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Journal of Materials Processing Technology 237 (2016) 31–47

Contents lists available at ScienceDirect

Journal of Materials Processing Technology


journal homepage: www.elsevier.com/locate/jmatprotec

Analysis of longitudinal weld seam defects and investigation of


solid-state bonding criteria in porthole die extrusion process of
aluminum alloy profiles
Junquan Yu, Guoqun Zhao ∗ , Liang Chen
Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials (Ministry of Education), Shandong University, Jinan, Shandong 250061, PR
China

a r t i c l e i n f o a b s t r a c t

Article history: In porthole die extrusion process of aluminum alloy profiles, the formation of longitudinal weld seams
Received 22 January 2016 (L-seams) is inevitable. Analysis of L-seam defects and investigation of solid-state bonding criteria are
Received in revised form 7 April 2016 important issues for practical production. In this study, a set of modular porthole extrusion dies with
Accepted 21 May 2016
different depths of welding chambers were designed and manufactured. The profiles extruded with dif-
Available online 24 May 2016
ferent depths of welding chambers were obtained by performing extrusion experiments.The welding
quality of extruded profiles was characterized by means of microstructure observation, tensile test and
Keywords:
fracture analysis. The true stress-strain curves of homogenized AA6063 aluminum alloy with various
Aluminum alloy profile
Extrusion
strain rates and deformation temperatures were obtained by means of isothermal hot compression test.
Weld seam defect Three-dimensional transient numerical simulation models of the porthole die extrusion processes were
Welding path established. Flow behaviors of aluminum alloy in porthole die extrusion process were investigated, and
Bonding criterion the formation processes of L-seams and their defects were revealed. The solid-state bonding processes
of metal particles were traced and their welding paths were determined. Finally, based on the plastic
deformation and diffusion mechanisms for closure behaviors of micro voids on contact interfaces, a new
dimensionless solid-state bonding criterion related to stress triaxiality, effective strain rate, temperature
and contact time was proposed. The bonding quality of L-seams of extruded profiles without any macro
defect was predicted successfully by using this new criterion. In addition, it was found that the forma-
tion of a macro hole in the profile extruded with a shallow welding chamber is attributed to metal flow
behavior, and does not relate to solid-state bonding process.
© 2016 Elsevier B.V. All rights reserved.

1. Introduction pose of high productivity, this kind of aluminum alloy profiles are
usually extruded by using porthole die direct extrusion process.
Due to the advantages of recyclability, light-weight and excel- In porthole die extrusion process of hollow section profiles,
lent corrosion resistance and mechanical properties, aluminum when a preheated aluminum alloy metal is extruded into portholes,
alloy profiles play an important role in many fields, such as railway it is firstly split into several separate streams by bridges, and then
transportation, shipbuilding, automobile industry, aerospace man- the streams are rejoined together in welding chamber. Finally, the
ufacturing, electronic equipment and engineering structure. As a rejoined metal breaks through the bearing of lower die and forms
typical plastic deformation process, hot extrusion process has been a profile with longitudinal weld seams (L-seams) inside. Owing to
widely used to produce various kinds of aluminum alloy profiles. improper extrusion process parameter or die structure, unsound
With the development of industry, the hollow section profiles with bonding may occur in the forming process of a hollow section pro-
large scale, thin-wall, multi-cavity and complex cross-section, as file. Kim et al. (2002) stated that the failure of a hollow section
shown in Fig. 1, are drawing more and more attention and the profile mostly occurs along or around L-seams when the profile is
demand for these profiles is increasing significantly. For the pur- subjected to severe internal pressure in the practical use. Therefore,
L-seams are usually the weakest areas of hollow section profiles.
In practice, the welding quality of profiles with large scale, multi-
∗ Corresponding author. cavity and complex cross-section can be detected by means of burst
E-mail addresses: yujunquansdu@163.com (J. Yu), zhaogq@sdu.edu.cn (G. Zhao), test. Fracture always occurs at the position where the L-seam has
chenliang@sdu.edu.cn (L. Chen).

http://dx.doi.org/10.1016/j.jmatprotec.2016.05.024
0924-0136/© 2016 Elsevier B.V. All rights reserved.
32 J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47

inside the welding chamber must exceed a critical limit to form


a sound weld seam. More recently, Plata and Piwnik (2000) pro-
posed the pressure-time criterion (Q criterion), which is stated
as that the integral of ratio of contact pressure to material flow
stress on time on welding surface must exceed a critical value to
obtain a sound weld seam. Finally, Donati and Tomesani (2004)
proposed the pressure-time-flow criterion (K criterion), which
is stated as that a sound weld seam can be formed once the
integral of ratio of contact pressure to material flow stress on
all possible welding paths on welding surface exceeds a critical
value.
(2) Numerical simulations. In the extrusion process with a port-
hole die, relevant physical variables such as pressure, effective
stress and metal flow velocity are important for welding quality
evaluation of L-seams, and these physical variables are usually
obtained by means of numerical simulation. Currently, the port-
hole die extrusion process is simulated mainly by using Deform
software based on Lagrange algorithm or HyperXtrude software
based on arbitrary Lagrange-Euler (ALE) algorithm. Based on
Fig. 1. Aluminum alloy profiles with large scale, thin-wall, multi-cavity and complex the bonding criteria and the numerical simulation softwares
cross-section. mentioned above, Güley et al. (2013) studied the effect of die
design on the welding quality during solid state recycling of
poor welding quality, as shown in Fig. 2. Consequently, investi- AA6060 chips, and Chen et al. (2011) evaluated the welding
gating the formation mechanism of L-seams and their defects and quality of a complex aluminum alloy multi-cavity wallboard of
establishing criterion for welding quality prediction have impor- high-speed train.
tant theoretical significance and engineering application values for (3) Physical simulations. In fact, the formation of an L-seam in pot-
extrusion die and extrusion process design to ensure the welding hole die extrusion process is belonged to solid-state bonding
quality of L-seams. process. Physical simulation means that the formation of an L-
Defects of L-seams of profiles extruded by porthole dies can be seam in porthole die extrusion process is simulated by means
classified into two categories: macro and micro defects. The macro of some basic solid-state bonding tests, such as the uniaxial
defects refer to macro holes or gaps which are formed on unbond- hot compression test used by Edwards et al. (2009) and the flat
ing surfaces. The micro defects refer to micro voids, cracks, oxide rolling experiment reported by Ceretti et al. (2009). By combin-
films, or other inclusions, which result in unsound bonding of metal ing numerical simulation with uniaxial hot compression test,
atoms on bonding interface. In practise, defects of L-seams are Tang et al. (2014) evaluated the weld seam quality of a micro
mainly caused by improper extrusion die structure. Den Bakkera channel tube according to the relationship of welding chamber
et al. (2014) found that a very shallow welding chamber can cause height, hydrostatic pressure and L-seam welding strength.
the appearance of a macro hole defect on profile’s cross-section.
Valberg et al. (1995) found that a relative shallow welding cham-
ber can lead to a transition of sticking friction to sliding friction at Although some research has been done to investigate the L-
the rear end of bridge. This transition results in the formation of seams’ defects and the bonding criteria in porthole die extrusion
free metal surfaces which are pressed into each other by classical process of aluminum alloy profiles, several critical problems still
pressure welding to form L-seams. As a result, some oxide particles need to be further classified.
may exist in L-seams. Furthermore, Donati and Tomesani (2005) Firstly, there are still some problems for the evaluation method
found that a deep and large welding chamber contributes to the of welding quality of L-seams. Most of previous studies took the
improvement of welding quality and extrusion speed limit. average effect of the whole bonding zone of an L-seam on profile’s
In order to evaluate the welding quality of L-seams of extruded cross-section as a standard to evaluate the welding quality of the
aluminum alloy profiles, researchers mainly carried out following L-seam. Namely, only the overall effect of relevant physical quanti-
studies. ties of all the particles in welding plane on the welding quality of an
L-seam is considered. However, the recent study of Yu et al. (2016)
(1) Bonding criteria. Several bonding criteria were established showed that the welding quality in the whole bonding zone of an L-
according to extrusion experimental results and theoretical seam on profile’s cross-section is usually variable. Since the failure
derivation. Akeret (1972) earliest proposed the maximum pres- is easy to originate at the weakest bonding position, the welding
sure criterion, which is stated as that the maximum pressure quality of each particle of an L-seam should be evaluated individ-

Fig. 2. Burst test for a hollow section aluminum alloy profile: (a) test equipment, (b) fracture location.
J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47 33

Fig. 3. Experimental extrusion dies.

Fig. 4. Dimensions of bridges (Unit: mm).

ually. For this purpose, the true welding path of each particle of an Based on the aforementioned reasons, in this study, firstly, a
L-seam should be determined. set of modular porthole extrusion dies with different depths of
Secondly, the existing bonding criteria are still not perfect. For welding chambers were designed and manufactured. The profiles
the solid-state bonding process of aluminum alloy extrusion, the extruded with different depths of welding chambers were obtained
existing bonding criteria mainly take pressure, effective stress, by performing extrusion experiments. Welding quality of extruded
velocity and time into consideration. Both the Q and K criteria con- profiles was systematically characterized by means of microstruc-
sider the effect of temperature on bonding quality just through the ture observation, tensile test and fracture analysis. After that,
effect of temperature on material flow stress. The experimental three-dimensional transient numerical simulation models of the
results of Bariani et al. (2006) showed that the increase of the ratio porthole die extrusion processes were established. Flow behaviors
of hydrostatic pressure to effective stress allows complete weld- of aluminum alloy in the porthole die extrusion process were inves-
ing to take place at a lower temperature. Ceretti et al. (2009) found tigated, and the formation processes of L-seams and their defects
that the critical value of the Q criterion is a function of tempera- were revealed. Solid-state bonding processes of metal particles
ture. In addition, the experimental results of Valberg et al. (1995) were traced and true welding paths were determined. Finally, based
demonstrated that improper extrusion die structure can result in on experimental results and solid-state bonding theory and by syn-
an incomplete filling of metal in welding chambers and the for- thesizing various factors affecting solid-state bonding process, a
mation of gas pockets. In this case, the surfaces of split metal new dimensionless solid-state bonding criterion was established.
streams are oxidized to some extent. Edwards et al. (2009) further This new criterion considered the actions of both plastic deforma-
revealed that the surface stretching parameter (strain) is the most tion and atomic diffusion from the viewpoint of closure behaviors
influential parameter for the bonding process of specimens that of micro voids on contact interfaces. According to this new bonding
were covered with oxide layers. However, the K criterion based on criterion, the bonding quality of L-seams obtained by means of the
the experiments of Valberg et al. (1995) does not take strain into extrusion experiments was successfully predicted.
consideration. Therefore, a more realistic and effective bonding cri-
terion needs to be established from the viewpoint of more extensive
2. Experimental methods and procedure
influencing factors.
Thirdly, although some welding defects of L-seams were discov-
2.1. Extrusion experiment
ered, there is still lack of a deep and detailed investigation on the
formation mechanism of the welding defects. Since the defects of
In this study, plate-shaped profiles were investigated, and the
L-seams directly impact the performance of extruded profile, it is
extrusion dies used to extrude these profiles were designed in a
necessary to study the formation mechanism of the welding defects
modular way, as shown in Fig. 3. This kind of extrusion die consists
from both the macro and micro levels.
of the upper die, lower die and bridge. The rear end of the bridges
34 J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47

Fig. 5. The position of different samples and the dimension of tensile specimen.

Fig. 6. Finite element model of the aluminum alloy profile extrusion process.

were arched and pointed. Fig. 4 gives the dimensions of the bridges, Table 1
Chemical compositions of AA6063 aluminum alloy.
where the h represents the depth of welding chambers. In order
to obtain the extruded profiles with different defects of L-seams, Element Si Fe Cu Mn Mg Cr Zn Ti Al
welding chambers were designed as four different depths, namely, (wt%) 0.2–0.6 ≤0.35 ≤0.10 ≤0.10 0.45–0.90 ≤0.10 ≤0.10 ≤0.10 Bal.
h of the bridges is 5, 15, 25 and 35 mm, respectively.
The as-cast billets of AA6063 aluminum alloy with dimensions
of Ø152 mm × 450 mm were selected and the homogenization was for microstructure observation of L-seams were polished and then
carried out at 530 ◦ C for 14 h and then cooled down to room tem- etched in the solution of 1.0 ml HF, 1.5 ml HCl, 2.5 ml HNO3 and
perature in the air. Table 1 gives the chemical compositions of 95.0 ml H2 O. The light optical microscopy was used for microstruc-
AA6063 aluminum alloy. Extrusion experiments were performed ture observation. Due to the limited width of extruded profile, the
on a 16 MN extrusion press. The temperatures of container and dimensions of the tensile specimens are not compliant with rel-
extrusion dies were 450 ◦ C and 500 ◦ C respectively, and the tem- evant standard tensile samples. Nevertheless, the results of the
perature of the billets was 500 ◦ C. The ram speed was set to be tensile tests are still reasonable for the comparison of the different
1.0 mms−1 . The extruded profiles were rapidly quenched with profiles obtained from extrusion experiments. The tensile speci-
spraying water. The extrusion loads were obtained by calculating mens are tested on a hydraulic testing machine with high pressure
the sum of products of one main hydraulic pressure and two side clamps. All the tensile tests were performed at a constant speed
hydraulic pressures with the areas of cylinders respectively. of 0.01 mms−1 , and repeated three times for each configuration to
ensure the accuracy and repeatability of the tests. After the tensile
2.2. Characterization of microstructure and mechanical test, the fracture surfaces of tensile specimens were observed by
properties of L-seams means of scanning electron microscopy (SEM).

After extrusion experiments, the plate-shaped profiles with 3. 3-D numerical simulation modeling
12 mm thickness, 80 mm width and about 8 m length were
obtained. The L-seam is located in the mid-plane of the profile in 3.1. Elements meshing
width direction, as shown in Fig. 5. In order to ensure the stability
of the samples’ performance, all the samples were taken from the The porthole die extrusion process was simulated by means of
middle parts of extruded profiles in length direction. The samples Deform-3D software. Due to the symmetry of extrusion die and
J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47 35

Fig. 7. True stress-strain curves of the homogenized AA6063 aluminum alloy under various strain rates and at the deformation temperatures of (a) 400 ◦ C, (b) 450 ◦ C, (c)
500 ◦ C, (d) 530 ◦ C.

Table 2
Physical properties of materials used for billet and extrusion tools.

Material Young’s modulus (Pa) Poisson’s ratio Density (Kg/m3 ) Thermal conductivity [N/(s ◦ C)] Heat capacity [N/(mm2 ◦ C)]

AA6063 6.9E + 10 0.33 2700 180.2 2.27


H13 tool steel 2.1E + 11 0.30 7760 28.4 5.6

deformation process, a quarter of the numerical simulation model 3500 thermo-simulation machine. The deformation temperatures
was setup to reduce computational time, as shown in Fig. 6. The were 400, 450, 500 and 530 ◦ C, and the strain rates were set to
components of the numerical simulation model include stem, con- be 0.01, 0.1, 1 and 10 s−1 , respectively. Fig. 7 gives the true stress-
tainer, billet, bridge, upper die and lower die. All these components strain curves of the homogenized AA6063 aluminum alloy under
were meshed into tetrahedral elements. Since the Lagrange algo- various strain rates and at different deformation temperatures.
rithm is used in Deform-3D software, the elements of deformation According to the obtained results of isothermal hot compression
metal are remeshed continuously in the simulation process. In tests, the values of true stresses and strains of a series of points on
order to ensure the accuracy of simulation, the absolute mesh- the true stress-strain curves were imported into Deform-3D soft-
ing method was adopted. This meshing method means that the ware. When strain is larger than 0.8, the corresponding flow stress
minimum and maximum sizes of elements of deformation metal is calculated by means of trend extrapolation.
are invariable in the extrusion process. However, the number of
elements increases accordingly with the increase of complexity of
geometrical shape of deformation metal. As a result, the geometri- 3.3. Extrusion parameters and boundary conditions
cal shape of deformation metal can be described accurately. Liu et al.
(2008) confirmed the advantage of the absolute meshing method All the extrusion process parameters in the numerical simula-
through simulating the extrusion process of a thin-walled square tion models were set in accordance with the extrusion experiments.
magnesium tube. In addition, in order to predict defects of L-seams, The extrusion ratio is 20.9. The physical properties of materials used
local mesh refinement was also used in welding area. for billet and extrusion tools are listed in Table 2.
The boundary conditions in the numerical simulation model
mainly include heat transmission boundary conditions and fric-
3.2. True stress-strain curves of homogenized AA6063 aluminum
tional conditions. According to the report of Fang et al. (2009),
alloy
the heat transfer coefficient between tooling and billet was set
as 11 N/s mm ◦ C, and the heat transfer coefficients between tool-
In order to precisely describe the high-temperature plastic
ing/billet and air were set as 0.02 N/s mm ◦ C. The friction behavior
deformation behavior and calculate the flow stress of homogenized
between the die and the billet was described with the following
AA6063 aluminum alloy used in this study. The cylindrical speci-
plastic shear friction model.
mens of 15 mm in height and 10 mm in diameter were machined
from the homogenized AA6063 aluminum alloy billet, and the
isothermal hot compression tests were carried out by using Gleeble  = my (1)
36 J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47

Fig. 8. The macroscopic and microscopic observation results of L-seams on the cross-sections of profiles extruded with different depths of welding chambers.

where  is the shear frictional stress,  y the shear yield stress and by the experimental dies with the depth of welding chambers h = 5,
m is the friction factor. Based on both numerical simulation and 15, 25 and 35 mm, respectively. The macro-observation results of
experimental work, Flitta and Sheppard (2003) found that the fric- L-seams show that there is no any macro welding defect on the
tion conditions should be variable in the extrusion process. In the cross-sections of profiles extruded with h = 15, 25 and 35 mm, as
research work of Zhou et al. (2003), the friction factor of 0.3 was shown in Fig. 8(e), (i) and (m). However, an elliptic macro hole
set on the interface between the billet and the bearing of lower exists in the central zone of cross-section of the profile extruded
die, and 0.9 between the billet and the container or the other areas with h = 5 mm, as shown in Fig. 8(a). This elliptic macro hole pen-
of the extrusion die. In this work, the friction factor on the inter- etrates through the whole profile along length direction and the
face between the billet and the bearing of lower die was selected dimensions of this hole are around 5.0 mm in thickness direction
as 0.3, while the friction factor on the interface between the bil- and 1.6 mm in width direction of the profile.
let and the container or the other areas of the extrusion die was Further metallographic observation results show that the
respectively selected as 0.8, 0.9 and 1.0. The numerical simulations microstructures of L-seams are very different along the thick-
of extrusion process for the above three pair of friction factors were ness direction of extruded profiles. For the profile extruded with
carried out by using Deform software. The results showed that sim- h = 5 mm, the microstructures of the zones B and C of the L-seam
ulated profile fronts and the maximum ram forces are the closest are respectively presented in Fig. 8(c) and (d). The white boundaries
to the experimental results when the friction factor m on the inter- in the middle of profile’s cross-section represent the bonding inter-
face between the billet and the container or the other areas of the face. For the profile extruded with h = 15 mm, the bonding interface
extrusion die was set as 0.9 and the friction factor on the interface in the central zone A exhibits a dark boundary, as shown in Fig. 8(f).
between the billet and the bearing of lower die was selected as 0.3. This dark boundary gradually narrows down from the center to the
side of the cross-section along the thickness directions of the pro-
4. Results and discussion file and transforms to be a white boundary at the position of the
transition point T1 in the zone B, as shown in Fig. 8(g). The bond-
4.1. Microstructure and mechanical properties of L-seams ing interface in the zone C exhibits a white boundary, as shown in
Fig. 8(h). Furthermore, by means of microstructure observation and
4.1.1. Microstructure measurement, the lengths of the dark and white boundaries were
Fig. 8 shows the macroscopic and microscopic observation finally determined as 2.5 mm and 9.5 mm respectively, as shown
results of L-seams on the cross-sections of the profiles extruded in Fig. 8(e). For the profile extruded with h = 25 mm, the L-seam’s
J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47 37

Fig. 9. The engineering stress-strain curves obtained by tensile tests and the fracture angles of tensile specimens.

microstructure is also different along the thickness direction of the seen from Fig. 9 that the difference of the fracture elongations of
profile. However, the dark boundary in the central zone A is rela- profiles extruded with h = 15, 25 and 35 mm is mainly attributed
tively narrow, and the length of this dark boundary is shortened to to the difference of non-uniform plastic deformations occurring
1.5 mm and the white boundary is increased to 10.5 mm, as shown in the process of necking, namely, ␧2 < ␧3 < ␧4 . In conclusion,
in Fig. 8(j) and (i). The transition position is defined as T3 . For the the depths of welding chambers have an obvious influence on the
profile extruded with h = 35 mm, only white boundary exists on the mechanical properties of extruded profiles. With the increase of the
whole bonding interface of the L-seam, as shown in Fig. 8(n)–(p), depth of welding chamber, the non-uniform plastic deformation
and thus the length of the white boundary is 12.0 mm. As a result, and the fracture angle of the tensile specimen increase.
it can be concluded that the depths of welding chambers have a In the ductile fracture process of tensile specimens, micro voids
significant influence on the microstructure of L-seams. easily originate at the positions where brittle substances exist such
as the second phase particles and impurities, or where the atomic
bonding is weak such as grain boundary, phase boundary and bond-
4.1.2. Mechanical properties and fracture feature analyses ing interface. With the increase of plastic deformation, these micro
Fig. 9 gives the engineering stress-strain curves and the frac- voids gradually grow and propagate, and finally macro cracks are
ture angles of tensile specimens. The T-1–T-4 represent the tensile formed and the specimen failure occurs. In this study, the fracture
specimens taken from the profiles extruded with h = 5, 15, 25 and locations, fracture angles and non-uniform plastic deformations
35 mm, respectively. According to the tensile test results, the profile obtained from tensile tests directly reveal the atomic bonding
extruded with h = 5 mm has the lowest tensile strength (264 MPa) degrees of the bonding interfaces of L-seams. Overall, the bonding
and elongation (0.054) due to the existence of the elliptic macro interface of the L-seam of the profile extruded with h = 15 mm has
hole. The fracture of the tensile specimen T-1 penetrates through a weak atomic bonding, and the bonding interface of the L-seam of
L-seam, and the fracture angle is about 40 ◦ . The yield and tensile the profile extruded with h = 35 mm has a strong atomic bonding.
strengths of profiles extruded with h = 15, 25 and 35 mm are about While, the atomic bonding degree of the bonding interface of the
175 and 275 Mpa, but the entire engineering strains before fracture L-seam of the profile extruded with h = 25 mm is mediate.
(fracture elongations) and the fracture angles of the tensile speci- Fig. 10 shows the facture morphologies of the tensile specimens
mens are obviously different. The profile extruded with h = 15 mm by means of SEM. Fig. 10(a) shows the morphologies of the unbond-
has a relatively large fracture elongation (0.398). However, the fail- ing surface and the fracture surface of the specimen T-1. Some
ure of the tensile specimen T-2 occurs almost along L-seam. The equiaxial dimples with very small size and some elongated dimples
fracture surface of T-2 is smooth, and the fracture angle is about 0 ◦ . with relative big size are found in the fracture surface. Fig. 10(b)
The profile extruded with h = 25 mm has a larger fracture elonga- shows the morphologies of the fracture surface of the T-2. There
tion (0.455) than the profile extruded with h = 15 mm. The fracture are a large number of small and shallow equiaxial dimples in the
surface of the tensile specimen T-3 is unsmooth, and the fracture central region of the fracture surface and some elongated dimples
angle is about 15 ◦ . The profile extruded with h = 35 mm has the in the edge region adjacent to profile’s surfaces. Fig. 10(c) shows
largest fracture elongation (0.500). The fracture surface of the ten- the morphologies of the fracture surface of the T-3. There are also
sile specimen T-4 is also unsmooth, but the fracture angle is about many equiaxial dimples in the central region of the fracture surface
30 ◦ . For the tensile specimens T-2–T-4, the larger the fracture angle and some elongated dimples in the edge region adjacent to profile’s
is, the larger the fracture elongation is. In addition, it also can be
38 J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47

Fig. 10. The fracture morphologies of the tensile specimens: (a) T-1, (b) T-2, (c) T-3, (d) T-4.

surfaces. However, the dimensions of the equiaxial dimples in the addition, since the failure of the tensile specimen T-2 occurs almost
central region have an obvious difference. The equiaxial dimples along the L-seam of the profile extruded with h = 15 mm and the
in the zone 2, which is around the center of the fracture surface, fracture surface has lots of small and shallow dimples, it can be con-
are small and shallow. While, the equiaxial dimples in the zone 1, cluded that the bonding quality of the central region of the L-seam
which is a bit far away from the center of the fracture surface, are on the cross-section of profile extruded with h = 15 mm is poor.
large and deep. The morphologies of the fracture surface of T-4 are While, the bonding quality of the central region of the L-seam on
shown in Fig. 10(d). It is observed that there are many large and the cross-section of profile extruded with h = 35 mm is good, since
deep quiaxial dimples in the center region of the fracture surface the fracture of the tensile specimen T-4 penetrates through the L-
and some elongated dimples in the edge region adjacent to pro- seam and the fracture surface has lots of large and deep dimples.
file’s surfaces. As a result, it can be seen that the shape and size of The fracture surface of tensile specimen T-3 has many small and
the dimples on the fracture surfaces of the tensile specimens are shallow dimples (in zone 2) similar to those in the central region of
different along the thickness direction of profiles. L-seam of the profile extruded with h = 15 mm and many large and
The theoretical and experimental research of Li et al. (2011) deep dimples (in zone 1) similar to those in the central region of L-
showed that the shape of the dimples on fractrue surface is deter- seam of the profile extruded with h = 35 mm. Therefore, the central
mined mainly by the stress state. In the process of ductile fracture of region of the L-seam of the profile extruded with h = 25 mm has a
tensile specimens, the equiaxial dimple is formed due to the action poor bonding quality, but the region adjacent to the central region
of normal stress, while the elongated dimple is formed owing to the has a good bonding quality.
action of shearing stress, which were also demonstrated by Achouri According to the aforementioned microstructure observation,
et al. (2013). In addtion, Guo et al. (2014) pointed out that the size mechanical properties and fracture feature analyses, it can be con-
and depth of the dimples on fractrue surface are influenced by the cluded that the dark bonding interfaces in Fig. 8 have poor bonding
second phase particles, inclusions, grain boundaries, bonding inter- quality and the white bonding interfaces have good bonding qual-
faces, dislocation pileups and so on. Furthermore, Den Bakkera et al. ity. The bonding interfaces of the L-seams of the profiles extruded
(2014) indicated that in the process of solid-state bonding, the size with h = 5, 15, 25 and 35 mm can be distinguished as the unbond-
and depth of the dimples on fractrue surfaces of weld seams reveal ing surfaces, unsound and sound bonding zones. Fig. 11 gives the
the atomic bonding degrees of the bonding interfaces and corre- dimension of each zone in detail. According to Cooper and Allwood
spond to the ductility of extruded profiles. More specifically, large (2014a), the unsound bonding is formed because that the bonding
and deep dimples represent strong atomic bonding and superior process does not establish close contact on the bonding interface
ductility, while small and shallow dimples represent weak atomic on the micrometer and millimeter scale, or that islands of con-
bonding and inferior ductility, which were also showed by Shen taminant (such as oxide) prevent full bonding of the interface at
et al. (2014). the nano scale. As a result, the unsound bonding zones exhibit
Overall, the fracture surface of the tensile specimen T-1 has dark boundaries in Fig. 8. In addition, although the sound bond-
equiaxial and elongated dimples, and the elongated dimples take ing zones have established close contact and have no contaminant,
the dominant place. This is because that the shearing stress takes their microstructure such as grain size may be different from the
the dominant place although the dimples were formed under the other zones without L-seam. As a result, the sound bonding zones
combined action of the normal and shearing stress. The central exhibits white boundaries in Fig. 8.
regions of the fracture surfaces of tensile specimens T-2–T-4 have
a large number of equiaxial dimples, but the edge regions of these
4.2. Formation processes of L-seams and defects
fracture surfaces have some elongated dimples. This is because that
micro voids firstly originate, grow, propagate and form micro cracks
4.2.1. Analysis of the accuracy of numerical simulation results
in the central regions of tensile specimens under the action of ten-
In order to reveal the formation processes of the L-seams and
sile stress, but with the propagation of the micro cracks, the edge
their defects and obtain relevant physical quantities, 3-D transient
regions of tensile specimens are subjected to shearing stress. In
numerical simulations for the porthole die extrusion processes
J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47 39

Fig. 11. The bonding quality of L-seams on the cross-sections of profiles extruded with different depths of the welding chambers: (a) h = 5 mm, (b) h = 15 mm, (c) h = 25 mm,
(d) h = 35 mm.

defects. However, there is an elliptic macro hole in the central


zone of cross-section of the profile extruded with h = 5 mm. Fig. 14
gives the formation process of the L-seam of the profile extruded
with h = 15 mm. In the porthole die extrusion process, when heated
metal flows into upper die cavity, it is firstly divided into two sepa-
rated metal streams by bridge. After that, the two separated metal
streams gradually flow toward the bottom of welding chamber.
When the metal streams have reached the bottom of welding cham-
ber, they flow sideways to fill welding chamber and a few of them
is pressed into the bearing of lower die to form profile fronts, as
shown in Fig. 14(a)–(d). This process can be called the dividing and
filling stage. With the extrusion proceeding, since the metal close
to the central axis of welding chamber has the fastest flow veloc-
ity, the two separated metal streams firstly contact to each other in
the central area of welding chamber and start to solid-state bond
to form welding seam under the conditions of high pressure and
temperature, as shown in Fig. 14(e)–(h). This process can be called
the contacting and partially welding stage. After metal fills welding
chamber completely and flows out of the bearing of the lower die to
form profile, the extrusion process enters into the steady welding
and forming stage (Fig. 14(i)–(l)), and a welding plane with stable
shape and size is formed in welding chamber and lower die bear-
ing, as shown in Fig. 14(l). From Fig. 14(k) and (l), it can be seen that
there is no any macro defect in the welding plane and in the L-seam
of extruded profile. In addition, the formation processes of the L-
seams of the profiles extruded with h = 25 and 35 mm are similar
to that extruded with h = 15 mm, and there are also no any macro
defect in welding planes and in L-seams of extruded profiles. There-
fore, it can be concluded that the welding quality of the L-seams of
Fig. 12. Load-time curves obtained from numerical simulation and experiment with the profiles extruded with h = 15, 25 and 35 mm depends on the
h = 15 mm.
solid-state bonding behavior in welding planes.
Fig. 15 gives the formation process of the elliptic macro hole
were conducted by using Deform-3D software. In order to verify in the central zone of cross-section of the profile extruded with
the reliability of the simulation results, the extrusion loads and h = 5 mm. In the extrusion process with h = 5 mm, the welding pres-
profile fronts obtained from extrusion experiments and numerical sure is quite low due to the small height of welding chamber. As a
simulations were compared accordingly. result, in the contacting and partially welding stage, the split metal
Fig. 12 compares the load-time curves obtained from numeri- streams can not contact to each other in the central area of the
cal simulation and experiment with the depth of welding chamber welding chamber and a hole is formed, as shown in Fig. 15(b) and
h = 15 mm. Their maximum extrusion loads are 7.60 and 7.73 MN, (c). With the extrusion proceeding, the hole gradually shrinks but
respectively. It is clear that the predicted maximum extrusion load the flow resistance in the radial direction increases. When the flow
is in good agreement with the experimental one. resistance in the radial direction is greater than that in lower die
Fig. 13 shows the comparison of the profile fronts obtained bearing, the metal flows out of the bearing and forms profile. After
from experiments and simulations. Although the effect of the weld- that, the shape and size of the hole are stable and the hole appears
ing quality of the areas just behind the fronts on the profile front in the extruded profile, as shown in Fig. 15(e) and (f). This hole
geometries was not taken into consideration in numerical sim- always exists in the steady welding and forming stage, and thus
ulations, it can be seen that the sizes and shapes of extruded it penetrates through the whole profile along length direction of
profile fronts are in good agreement with the experimental results. the extruded profile. It can be concluded that the macro hole in the
According to the aforementioned comparisons between the exper- profile extruded with h = 5 mm is caused by metal flow behavior,
imental and simulation results, it can be concluded that the and does not relate to solid-state bonding process.
numerical simulation models and results are reliable. In porthole die extrusion process, the macro defect of L-seams
is easy to be obversed and can be directly predicted by means of
4.2.2. Formation processes of L-seams and the macro hole numerical simulation. However, the bonding quality of the L-seams
Extrusion experimental results have shown that the L-seams of without any macro defect is difficult to be directly determined by
the profiles extruded with h = 15, 25 and 35 mm have no macro means of numerical simulation. Since the bonding quality of the
40 J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47

Fig. 13. Comparison of profile fronts obtained from the experiments and simulations with different depths of welding chambers: (a) h = 5 mm, (b) h = 15 mm, (c) h = 25 mm,
(d) h = 35 mm.

Fig. 14. Three stages of the formation process of an L-seam during porthole die extrusion: (a)–(d) dividing and filling stage, (e)–(h) contacting and partially welding stage,
(i)–(l) steady welding and forming stage.
J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47 41

Fig. 15. Formation process of the macro hole of the profile extruded with h = 5 mm: (a)–(c) contacting and partially welding stage, (d)–(f) steady welding and forming stage.

L-seams without any macro defect is determined by the solid-state solid-state bonding, are also determined. In this way, in the welding
bonding behavior in welding planes, investigating the bonding plane, the welding path of each tracing point is finally determined,
mechanism and establishing bonding criterion become particularly as shown in Fig. 16(f). By the same way, the metal particle flow
important. In the following sections, the extrusion processes of the lines, initial welding positions and the welding paths in the steady
profiles extruded with h = 15, 25 and 35 mm are used to establish a welding and forming stages for the extrusion processes with h = 25
new bonding criterion. and 35 mm can also be determined.
The velocity distributions in Fig. 16(e) and (f) show that there
is a dead metal zone in the welding chamber and welding plane.
4.3. Evaluation of solid-state bonding quality According to the flow lines f1 –f5 shown in Fig. 16(c) and (d) and
the velocity distributions shown in Fig. 16(e) and (f), it can be seen
4.3.1. Metal flow behavior and welding paths that, in the steady welding and forming stage, most of the metal in
In steady welding and forming stage, the separated metal the welding chamber bypasses the dead metal zone and flows into
streams always encounter in the welding plane shown in Fig. 14(l) the welding plane from initial welding positions with a relatively
and form an L-seam inside profile by means of solid-state bonding. high velocity. Then, the bypassed metal starts to solid-state bond
Therefore, for the profiles extruded with h = 15, 25 and 35 mm, the in the welding plane and gradually flows into the die bearing to
flow behavior and the solid-state bonding process in the welding form the L-seam. Since the metal in the dead zone has a very low
planes directly determine the bonding quality of the profiles. velocity, it hardly flows into the bearing to form the L-seam. As a
The extrusion experimental results in this study have shown result, the L-seam of profile is formed almost by the metal in the
that the bonding quality of the L-seams of profiles extruded with main welding zone of the welding plane, as shown in Fig. 16(f).
h = 15, 25 and 35 mm are variable along the thickness direction of According to the welding paths of tracing points, the changes of
profiles. In order to investigate the solid-state bonding processes physical qualities during the solid-state bonding can be obtained.
of some special particles in each L-seam, five tracing points named Fig. 17 gives the changes of the hydrostatic pressure, effective
as P1 , P2 , P3 , P4 and P5 were set up in each L-seam at the position stress, effective strain rate and temperature along the welding
of the die exit, as shown in Fig. 16(b). The distance between each paths of tracing points P1 –P5 in the solid-state bonding process for
tracing point and the center of the profile’s cross-section is 0, 0.75, the extrusion die with h = 15 mm. The solid-state bonding time for
1.25, 3.0 and 5.0 mm, respectively. After that, based on the particle tracing points P1 –P5 are 1.71, 4.73, 6.93, 13.99 and 14.19 s, respec-
tracing algorithm of Deform-3D software, the position change of tively. During the solid-state bonding, no matter which welding
each tracing point during extrusion is obtained. According to the path the metal flows along, with the increase of the bonding
coordinate values of each tracing point, the metal particle flow lines time, the hydrostatic pressures overall show downward trends
were determined, as shown as f1 –f5 in Fig. 16(c) and (d). In addition, and finally decrease to 0 Mpa (Fig. 17(a)), and both the effective
the initial welding positions of five tracing points, named as I1 , I2 , I3 , stresses and effective strain rates increase firstly and then decrease
I4 and I5 , where metal just flows into the welding plane and starts
42 J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47

Fig. 16. Related information in steady welding and forming stage for the extrusion process with h = 15 mm: (a) a quarter of geometric model, (b) five tracing points, (c) flow
lines in Y–Z plane, (d) flow lines in X–Y plane, (e) 3-D velocity distribution, (f) velocity distribution, initial welding positions and welding paths in welding plane.

Fig. 17. The changes of physical quantities along welding paths of tracing points P1 –P5 in the solid-state bonding process for the extrusion die with h = 15 mm: (a) hydrostatic
pressure, (b) effective stress, (c) effective strain rate, (d) temperature.

(Fig. 17(b) and (c)), and the temperatures increase slightly (Fig. 17 state bonding processes for extrusion dies with h = 25 and 35 mm,
(d)). In addition, compared to the metal flowing along the welding the change rules of the hydrostatic pressure, effective stress, effec-
path of tracing points P5 , the metal flowing along the welding path tive strain rate and temperature along their corresponding welding
of tracing points P1 is subjected to a lower hydrostatic pressure, paths of tracing points P1 –P5 are similar to those for the extrusion
larger effective stress and effective strain rate, and lower tempera- die with h = 15 mm. Consequently, the changes of physical quali-
ture. As a result, the bonding quality in the center of the L-seam ties obtained from the numerical simulation results qualitatively
of profile extruded with h = 15 mm is worse, while the bonding explain the differences of the bonding quality of L-seams of profile
quality in the region far away from the center is good. In the solid- extruded with h = 15, 25 and 35 mm along the thickness direction.
J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47 43

4.3.2. Extrusion bonding mechanism and a new bonding criterion models are complex and the assumed shape of void directly deter-
Inspired by the above research results, the authors of this paper mines the prediction precision, they are difficultly used to guide
proposed a solid-state bonding mechanism of the L-seam in the practical process. Since the temperature, time and material have
process of porthole die extrusion, as shown in Fig. 18. When sep- obvious influences on the atomic diffusion, which were reported
arated metal streams just flow into the welding plane and contact by Cooper and Allwood (2014b), in order to describe the influence
to each other, on a microscopic scale, the surfaces for bonding of the atomic diffusion on the void closure behavior in porthole
are irregular and have many asperities. Therefore, there are many die extrusion process, a diffusion integration GD was proposed as
micro voids on the contact interface, as shown in Fig. 18(a). With follows,
the solid-state bonding proceeding along welding paths, the micro
 t  RT 
voids gradually close to create a micro-level intimate contact under
the actions of plastic deformation and atomic diffusion, as shown in GD = k0 exp dt (3)
0
QD
Fig. 18(b). According to the report of Cooper and Allwood (2014a),
the inter-atomic and van der Waals forces are the major sources where, t is the time (s), R is the universal gas constant
of attraction between the atoms, and the inter-atomic force is (8.314 J mol−1 K−1 ), T is the absolute temperature (K), QD is the dif-
far greater than the van der Waals force. When intimate con- fusion activation energy (J mol−1 ), and k0 is a coefficient related to
tact is achieved, namely, the distances (d) of the atoms on the material and the surface conditions of metal for bonding.
contact interface are reduced to the 10 atomic spacings, the inter- It should be pointed out that, in the Eq. (3), the effect of temper-
atomic attractive forces will form a joint, which means that a sound ature on the void closure behavior is described as the exp(RT/QD )
solid-state bonding for L-seam of profile is achieved, as shown in instead of the Arrhenius type relationship exp(-QD /RT) used in dif-
Fig. 18(c). fusion equations. The reason of this modification is as follows. In
In order to predict solid-state bonding quality of L-seams in port- porthole die extrusion process, usually, the ratio of mean normal
hole die extrusion process, investigating void closure mechanism stress to effective stress, stress triaxiality  m /,
¯ is about 1.0–10.0.
and developing mathematical model of void closure behavior are of On the one hand, if the product of  m /¯ and exp(-QD /RT) is used to
great importance. Main void closure mechanisms include the plas- describe the effect of stress triaxiality and temperature on the void
tic deformation mechanism and the diffusion mechanism. In the closure behavior, since the orders of magnitude of the values of
porthole die extrusion process, the plastic deformation mechanism  m /¯ and exp(-QD /RT) are considerably different, the effect of tem-
of the void closure can refer to that in other plastic deformation perature on the void closure behavior almost can not be reflected.
processes such as forging and rolling. With the effect of the plas- On the other hand, if the values of exp(-QD /RT) are modified as
tic deformation, the voids gradually shrink and become flatten, as the same order of magnitude of the values of  m /, ¯ a small tem-
shown in Fig. 18(1). Nakasaki et al. (2006) showed that the ratio of perature difference will result in a large difference of the values
mean normal stress to effective stress (stress triaxiality) and effec- of exp(-QD /RT), which means that the exp(-QD /RT) gives an over
tive strain in the region surrounding the void are the dominant emphasis on the effect of temperature on the void closure behav-
factors for the void closure behavior, which can be described by ior. As a contrast, the values of exp(RT/QD ) have the same order of
using following hydrostatic integration Gm , magnitude of the values of  m /¯ and can properly reflect the effect
 ε̄   of temperature on the void closure behavior. Therefore, this study
m used exp(RT/QD ) in the Eq. (3) to describe the effect of temperature
Gm = dε̄ (2)
0
¯ on the void closure behavior in porthole die extrusion process.
This study considers that in the whole process of void clo-
where,  m is the mean normal stress (Mpa), ¯ is the effective stress sure and sound bonding formation, both plastic deformation and
(Mpa), and ε̄ is the effective strain. atomic diffusion are indispensable two steps. The dominant fac-
The diffusion mechanism of the void closure can refer to that tors affecting void closure and sound bonding are temperature,
in the solid-state diffusion bonding process. Derby and Wallach stress, strain, strain rate, time and material. Firstly, temperature
(1982) demonstrated that the diffusion mechanism of the void not only influences the flow stress of material but also affects
closure mainly includes the surface source diffusion and the inter- the atomic diffusion. Secondly, stress state influences the plas-
face source diffusion. The surface source diffusion means that the tic deformation behavior, while the stress gradient is a driving
atoms on or near the surface of void are transferred from the parts force for atomic diffusion. Thirdly, strain and strain rate not only
with larger curvatures to those with smaller curvatures under the influence the degree of contaminant broking and virgin material
driving of the difference of surface free energy by means of vol- exposing but also reveal the dislocation density surrounding voids.
ume diffusion (path 2 in Fig. 18(2)) and surface diffusion (path The dislocation density influences the atomic diffusion. Strain can
3 in Fig. 18(2)). While, the interface source diffusion means that be expressed as an integral of strain rate on time. Fourthly, time
the atoms on or near the contact interface are transferred to the influences the degree of atomic diffusion and plastic deformation.
void necks under the driving of the chemical potential gradient by Finally, the thermo-physical properties of material and the sur-
means of volume diffusion (path 4 in Fig. 18(3)) and surface diffu- face conditions of metal for bonding also influence void closure
sion (path 5 in Fig. 18(3)). Furthermore, Ma et al. (2012) considered behavior and atomic diffusion. The surface conditions of metal for
that the surface source diffusion only results in the distribution bonding include the roughness, oxide and contaminant films. Dur-
change of the atoms on the void surface, and not results in the ing porthole dies extrusion, sometimes a certain amount of oxide
change of the void volume. Therefore, when the void closure occurs layers or contaminant films exist on the surfaces of the split metal
under the action of the diffusion mechanism, the volume of void streams due to the formation of gas pockets behind the die bridge.
is directly determined by the interface source diffusion. In order As a result, in this study, a new dimensionless solid-state bonding
to quantitatively predict the volume evolution of void, some geo- criterion named as the J criterion was proposed as follows,
metric models are proposed to describe the shape of void and
some mathematical models of void closure were established. For  t  RT 
m ˙
example, Hill and Wallach (1989) assumed that the initial shape of J= k0 ε̄ exp dt (4)
¯ QD
void is an ellipse, while Orhan et al. (1999) assumed that is a sine 0
wave, and the models for void closure in the diffusion bonding pro-
cess were derived respectively. However, since these mathematical where, ε̄˙ is the effective strain rate (s−1 ).
44 J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47

Fig. 18. Schematic diagram of solid-state bonding mechanism in porthole die extrusion process.

 t
4.3.3. Experimental validation and evaluation of the new bonding p
criterion Qad = dt (6)
0

In order to validate the accuracy of the J criterion for predicting
solid-state bonding quality in porthole die extrusion process, the
where,  is the metal flow velocity (mm s−1 ), p is the contact pres-
values of J, which are integrals along the welding paths of tracing
sure (Mpa), i.e. the normal contact stress ( n ) on the welding plane.
points mentioned previously, were calculated. Since the L-seams
In order to comprehensively evaluate the action of p in Eqs. (5)
in this study are formed by the same material and the alloy ele-
and (6), this paper tried to use two definitions of p. One is the nor-
ments such as Mg and Si in AA6063 are very few, thus the void
mal contact stress ( n ) on the welding plane originally defined by
closure behavior with the action of the atomic diffusion is mainly
the K and Q criteria, another is the mean normal stress ( m ). The
due to the self-diffusion behavior of aluminum atoms. According to
corresponding Kad is respectively expressed as Kad  n and Kad  m ,
the report of Sohn (2004), the activation energy of self-diffusion of
and the corresponding Qad is respectively expressed as Qad  n and
aluminum atoms is 1.42 × 105 J mol−1 at the temperature range of
Qad  m .
450–650 ◦ C (QD = 1.42 × 105 J mol−1 ). Since the extrusion parame-
The above mentioned microstructure observation, mechanical
ters are the same for the extrusion experiments with h = 15, 25 and
properties and fracture feature analyses have shown that the L-
35 mm and there are no gas pockets behind the die bridges during
seams of profiles extruded with h = 15 and 25 mm respectively have
extrusion, thus the surface conditions of metal for bonding should
an unsound bonding zone with the length of 2.5 and 1.5 mm in their
be the same. Therefore, for simplicity, the value of k0 is assumed
central zones, and the L-seam of profile extruded with h = 35 mm
as 1.0. In addition, for comparison, the values of the Kad and the
has no unsound bonding zone. The distance from the centers to
Qad for each tracing point were also respectively calculated accord-
the bonding quality transition positions for L-seams of profiles
ing to the K criterion proposed by Donati and Tomesani (2004) and
extruded with h = 15 and 25 mm are 1.25 and 0.75 mm, respectively.
the Q criterion proposed by Plata and Piwnik (2000). The K and Q
Fig. 19(a) represents the bonding quality of five tracing points
criteria are expressed as follow,
on L-seams summarized according to the experimental results,
where 䊉 indicates sound bonding,  indicates unsound bonding,
 t and  indicates the transition point from unsound to sound bond-
p
Kad = dt (5) ing, i.e. sound bonding critical point. The dotted rectangle indicates
0
¯ unsound bonding area. For h = 15 mm, P1 and P2 are the unsound
J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47 45

Fig. 19. The values of Kad , Qad and J calculated according to the welding paths of the tracing points P1 –P5 for the L-seams of profiles extruded with h = 15, 25 and 35 mm: (a)
bonding quality of the tracing points P1 –P5 on the L-seams, (b) Kad  n , (c) Qad  n , (d) Kad  m , (e) Qad  m , (f) J.

bonding points, P3 is the transition point (corresponding to T1 in the Therefore, according to the experimental results, the values of
above Section 4.1.1), and P4 and P5 are the sound bonding points. the Kad , Qad and J for five tracing points should satisfy the following
For h = 25 mm, P1 is the unsound bonding point, P2 is the transition conditions.
point (corresponding to T3 in the above Section 4.1.1), and P3 –P5
are the sound bonding points. For h = 35 mm, P1 –P5 are all the sound
(1) The values of the Kad , Qad and J for P1 and P2 with h = 15 mm
bonding points.
and P1 with h = 25 mm should be respectively less than the cor-
responding values of the Kad , Qad and J for P1 with h = 35 mm.
46 J. Yu et al. / Journal of Materials Processing Technology 237 (2016) 31–47

(2) The values of the Kad , Qad and J for P1 and P2 with h = 15 mm Therefore, the J criterion can be used to evaluate the bonding quality
should be respectively less than the corresponding values of of different shaped profiles.
the Kad , Qad and J for P3 with h = 15 mm.
(3) The values of the Kad , Qad and J for P1 with h = 25 mm should be 5. Conclusions
respectively less than the corresponding values of the Kad , Qad
and J for P2 with h = 25 mm. In this study, a set of modular porthole extrusion dies with
(4) The values of the Kad , Qad and J for P3 with h = 15 mm should be different depths of welding chambers were designed and manu-
respectively equal to the corresponding values of the Kad , Qad factured. The profiles extruded with different depths of welding
and J for P2 with h = 25 mm. chambers were obtained by performing extrusion experiments.The
welding quality of these extruded profiles was characterized by
means of microstructure observation, tensile test and fracture anal-
For the K and Q criteria, when p in Eqs. (5) and (6) is the nor- ysis. True stress-strain curves of homogenized 6063 aluminum
mal contact stress ( n ), the values of the Kad  n , Qad  n calculated alloy with various strain rates and deformation temperatures were
according to the welding paths of the tracing points P1 –P5 for the obtained by means of isothermal hot compression test. Three-
L-seams of profiles extruded with h = 15, 25 and 35 mm are respec- dimensional transient numerical simulation models of porthole
tively shown in Fig. 19(b) and (c). It can be seen from Fig. 19(b) die extrusion processes were established. Flow behaviors of alu-
that the value of the Kad  n for P1 with h = 25 mm is larger than that minum alloy in porthole die extrusion process were investigated,
for P2 with h = 25 mm. Obviously, the values of Kad  n in Fig. 19(b) and the formation processes of L-seams and their defects were
do not satisfy the condition (3). In addition, the value of Kad  n for revealed. Solid-state welding processes of metal particles were
P3 with h = 15 mm is equal to 57.00 mm, and the value of Kad  n for traced and welding paths were determined. Finally, based on the
P2 with h = 25 mm is equal to 52.50 mm. The relative error of these plastic deformation and diffusion mechanisms for closure behavior
two values is 7.89%. It can be seen from Fig. 19(c) that the value of micro voids on contact interfaces, a new dimensionless solid-
of Qad  n for P3 with h = 15 mm is equal to 16.18 s, and the value of state bonding criterion related to stress triaxiality, effective strain
Qad  n for P2 with h = 25 mm is equal to 17.68 s. The relative error of rate, temperature and contact time was proposed. According to this
these two values is 8.48%. new bonding criterion, the bonding quality of L-seams obtained
For the K and Q criteria, when p in Eqs. (5) and (6) is the by means of extrusion experiments was successfully predicted.
mean normal stress ( m ), the values of the Kad  m , Qad  m calculated According this study, the following conclusions were drawn:
according to the welding paths of the tracing points P1 -P5 for the
L-seams of profiles extruded with h = 15, 25 and 35 mm are respec- (1) The welding quality of an L-seam on the cross-section of the
tively shown in Fig. 19(d) and (e). It can be seen from Fig. 19(d) that profile extruded by the modular die with an arched and pointed
the value of the Kad  m for P1 with h = 25 mm is also larger than that bridge is variable along the thickness direction of profile and
for P2 with h = 25 mm. Obviously, the values of Kad  m in Fig. 19(d) the welding defect tends to be formed in the central zone of
also do not satisfy the condition (3). In addition, the value of Kad  m the profile’s cross-section. With the increase of the depth of
for P3 with h = 15 mm is equal to 45.92 mm, and the value of Kad  m the welding chamber, the macro hole in the central zone of the
for P2 with h = 25 mm is equal to 43.64 mm. The relative error of profile’s cross-section disappears and the length of the unsound
these two values is 4.97%. It can be seen from Fig. 19(e) that the bonding zone decreases.
value of Qad  m for P3 with h = 15 mm is equal to 14.20 s, and the (2) The welding quality of L-seam of profile extruded by porthole
value of Qad  m for P2 with h = 25 mm is equal to 15.71 s. The relative die is determined by two key factors: metal flow behavior and
error of these two values is 9.61%. solid-state bonding process. The metal flow behavior deter-
Fig. 19(f) gives the values of the J criterion calculated according mines whether the macro welding defect is formed and the
to the welding paths of the tracing points P1 -P5 for the L-seams solid-state bonding process determines the bonding quality of
of profiles extruded with h = 15, 25 and 35 mm. The value of J for the bonding interface. The formation of a macro hole in the pro-
P3 with h = 15 mm is equal to 9.65, and the value of J for P2 with file extruded with a shallow welding chamber is attributed to
h = 25 mm is equal to 9.63. The relative error of these two values is metal flow behavior, and does not relate to solid-state bonding
0.21%. Obviously, in comparison with the K and Q criteria calculated process.
whether by using the normal contact stress ( n ) on the welding (3) There is a dead metal zone in the welding plane and the metal
plane or the mean normal stress ( m ), the J criterion proposed in in the dead metal zone almost does not participate the solid-
this study has the highest prediction accuracy. state bonding. The L-seam of profile without any macro welding
It should be pointed out that the points above the critical lines in defect is formed almost by the metal in the main welding zone
Fig. 19(b)–(f) only indicate that the corresponding zones of bonding of the welding plane through solid-state bonding.
interfaces have sound bonding, and the magnitudes of values of
these points do not represent the difference of bonding quality in
Acknowledgements
these zones. Therefore, the magnitudes of values of the points above
the critical lines can not be used to evaluate the accuracy of the
The authors would like to acknowledge the financial support
bonding criteria.
from National Natural Science Foundation of China (51375270
In this work, the welding process of a plate-shaped profile in
and 51405268), Encouragement Foundation for Young Scholars of
porthole die extrusion process was studied in detail. Generally
Shandong Province (BS2014ZZ001).
speaking, different shaped profiles may have different metal flow
behaviors, L-seam formation processes, welding defects, bonding
quality and microstructure. However, the formation mechanisms of References
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