You are on page 1of 15

Wear 255 (2003) 975–989

Abrasive machining of porcelain and zirconia with a dental handpiece


L. Yin1 , S. Jahanmir∗ , L.K. Ives
National Institute of Standards and Technology, 100 Bureau Drive, Gaithersburg, MD 20899-8521, USA

Abstract
The machining characteristics and material removal mechanisms of two dental ceramics—feldspathic porcelain and yttria-stabilized
tetragonal zirconia—were investigated using a dental handpiece and diamond burs with different grit sizes. The material removal rates
were measured as a function of total machining time using a constant load of 2 N on the bur, consistent with clinical cutting conditions.
As the diamond grit size was increased from ultrafine (UF) (10 ␮m) to fine (F) (41 ␮m) and coarse (C) (172 ␮m), the removal rate
and the resulting surface roughness for each material increased substantially. The mechanisms of material removal determined through
microscopic examination of the machined surfaces and the machining debris on the burs were found to consist of a combination of
ductile and brittle-type chip formation processes. The occurrence of brittle fracture increased as the diamond grit size was increased.
While the material removal process in porcelain was dominated by brittle fracture, zirconia was primarily subjected to ductile cutting.
Four wear processes were identified on the burs in prolonged cutting tests: grit microfracture, grit pullout, wear flat generation, and
matrix abrasion. The results demonstrated that while the material removal rate for the zirconia evaluated in this study was lower than
those for porcelain and many other dental ceramics, the zirconia could be machined under clinical conditions with no edge chipping
damage.
© 2003 Elsevier Science B.V. All rights reserved.
Keywords: Dental restorations; Diamond burs; Dental handpiece; Yttria-stabilized tetragonal zirconia; Felspathic porcelain; Material removal mechanism;
Tool wear; Surface integrity

1. Introduction design and computer-aided manufacturing (CAD/CAM)


systems [9,10]. The desired shapes for crowns, onlays, or
Abrasive machining is routinely used in dentistry for the inlays are obtained fairly rapidly using either a milling cut-
preparation of teeth for filling, crowns, and bridgework, and ter or an abrasive tool depending on the properties of the
for making final fit adjustments on dental restorations [1]. In workpiece material. The data obtained in abrasive machin-
these machining procedures, a high-speed, air-driven den- ing of porcelain and zirconia with the dental handpiece can
tal handpiece with a diamond bur is often used. In spite of also be used as a guide for CAD/CAM preparation of dental
the importance of diamond machining in dentistry, there are restorations with these ceramics, where similar machining
only a few published studies on the subject [2–8]. Recent conditions apply.
studies have provided data on the machining characteris- Porcelains have been widely used for dental restora-
tics of tooth enamel [4], machinable glass-ceramics [6], and tions as veneers mainly because of their excellent esthetics
glass-infiltrated alumina [7] using a dental handpiece and [11–13]. More recently, modified feldspathic porcelains
diamond burs. The purpose of the present study is to inves- containing crystalline reinforcements have been used as
tigate the abrasive machining characteristics of a commonly onlays and inlays due to their high-longevity, comparable
used dental porcelain and a new tetragonal zirconia. wear resistance to natural tooth enamel, natural translu-
In addition to handpiece machining performed by the cency, radiopacity, and biocompatibility [14–18]. One ma-
dentist, abrasive machining is used to prepare ceramic jor problem in the use of porcelains in dentistry is their
restorations in the dental laboratory using computer-aided potential for brittle, catastrophic fracture [12,19] that may
be accentuated by machining damage [20,21]. As there is
little published information available on the machining be-
∗ Corresponding author. Present address: MiTiHeart Corporation, P.O.
havior of porcelains, one objective of the present study is
Box 83610, Gaithersburg, MD 20883, USA. Fax: +1-301-869-9724.
E-mail address: sjahanmir@mitiheart.com (S. Jahanmir).
to evaluate the machining responses of porcelains.
1 Present address: Gintic Institute of Manufacturing Technology, Singa- The second objective is to characterize the machining
pore 638075, Singapore. behavior in a high-toughness zirconia ceramic recently

0043-1648/03/$ – see front matter © 2003 Elsevier Science B.V. All rights reserved.
doi:10.1016/S0043-1648(03)00195-9
976 L. Yin et al. / Wear 255 (2003) 975–989

developed [22] as an alternative to porcelains or glass- dine [27]. Reported [28] mechanical properties are: Vickers
ceramics in posterior restorations. The surgical grade hardness = 6.3 ± 0.3 GPa, Young’s modulus = 69.7 GPa,
yttria-stabilized tetragonal zirconia polyscrystal (Y-TZP) and fracture toughness = 1.19 ± 0.05 MPa m1/2 . Specimens
with a high-fracture strength and toughness and an out- 3 mm × 4 mm × 25 mm in dimension were cut from blocks
standing biocompatibility have been used in orthopedics and all the surfaces were sand-blasted to achieve a uniform
for joint replacement for more than a decade [23,24] and in surface roughness.
dentistry as implants, abutments, inlays, onlays, and crowns The yttria-stabilized tetragonal zirconia evaluated in this
for several years [25]. The new colored zirconia ceramics study was a commercial, surgical grade zirconia, Prozyr
are aesthetic and can be made to closely match the color (Norton-St. Gobain, Northboro, MA), containing 3% mole
of human teeth [22]. Y-TZP ceramics are fully dense with fraction (5.1 ± 0.3% mass fraction) of yttria. It was prepared
a fine microstructure consisting of submicrometer tetrago- by isostatic pressing followed by sintering. The grain size
nal grains. The tetragonal to monoclinic transformation is distribution determined on a polished surface was relatively
accompanied by volume dilatation that produces compres- uniform with an average grain size of 0.6 ␮m [27]. The re-
sive stresses, making crack propagation more difficult and ported [28] mechanical properties are: Vickers hardness =
surface flaws less detrimental to fracture. Growth of micro- (13.9 ± 0.4) GPa, Young’s modulus = 210 GPa, fracture
scopic flaws that form during processing or surface damage toughness = (4.9±0.2) MPa m1/2 . The test specimens were
generated during service [12,19] is also impeded by the received in the form of bars with a rectangular cross-section
compressive stresses in the zirconia. Although the grinding (3 mm × 5 mm × 25 mm). The received specimens had been
behavior of zirconia with diamond wheels, and especially prepared by grinding with a 320-grit diamond wheel on all
the effect of grinding on strength, have been studied (see surfaces.
for example [26]), the abrasive machining of zirconia with
the dental handpiece and dental burs have not been inves- 2.2. Test apparatus
tigated. The surface integrity after machining, achievable
removal rates, and bur life are of primary interest when The machining apparatus utilized in this investigation has
machining the tough zirconia. been described previously [6]. It incorporated a high-speed
The purpose of the present study, therefore, is to inves- air-turbine-type handpiece equipped with an air–water mist
tigate the abrasive machining characteristics of feldspathic delivery system (625C Super Torque, KaVo American
porcelain and tetragonal zirconia with a dental handpiece Corp.). The dental handpiece was clamped to an arm that
and diamond burs that are commonly used in dentistry. The pivoted freely on a ball bearing support. The load between
removal rates are measured for burs with three diamond grit the bur and workpiece was established by a pulley and
sizes and the wear of burs is examined. The surface integrity, suspended weight arrangement.
including surface roughness and edge chipping is evaluated
as a function of diamond grit size. Microscopic examina- 2.3. Diamond burs
tion of machined surfaces and machining debris is used to
determine the mechanisms of material removal. The results Disposable dental diamond burs manufactured by NTI Di-
of this study are compared with results of similar studies on amond (Axis Dental Corporation, Irving, TX) were used.
other dental ceramics. Each bur comprised a steel blank of fixed diameter for

2. Experimental procedure

2.1. Workpiece materials

The dental porcelain selected for this study was Vita


Mark II (Vita Zahnfabric, Bad Sackingen, Germany)2 com-
monly used for inlays, onlays and veneer restorations in
the CAD/CAM Cerec system (Siemens, Bensheim, Ger-
many). The microstructure analyzed in a scanning elec-
tron micrograph of a polished cross-section consisted of a
glass matrix containing approximately 30% (volume frac-
tion) of irregularly-shaped crystalline particles measuring
from 1 to 7 ␮m in size, some of which were crystalline sani-
Fig. 1. Schematic representation of groove cut into a test sample with
2 Information on product names, manufacturers, and suppliers is in- a diamond bur, showing the designations used in the text for different
cluded for clarification. This does not imply endorsement of the products surfaces: (1) top surface, (2) bottom surface, (3) inside surface, (4) side
or services by the National Institute of Standards and Technology. surface, and (5) front surface.
L. Yin et al. / Wear 255 (2003) 975–989 977

mounting in the handpiece and a cutting portion that con- The actual bur diameter in the diamond section was larger
sisted of a single layer of synthetic diamond grit, elec- than the nominal diameter due to the added thickness of the
trolytically codeposited with nickel. Burs of three different plated layer and the diamond grit [6].
grit sizes designated by the manufacturer as ultrafine (862
012UF), fine (862 012F), and coarse (862 012C) were used. 2.4. Machining procedure
The average diameter of the diamond particles were esti-
mated from a series of micrographs obtained by scanning The orientation of the bur during machining with respect
electron microscopy (SEM) on new burs to be 10±3, 41±17, to the specimen is illustrated in Fig. 1, which also shows
and 172 ± 49 ␮m, respectively. The burs had a pre-plated schematically the various features associated with a single
nominal diameter of 1.2 mm and a straight cylindrical ge- groove cut in the specimen. The bur was oriented approxi-
ometry with a flame-shaped tip at the end. The burs were mately parallel to the 3 mm × 25 mm surface of the speci-
positioned so that only the straight cylindrical portion was in men (designated 5 in Fig. 1). A series of grooves was made
contact with the porcelain and zirconia workpieces (Fig. 1). along the length of each specimen.

Fig. 2. The volumetric removal rate as a function of total machining time for (a) porcelain and (b) zirconia cut with diamond burs of three different
grit sizes (UF: ultrafine, F: fine, and C: course). The mean value from the repeat tests with three new burs of each grit size is represented by the data
symbols. The uncertainty bars represent ± one standard deviation of the measured removal rates. The lines are empirical best fit to the data. Before the
fourth cut at 40 s, the burs were ultrasonically cleaned for 30 s.
978 L. Yin et al. / Wear 255 (2003) 975–989

Water coolant was delivered to the handpiece at a constant (Rz ) were used to characterize surface roughness. Three
flow rate of (15 ± 2) ml/min during cutting. The handpiece traces were made at different positions along each groove.
was positioned such that the water spray nozzle was located The mean values and the standard deviations of measure-
at 180◦ with respect to the bur–specimen contact. Before ments were determined from the three repeat measurements
each test series was begun, a light hydrocarbon lubricant on the three grooves cut with the three burs of each grit
(KaVo lubricant spray, KaVo American Corp.) was applied size.
for approximately 1 s to lubricate the handpiece bearings. Several machined specimens were ultrasonically cleaned,
The handpiece was then run without load for 60 s, as sug- sputter coated with gold, and examined in the SEM to assess
gested by Siegel and Von Fraunhofer [5], to remove the ex- the mechanisms of material removal during machining and
cess lubricant. to examine the groove edges for chipping damage. The quan-
A constant applied load of 2 N, typical of that used by tity used to determine the degree of edge chipping at each
clinicians in finishing operations [3,5], was used in the cut- groove was the projected chipped area per unit length (or
ting experiments. At a constant air pressure of 241 ± 7 kPa average chipping width) measured along the groove edges
(35 ± 1 psi), the pressure used throughout out this investi-
gation, the rotational speed of the bur was approximately
320,000 rpm, measured by means of a strobe-type tachome-
ter (Strobotac 1538-A, General Radio Company). On con-
tacting the specimen under the 2 N load the speed dropped
to 260,000 rpm where it remained until the handpiece was
removed from the specimen.
Three burs of each diamond grit size were used in the
study for each test condition to allow for evaluation of the
repeatability of the results. The machining sequence con-
sisted of cutting a series of four grooves with each bur along
the length of the porcelain and zirconia bars. The cutting du-
ration for each groove was approximately 5 s for porcelain
and 10 s for zirconia. A longer cutting duration was used for
the zirconia to account for the lower removal rate. The burs
were removed from the handpiece prior to the fourth cut and
were ultrasonically cleaned in water for 30 s (Cole-Parmer
Instrument Company, Chicago, IL). Bur cleaning was done
to reduce the possible effect of bur loading on the removal
rate.

2.5. Characterization methods

The volume removal rate for each groove was determined


by dividing the groove volume by the time to cut the groove.
The groove volume was determined by multiplying the av-
erage of the top and bottom groove areas by the specimen
thickness. An image analysis system (Leica Microimage
Video System with Image-Pro Plus) was used to measure
the top and bottom groove areas. The actual cutting dura-
tion was determined from the cutting force data that were
recorded as a function of time [6]. The means and standard
deviations were determined from the measurements on the
grooves that were cut with the three burs of each grit size
for the same machining duration.
Surface roughness was measured by means of a stylus
profilometer (Perthen, Mahr GmbH). The traces perpendic-
ular to the machining direction were made across the bottom
of the grooves (designated 3 in Fig. 1) using a trace length of
1.75 mm and a cut off length of 0.25 mm. Arithmetic mean
roughness (Ra ), maximum roughness (Rmax ), and mean
roughness, i.e. the average of five largest distances between Fig. 3. SEM micrographs of the burs after machining porcelain: (a)
the highest and the lowest points within the sampling length ultrafine bur, (b) fine bur, and (c) coarse bur.
L. Yin et al. / Wear 255 (2003) 975–989 979

on the top and bottom surfaces of the specimens (designated burs were ultrasonically cleaned, sputter coated with gold,
1 and 2 in Fig. 1). The projected chipped area is the area of and examined in the SEM to check for wear and grit pull
the chip projected on the plane of the top or bottom spec- out.
imen surfaces. Measurements of the chipped area and the
edge length of the grooves were made with the same image
analysis system used to determine the groove volume. Fol- 3. Results
lowing the cutting experiments, the burs were sputter coated
with gold and examined by SEM, without prior cleaning, 3.1. Material removal rate
to determine the condition of the burs with respect to bur
loading and grit wear and to identify the types of machining The removal rates achieved with the diamond burs were
chips that were left on the burs. higher for porcelain (Fig. 2(a)), than for zirconia (Fig. 2(b)),
by at least one order of magnitude. The removal rate for
2.6. Evaluation of bur wear both materials increased with an increase in the diamond
grit size. The removal rate for porcelain with the coarse burs
A series of prolonged cutting tests was conducted to fur- was approximately 15% higher than the removal rate with
ther evaluate the wear of diamond burs. In these tests, one the fine burs (Fig. 2(a)), even though the grit size was more
bur of each grit size was used to cut 60 grooves in the porce- than three times larger. The removal rate for porcelain with
lain (5 s duration each) for a total machining time of 300 s. the coarse burs was four to six times larger than the removal
Similarly, one fine bur was used to cut 72 grooves in the rate with the ultrafine burs. The removal rate for zirconia
zirconia (10 s duration each) for a total machining time of with the coarse burs was approximately 50% higher than the
720 s. The burs were ultrasonically cleaned in water for 30 s removal rate with the fine burs and 150% higher than the
several times during the tests. This procedure was followed removal rate with the ultrafine burs (Fig. 2(b)).
to minimize the influence of bur loading by removing the ma- In general, the removal rates for both materials decreased
chining debris attached to the bur. At the end of the tests, the as the total machining time was increased (Fig. 2). Ultrasonic
material removal rate was measured for each groove; and the cleaning of the burs prior to the fourth cut to remove bur

Fig. 4. SEM micrographs of zirconia machining debris on the burs: (a) small debris on an ultrafine bur, (b) a curled cutting chip on a fine bur, (c) debris
on a coarse bur, and (d) elongated chips on a coarse bur.
980 L. Yin et al. / Wear 255 (2003) 975–989

loading did not substantially affect the removal rate, with bris on the ultrafine and fine burs as well as a few larger
one exception. The removal rate for zirconia with the coarse particles (Fig. 3(a)), and agglomerated debris (Fig. 3(b)).
burs stayed relatively constant for the first three cuts, but No debris was seen on the coarse burs (Fig. 3(c)). The
it decreased for the last cut, in spite of ultrasonic cleaning sharp edges on the larger particles and the fragmented na-
prior to making the cut. ture of the fine debris suggest material removal by brittle
fracture.
3.2. Material removal mechanisms Four types of machining debris were observed on the burs
after cutting zirconia. The debris on the ultrafine burs con-
Examination in the SEM of the burs after machining did sisted mostly of small acicular particles 1–2 ␮m in length
not reveal clear evidence of wear, despite a trend towards (Fig. 4(a)). Several ribbon-like curled chips, often associated
decreasing removal rate with increasing cutting time in with ductile cutting, as well as small fragmented particles
these short tests. Examination of the burs used to cut the were seen on the fine burs (Fig. 4(b)). Debris on the coarse
porcelain showed numerous, very fine, submicrometer de- burrs (Fig. 4(c)), consisted primarily of small equiaxed

Fig. 5. SEM micrographs of porcelain machined surfaces cut with ultrafine burs (a and d), fine burs (b and e), and coarse burs (c and f). The micrographs
in (d–f) show the same surfaces as in (a–c) but at a higher magnification.
L. Yin et al. / Wear 255 (2003) 975–989 981

particles with dimensions on the order 1 ␮m or less, that are also contained features (pits with clearly defined edges) that
characteristic of chip formation by brittle fracture. Elongated were characteristic of a brittle removal process (i.e. brittle
chips, 20 ␮m in length and 1–2 ␮m in width, characteristic fracture). Examination of the machined surfaces at a higher
of segmented chips produced by ductile cutting, were also magnification (Fig. 5(d–f)), indicated an increasing trend
seen on the coarse burs (Fig. 4(d)). X-ray energy dispersive for microfracture as the grit size was increased. In contrast,
analysis in the SEM confirmed that the debris in Figs. 3 the scratches on zirconia surfaces did not contain much
and 4 originated from the respective porcelain and zirconia evidence for brittle fracture and the smooth scratches were
workpieces. characteristic of a ductile removal process (i.e. plastic defor-
The machined porcelain and zirconia surfaces viewed in mation). The zirconia surfaces machined with the ultrafine
the SEM consisted mostly of a series of parallel scratches burs were mostly characterized with very smooth scratches
(Figs. 5 and 6). The width of these scratches that appeared associated with plowing or ductile cutting (Fig. 6(d)). The
to be formed by plastic deformation increased as the grit zirconia surfaces machined with the coarse burs contained
size was increased (see Fig. 5(a–c) for porcelain, and characteristic features associated with plastic flow, delami-
Fig. 6(a–c) for zirconia). The machined porcelain surfaces nation of deformed layer, and side flow across the scratches

Fig. 6. SEM micrographs of zirconia machined surfaces cut with ultrafine burs (a and d), fine burs (b and e), and coarse burs (c and f). The micrographs
in (d–f) show the same surfaces as in (a–c) but at a higher magnification.
982 L. Yin et al. / Wear 255 (2003) 975–989

(Fig. 6(f)). Similar features were seen on the zirconia sur- and deeper scratches as the grit size was increased (Figs. 5
faces machined with fine burs (Fig. 6(e)), but the occurrence and 6).
of microfracture and delamination was less with the fine Examination in the SEM of the machined grooves in the
burs. porcelain showed no chipping damage with the ultrafine burs
(Fig. 9(a)), only slight chipping with the fine burs (Fig. 9(b)),
3.3. Surface integrity and relatively large chipped areas along the edges when
coarse burs were used (Fig. 9(c)). Examination of the ma-
The measured surface roughness values, Ra , Rz , and Rmax , chined grooves in zirconia showed no evidence for edge
increased for both materials as the grit size was increased chipping (Fig. 10(a–c)), even for the grooves cut with the
(Figs. 7 and 8). There was no effect of total machining time coarse burs (Fig. 10(c)). The average chipping width mea-
on the roughness parameters. The roughness appeared to sured for porcelain (Fig. 11), confirmed the strong influence
be independent of the material being machined, and only of diamond grit size on edge chipping in that material. The
the grit size had a major influence on roughness. The Ra porcelain samples showed a 5–10-fold increase in the ex-
roughness generated with the coarse burs was about three tent of chipping with the coarse burs compared with the fine
times as high as the Ra for the fine burs and 18 times as high burs. The standard deviations (Fig. 11), were much larger for
as the Ra for the ultrafine burs. The increase in roughness the coarse burs than the fine burs, indicating the difficulty in
was consistent with the SEM observations that showed wider maintaining a consistent edge quality with the coarse burs.

Fig. 7. Arithmetic average roughness (Ra ), 10 point height roughness (Rz ) and maximum roughness (Rmax ) for the grooves cut in porcelain with coarse,
fine, and ultrafine diamond burs. Each data point is the mean value from three repeat cuts with three different burs under the same machining condition;
the error bars represent ± one standard deviation for the cuts.
L. Yin et al. / Wear 255 (2003) 975–989 983

Fig. 8. Arithmetic average roughness (Ra ), 10 point height roughness (Rz ) and maximum roughness (Rmax ) for the grooves cut in zirconia with coarse,
fine, and ultrafine diamond burs. Each data point is the mean value from three repeat cuts with three different burs under the same machining conditions;
the error bars represent ± one standard deviation for the cuts.

The average chipping widths with the ultrafine burs were dislodgment or pullout (Fig. 13(a)), probably due to poorly
negligible. held particles in the matrix or application of excessive grit
load, accounted for about 20% diamond loss in the ultrafine
3.4. Wear of diamond burs bur when machining porcelain. Although grit dislodgment
accounted for about 8 and 9% diamond loss after machining
The removal rate of porcelain after prolonged tests (300 s porcelain with the fine and coarse burs, grit fracture, where
of machining) was reduced by 70, 90 and 80% for the ul- large portions of the grit were cleaved off (Fig. 13(b–c)),
trafine, fine and coarse burs (Fig. 12(a)), presumably due to was found to be the dominant wear process in these burs.
wear of the burs. The removal rate of zirconia after 720 s Similarly, while grit dislodgment accounted for about 15%
of machining with the fine bur was reduced by only 50% diamond loss (Fig. 14(a)), when machining zirconia with
(Fig. 12(b)). Examination of the burs in the SEM after the the fine burs, grit fracture (Fig. 14(b)), was found to be the
prolonged cutting tests and following ultrasonic cleaning to dominant wear process. Several diamond grit were found to
remove the machining debris revealed four types of wear contain wear flats, where the grit edges had been worn pro-
damage: grit dislodgment, grit fracture, attritious wear, and ducing small flat surfaces (Fig. 14(c)). Wear flat generation,
matrix abrasion. The extent of each damage type was dif- or attritious wear, was also observed in burs used for porce-
ferent for each workpiece and the diamond grit size. Grit lain machining, but it was not a common wear process with
984 L. Yin et al. / Wear 255 (2003) 975–989

Fig. 9. SEM micrographs showing typical chipping damage around the


groove top surfaces for porcelain cut with (a) an ultrafine bur, (b) a fine Fig. 10. SEM micrographs showing no chipping damage around the groove
bur, and (c) a coarse bur. top surfaces for zirconia cut with (a) an ultrafine bur, (b) a fine bur, and
(c) a coarse bur.

either material. Abrasion damage to the nickel matrix was


also observed (Fig. 14(b)). rates for the porcelain were equivalent to that of Dicor, a
machinable glass ceramic [6], the removal rate of zirconia
was close to the rate obtained for InCeram alumina [7].
4. Discussion These four ceramics seem to show a correlation between
the removal rate and hardness. However, a more systematic
In this study, we have compared the abrasive machining analysis is needed before an authoritative statement can be
behavior of dental porcelain with a high-strength zirconia made. Although the removal rates of porcelain and zirconia
using dental burs of three different grit sizes. The results are significantly different, the surface roughness parameters
clearly show a distinct difference in response for the two are almost indistinguishable when the same bur grit size is
materials, both with respect to the removal rates achieved used. This material-independent roughness behavior is con-
during cutting and the basic removal mechanisms. The re- sistent with the previous results for glass-ceramics [6] and
moval rates for the porcelain were larger by at least one glass-infiltrated alumina [7], and with a Monte Carlo simu-
order of magnitude than for zirconia. While the removal lation of surface roughness generated by abrasive machining
L. Yin et al. / Wear 255 (2003) 975–989 985

Fig. 11. Average chipping width around the groove surfaces in porcelain cut with coarse, fine, and ultrafine diamond burs. Each data point is the mean
value from three repeat cuts with three different burs under the same machining conditions; the error bars represent ± one standard deviation for the cuts.

[29]. In that study, surface roughness was shown to be pri- increase in the grit size is accompanied by a reduction in the
marily sensitive to the grit size, consistent with the present number of diamond particles in dental burs [6]. Therefore,
results. with the same load is applied to the bur, the grit load can be
Diamond grit size plays an important role in abrasive ma- much larger with a coarser bur. The higher grit load causes
chining. It is generally believed that higher removal rates an increased grit penetration into the ceramic workpiece re-
can be achieved by coarser grit burs, and therefore, coarse sulting in a higher removal rate and generation of surface
burs are often used for gross tooth reduction [8]. The rela- and subsurface cracks. Both the removal rate and the ex-
tionship between the removal rate and grit size, however, is tent of chipping damage depend on the same properties that
not necessarily linear for all materials. While the removal control deformation and fracture of the ceramics, i.e. hard-
rate for porcelain was higher by about 15% with coarse burs ness and toughness [30], that also control the mode of ma-
than with fine burs, the removal rate for zirconia increased terial removal, i.e. brittle fracture versus plastic deformation
by nearly 50% upon the use of coarse burs. The removal rate [20].
for machinable glass-ceramics did not always increase with The material removal mechanism in abrasive machining
the use of coarse burs [6]. However, coarse burs substantially of porcelain was dominated by brittle fracture, as seen by the
increased the extent of chipping damage along the edges of pits with sharp edges on the machined surfaces (Fig. 5) and
the grooves cut in glass-ceramics [6], similar to the results on the fragmented appearance of the machining debris (Fig. 3).
porcelain in the present study. The zirconia ceramic, unlike However, the removal mechanisms for zirconia were primar-
the porcelain, did not exhibit any visible edge chipping with ily plastic deformation and microcutting, as evidenced by
any of the burs used in this study. Since edge retention at the smooth furrows on the machined surfaces (Fig. 6) and
the margins and the achievement of close dimensional toler- the ribbon-like shape of the machining debris (Fig. 4). The
ances are important issues in obtaining high-quality restora- difference in the behavior of these two materials with respect
tions, one must balance the high-removal rates often asso- to the predominance of brittle fracture or plastic deforma-
ciated with the use of coarse burs with the potential loss tion is consistent with Hertzian contact studies [27]. For the
of surface/edge integrity. The use of coarse burs could also porcelain, the response to indentation with a tungsten car-
increase the propensity for generation of subsurface cracks bide sphere was classical brittle fracture, i.e. formation of
with concomitant strength degradation [20]. The strength a well defined cone crack [27]. The response for zirconia,
reduction due to machining-induced damage is, however, however, was primarily plastic or quasi-plastic, i.e. evolu-
material-dependent. The yttria-stabilized tetragonal zirconia tion of a diffuse subsurface zone of microscopic shear cracks
is less sensitive to machining damage compared to many [27]. The brittle/ductile response of these two materials to
other polycrystalline ceramics [26]. indentation can also be predicted by using a brittleness in-
The effect of grit size on removal rate and edge chip- dex proposed by Rhee et al. [31], derived from the ratio of
ping is not necessarily a simple phenomenon. Usually, an the contact load needed for initiation of subsurface plastic
986 L. Yin et al. / Wear 255 (2003) 975–989

Fig. 12. The volumetric removal rate as a function of total machining time in prolonged cutting tests for (a) porcelain and (b) zirconia. Diamond burs of
three different grit sizes (ultrafine, fine, and course) were used in the tests with porcelain, while only a fine bur was used with zirconia. The burs were
ultrasonically cleaned several times during the test series.

yield to the threshold load for the formation of ring cracks. The cutting efficiency is measured by the reduction in the
The distinction between the brittle/ductile behavior of these removal rate as a function of cutting time. The decrease in
two materials can also be predicted by using a similar brit- the removal rate as a function of cutting time is generally
tleness index proposed by Quinn and Quinn [32], related to due to bur loading (attachment of machining debris to the
the ratio of deformation energy to fracture energy. bur) and wear of the diamond particles. The influence of bur
The disposable or single-patient diamond burs employed loading in our study, however, was minimal since ultrasonic
in the present study are chosen by the clinicians to minimize cleaning of the burs prior to the fourth cuts did not signifi-
cross-contamination risks of bloodborne pathogens [33]. It cantly increase the removal rate (Fig. 2).
is likely that such burs would be used no more than a few Wear of the burs occurred through grit fracture, grit
tens of seconds before being discarded. However, our results pullout, wear flat generation or attritious wear, and matrix
indicate that these single-patient burs can be used for sev- damage. These results are consistent with the observed
eral minutes without a significant loss of cutting efficiency. wear mechanisms previously discussed for dental cutting
L. Yin et al. / Wear 255 (2003) 975–989 987

Fig. 13. SEM micrographs of the burs after prolonged cutting tests on
porcelain: (a) grit dislodgment on the ultrafine bur, (b) grit fracture on
the fine bur, and (c) grit fracture on the coarse bur. Fig. 14. SEM micrographs of a fine bur prolonged cutting tests on zirconia
showing different types of wear and damage: (a) grit dislodgment, (b)
grit fracture and matrix abrasion, and (c) wear flat generation.
of glass-infiltrated alumina [7]. The observed grit fracture
suggests that a friable (self-sharpening) diamond had been
used in the burs, which may explain the fairly high-cutting ing debris could cause abrasion damage on the metal matrix
efficiency of the burs in prolonged tests. used to hold the diamond particles on the bur, weakening
The wear mechanisms in diamond burs can also be influ- the bond between the diamond particles and the matrix, and
enced by the grit size. It is generally accepted that finer di- resulting in grit loss. Therefore, grit loss becomes a more
amond particles are stronger than the larger ones due to the dominant wear process for finer burs.
lower flaw population as the original flaws in the large par-
ticles are eliminated by fracture when finer grit is made by
crushing the coarse diamond particles [34]. Therefore, less 5. Conclusions
grit fracture is expected for finer burs. However, fine burs
are more prone to matrix damage since the space available In this study, we investigated the machining character-
for debris removal is smaller for the fine burs. The machin- istics of feldspathic porcelain and tetragonal zirconia with
988 L. Yin et al. / Wear 255 (2003) 975–989

a dental handpiece and diamond burs of varying grit sizes [5] S.C. Siegel, J.A. Von Fraunhofer, Effect of handpiece load on the
under simulated clinical cutting conditions. The following cutting efficiency of dental burs, Mach. Sci. Technol. 1 (1) (1997)
conclusions are drawn from the results: 1–13.
[6] X. Dong, L. Yin, S. Jahanmir, L.K. Ives, E.D. Rekow, Abrasive
(1) As the diamond grit size was increased from ultrafine machining of glass-ceramics with a dental handpiece, Mach. Sci.
Technol. 4 (2) (2000) 209–233.
(10 ␮m) to fine (40 ␮m) and coarse (151 ␮m) the re-
[7] L. Yin, L.K. Ives, S. Jahanmir, E.D. Rekow, E. Romberg, Machining
moval rate and the resulting surface roughness for both characteristics of glass-infiltrated alumina with diamond burs, Mach.
materials increased substantially. Sci. Technol. 5 (1) (2001) 43–61.
(2) The removal rate for porcelain was much higher than [8] S.C. Siegel, J.A. Von Fraunhofer, Dental cutting: the historical
for zirconia for all grit sizes. development of diamond burs, J. Am. Dent. Assoc. 129 (6) (1998)
740–745.
(3) The porcelain sustained severe edge chipping with both [9] E.D. Rekow, A.G. Erdman, D.R. Riley, B. Klamecki, CAD/CAM
coarse and fine burs, but edge chipping was essentially for dental restorations—some of the curious challenges, IEEE Trans.
absent with the ultrafine burs. The zirconia was free of Biomed. Eng. 38 (4) (1991) 314–318.
edge chipping for all grit sizes. [10] E.D. Rekow, Dental CAD/CAM systems, J. Am. Dent. Assoc.
122 (13) (1991) 42–48.
(4) The surface roughness increased with increasing grit
[11] M. Friedman, Augmenting restorative dentistry with porcelain
size for both porcelain and zirconia, and it was material- veneers, J. Am. Dent. Assoc. 122 (6) (1991) 29–34.
independent. [12] J.R. Kelly, Ceramics in restorative and prosthetic dentistry, Mater.
(5) The mechanisms of material removal determined Sci. 27 (1997) 443–468.
through microscopic examination of the machined sur- [13] M. Rosenblum, A. Schulman, A review of all-ceramic restorations,
J. Am. Dent. Assoc. 128 (3) (1997) 297–307.
faces and the machining debris on the burs were found [14] I. Denry, J. Mackert, L. Holloway, S. Rosentiel, Effect of cubic
to consist of a combination of ductile and brittle-type leucite stabilization on the flexural strength of feldspathic dental
chip formation processes. The occurrence of brittle porcelain, J. Dent. Res. 75 (12) (1996) 1928–1935.
fracture increased as the diamond grit size was in- [15] R. Seghi, I. Dnery, S. Rosenstiel, Relative fracture toughness and
hardness of new dental ceramics, J. Prosthet. Dent. 74 (2) (1995)
creased. While the material removal process in the
145–150.
porcelain was dominated by brittle fracture, the re- [16] I. Krejci, F. Lutz, M. Reimer, Wear of CAD/CAM ceramic inlays:
moval process in zirconia was dominated by ductile restorations, opposing cups, and luting cements, Quintessence Int.
cutting. 25 (3) (1994) 199–207.
(6) Four wear processes were identified on the burs in pro- [17] H. Schwickerath, The strength characteristics of cerec, Quintessenz
43 (1992) 669–677.
longed cutting tests: grit microfracture, grit pullout, wear [18] I. Krejci, in: W. Mormann (Ed.), Wear of cerec and other restorative
flat generation, and matrix abrasion. materials, Proceedings of the International Symposium on Computer
Restorations, Quintessence Publishing, Chicago, IL, USA, 1991,
pp. 245–251.
[19] J.R. Kelly, I. Nishimura, S.D. Campbell, Ceramics in dentistry:
Acknowledgements historical roots and current perspectives, J. Prosthet. Dent. 75 (1)
(1996) 18–32.
[20] S. Jahanmir, H.H.K. Xu, L.K. Ives, in: S. Jahanmir, P. Koshy,
We acknowledge the generous supply of materials from
M. Ramulu (Eds.), Mechanism of Materials Removal in Abrasive
Norton St. Gobain and Vita Zhanfabrik. This project Machining of Ceramics, Machining of Ceramics and Composites,
was supported by NIDCR Program Project Grant No. Marcel Dekker, New York, 1999, pp. 11–84.
P01 DE 10976. We are grateful to Professors E.D. [21] H.H.K. Xu, S. Jahanmir, L.K. Ives, Material removal and damage
Rekow and V.P. Thompson of the New York University formation mechanisms in grinding silicon nitride, J. Mater. Res.
11 (7) (1996) 1717–1724.
College of Dentistry for their overall guidance of this [22] B. Cales, Colored zirconia ceramics for dental applications,
program. Bioceramics 11 (1998) 591–594.
[23] B. Cales, Zirconia ceramic for improved hip prosthesis—a review,
in: Proceedings of the Sixth Biomaterials Symposium on Ceramic
Implant Materials in Orthopedic Surgery, Gottingen, Germany,
References 1994.
[24] J. Chevalier, J.M. Drouin, B. Cales, in: L. Sedel, C. Rey (Eds.),
Low Temperature Aging Behavior of Zirconia Hip Joint Heads,
[1] C.M. Stuedevant, T.M. Roberson, H.O. Heymann, J.R. Sturdevant,
Proceedings of the Tenth International Symposium on Ceramics in
The Art and Science of Operative Dentistry, third ed., Moshy-Year
Medicine, Elsevier, Amsterdam, 1997.
Book Inc., St. Louis, 1995, pp. 345–357.
[25] Active Biomedicale, Norton Desmarquest, 1998.
[2] J.A. Von Fraunhofer, T.J. Overmyer, A.A. Johnson, Improved cutting [26] H.H.K. Xu, S. Jahanmir, L.K. Ives, Effect of grinding on strength
of tooth enamel with dental burs, Quintessence Int. Oper. Dent. of tetragonal zirconia and zirconia-toughened alumina, Mach. Sci.
18 (6) (1987) 383–385. Technol. 1 (1) (1997) 49–66.
[3] J.A. Von Fraunhofer, C.D. Givens, T.J. Overmyer, Lubricating [27] I.M. Peterson, A. Pajares, B.R. Lawn, V.P. Thomspon, E.D. Rekow,
coolants for high-speed dental handpieces, J. Am. Dent. Assoc. Mechanical characterization of dental ceramics by hertzian contacts,
119 (8) (1989) 291–295. J. Dent. Res. 77 (4) (1998) 589–602.
[4] H.H.K. Xu, J.R. Kelly, S. Jahanmir, V.P. Thompson, E.D. Redow, [28] J. Quinn, L. Su, L. Flanders, L. Lloyd, Edge toughness and material
Enamel subsurface damage due to tooth preparation with diamonds, properties related to the machining of dental ceramics, Mach. Sci.
J. Dent. Res. 76 (10) (1997) 1698–1706. Technol. 4 (2) (2000) 291–304.
L. Yin et al. / Wear 255 (2003) 975–989 989

[29] P. Koshy, L.K. Ives, S. Jahanmir, Simulation of diamond ground [32] J.B. Quinn, G.D. Quinn, Indentation brittleness of ceramics: a fresh
surfaces, Int. J. Mach. Tools Manufac. 39 (1999) 1451–1470. approach, J. Mater. Sci. 32 (1997) 4331–4346.
[30] B.R. Lawn, Fracture of Brittle Solids, Cambridge University Press, [33] G.J. Christensen, R.P. Christensen, Single patient-use diamond rotary
Cambridge, UK, 1993. instruments, Clin. Res. Assoc. Newslett. 15 (6) (1991) 1–2.
[31] Y.-W. Rhee, H.-W. Kim, Y. Deng, B.R. Lawn, Brittle fracture versus [34] M.C. Shaw, Principles of Abrasive Processing, Oxford Science
quasi plasticity in ceramics: a simple predictive index, J. Am. Ceram. Publications, Oxford, 1996.
Soc. 84 (3) (2001) 561–565.

You might also like