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International Journal of Mechanical & Mechatronics Engineering IJMME-IJENS Vol:19 No:01 160

Experimental Investigation on Low Velocity Impact


of a Novel Fibre Metal Laminate (FML) Tube
M. A. Mansor1, Z. Ahmad2 and M. R.Abdullah2
1
Faculty of Engineering Technology, Universiti Teknikal Malaysia Melaka
2
Faculty of Mechanical Engineering, Universiti Teknologi Malaysia
mazlan.mansor@utem.edu.my

Abstract-- The experimental study of new tubular type of to be considered in the industry, composite gains popularity
Fibre Metal Laminate (FML) with braided fibreglass sleeve and among researchers for its strength compare to metal structures
aluminium alloy tubes was performed and its manufacturing [3] [4]. In the event of an axial impact, composite materials
process was proposed. Aluminium tubes was machined to specific such as GFRP encounter fractures to absorb energy that differ
thickness and chemically treated to improve the adhesive from metals which deformed plastically [5] [6]. Failure modes
bonding. Sleeve type braided fibreglass was selected as it comes
of composite are far more complicated compared to metallic,
in specific dimension and more importantly it is seamless and
perfectly produces an excellent composite tube. Tubes carefully involving fibre breakage, fibre buckling, fibre-matrix
assembled to form 2/1 and 3/2 layup configurations and highly de-bonding, matrix cracking, matrix crushing, and
adhesive resin was introduced as interlayer, which is composed of delamination [7] [8] that are contributing to the energy
two layers of aluminium tubes and one layer of fibreglass braided absorbing characteristics.
sleeve in between for 2/1 layup. The new design tube was tested to
evaluate the behaviour and impact characteristics under low In crushing event, the energy absorption (Ea)
velocity axial impact loading, where its intended purpose of measures the total strain energy absorbed by the structure,
application. This tube crushed progressively and was able to which is determined in terms of the area under the
avoid catastrophic failure. The results also indicate that the
force-displacement curve as,
mechanical performance of the new FML tube could be applied
as a new and efficient energy absorber.
𝑑
𝐸𝑎 = ∫0 𝐹(𝛿)𝑑𝛿
Index Term-- Fibre Metal Laminate, Energy Absorption, (1)
Crashworthiness, Low Velocity, Impact Loading.
where F(δ) denotes the instantaneous crushing force and d is
1. INTRODUCTION the crushing distance concerned. Specific Energy Absorption
Over the last decade, thin-walled structures have (SEA) is energy absorption capability, which is calculated as
been widely used as energy-absorbing devices to protect the per unit mass absorbed. To account for the effect of mass (m),
occupants from injury in the event of collision. Continuous specific energy absorption (SEA) defined as
efforts have been devoted to investigate the crashworthiness
characteristics for a variety of thin-walled structures. In the 𝑑
𝐸𝑎 ∫0 𝐹(𝛿)𝑑𝛿
event of an accident, the best chance of survival is the ability 𝑆𝐸𝐴 = =
𝑚 𝑚
to absorb or divert kinetic energy. Different geometries and (2)
materials of tubular structure members have been widely used
as energy absorber. They have the ability to absorb and SEA is frequently used as one of most critical crashworthiness
convert large kinetic energy into plastic strain energy when criteria. A higher SEA indicates better material usage
deformed under compression in the state of impact. Used as a efficiency for energy-absorption structure.
crash absorber located in the crash box, this device absorbs the
kinetic energy from an impact and collapse progressively in Prior to material failure due to buckling, initial
controlled manner. The collapse is usually in a concertina crushing peak load is measured [9]. Further failure will lead to
mode or diamond mode, or combination of both modes [1]. either catastrophic or progressive failure [10]. For an
occurrence of progressive failure, a larger area under the curve
Contemporary land vehicles prefer to use a will be gained with a constant load as the crush distance
lightweight material that is strong enough to sustain high increased. Contrarily the catastrophic failure will cause the
impact energy. Traditionally in the metal family, steel and drastic load drop causing lower energy absorption due to the
aluminium are the material of choice for its lightweight, structure integrity has been compromised horizontally [11] or
strength and cost. There is also non-metallic material from longitudal cracks happen [12]. In an axial crushing of
composite family such as glass fibre reinforced plastic (GFRP) composite structure, there will be two fracture failure types
and carbon fibre reinforced plastic (CFRP) that is very popular that are progressive failure that results in desirable
to substitute the metallic as the crash absorber. It has very high high-energy absorption and catastrophic failure results in
strength to weight ratio when compared to steel or aluminium minimal energy absorption [13].
[2]. As the weight savings became an important improvement
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With the lightweight features and good in specific is extracted from the composite tube during the curing
energy-absorption (SEA) capability, the composite materials process. This hybrid tubes with 90º ply oriented composite
are still not suitable to replace metallic components structure. tubes demonstrate the best energy absorption capability among
For this reason, the metal/composite hybrid structures were all hybrid tubes. When aluminium tube deform, the composite
introduced by combining the low density and high strength of material prevents the aluminium tube from folding. Hybrid
composite materials with low cost and high plasticity metallic tube failure is stable and progressive without any trigger
materials such as aluminium in crushing structures. It has mechanism because the internal aluminium tubes can play the
proven that catastrophic failure mode of composite structure role of crack initiator and controller. El-Hage et al. [22]
can be changed to a progressive failure mode when the studied the behaviour of aluminium composite hybrid tubes
fracture process of the composites is guided by the plastic containing glass fibre reinforced epoxy wrap around
deformation of aluminium, thereby improving energy aluminium tubes in the static quasi-destructive static axis. The
absorptions for the whole structures [14] [2]. fibre orientation is 45º to the tube axis. The fold initiation
force is lower with adhesive between aluminium tubes and
The study of tubes with two different materials, also composites than without adhesive. The high bond failure limit
called hybrid tubes was carried out by Mamalis et al [15]. In produces a lower folding initiation force and mean crush
this study, the effects of different parameters such as force.
geometrical construction, material properties, and metal
thicknesses were investigated. The changes in these Most all the study in the hybrid tubes shows of better
parameters may affect the energy absorption and tube failure energy absorption capacity than the single metallic or
modes. Kim et al. [16] and Zhu et al. [7] study the axial composite tubes. However there is still a catastrophic failure
crushing of metal tubes reinforced by a composite layer from happen in the test that resulting low energy absorption makes
experiments and El-Hage et al. [17] and Huang et al. [18] did the hybrid tubes not completely able to replace metal
in numerical. The results show that various parameters could components in the particular structures. A new design for
contribute to collapse and affect the characteristics of hybrid is introduced in this study to add another metallic
crashworthiness in form of absorbed and specific energy, seamless layer to the outer most tube of hybrid tube. The
minimum and peak load and crush force efficiency. The design is similar to the layer of panels in fibre metal laminates
crushing behaviour of a metal/composite hybrid structure can panels except in the form of seamless tube. This design could
be influenced by geometry, composition of composite be called fibre metal laminate (FML) tubes as well. At the
arrangement, surface treatment, strain rate, and others. The present, this FML tubes design and its performance as energy
idea of increasing the energy absorption capability of the absorber has not been studied and discussed in open literature
metal tubes through composite reinforcement was introduced which makes this research more interesting.
by Song et al. [19] studies. In the experiment, the effects
factors such as strain rate, composite wall thickness, fibre In this study, aluminium was chosen to make the
orientation and mechanical properties of the metal tubes are inner and outer metallic tube; the glass fibre was chosen as
subject to impact loads. They obtained four major modes of reinforcement and epoxy resin as matrix materials to
collapse for hybrid tubes including: compound diamonds, manufacture the aluminium/GFRP FML tube by using new
compound fragmentation, delamination and catastrophic method that will be established. Dynamic low velocity impact
failure. Bouchet et al. [20] analyses the effects of crushing tests were carried out for investigating the effects
reinforcement and different surface treatment of metal tubes to reinforcing external and internal layer of composite tube with
enhance practical adhesion between composites and metal aluminium tube on the crashworthiness. A study on energy
tubes. The value obtained from specific energy absorption absorption and crushing mode of the FML tubes was
indicates that the influence of multi-material structures surface performed to evaluate this new design as a potent energy
treatment do not have significant contribution, whereas the use absorber.
of reinforcement can improve the performance of
crashworthiness if the same crushing mode is maintained. For 2. MATERIAL PREPARATION AND FABRICATION
thin aluminium alloy tubes, with or without reinforced fibre METHOD
plastic composites, diamond modes have been observed. On The FML tubes were built in the form of 2 × 1 (m ×
the contrary, a thick tube without reinforcement produce the n) and 3 × 2 stacking layers with a maximum diameter of
concertina collapse mode while a thick tube with 49.6mm and length of 100 mm. The fabrication was carried
reinforcement observed the diamond collapse mode. When the out using a conventional machining technique. In particular, m
crushing mode changes, the reinforcement used on the and n signify the number of layer for metallic and composite
aluminium tube decreases the capacity of the structure to layers, respectively.
absorb energy. On the other hand, the reinforcement used on
the thinner tube increases the SEA of the tube.
2.1. Material selection
Shin et al. [21] wrapped glass fibre-epoxy composite
pre-impregnated around an aluminium tube and cured 2.1.1. Aluminium
completely in the autoclave. The bonds between composite For metal part, aluminium 6063-T5 tube is used due
tubes and aluminium are performed by excessive resin which
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to its ductility and predominant impact properties compared to viscosity, odourless and cures at room temperature. This
other metals. A long piece of aluminium alloy AA6063-T5 matrix also can be used with other applications such as
[23] circular tubes with 50.4mm outer diameter and thickness S-Glass, Kevlar and Carbon fibres for lay-up of composite
3mm was acquired. These tubes were cut into specific parts.
diameter with thickness 0.4 mm using conventional lathe
machine. 2.2. Manufacturing process

2.1.2. Composite In this section, the process of producing effective


For continuous fibre reinforced thermoplastic FML thin-walled tubes will be presented. The fabrication
composites, a biaxial fibreglass sleeve from Soller Composite method for the FML tube here is a bold process. Detail
of USA was used. This sleeve type e-glass fibre is the best material preparations and manufacturing methods are
option for composite tubes as it is seamless. A sleeve or tube describes in this section.
of braided material behaves like a Chinese finger trap.
Because the fibres are woven together at 45 degrees, it can 2.2.1 Aluminium tubes cutting process
simply pull the braid to lengthen it or compress to shorten it. AL6063 aluminium tube will be cut to the thickness
This pull will reduce the fibre orientation to about 35 0.4 mm using conventional lathe machine. Machining
degrees. As the total surface area remains constant, the more it tolerance was set at +50 microns to avoid over cutting and for
is lengthening, the more the diameter shrinks or tightens. A safety reason. As the final tube is very thin, special made jigs
commercially available diameter 50.4mm sleeve with are required for the cutting process.
thickness of 0.28 mm was selected as the composite
reinforcement 2.2.2. Surface treatment of the aluminium tube
Table I indicates the surface treatment methods,
2.1.3. Matrix systems namely mechanical abrasion, solvent degreasing, alkaline
Epoxamite 100 is the liquid epoxy system for degreasing, and plasma, which were used to modify the
fibreglass product fabrication applications produced by surface properties of the aluminium tubes so that the adhesive
Smooth-On Inc of the USA. The epoxy with its 101 hardener strength between the composites and aluminium plate can be
was used in the study. When mixed, the matrix liquid is low in improved.
Table I
Applied surface treatment methods for aluminium tube.
Surface treatment methods Solutions Applied conditions
Solvent degreasing Ethanol Wipe with clean cloth
Chemical Etch - Kellers Distilled Water 190ml 2 minutes immersion.
Nitric Acid 5ml Use fresh
Hydrochloric Acid 3ml
Hydroufluoric Acid 2ml
Rinse Hot water 10 second
Clean Distilled water Ultrasonic bath 1 hour

The machined tubes were etched in Kellers etchant water and later were cleaned using ultrasonic bath to remove
solution for 2 minutes to remove their unwanted interior unwanted chemical residue left throughout the process. Finally
extrusion surfaces. Kellers etchant is a solution consists of the tube will be rinsed using distilled water and left for 24
nitric acid, hydrochloric acid and hydroflouric acid diluted hours to dry out in the room temperature.
with distilled water. The tubes then will be rinsed with hot

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Fig. 1. Assembly procedure (a) push the outer tube to cover the composite sleeve (b) access material will be trimmed after it is cured

2.2.3. FML tube assembly process removed and trim to the sizes. Figure 2 illustrates the
The assembly process of FML tubes is the core geometries of the circular tube, with the length (L), wall
novelty in the research. The method was to impregnate the thickness (t) and outer diameter (D).
fibreglass sleeve with epoxy, tie one end with cable tie. Cover
the inner tube with this sleeve; carefully push the outer tube to The sample preparation has produced two types of
the sub-assembly as in Figure 1. FML, 2/1 and 3/2 tubes as in Figure 3. All of these tubes have
an outer diameter of 49.6mm while the thickness are
The procedure is applicable for any number of FML according to the number of layers constructed. As a
tube layup. It is important to start with the most inner tube, comparisons, a set of bare aluminium tube with equivalent
followed by fibreglass sleeve and finally with the most outer mass to 2/1 FML tube and similar internal diameter were
tube. The material stack up should be alternately assembled prepared and tested all together. Tables 2 to 4 then show the
with aluminium and composite materials. After the FML tubes measurements of 2/1, 3/2 FML tubes and aluminium bare tube
successfully produced, the FML tubes should be clean from respectively that have been taken. Both 2/1 FML tubes and
access epoxy using clean cloth, kept and cure at the room aluminium bare tube have a general inner diameter of 46.6mm
temperature for 24 hour. Later the access material should be while 3/2 FML tubes is 44.4mm.

Fig. 2. Schematic of FML tube parameters.

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Fig. 3. 2/1 FML tubes and 3/2 FML tubes.


2.2.4. GFRP layer observation can be cut into pieces and stack together. The edge of the plate
The critical point in building this FML tube is to also open ended makes it easy to assemble. While in the FML
make sure the composite layer intact in between two metal tube, all the layers are seamless and in a tube form makes it
layers. As in a FML plate, the metal and composite materials very hard to laminate all the tubes become a FML tube.

Table II
2/1 FML tube measurement
Label Mass (g) Length ( L ) Diameter ( D ) Thickness ( t )
DB1 48.92 100.03 47.70 1.55
DB2 48.82 100.05 47.60 1.54
DB3 49.11 100.11 47.67 1.54
DB4 47.69 100.06 47.60 1.54
DB5 48.68 100.07 47.65 1.60
Mean 48.64 100.07 47.64 1.55
Std Dev 0.56 0.03 0.05 0.03

Table III
3/2 FML tube measurement
Label Mass (g) Length ( L ) Diameter ( D ) Thickness ( t )
DC1 81.67 100.07 49.59 2.53
DC2 81.37 100.06 49.64 2.57
DC3 80.64 100.01 49.62 2.59
DC4 80.06 99.85 49.65 2.55
DC5 80.54 99.98 49.66 2.57
Mean 80.86 99.99 49.63 2.56
Std Dev 0.65 0.09 0.03 0.02

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Table IV
Aluminium bare tube measurement
Label Mass (g) Length ( L ) Diameter ( D ) Thickness ( t )
T1 48.60 99.64 49.15 1.17
T2 48.27 99.70 49.13 1.19
T3 49.73 99.83 49.22 1.23
T4 48.44 99.78 49.20 1.17
T5 48.36 99.96 49.21 1.21
Mean 48.68 99.78 49.18 1.19
Std Dev 0.60 0.12 0.04 0.03

After the FML tube was fabricated, the best way to bubble area detected on the composite layer indicates the
ensure that the composite layer was successfully installed is to process was successfully done. The layer also shows the
observe it with naked eye. The external aluminium layer was thickness is even at all area and the measurement indicates
ply open and to expose internal composite layer. constantly 0.6mm. The information given by the manufacturer
tells that the thickness of a single layer of this glass fibre
The composite layer in Figure 4 shows the resin was sleeve is 0.28mm, thus 2 layers was used in the build.
properly impregnated into fibres. There was no non-smear or

Fig. 4. External aluminium layer was open exposing internal composite layer.

2.3 Crashworthiness criteria (Fmax), mean crushing force (Favg), crush force efficiency
(CFE), energy absorption (Ea) and specific energy absorption
Figure 5 shows the typical force–displacement curve (SEA). The initial peak force (Fmax) is available directly from
of the tube displacement in a quasi-static and dynamic-impact the load-displacement curve separating the process of loading
compression test. To measure the crashworthiness, several to the pre-crushing stage and the post-crushing phase.
different criteria are often used, namely the initial peak force

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Fig. 5. Typical force–displacement curve for crushing of empty circular tube [24].

The mean value of crushing force (Favg) for a given


crushing distance d is mathematically defined as: 3. AXIAL CRUSHING BEHAVIOUR AND ENERGY
ABSORBTION
1 𝑑
𝐹𝑎𝑣𝑔 = ∫0 𝐹(𝛿)𝑑𝛿
𝑑
3.1. Dynamic experimental test
(3)
The dynamic-impact loading test was performed
where d is the collapse distance, and F(δ) is the instantaneous
using Instron-CEAST 9350 Drop Tower Impact System
crush force. (Favg) is an important design variable for a
machine in Universiti Teknologi Malaysia (UTM) Sekudai.
crashworthy structure, a higher (Favg) can absorb more energy
The working principle is using gravity pull to generate
with a certain deformation.
acceleration and weight plate is used to obtain the required
energy. With drop height set to maximum 1.1 meter and
The initial peak force (Fmax) means the force reached
maximum drop weight is 70kg, the machine generates 757J of
maximum load during the crashing process. Crush force
energy. Since the machine is also fitted with impact speed
efficiency (CFE), defined as the ratio of the average crushing
accelerator, the drop height can be simulated up to 30 meter
force (Favg) to the initial peak force (Fmax), is used to measure
thus giving the maximum energy range up to 1800J. All the
the uniformity of crushing force, as
measurements are carried out by strain gauges inside the
𝐹𝑎𝑣𝑔 transducer box attached to the striker shaft. The signals are
𝐶𝐹𝐸 = collected by data acquisition system then calculated by the
𝐹𝑚𝑎𝑥
(4) computer using software provided by the manufacturer. Load,
displacement and time characteristics were then obtained.
The CFE should be as high as possible as a high
(Fmax) may lead to severe injury or even death of occupants For the test, the energy was set to 871J. This value
during vehicle crash. was used to compress about 50% of the original length. The
test data for the tubes are listed in Table 5. The representative
The energy absorption (Ea) measures the total strain deformed mode pictures for each configuration can be found
energy absorbed by the structure during the crashing process, in Figure 6. When the specimen was axially crushed, it
which is determined in terms of the area under the normally deforms in some mode. The localization of the
force-displacement curve, mathematically, as in equation (1), axisymmetric and mixed mode of deformation for all tested
where F(δ) denotes the instantaneous crushing force and d is specimen, started at the impacted end. The progressive
the crushing distance concerned. Obviously, the higher energy collapse of the tube is started by forming a folding lobe from
absorption (Ea), the better is crashworthiness. To account for one end. Then, as the previous lobe is completed, the adjacent
the effect of mass (m), specific energy absorption (SEA) folding lobe is formed on top and stack on each other. This
defined as in equation (2), is frequently used as one of most process continues in series until the test is terminated. In
critical crashworthiness criteria. A higher SEA indicates better general, there are 4 modes of collapse could be found in
material usage efficiency for energy-absorption structure. compressed tube. They are concertina mode (axisymmetric),
diamond mode (asymmetric), buckling mode (asymmetric)
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and mixed mode (asymmetric) [1]. These modes are closely Onsalung et al. [25]. There are 3 collapse modes found in this
depending on geometry of specimens. They are different in study that are concertina mode, diamond mode and mixed
appearance and energy absorption capacity, as discussed by (concertina with diamond) mode as shown in Figure 7.

Table V
Mean value of dynamic test results for 2/1 FML tubes (DB), 3/2 FML tubes (DC) and aluminium tubes (T)
Max Mean
Absorbed Crush CFE SEA
Force, Load,
Specimen Mass, M Fmax Energy, Ea Length, d Fave=Ea/d Fave/Fmax Ea/M
(g) (kN) (Nm) (mm) (kN) (Nm/g)
DB 48.66 49.99 659.37 55.6 11.93 0.24 13.56
DC 80.86 89.34 479.89 16.83 28.55 0.32 5.93
T 48.68 41.96 710.2 44.27 16.71 0.41 14.59

Fig. 6. Deformed modes of bare aluminium tube (T1), 2/1 FML tube (DB4) and 3/2 FML tube (DC3) in dynamic impact tests.

Fig. 7. Typical collapse mode under impact: (a) concertina mode, (b) diamond mode, (c) mixed mode.

For the empty tubes T, they collapse in concertina initial peak load followed by oscillations. The curves are
mode followed by diamond that is called mixed mode. For normally fluctuating in wavy shape. Each loop of the curve is
both FML tubes DB and DC in Figure 6, they collapse in corresponding to a lobe in the deformed tubes. The high
diamond only. One reason why different modes were found frequency content was assumed to be associated with the
here might be because of the difference in tube density while vibration of the test rig. At the final displacement, all the
the diameter D is the same. impact energy was absorbed by the specimen. Absorb energy
versus crush displacement for all specimens are shown in
Typical plot of impact force versus axial crushing Figure 9. An approximately linear relationship between
displacement curve for one sample from each configuration is energy and displacement was found for all tests.
shown in Figure 8. These curves were characterized by a high

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Fig. 8. Dynamic tests impact force-displacement curves

Fig. 9. Absorbed energy-displacement curves

In the case of 2/1 tubes labelled with DB4, it can be


seen that the initial peak load of 48.8 kN occurred at the Normally, the load-displacement curve of concertina
displacement of 1.9 mm. The region before reaching the initial mode is more uniform than other modes. As the result, the
peak value was named the pre-crushing stage, in which the mean crushing load is high compared to peak load and helps to
force–displacement relationship is linear deformation of FML reduce deceleration while impacting. This has been confirmed
tube was observed. The region after the initial peak load is by many investigators such as Andrews et al. [1] and Pled et
known as the post-crushing stage for composite materials and al.[27] who indicated that the concertina mode is better than
progressive folding stage for metals. After the initial peak other modes and higher specific energy absorption than the
load, a progressive folding stage follows, which represents the diamond mode. In addition, the study of Gupta et al.[28] also
main phase for energy absorption. In this stage, the aluminium revealed that the crushing load of concertina mode is higher
tubes started deforming plastically with development of one than diamond mode in the specimen with same geometry and
lob in a concertina mode at the incident [26] end and with boundary condition. On the crash behaviour, this progressive
increase in the crushing displacement, it was followed by crush mode is the better for body tolerance in respect to
several folds in a diamond mode. This is quite typical pattern reducing of acceleration and deceleration of human body. It is
for the aluminium tube to see several corresponding postulated that composite layer which filled in between the
oscillations in the force–displacement curves around the aluminium tube helps distributing impact load to the tube wall
average value. However, in the FML tubes, the corresponding more effective, resulting more uniform mode and higher
oscillations are much lower compare to the initial peak load. number of folds. This implies that one may achieve preferable
While in the single composite tube case, post crushing stage mode and increase number of folds by configuring the
will be resulting in a series of small fluctuations of load value aluminium and composite thicknesses.
around the mean crush load. Additionally, friction effect
between fronds and platen can be observed during the 4. CONCLUSION
crushing, and this effect may be a significant contributor to the In this study, a new method has been established to
energy absorption of composite tube from the literature [3]. fabricate a new type of fibre metal laminate in a seamless
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cylindrical tube to be called fibre metal laminate (FML) tube. [10] M.A Jiménez, A.M., E Larrodé, D Revuelta, Effect of trigger
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[17] El-Hage, H., P.K. Mallick, and N. Zamani, A numerical study on
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