Duy CH20

1.80
2.445

1.60

1.40

1.20

1.00
AU

0.80

0.60
3.552

8.442

0.40
12.550

0.20
18.102
11.520
7.870

0.00

0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00
Minutes
Sample Name: DDH_HCl; Date Acquired: 6/19/2023 3:53:20 PM ICT; Vial: 3; Injection: 1

Peak Summary with Statistics

Name:
Retention Purity1 Purity1
Area % Area Height K Prime Resolution Selectivity USP Plate Count USP Tailing
Time (min) Angle Threshold

1 2.445 7.057 0.785 9816835 59.62 1726837 -0.2 4269 1.3

2 3.552 5.545 0.354 1316365 7.99 419622 0.2 10.3 -1.4 62158 2.7

3 7.870 2.997 2.753 28643 0.17 3748 1.7 34.7 7.6 25123 0.8

4 18.102 1.074 0.945 480720 2.92 6711 5.2 4.6 1.6 1385 1.0

Reported by User: System Project Name: Duy CH20

Report Method: Duy CH20 Date Printed:
Report Method ID:1154
1154 9/6/2023
Page: 1 of 8 11:01:03 AM Asia/Ho_Chi_Minh
 Peak Summary with Statistics
Name:
Retention Purity1 Purity1
Area % Area Height K Prime Resolution Selectivity USP Plate Count USP Tailing
Time (min) Angle Threshold

5 11.520 6.861 8.155 8119 0.05 781 3.0 13.1 1.6 45244 0.9

6 12.550 0.194 0.302 2702713 16.41 179084 3.3 3.2 1.1 16993 1.4

7 8.442 0.916 0.439 2112166 12.83 290192 1.9 2.9 1.1 34285 1.0

Mean 9.212

Std. Dev. 5.412

% RSD 58.75

3D Plot

1.50

1.00

AU
0.50

0.00

300.00
400.00
0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00
Minutes

Purity Plot
Purity
Auto Threshold 80.00
2.445

1.50

60.00
M
Degrees
1.00
AU

40.00

0.50
20.00

0.00
0.00
2.30 2.40 2.50 2.60 2.70 2.80 2.90 3.00
Minutes
PA: 7.057 TH: 0.785
Peak:
Purity
Auto Threshold

Reported by User: System Project Name: Duy CH20

Report Method: Duy CH20 Date Printed:
Report Method ID:1154
1154 9/6/2023
Page: 2 of 8 11:01:03 AM Asia/Ho_Chi_Minh
 Purity Plot
Purity
0.40 Auto Threshold

3.552
40.00

0.30
30.00

Degrees
AU

0.20
20.00

0.10
10.00
M
0.00
0.00
3.50 3.60 3.70 3.80 3.90 4.00
Minutes
PA: 5.545 TH: 0.354
Peak:
Purity
Auto Threshold
Purity Plot
Purity
0.008
Auto Threshold 7.870 80.00

60.00
0.007

Degrees
AU

40.00
0.006

20.00
0.005
M
0.00
7.70 7.75 7.80 7.85 7.90 7.95
Minutes
PA: 2.997 TH: 2.753
Peak:
Purity
Auto Threshold

Reported by User: System Project Name: Duy CH20

Report Method: Duy CH20 Date Printed:
Report Method ID:1154
1154 9/6/2023
Page: 3 of 8 11:01:03 AM Asia/Ho_Chi_Minh
 Purity Plot

0.30 Purity
Auto Threshold 80.00

8.442
0.20 60.00
M

Degrees
AU

40.00
0.10
20.00

0.00 0.00
8.30 8.35 8.40 8.45 8.50 8.55 8.60
Minutes
PA: 0.916 TH: 0.439
Peak:
Purity
Auto Threshold
Purity Plot
Purity
0.0038 Auto Threshold 80.00
11.520

0.0036 60.00

Degrees
AU

0.0034 40.00

0.0032 20.00
M

0.0030 0.00
11.35 11.40 11.45 11.50 11.55 11.60 11.65 11.70
Minutes
PA: 6.861 TH: 8.155
Peak:
Purity
Auto Threshold

Reported by User: System Project Name: Duy CH20

Report Method: Duy CH20 Date Printed:
Report Method ID:1154
1154 9/6/2023
Page: 4 of 8 11:01:03 AM Asia/Ho_Chi_Minh
 Purity Plot
0.20
Purity
Auto Threshold 80.00

12.550
0.15

60.00

Degrees
0.10 M
AU

40.00

0.05
20.00

0.00 0.00
12.40 12.60 12.80 13.00 13.20
Minutes
PA: 0.194 TH: 0.302
Peak:
Purity
Auto Threshold
Purity Plot
0.012 Purity
Auto Threshold 80.00
18.102

0.010
60.00

Degrees
0.008
AU

M 40.00
0.006
20.00
0.004
0.00
17.00 17.20 17.40 17.60 17.80 18.00 18.20 18.40 18.60 18.80 19.00 19.20
Minutes
PA: 1.074 TH: 0.945
Peak:
Purity
Auto Threshold

Reported by User: System Project Name: Duy CH20

Report Method: Duy CH20 Date Printed:
Report Method ID:1154
1154 9/6/2023
Page: 5 of 8 11:01:03 AM Asia/Ho_Chi_Minh
 Match Plot
210.6 Peak #1

1.50

1.00
AU

0.50

0.00
220.00 240.00 260.00 280.00 300.00 320.00 340.00 360.00 380.00 400.00
nm

Match Plot
Peak #2
1.20

1.00

0.80
240.1
AU

0.60

0.40 301.9

0.20

0.00
220.00 240.00 260.00 280.00 300.00 320.00 340.00 360.00 380.00 400.00
nm

Match Plot
Peak #3
0.008

0.006
AU

0.004 304.3

0.002

353.3 397.6
0.000

220.00 240.00 260.00 280.00 300.00 320.00 340.00 360.00 380.00 400.00
nm

Reported by User: System Project Name: Duy CH20

Report Method: Duy CH20 Date Printed:
Report Method ID:1154
1154 9/6/2023
Page: 6 of 8 11:01:03 AM Asia/Ho_Chi_Minh
 Match Plot
1.50 Peak #4

1.00
AU

0.50 285.2

0.00
220.00 240.00 260.00 280.00 300.00 320.00 340.00 360.00 380.00 400.00
nm

Match Plot
Peak #5
0.004

0.003
AU

0.002

244.9 278.1
0.001

335.4348.5 377.1395.2
0.000

220.00 240.00 260.00 280.00 300.00 320.00 340.00 360.00 380.00 400.00
nm

Match Plot
0.50
Peak #6

0.40

0.30
AU

0.20 286.4

0.10

0.00
220.00 240.00 260.00 280.00 300.00 320.00 340.00 360.00 380.00 400.00
nm

Reported by User: System Project Name: Duy CH20

Report Method: Duy CH20 Date Printed:
Report Method ID:1154
1154 9/6/2023
Page: 7 of 8 11:01:03 AM Asia/Ho_Chi_Minh
 Match Plot
211.8 Peak #7

0.030

0.020
AU

0.010 248.4 276.9

0.000
220.00 240.00 260.00 280.00 300.00 320.00 340.00 360.00 380.00 400.00
nm

Reported by User: System Project Name: Duy CH20

Report Method: Duy CH20 Date Printed:
Report Method ID:1154
1154 9/6/2023
Page: 8 of 8 11:01:03 AM Asia/Ho_Chi_Minh