERS
plastic block into which an industrial blade is clamped. The amount of exposed
blade can be adjusted to the caliper of board to be cut. The block rides on the
combined board, which rests on a plywood base. The base has two metal guides at
right angles to each other which hold the combined board in place. The operator
cuts the board by pushing the plastic block along one of the guides. Both
machine and cross-machine direction cuts can be made, but only in two-inch
widths. ,
device which uses air pressure to drive the cutting blades (Fig. 2). Two
blades are mounted on a moving carriage one or two inches apart, depending
on the cutter. The cutting edge of each blade is beveled on one side only and
Project 2695-24 -6- Report One
mounted with the beveled edge facing outward. The specimen is cut cleanly by
the inside, unbeveled edge on each blade. To cut a specimen the operator simply
places a piece of combined board in front of the blades and activates the
carriage. The cross-direction cuts are made with this cutter; the board is
Care must be taken to make sure the blades are mounted squarely; shims are some-
times necessary. The blades must also be replaced after approximately 150 cuts
because of dulling.
guides and cut by pushing a carriage containing a blade over the board. The
-- Z
are 2 x 2 x 20-cm metal ungrooved blocks which are used to hold the specimen
vertical. Once the upper platen begins loading the specimen, the blocks are
removed. Very similar to the TAPPI method, they do not supply any support
;<
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slightly, which clamp the upper and lower 1/4 inch of the specimen. Specimens
the loaded edges of an unwaxed sample (Fig. 6). The clamps, unbeveled, support
a full 2 cm of the specimen on the top and bottom. The fixture is designed for
60-mm-height specimens; two-inch heights work very well. ECT values must be
corrected by adding 1.12 lb. to the reading taken from the compression tester to
take into account the weight of the upper half of the fixture. In the original
design these clamps were tightened by hand. Later versions used a torque wrench
later pages.
Project 2695-24 -10- I Report One
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have a stiff upper platen which is driven at a constant rate, and a rigid lower
platen equipped with a load cell. The test fixtures described above are placed
directly on the lower platen. These machines, pictured in Fig. 7 and 8, are
made by Testing Machines, Incorporated (TMI) and L&W, respectively. We also set
up one of our Instron machines to test in the same manner. These three testers
were compared to the Hinde & Dauch (H&D) flexible-platen testing machine.
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Project 2695-24 -13- Report One
specimens. Thus sample height does not:appear to be a major factor, while wax-
ing does. This should permit using one height for ECT specimens from A-, B-, C-
aL&W tester.
wedges which clamp the top and bottom of the specimen. The wedge spacing is
usually set so that the specimen is held at middepth of the lower holder when
resting-in the groove under its own weight. This wedge setting gives a pinch
fit. Unwaxed specimens were tested on the L&W tester at several wedge settings
other than the pinch-fit setting, using both.saw-cut and Weyerhaeuser-cut speci-
Saw-Cut Specimens
Weyerhaeuser Knife-
Cut Specimens
Waxed-specimen
average from
Table 1 34.7 43.8 67.0 74.0
tester. In Table 4 it is shown that ECT results obtained with the knife cut-
ters are only a few percent below those obtained from saw-cut specimens. This
indicates that either knife cutting method should work satisfactorily in place of
Billerud cutter
(1-inch height)b 31.1 36.8 54.5 - 63.0 46.4 -3.3
Weyerhaeuser cutter
(2-inch height) 29.4 35.8 58.0 63.2 -46.6 -2.9
Saw cut
(2-inch height) 32.2 37.2 54.5 68.0 48.0
variations in wedge spacing of the Weyerhaeuser test fixture do not have a major
effect on ECT results. All of the alternate sample cutting methods appeared to
work satisfactorily. These are examined further in the next section using dif-
methods:
tested on the H&D and L&W testers. The average ECT results for each series are
given in Tables 5 and 6, and the individual data are tabulated in Tables A1-A14
in the appendix. The Weyerhaeuser and SCAN/Billerud methods give about equal
load levels; however, both are about 16% lower than the. TAPPI standard results.
ECT, lb/inch
Weyer- SCAN/ No.
TAPPI, haeuser, Diff., Billerud, Diff., of
waxed no wax % no waxa, % Lots
Composite
average 46.74 39.25 -16.37 38.69 -17.27 69
Total
1001
75.
C
"Z *fa a
hJ 2 5
0
1001
75. a
C
50* a~j~ -
a
a
a
a
1AJ 2 3 -
wi 2 - ___ _ _ _ __ _ __ _ _ _ _ _ __ _ _ _ _ __ _ _ _
I_
75.-
C
a3
50-
Liiw--
251
0i 25 5I 75.,i 160
ECT. TAPPI, H&DI lb/In
IFigure It.. TAPPI ECT tests, L&W tester vs. H&D tester.
~75.
3:~~~~~~~~~~~~~~c1
500
.25-
0
0 25 50 75~~; 100
ECT, WEYERHAEUSER. H&D, lb/in
Figure. 12.,. Weyerhaeuser untaxed ECT tests, L&W tester vs. H&D tester.
Project 2695-24 -21- Report One
100
C:
.0 235
5
I50
Ns
0
0 E25 SC 75 100
ECT, SCAN/BILLERUD, H&D, Ib/in
Figure 13. SCAN/Billerud unwaxed ECT tests, L&W tester vs. H&D tester.
Table 8. Both the Weyerhaeuser and the SCAN/Billerud methods gave lower coef-
ficients of variation than the Standard TAPPI Method, with the SCAN/Billerud
method results exhibiting the lowest variation. This is probably due to the
Japanese cutter and ECT test fixture (JTF). He obtained ECT values which
averaged about 5% lower than TAPPI values, and within-lot variabilities which
were also lower than TAPPI's. We sent Mr. Friedman samples of the four lots on
which we did our preliminary work. He tested the lots using the Japanese cutter
Project 2695-24 -22- Report One
and test fixture, and also using the TAPPI method. His results are summarized
t
in Table 9.
this project. We carried out a similar set of tests which are summarized in
Table 10. The results were again encouraging, with ECT results close to the
most encouraging results were obtained using the recently acquired 2-inch
,rr
Table 9. ECT results obtained with Japanese test fixture by Stone Container. O
0o
cn
ECT, Ib/inch
150 lb SW 200 lb SW 275 lb SW 350 lb IW Composite
(64100A) (64101) (64102A) (64104) (Av.)
Av. Diff., %a Av. Diff., Za Av. Diff., Xa Av. Diff., Xa Av. Diff., Za
Stone, saw-cut, waxedb (TAPPI) 31.0 -4.02 47.1 5.84 68.4 -3.53 74.3 -2.24 55.2 -1.25
Japanese-cut, waxedb 32.3 0.00 47.5 5.74 70.4 -0.71 79.6 4.74 57.5 2.86
Japanese-cut, JTFb 33.4 3.41 43.1 -3.15 65.0 -8.32 70.1 -7.76 52.9 -5.37
Japanese-cut, no JTFb 28.6 -11.46 34.8 -21.80 52.5 -25.95 64.5 -15.13 45.1 -19.32
IPC, Weyerhaeuser method 27.9 -13.62 38.5 -13.48 56.7 -20.03 57.8 -23.95 45.2 -19.14
0
ID
o
rr
O0
1o
Table 10. IPC results with Japanese test fixture. I
4>
ECT, Ib/inch
150 lb SW 200 lb SW 275 lb SW 350 lb DW Composite
Test (64100A) (64101) (64102A) (64104) (Av.)
Lab. Av. Diff., Za Av. Diff., %a Av. Diff., Xa Av. Diff., %a Av. Diff., %a
Japanese-cut, JTFb Stone 34.0 5.26 43.7 -1.80 65.6 -7.48 70.7 -6.98 53.5 -4.29
*
Billerud-cut, JTF IPC 36.0 11.46 43.2 -2.92 66.6 -6.06 72.6 -4.47 54.6 -2.33
Japanese-cut, JTF IPC 32.6 0.93 39.1 -12.13 59.6 -15.94 69.5 -8.55 50.2 -10.20
I
4:'
I
ECT, Coefficient of Variation, X
150 lb SW 200 lb SW 275 lb SW 350 lb DW Composite
(64100A) (64101) (64102A) (64104) (Av.)
o
0
Project 2695-24 -25- Report One
Table 11 summarizes the results by board series, with the actual data
JTF/Billerud ECT results are in very close agreement with the TAPPI tests.
Within-grade correlations with the TAPPI method are good, as is the correlation
over all board grades, shown in Fig.. 14. These coefficients are tabulated in
Table 12. Within-lot variability, shown in Table 13, was much lower with the
ECT, lb/inch
JTF/ No.
TAPPI, Billerud, Diff., of
waxed no waxa % Lots
Composite
average 45.26 45.28 1.13 67
Total
100
75
C 0
Oua
.1
1B
- 350
cP a
25*
0 25 50 75 100
ECT, JTF/BILLERUD, L&W, Ib/ln
Figure 14. TAPPI ECT tests vs. JTF/Billerud unwaxed tests, L&W tester.
Correlation Coefficient
Within-Grade (SW) All Grades
150 175 - 200 · 275
ECT Method
Tests on L&W
TAPPI vs.
Weyerhaeuser 0.80 0.87 0.76 0.87 0.965
TAPPI vs.
SCAN/Billeruda 0.82 0.68 0.57 0.68 0.946
TAPPI vs.
JTF/Billerudb 0.67 0.68 0.75 0.80 0.955
"snug." FKBG members pointed out that this is a possible source of operator
Initially each clamp was tightened with a torque wrench as shown in Fig. 15.
Using an Instron we were able to determine the relationship between the torque
applied and clamping pressure plotted in Fig. 16. Using one single-wall lot,
we tested ECT values over a range of torques, i.e., clamping pressures, as shown
in Fig. 17. While the ECT results are somewhat erratic, it would appear from
this limited study that ECT is relatively constant over a broad range of
clamping pressures. We next retested nine of the original lots at two clamping
pressures (torques) in the middle of this range, 12.1 psi and 15.6 psi. The
results, listed in Table 14, were promising, and we relayed this information to
the Sumitomo Corp. along with our request for a modified fixture.
to clamp. -. i ]_'
, , . . . fs
^v^
. ''' P., ., * C -,
Figure
Figure 15.
15. Sumitomo's Japanese test fixture (JTF)
Sumitomo's (JTF) with torque wrench attached
to clamp.
Project 2695-24 -29- Report One
25'
a
20' a
a X
a x
x
x
UlS
x x
x
0 X
*10. a x
I.
g ax
0
0 5 10 iS 20 25
TORQUE, in-oz
a
o
0
130
r_ oa
0D a
20 O.
a
a
120
110
0 5 10 15 20 25
PRESSURE, psi
Figure 17. Effect of clamping pressure on ECT.
I I I
Project 2695-24 -30- Report One:
ECT, lb/inch
Original
Fixture K=10.1
(Hand- Torque Wrench lb/inch
Series Lot TAPPI Tightened) 12.1 psi 15.6 psi Springs
constant clamping pressure. The clamps lock open for removal and insertion of
the specimen, then slide closed when released to exert a stable, repeatable
clamping pressure for a given caliper. Since the clamping pressure increases
with increasing board caliper, 150 mil spacers were included to be used with
over all single-wall and double-wall board calipers. The fixture came with
springs which had a spring constant of 10.1 lb/inch and produced a clamping
pressure of only 5.3 psi at a clamp opening of 300 mils. (See the top of Table
15.) While this pressure was lower than desired, the arrangement was tested
using the same nine lots mentioned above. These results, listed in the last
column of Table 14, compared fairly well with our previous work. Next, about 20
of the new lots were tested and compared with the corresponding TAPPI values.
Project 2695-24 -31- Report One
Because they compared favorably, all 150 new lots were tested with the modified
fixture as is.
;i i'.-1
PWK
1~~~~~~~~1
I I·
Figure 18. Modified Japanese test fixture (JTF) received from Sumitomo.
Top clamp is locked open.
boards. The modified Japanese test fixture was used with the K=10.1 lb/inch
springs. The 150-mil spacers were inserted when single-wall specimens were
Project 2695-24 -32- .1' ---"Report One
5.3 psi. These results are summarized in Table 16 and Fig. 19; detailed-
averaged lower than the TAPPI method's in all but one series, with the overall
average being lower than TAPPI's. The overall average ECT is 2.7% lower than
the corresponding TAPPI value, which is not as good as with the original fix-
ture. Close examination of the average percent difference reveals that the dif-
ference is about 0.5% low up to and including 200-lb single-wall boards, about
3.0% low for the 275-lb single-wall to 350-lb double-wall series, and about 6.6%
low for the 500-lb double-wall series. The discovery that the differences become
greater as the board gets heavier, along with the weaker than desired clamping
fixture.
140 - o n
125 - S
re0
95 -
65-
E o 0
Figure 19. TAPPI ECT vs. JTF/Billerud ECT, K= 10.1 lb/inch springs, all 150
lots.
Project 2695-24 -33- Report One
from the Institute's shop. These springs were slightly longer, and this prevented
the use of the 150-mil spacers. However, since the heavier weight boards appear
to require a higher clamping pressure, the tests were performed without spacers.
15. Twenty nine lots were retested and compared with the corresponding TAPPI
I
Project 2695-24 -34- IReport One
results, shown in Tables 17 and A30. The average percent difference dropped
from -2.8 to -2.1%. The trend of increasing differences with increasing board
weight is still evident, but to a lesser degree, as can be seen in Fig. 20 and
21. Next, even stronger springs were acquired from the Sumitomo Corp. With a
spring constant of 20.4 lb/inch, these springs exerted a clamping: pressure of 7.1
and 11.6 psi for board calipers of 150 and 300 mils, respectively. (See the
last row in Table 15.) For the same 29 lots, the average percent difference
dropped to -0.7%, as shown in Table 17 and Fig. 22. Only the 500-lb double-
constant with increasing clamping pressure, always remaining lower than TAPPI
140-
125 o
110 -
95-
os
50-
35
Figure 20. TAPPI ECT vs. JTF/Billerud ECT, K = 10.1 lb/inch springs,
29 retested lots.
140 -
r'
r.
125 -
110
|c 0.989
95.
80 o
u
65
35-
Figure 21. TAPPI ECT vs. JTF/Billerud ECT, K = 16.6 lb/inch springs,
29 retested lots.
Project 2695-24 -36- ' Report One,
1I
.S
l-.
u
U
'U
a:
0.
4:
140
JTF/Billerud ECT, lb/inch
Figure 22. TAPPI ECT vs. JTF/Billerud ECT, K = 20.4 lb/inch springs,
29 retested lots.
Coefficient of Variation, %
JTF/Billerud Methoda No.
K = 10.1 K = 16.6 K = 20.4 of
lb/inch lb/inch lb/inch Lots
Series TAPPI Springs Springs Springs Retested
While the agreement between the TAPPI and JTF/Billerud ECT test
methods using the K=20.4 lb/inch springs is excellent, one problem was encountered
with these strong springs, namely, difficulty in operating the clamps repeatedly.
Several hundred repetitions, necessary to test many lots, would be tiring for
the operator. However, the clamps of the original fixture are relatively easy
to operate with these springs, and a simple way was found to eliminate operator
error when hand-tightening these clamps. A schematic of the top view of the
fixture's clamps is shown in Fig. 23. Figure 24a is a schematic of the interior
of the clamp, viewed from the side, when the clamp is open. There is a region
where the clamp knob, while being tightened, becomes loose as the specimen takes
up the load from the springs. This point, where only the springs are allowed to
achieved, and operator error is removed. Figure 24c shows a clamp which is
over tightened, applying additional pressure. As a final test, the 29 lots were
rechecked with this arrangement, see Tables 19 and A31. The results were in
good agreement with the TAPPI ECT test results. This arrangement has been
edge failure is still the predominant mode of failure with this fixture.
However, there is still no evidence to suggest that this results in low ECT
readings.
results. The K = 20.4 lb/inch springs reach the lower end of the "safe pressure
range" discussed earlier, and it is desirable to stay on the low end of this
Japanese test fixture with the 20.4 lb/inch springs gives ECT results which are in
Project 2695-24 -38- Report One
very good agreement with the TAPPI values, in addition to lower variability.
Using these springs in the original fixture results in a quick; easy to operate
Sample
I Clamp
Area Shown in Next Fig
Figure 23. Schematic of Japanese test fixture (JTF) clamp, top view.
Project 2695-24 -39- Report One
Set Screw
To
Knob
of Clamp
Figure 24. Schematic of Japanese test fixture (JTF) clamp, interior view.
a. Clamp open.
b. Clamp properly closed; springs only applying pressure
to specimen.
c. Clamp overtightened; operator has applied additional
pressure to specimen.
Project 2695-24 -40-. '.Report ...One
ECT, lb/inch
JTF/Billerud Methoda
K = 20.4 lb/inch Springs
Number
Modified Diff.,. Original Diff., of Lots
Series TAPPI Fixture % Fixture % Retested
McKee Formulas
box compression predictions were made using each ECT method and compared to
actual box compression values. Predictions were made using the McKee box
compression formula: 1
Z = box perimeter
a,b = constants
4
P = 2.028 (ECT) 0 .7 46 [(DxDy)0.5]0.25 Z0.4 9 2
This equation was used to predict the top-load box compression strength of some
JTF/Billerud (original fixture) ECT test values. The data necessary for these
calculations are listed in the appendix in Table A32. Actual box compression
values and predictions are tabulated in Table A33 and summarized on the top of
Table 20. The percent difference between predicted and actual box compression
is given by:
[(Predicted/Actual)-1] * 100
with regard to sign indicate whether the predictions are in general high or low,
while the average percent differences without regard to sign represent the
overall accuracy of the predictions. Results are given for single-wall data
with and without the double-wall data because the McKee equation was derived
using only single-wall data. Double-wall predictions are generally high. The
last column lists McKee's results for comparison. Note that the JTF/Billerud
method agrees very well with the TAPPI method with both sets of predictions
averaging 7-10% high. The SCAN/Billerud and Weyerhaeuser methods average about
4-7% low. This is expected because of the lower ECT values. Correlation coef-
ficients are all good, improving with the addition of the double-wall data.
McKee et al. 1 simplified their equation when they noticed the linear
Box compression predictions using this equation are listed in Table A34 and sum-
marized at the bottom of Table 20. Again the TAPPI and JTF/Billerud methods are
almost the same as with the long form, but the average percent differences with
regard to sign are only a few percent below zero. The SCAN/Billerud and
Weyerhaeuser methods are both around 20% low, again due to the lower ECT values.
IPC
SCAN/ Weyer- JTF/
TAPPI Billeruda haeuser Billerudb McKee
Long Formula
Short Formula
The most important result is the close agreement between TAPPI and
JTF/Billerud results, for both forms of the equation. Figures 25-26 show the
good agreement between actual and predicted box compression for the two methods
using the McKee short formula. Note how the double-wall predictions are not as
accurate.
2000
1500
X
X
X
I0 X
.0
X
1000- X
a
a
0
500- 0 SINGLE-WALL
x DOUBLE-WALL
Figure 25. Box compression, actual vs. predicted, using McKee short formula,
TAPPI ECT data.
0 0 0 0 0
Project 2695-24 -44- IReport One
2000-
1500-
A
Iwf
X
0)
.0 XS
41000- 00 X
1()B e a
500 1
0 SINGLE-WAU.
a x DOUBLE-WALL
0+
0 500 1000 1500 2000
PREDICTED Ilbs
Figure 26. Box compression, actual vs. predicted, using McKee short formula,
JTF/Billerud ECT data.
Modified Formulas
box compression, the constants in the McKee long formula were rederived using
our TAPPI single-wall ECT data. Our "TAPPI Long Formula" is:
The McKee short formula was also rederived using the relation between flexural
stiffness, caliper, and TAPPI ECT shown in Fig. 27. Our "TAPPI Short Formula"
is:
Project 2695-24 -45- Report One
Using these equations box compression predictions were again made using all four
ECT methods and compared to the actual box compression values. The results are
tabulated in Tables A35-A36 and summarized in Table 21. Using these equations
the TAPPI predictions are now as accurate as McKee's predictions were, which is
expected. The TAPPI and JTF/Billerud predictions still correlate best with the
200-
13
Q 1
en 0
Z 15 0, a
10o
a
a
o o
Q X
E 50
0
0C.,
o F I --
0 .5 1 1.5 2
CALIPER SQUARED X TAPPI ECT
Long Formula
Short Formula
Finally, the constants for the long and short forms of the McKee
Long Formula
P = 2.595 (ECT)0 * 7 22 [(DXDy)0O5].0 27 8 zO.44 4
' 0 7 29
P = 2.445 (ECT) [(DXDY)0.5] 0 .2 7 1 z0. 4 5 8
P = 2.049 (ECT) 0 '7 3 3
[(DXDY)0.5] 0 .2 6 7 z0. 4 66
Short Formula
P = 9.953 (ECT) H0 .5 5 6 Z0 44 4 '
P = 9.010 (ECT) H0 .5 4 2 Z 0 .4 58
P = 7.044 (ECT) H0O 5 34 Z0 4 66
Project 2695-24-4-RprOe -47 Report One
1300,
K
K
K
A K
K
100 03 K
lb o
a
a3UINOL-WA.LL
X DOUBLE-WALL
s0o
2000-
1500w
K
K
~1000. 00a
a 03
03
500-
o UNOLE-WALL
x DOUBLE-WALL
Predictions made with these formulas are listed in Tables A37-A38 and summarized
in Table 22. In all cases the average percent differences without regard to
sign remains relatively constant; however, the average difference with regard to
Long Formula
Short Formula
2000-
1500-
a x
x
XS
X 1000- x
D o
500-
13 1 SINGLE-WALL
x DOUBLE-WALL
0+
0 500 1000 1500 2000
PREDICTED, Ibs
Figure 30. Box Compression, actual vs. predicted, using "JTF/Billerud Short
Formula", JTF/Billerud ECT data.
ECT box compression predictions, it appears that the JTF/Billerud method is the
M M
Project 2695-24 -50- .. Report .One -
CONCLUSIONS
In the exploratory study it was shown that sample height was not a
major factor in ECT results in the range of 1-2 inches. Gap width in the
Weyerhaeuser test fixture was also not critical in the range of (-2)-(+4) mils
around a "snug fit." Waxing was found to be important, indicating the need for
The JTF/Billerud method was found to most closely duplicate the TAPPI.
results. Springs with a spring constant of K.= 20.4 lb/inch in the Japanese test
fixture appear to supply the appropriate pressure for all series boards from
with the Japanese test fixture, but this does not cause a decrease in measured
ECT. The Billerud cutter appears to be the best alternate cutting procedure.
This is partly due to the dual blade setup which cuts specimens quickly and
cleanly. Also, because the beveled edge of each blade faces outward, the cut
edges of the specimen are less damaged. This is not always the case with the
other cutters. The Billerud cutter must be properly maintained to ensure that
The box compression study again showed the JTF/Billerud method-to most
closely duplicate the TAPPI results.' Using the Mckeel and "TAPPI" equations,
both the TAPPI and JTF/Billerud method's average predictions were very similar.
The SCAN/Billerud and Weyerhaeuser method's average predictions were also simi-
ACKNOWLEDGMENTS
The authors wish to thank the Fourdrinier Kraft Board Group for its
staff members Ann Mahoney, Gerald Hoffman, and Carl Smith for their work and
advice.
Project 2695-24 -53- Report One
LITERATURE CITED
Kurt E. Schrampfer /
Research Fellow
Paper Materials Division
Will'm J. WhitsitF
Research Associate
Containers Group Leader
Paper Materials Division
Gary A. Baum
Director
Paper Materials Division
Project 2695-24 -54- Report One,·
Table Al. 150-Lb series single-wall ECT results, TAPPI method vs.
Weyerhaeuser method.
ECT, lb/inch
H&D Tester L&W Tester
Weyer- Weyer-
Lot, TAPPI, haeuser, Diff., TAPPI, haeuser, Diff.,
flute waxed no wax waxed no wax %
Standard
deviation 3.47 2.57 -- 3.43 2.15
Project 2695-24 -55- Report One
Table A2. 175-Lb series single-wall ECT results, TAPPI method vs.
Weyerhaeuser method.
ECT. lb/inch
H&D Tester L&W Tester
Weyer- Weyer-
Lot, TAPPI, haeuser, Diff., TAPPI, haeuser, Diff.,
flute waxed no wax waxed no wax %
Standard
deviation 4.37 4.22 4.75 3.54
Project 2695-24 -56- Report One
Table A3. 200-Lb series single-wall ECT results, TAPPI method vs.
Weyerhaeuser method.
ECT, lb/inch
H&D Tester L&W Tester
Weyer- Weyer-
Lot, TAPPI, haeuser, Diff., TAPPI, haeuser, Diff.,
flute waxed no wax % waxed no wax ., % . *
Standard
deviation 4.75 3.37 4.59 2.81
Project 2695-24 -57- Report One
Table A4. 275-Lb series single-wall ECT results, TAPPI method vs.
Weyerhaeuser method.
ECT. lb/inch
H&D Tester L&W Tester
Weyer- Weyer-
Lot, TAPPI, haeuser, Diff., TAPPI, haeuser, Diff.,
flute waxed no wax % waxed no wax
Standard
deviation 7.25 4.58 7.06 4.64
Project 2695-24 -58- .Reo~ort· One
Table A5. 200-Lb series double-wall ECT results, TAPPI method vs.
Weyerhaeuser method.
ECT, lb/inch
H&D Tester L&W Tester
Weyer- Weyer-
TAPPI, haeuser, Diff., TAPPI, . haeuser, Diff.,
Lot waxed no wax % waxed ; no wax 0
Standard
deviation 3.08 2.58 0.57 2.26
Project 2695-24 -59- -'Report One
Table A6. 275-Lb series double-wall ECT results, TAPPI method vs.
Weyerhaeuser method.
ECT, lb/inch
H&D Tester L&W Tester
Weyer- Weyer-
TAPPI, haeuser, Diff., TAPPI, haeuser, !Diff.,
Lot waxed no wax % waxed no wax %
Standard
deviation 4.03 4.56 4.14 4.79
Project 2695-24 -60- Report.One.
Table A7. 350-Lb series double-wall ECT results, TAPPI method vs.
Weyerhaeuser method.
ECT, lb/inch
H&D Tester L&W Tester
Weyer- Weyer-
TAPPI, haeuser, Diff., TAPPI, haeuser, Diff.,
Lot waxed no wax waxed no wax %
Standard
deviation 7.14 5.15 6.24 3.95
Project 2695-24 -61- Report One
Table A8. 150-Lb series single-wall ECT results, TAPPI method vs.
SCAN/Billerud method.
ECT. lb/inch
H&D Tester L&W Tester
SCAN/ SCAN/
Lot, TAPPI, Billerud, Diff., TAPPI, Billerud, Diff.,.
flute waxed no wax % waxed no wax %
Standard
deviation 3.47 3.59 3.43 3.21
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Project 2695-24 -63- Report One
Table A10. 200-Lb series single-wall ECT results, TAPPI method vs.
SCAN/Billerud method.
ECT. lb/inch
H&D Tester L&W Tester
SCAN/ SCAN/
Lot, TAPPI, Billerud, Diff., TAPPI, Billerud, Diff.,
flute waxed no wax % waxed no wax %
Standard
deviation 4.75 2.92 4.59 2.91
Project 2695-24 -64- Report One
Table All. 275-Lb series single-wall ECT results, TAPPI method vs.
SCAN/Billerud method.
ECT. lb/inch
H&D Tester L&W Tester
SCAN/ ,SCAN/
Lot, TAPPI, Billerud, Diff., TAPPI, Billerud, Diff.,
flute waxed no wax % waxed no wax %
Standard
deviation 7.25 4.76 7.06 5.10
'7L' LS'0 1tL0 90 * uoTI PAO1'
.Pjepuels
06'L- 0V'6~ E6'ZS 92e.Ay
E1£*9- 01.ES LO'l- 096O SLIOS 9il1
0 L67
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Po am iddvi '8:1nsa.i 10 TIL--aTqnop sea~s q'i-!OOZ ,ZIV aTqul
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Project 2695-24 -66- .Report-One:
Table A13. 275-Lb series double-wall ECT results, TAPPI method vs.,
SCAN/Billerud method.
ECT. lb/inch
H&D Tester L&W Tester
SCAN/ SCAN/
TAPPI, Billerud, Diff., TAPPI, Billerud, Diff.,
Lot waxed no wax % waxed no wax %
Standard
deviation 4.03 2.54 4.14 2.29
Project 2695-24 -67- Report One
Table A14. 350-Lb series double-wall ECT results, TAPPI method vs.
SCAN/Billerud method.
ECT. lb/inch
H&D Tester L&W Tester
SCAN/ SCAN/
TAPPI, Billerud, Diff., TAPPI, Billerud, Diff.,
Lot waxed no wax % waxed no wax
Standard
deviation 7.14 2.50 6.24 3.36
Project 2695-24 -68- ~,. Report One
ECT, lb/inch
L&W Tester
T-1:
J Lr/
Lot, TAPPI, Billerud, Diff.,
flute waxed no wax
Standard
deviation 3.43 3.08
Project 2695-24 -69- Report One
Table A16. 175-Lb series single-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT, lb/inch
L&W Tester
JTF/
Lot, TAPPI, Billerud, Diff.,
flute waxed no wax %
Standard
deviation 4. 75 3. 5
Project 2695-24 -70- , .; RiRport- One'
Table A17. 200-Lb series single-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT, lb/inch
L&W Tester
JTF/
Lot, TAPPI, Billerud', Diff.,
flute waxed no wax %'
Standard
deviation 4. 59 2. 58
Project .2695-24 -71- Report One
Table A18. 275-Lb series single-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT. lb/inch
L&W Tester
JTF/
Lot, TAPPI, Billerud, Diff.,
flute waxed no wax %
Standard
deviation 7.29 5.99
Project 2695-24 -72- Report One
Table A19. 200-Lb series double-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT, lb/inch
L&W Tester
JTF/
Lot, TAPPI, Billerud, Diff.,
flute waxed no wax %
Table A20. 275-Lb series double-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT, lb/inch
L&W Tester
JTF/
TAPPI, Billerud, Diff.,
Lot waxed no wax %
Standard
deviation 4.14 2.97
Project 2695-24 -74- Re'port:.One
Table A21. 350-Lb series double-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT. lb/inch
L&W Tester
JTF/
TAPPI, Billerud, Diff.,
Lot waxed no wax %
Standard
deviation 6.24 2.17
Project 2695-24 -75- Report One
Table A22. 150-Lb series single-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT, lb/inch
JTF/
Lot, TAPPI, Billerud, Diff.,
flute waxed unwaxed %
Standard
deviation 2.48 2.38
Project 2695-24 -76- I. 'Report. One
Table A23. 175-Lb series single-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT, lb/inch
JTF/
Lot, .TAPPI, Billerud, Diff.,
flute waxed unwaxed %
Standard
deviation 3.68 3.55
Project 2695-24 -77- Report One
Table A24. 200-Lb series single-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT, lb/inch
Lot, TAPPI, Billerud, Diff.,
flute waxed unwaxed %
Standard
deviation 3.73 3.94
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Project 2695-24 -79- Report One
Table A26. 350-Lb series single-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT, lb/inch
JTF/
Lot, TAPPI, Billerud, Diff.,
flute waxed unwaxed
Standard
deviation 5.50 . 3.80
Project 2695-24 -80- -Report ,One
Table A27. 275-Lb series double-wall ECT results, TAPPI method vs.
JTF/Billerud method. -
ECT, lb/inch
JTF/
Lot, TAPPI, Billerud, Diff.,
flute waxed unwaxed
Standard
deviation 6.55 6.23
Project 2695-24 -81- Report One.
Table A28. 350-Lb series double-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT. lb/inch
JTF/
Lot, TAPPI, Billerud, Diff.,
flute waxed unwaxed
Standard
deviation 8.83 7.93
Project 2695-24 -82- Report-·One
Table A29. 500-Lb series double-wall ECT results, TAPPI method vs.
JTF/Billerud method.
ECT. lb/inch
JTF/
Lot, TAPPI, Billerud, Diff.,
flute waxed unwaxed %
Standard
deviation 9.52 7.30
Project 2695-24 -83- Report -One
ECT, lb/inch
JTF/Billerud Method
K = 10.1 K = 16.6 K = 20.4
Series, lb/inch lb/inch lb/inch
flute Lot TAPPI Springs % Diff. Springs % Diff. Springs % Diff.
E( :T, lb/inch
JTF/Billerud Method
K = 20.4 lb/inch Springs
Sseries, Modified Original
flute Lot TAPPI JTF % Diff. - JTF % Diff.
Table A33. Box compression predictions using McKee equation: long formula.
105 150 C 587 677 15.41 567 -3.35 595 1.34 651 10.98
113 150 C 346 419 21.09 362 4.73 349 0.92 435 25.85
123 150 C 603 594 -1.51 521 -13.68 541 -10.26 653 8.36
134 150 C 492 512 3.99 467 -5.06 447 -9.20 494 0.47
159 150 C 500 608 21.58 492 -1.69 527 5.40 571 14.28
166 150 C 643 742 15.42 636 -1.04 648 0.82 740 15.04
169 150 C 444 414 -6.79 343 -22.70 389 -12.34 443 -0.18
127 150 B 508 459 -9.64 415 -18.26 400 -21.27 479 -5.62
130 150 B 504 550 9.22 497 -1.30 452 -10.22 595 18.10
137 150 B 471 470 -0.25 403 -14.53 394 -16.44 458 -2.71
150 150 B 395 400 1.18 390 -1.32 387 -1.98 453 14.79
112 175 C 602 685 13.74 524 -12.93 569 -5.42 645 7.22
120 175 C 550 561 1.96 476 -13.48 469 -14.70 554 0.66
133 175 C 656 751 14.54 681 3.78 624 -4.84 730 11.33
142 175 C 601 665 10.65 589 -2.04 569 -5.38 642 6.86
144 175 C 466 524 12.45 472 1.36 466 0.09 538 15.46
149 175 C 489 462 -5.52 472 -3.50 443 -9.34 543 11.12
154 175 C 701 731 4.32 638 -8.96 622 -11.26 739 5.41
163 175 C 746 788 5.56 660 -11.51 687 -7.84 775 3.95
165 175 C 946 992 4.86 864 -8.71 839 -11.29 961 1.57
167 175 C 547 612 11.94 541 -1.06 524 -4.28 626 14.36
109 175 B 421 407 -3.42 355 -15.57 323 -23.39 425 0.97
117 175 B 565 566 0.11 440 -22.11 459 -18.77 571 0.99
126 175 B 465 480 3.22 442 -4.98 412 -11.30 495 6.55
136 175 B 553 523 -5.51 536 -3.10 493 -10.84 628 13.49
151 175 B 448 555 23.87 480 7.10 480 7.10 550 22.82
111 200 C 695 735 5.69 641 -7.83 681 -1.98 773 11.28
115 200 C 680 698 2.60 639 -5.97 656 -3.51 709 4.33
119 200 C 788 770 -2.24 618 -21.57 662 -16.02 734 -6.80
122 200 C 642 649 1.07 531 -17.21 556 -13.43 673 4.84
158 200 C 714 727 1.89 588 -17.58 621 -12.97 724 1.42
108 200 B 541 635 17.34 543 0.45 543 0.34 640 18.38
116 200 B 578 636 9.98 497 -13.98 499 -13.68 603 4.30
118 200 B 583 658 12.86 539 -7.59 583 -0.03 666 14.22
125 200 B 502 597 18.84 565 12.55 558 11.14 635 26.47
135 200 B 571 566 -0.87 472 -17.40 486 -14.90 545 -4.52
100 275 C 800 813 1.57 657 -17.90 718 -10.31 797 -0.41
101 275 C 910 972 6.78 791 -13.09 849 -6.70 923 1.46
110 275 C 751 914 21.73 671 -10.67 743 -1.06 873 16.29
121 275 C 830 833 0.33 687 -17.19 724 -12.82 832 0.22
128 275 C 705 847 20.12 797 13.10 775 9.97 851 20.73
132 275 C 892 967 8.40 845 -5.30 890 -0.27 975 9.29
147 275 C 973 950 -2.40 970 -0.31 915 -5.94 142 17.37
Project 2695-24 -88- -Report Owe
152 275 C 705 754 6.94 650 -7.83 640 -9.21 733 4.03
124 275 B 800 964 20.55 804 0.50 813 1.67 980 22.46
140 275 B 643 767 19.22 597 -7.09 627 -2.47 782 21.61
106 200 IW 1219 1353 11.00 1254 2.91 1310 7.45 386 13.72
102 275 DW 1427 1477 3.48 1455 1.98 1481 3.75 557 9.10
114 275 DW 1101 1220 10.81 1084 -1.54 1148 4.30 277 16.00
141 275 DW 1003 1091 8.77 '1001 -0.16 969 -3.41 131 12.71
153 275 DW 1463 1687 15.28 1397 -4.50 1398 -4.42 533 4.80
161 275 DW 1111 1476 32.85 1290 16.09 1377 23.91 407 26.60
143 350 DW 1278 1683 31.67 1405 9.92 1502 17.53 491 16.70
145 350 DW 1072 1380 28.74 1162 8.36 1235 15.24 384 29.06
152 275 C 705 663 -5.92 543 -22.92 533 -24.47 639 -9.34
124 275 B 800 882 10.24 691 -13.62 702 -12.27 901 12.59
140 275 B 643 665 3.41 476 -25.97 508 -21.00 683 6.20
106 200 DW 1219 1382 13.34 1248 2.40 1323 8.50 1427 17.08
102 275 DW 1427 1413 -0.95 1386 -2.88 1418 -0.60 1517 6.32
114 275 DW 1101 1219 10.70 1040 -5.51 1124 2.07 1296 17.70
141 275 DW 1003 1050 4.67 936 -6.68 895 -10.74 1101 9.78
153 ' 275 DW 1463 1737 18.73 1350 -7.75 1351 -7.65 1529 4.48
161 275 ID 1111 1490 34.10 1243 11.92 1357 22.15 1397 25.72
143 350 DW 1278 1621 26.83 1272 -0.44 1392 8.91 1379 7.88
145 350 DW 1072 1377 28.45 1093 1.96 1187 10.72 1382 28.88
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Table A37 (Continued). Box compression predictions using modified long formulas.
#
Modified Eauation
.....
S;CAN/ Weyer- JTF/
Series/ Actual, Bil lerud, Diff., haeuser, Diff. , Billerud, *Diff.,
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Table A38 (Continued). Box compression predictions using modified short formulas.
Modified Equation
SCAN/ Weyer- JTF/
, Series/ Actual, Billerud, Diff., haeuser, Diff., Billerud, Diff.,
Lot Flute lb lb % lb % lb %
A
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