Professional Documents
Culture Documents
Gas Analyzer
Gas Analyzer
Page
1. General information 4
▪ 1.1 Specific safety notes and standard symbols 4
▪ 1.2 Correct use of the device 5
▪ 1.3 Obligation to exercise due care 5
▪ 1.4 Transport and disposal 6
2. MULTI-ANALYSERSF6 - Overview 8
▪ 2.1 Technical data 10
▪ 2.2 Standard equipment 14
3. Functional description 15
4. Operation 17
▪ 4.1 Description of the device 18
▪ 4.2 Operation 19
▪ 4.2.1 Commissioning 19
▪ 4.2.2 Switching on the MULTI-ANALYSER SF6
21
▪ 4.2.3 Settings 22
▪ 4.2.4 Measurement and storage of the measuring data 35
▪ 4.2.5 Manual pumping back 40
▪ 4.2.6 Handling the measured gas and automatic function 41
▪ 4.2.7 Continuous operation 43
▪ 4.2.8 Remote control via LAN/WLAN 44
▪ 4.2.9 Transmission of measuring data 45
▪ 4.2.10 Access to the internal storage via FTP server 46
▪ 4.2.11 Switching off the MULTI-ANALYSER SF6
47
▪ 4.3 Special functions 47
▪ 4.4 Charging the battery 49
Please read this operating instruction before putting the device into operation. Therefore, operating faults can be
avoided. In case of non-observance of the operating instructions the manufacturer cannot assume any liability or
warranty.
The copyright of this documentation remains with DILO Armaturen und Anlagen GmbH, D-87727 Babenhausen. Any
use not permitted by the author (multiplication, leaving to third persons etc.) is subject to penalty and indemnification.
1. General information
In the following operating manual specific safety warnings are given in order to draw your attention to
residual risks which cannot be avoided during the operation of the device.
The symbols used in the operating manual should draw your attention specially to the
safety notes! If the device is used incorrectly or for purposes other than those for which it is intended,
hazards may arise from it. For this reason, please pay attention to the safety instructions of the operating
manual, marked with the following pictograms:
This symbol refers to risks for people (danger to life, danger of injury)
Danger
This symbol refers to risks for machines, material and the environment.
Warning
The most important aim of the safety notes is to prevent personal injuries.
▪ If the warning sign „Danger“, appears, danger from machines, materials and the environment are
not excluded.
The corresponding symbol which is used cannot replace the text of the safety note.
Therefore the complete text must always be read.
This symbol is not for safety notes, but for information to understand the
device better.
We recommend that all persons who are involved in the operation and repair of DILO devices are properly
and specially trained.
Do not use the device to exhaust or compress liquids or other gases.
Use of the device for any other purpose may not be safe.
The manufacturer will not accept any liability in case of injury and damage caused by use of the device
for applications for which it was not intended. The operator alone shall be responsible for any damage
arising from improper use.
For correct use, the operating conditions as well as indications and instructions of this operating manual
must be observed.
The use of components not contained in the scope of supply must be approved by DILO beforehand.
The device has been designed and constructed bearing in mind the standards to be observed as well as
additional technical specifications.
All data and reference within this manual are compiled under the valid regulations, the state- of-the-art, as
well as DILO experiences over several years. It is advisable to have the manual stored with the device at
any time and accessible to all persons, who work with it. This manual must be read carefully before starting
to work with the equipment!
Warranty or guarantee is provided in accordance with the general terms and conditions of DILO (www.dilo-
gmbh.com). The text and graphics do not correspond necessarily to the scope of supply. The figures and/or
diagrams do not correspond to the 1:1 yardstick.
The actual scope of supply might deviate from special (customised) equipment, the recourse of additional
order options or due to latest technical changes concerning the data and references described herein as
well as the graphic representations.
DILO reserves the right to realise technical changes of the product due to improvements without explicitly
mentioning them. For further questions please contact the DILO-hotline.
▪ the device is only used for the purposes for which it is intended (see 1.2).
▪ the device is only operated in accordance with the instructions and in good condition.
▪ complete and legible operating manuals are available on the site of the device.
▪ only qualified and authorised personnel operate or carries out repairs to the device.
▪ personnel are regularly instructed in safety procedures and environmental protection and that these
persons are fully aware of the complete operating manuals and in particular the safety notes.
▪ the safety and warning notes mounted on the device are legible and not removed.
If the power cable is connected, be aware that parts inside the device will have an
electrical current within them. Prior to opening the housing, switch off and unplug
the device.
Danger
Transport
Check the device immediately after delivery concerning its completeness and any transport damages.
If outwardly recognisable transport damage is detected, do not receive the goods, or only under
reservation. State the extent of the damage on the provided delivery note and/or the transport
documents of the forwarding agent.
Lodge a complaint of covered defect immediately after recognising, as claims due to transport damages
can only be made valid within the complaint period (usually 7 days).
The equipment has to be moved only in the provided carrying case. Thus, transport damages can be
avoided.
ADR regulations
SF6 (Sulphur hexafluoride) filled service carts are exempt from the ADR transport regulations if the
pressure of the gas in the vessel or tank is not exceeding 200 kPa (2 bar) at a temperature of 20°C
and the gas is neither liquid nor refrigerated liquefied gas.
This includes each kind of vessel or tank as well as machinery parts (see ADR 1.1.3.2 c exemptions
with regard to the transport of gases).
For carriage of the device by air and sea the integrated pressure vessels must be emptied to
atmospheric pressure in accordance with EC directive 859/2008. Contaminated SF 6 must not
remain in the pressure vessels.
Installation
Disposal
The device must be disposed of in accordance with the local regulations or returned to the manufacturer
or a company authorised by the manufacturer for proper disposal!
The equipment contains the greenhouse gas SF6 as stipulated in the Kyoto
Protocol, with a global warming potential (GWP) of 22800. SF 6 needs to be
recovered and must not be released into the atmosphere.
When using and handling SF6 please observe IEC 62271-4 (High-voltage
switchgear and controlgear – Part 4: Handling procedures for sulphur
Danger hexafluoride (SF6) and its mixtures).
2. MULTI-ANALYSERSF6- Overview
Depending on the version, the battery-operated MultiAnalyserSF6 is equipped with the following main
components:
▪ one measuring module with a SF6 volume percentage sensor for determination of the SF6
concentration
▪ one moisture sensor for determination of the moisture content
▪ one SO2 sensor module for the determination of the SO2 concentration
as an indicator for the total concentration of decomposition products
(or optionally: SO2/HF module or SO2/HF/CO/H2S module).
The standard version of the SF6 volume percentage sensor is calibrated to a SF 6/N2 or SF6/air mixture and
measures the SF6 content in volume percent in such gas mixture. The SF 6 volume percentage sensor
works independently of air pressure and installation position.
The moisture sensor measures the dew point temperature of the SF 6 gas in °C dew point at inlet pressure.
The measuring value of the dew point in °C can automatically be indicated or converted into all established
indicating units in case of a modified setting. Measuring the dew point at inlet pressure, a higher accuracy
of the measurement is achieved with a reduced measuring time. The dew point at ambient pressure is
calculated based on this value.
With the SO2 sensor module for determining the SO 2 concentration, it is possible to draw conclusions
regarding the total concentration of decomposition products. The SO 2 value is used as an indicator for
the total concentration and the respective ratio is approx. 1:4 (see Cigré “SF 6-Recycling guide” page 49).
Additionally to a SO2 sensor the following modules are available as option: SO2/HF module or
SO2/HF/CO/H2S module: The lifetime of the integrated electrochemical sensors is two years. During the
operation of the device the residual lifetime of the electrochemical sensors (SO2/HF/H2S/CO) is indicated
on the info page of the sensor (see chapter 4.2.3 settings /sensor specific settings) so that the sensor
can be exchanged without any problems.
The modular construction of the Multi-AnalyserSF6 enables the user to replace each individual sensor
module for verification, calibration and exchange. In principle, it is also possible to measure with only one
measuring module.
For further versions of the MultiAnalyserSF6 please see the latest leaflet.
In addition to the individual sensor modules the MultiAnalyserSF6 is provided with a gas return system
consisting of the following components, a compressor, an internal gas storage vessel allowing to store at
least two measurements, a control unit, a 7“ capacitive touch screen and a high-performance battery.
It is also possible to work with the device in charging mode or in mains operation. (The battery is charged
in parallel to the mains operation).
The operating pressure of the connected SF6 filled equipment or SF6 vessel (cylinder or container) is
registered at the inlet of the device by means of the pressure sensor. The internal gas flow will be
monitored and controlled by pressure sensors, proportional valves and solenoid valves.
The control menu can be operated intuitively by the adjustable user languages (DE, EN, FR, ES, IT, PT,
CZ, PL, RUS, CN, JPN).
Purging the measuring hose before each measuring process guarantees precise and correct results for
subsequent measurements.
The final value of a measurement is recognised automatically. The measurement can be named
individually and saving the measuring data under consecutive number avoids overwriting of
measurements with same name. Results of up to 500 measurements can be saved with the
MultiAnalyserSF6 and can be read out and processed easily via the USB interface.
Remote control of the device and downloading of stored data is possible with a LAN and WLAN connection
via mobile devices. WLAN settings can be selected for Europe (Austria, Belgium, Bulgaria, Croatia,
Denmark, Finland, France, Germany, Greece, Italy, Liechtenstein, Luxembourg, Netherlands, Norway,
Poland, Portugal, Romania, Serbia, Slovenia, Spain, Sweden, Switzerland) as well as for Turkey, India
and USA.
All MultiAnalyserSF6 components are integrated in a compact and lightweight plastic case for comfortable
transportation (trolley).
The user and maintenance-friendly device allows different types of measurements and treatment of the
measured gas:
▪ Internal storage of the measured gas and pumping the gas back to the gas compartment
(up to 10 bar pe) after the measurement.
▪ For measurements in cylinders, vessels or gas compartments with a higher pressure (max.
inlet pressure 35 pe) or if the measured gas should not be pumped back into the unit, it is
possible to connect a cylinder directly to the outlet (max. 10 bar pe). For this purpose, a
pressure reducer is not necessary and a separation of the device from the gas cylinder or
the gas compartment is not required.
▪ Connecting an external gas collecting bag allows continuous measurements (inlet pressure
max. 35 pe) without pumping the gas back.
The external bag is emptied via the MultiAnalyserSF6 or by connecting a service cart or
compressor unit.
For all types of measurements, no SF6 gas is released into the atmosphere.
3-038R-R... MultiAnalyserSF6
Dimensions:
Length: 406 mm
Width: 538 mm
Height: 269 mm
Weight: 24 kg
General data:
Supply voltage: 85 – 264 VAC, 47 – 63 Hz
Internal battery: 21,6V; 4,0Ah; 86,4Wh
Operating temperature: -10° to +50 °C
Storage temperature: -10° to +60 °C
Inlet pressure: pe 0.2 – 35 bar
Air humidity: up to 90% non-condensing
Interface: USB, LAN
Measuring time (individual measurement): ≤ 7 min. (calculated automatically)
Limit value: volume percentage: 0.0 to 100.0 Vol.-%
Limit value: dew point: -60 °C to +20 °C
SO2 limit value: 0.0 to 500.0 ppm
Flow rate (all sensors): 18.3 – 20.5 lN SF6/h = 111 – 125 g SF6/h
Number of measured values to be saved: max. 500
Recommended calibration interval of the sensors: 2 years
Protection class (device closed /opened): IP65 / IP20
Moisture sensor:
Measuring range: -60 °C to +20 °C dew point temperature
Measuring accuracy: ± 2 at > – 40°C dew point temperature
± 3 at < – 40°C dew point temperature
Measuring condition: Measurement is carried out at inlet pressure.
Atmospheric dew points and ppmv values
are converted by the device
Flow rate: 18 – 20 lN SF6/h = 109 – 122 g SF6/h
Operating temperature: -10 °C to +60 °C
SO2 sensor:
Measuring range: 0 – 20 ppm
0 – 100 ppm
0 – 500 ppm
Measuring accuracy: < ± 2% of the measuring range
Measuring condition: Measurement is carried out at atmospheric pressure.
Flow rate: 1 – 3 lN SF6/h = 6.2 – 18.6 g SF6/h
Operating temperature: -20 °C to +50 °C
Optional:
Cross-sensitivity:
Cross-sensitivity:
3. Functional description
For the determination of the SF6 quality the following parameters can be measured with the
MultiAnalyser SF6 in its maximum version:
The measuring principles of the individual components are described in the following sections.
The measuring principle is based on the evaluation of the different velocities of sound in gases. The
velocity of sound in air is normally about 330 m/s, while in pure SF 6 gas it is only about 130 m/s. The
velocity of sound measured in the measuring cell is temperature compensated and converted into SF 6
volume percent by means of a microprocessor.
The measuring results are transmitted to the host computer.
The SF6 concentration in SF6/CF4 mixtures (optional) is determined analogously. In contrast to the
determination of the SF6 percentage in SF6, the residual concentration is ideally not air but CF 4.
The moisture sensor is based on the absorption of water molecules in a special polymer acting as
dielectric in a capacitor. This changes the electrical capacity of the capacitor which is recorded by the
electronic evaluation system and converted into a standard signal. This signal is forwarded to the main
computer.
These sensors are based on the electrochemical measuring principle and consist of three gold-plated
electrodes and a water-based acidic electrolyte. The structure of the sensors is the same for both SO 2
and HF, but different electrolytes are used and the reactions to determine the concentrations vary:
Electrochemical sensors:
The change in current generated by the released electrons is recorded by the electronic evaluation
system including temperature compensation and calibration in that area and converted into a standard
signal. This signal is forwarded to the main computer and converted into ppm value. The sensors have a
lifetime of two (2) years.
The CO and H2S sensors are identical to the SO2 and HF sensors with the
difference that other electrolytes are used for CO and H2S sensors which are
adjusted to the substance to be measured.
SO2-Sensor:
The SF6 filled-in diffuses into the SO2 sensor and reacts on the measuring electrode in an oxidative process
according to the equation below:
The counter electrode tries to keep the occurring reaction at equilibrium by means of an oxygen
reduction producing water.
If the SF6 gas to be examined contains SO2, electrons are released according to equation 1 by shifting
the electrochemical equilibrium.
HF sensor:
The SF6-filled in diffuses into the HF sensor and in the case that HF is contained, a PH reduction takes
place in an electro-catalytic reduction. By means of the following CL 2 reaction and subsequent redox
reaction, electrons are released.
4. Operation
The following parts can be found on the front panel of the measuring device:
▪ One “Gas inlet“ (101) coupling to input the measured gas (max. 35 bar pe) and to directly
pump back the measured gas (max. 10 bar pe). For pressures higher than 10 bar pe the
measured gas must either be pumped into another vessel (up to 10 bar pe) or stored
temporarily depressurised in a gas collecting bag.
▪ One “Gas outlet“ (102) coupling for pumping the measured gas into an external vessel to
max. 10bar pe.
▪ One gas outlet coupling (103) for depressurised storage (connection of external bag)
▪ One cable socket for mains cable
▪ One 7“ colour touch screen
▪ ON/Off key
▪ One LED indicating the power / battery status indication
▪ One USB connection
▪ One LAN connection
▪ Two fixing facilities for couplings with DN8 & DN20 hose connection
▪ One storage compartment (with 6 m long hose, 2 m long power cable,
adapter kit and USB stick
▪ One connection for potential equalisation
Cable connection
4.2 Operation
4.2.1 Commissioning
A standard device with battery (3-038R-XXX-B) is delivered without being connected to the battery.
For battery operation, connect the battery before commissioning.
Proceed as follows:
1) Make sure that the device is switched off (if the mains cable has already been plugged in).
2) Remove the label indicating that the battery is not connected.
3) Loosen the screws of the battery compartment.
For devices without battery (3-038R-XXX-N) or if battery operation is not possible/desired, the power
connection must be established using the supplied cable. The corresponding socket is located on the
left side of the display (see page 18).
In mains operation and when charging the battery, the following mains connection requirements apply:
The socket used must be easily accessible, earthed and fused with a 16A fuse.
In addition, the earthing must be checked by a skilled person.
Warning
Switch on the Multi-AnalyserSF6 by pressing the “ON/OFF” key. After the booting process the device is
ready for use and the following start screen appears.
Automatic operation
This page displays all connections and parameters of the MultiAnalyserSF6. From here, all settings and
functions can be selected and carried out. After having started the device the “Measurement” function is
preselected. The designations of the gas connections correspond to the labelling on the device.
When starting the device, the “user” is selected as login.
Active menu fields are orange and functions or settings which can be activated or made by the logged-in
user are highlighted in white. Functions or settings which are not possible are greyed out.
4.2.3. Settings
- General settings of the device: Left menu bar of the device (settings, messages, measurement
data archive, access authorisation)
- Sensor specific settings: Press the individual sensor in the measuring data indication (limit value
settings, sensor info, indication residual lifetime of electrochemical sensors)
General settings:
(Setting selection)
The following settings can be carried out and/or seen on this page.
Indication/Display:
Language selection:
Units selection:
The units can be changed by
pressing the corresponding
drop-down menu.
Pressure units:
bar pa, bar pe, psi pa, psi pe,
kPa pa, kPa pe, MPa pa, MPa
pe (pa= absolute value and
pe=differential value)
Temperature units:
°C, °F and °K
Humidity units:
°C atm., °C p., °F atm., °F p.,
ppmv and ppmw
CSV export:
Decimal separator: or,
(automatically combined with
the corresponding CSV
separator: , or ; )
If a SF6 percentage
module with
additional SF6-CF4-
calibration for
measurement of SF6-CF4-
mixutures is integrated it is
possible to switch between the
SF6-N2- standard and SF6-CF4-
calibration.
Operating hours:
yellow
Then the supervisor must carry
out the maintenance works and
acknowledge in this window.
After having acknowledged, a
registration is automatically
generated by whom and when
the maintenance works were
carried out.
System information:
Manual operation:
The manual functions can only be carried out in the “Supervisor“ login.
The user has read-only access.
The following components are displayed and can be individually selected and carried out except for the
sensors:
Components
Solenoid valves
Pressure sensors
By pressing the start key all selected components / solenoid valves are started or activated in
manual mode. They are stopped or deactivated by pressing the stop key.
Start / Stop is only possible with supervisor authorisation and should only be carried out on the
instructions of DILO staff.
WLAN:
Change of country
configuration (drop-down
menu)*
Current messages:
Current messages and history are described separately in chapter 5 “Current messages, history and
fault correction”.
In the archive of measuring data, measurements already saved can be read and processed. It is also
possible to delete individual as well as all measurements and to save measurements as CSV files
(comma separated value) in the internal storage or on a storage medium connected to the USB
connection. The archive of the measuring data is indicated and operated as follows:
Indication of all measured data (position of the measurement, date/time, logged-in user, SN of the
device, titel of the measurement, type of gas compartment, note, inlet pressure, temperature of device
and the climate data (air humidity and air pressure) if activated.
Access authorisation :
Below the icon, the user currently logged in is displayed and the following functions can be selected:
Login: .
Procedure:
1. Select user in the upper text field
via the drop-down menu (Logged in
users are displayed above)
Important: In order to be able to operate the device, at least one user must be logged in.
Logout:
When pressing the ‘Logout‘ key the user is directly logged out. No user is logged-in then and the display
jumps directly to the “Login” page. In order to continue working with the device a user has to be selected
(see ‘Login’ chapter).
My profile:
In this menu item the following functions or changes can be carried out:
(Change password)
User administration
(only with “supervisor” login)
On this page, the user has the following
possibilities:
1. To delete a user, press the
Regarding point 1:
Delete user :
After pressing the “Delete user“ key the
following window opens:
When pressing the “User“ key the
keyboard opens and the user can be
entered.
Or the user can be selected from a list
by pressing the key.
The selected user must be confirmed with
the RET key in order to close the keyboard
or list. Then reconfirm with the RET key to
delete the user permanently.
ATTENTION:
(View - delete user with logged-in supervisor) The supervisor or user is deleted
irrevocably and cannot be cancelled!
Regarding point 2:
Create a new user :
After pressing the “Create new user“ key the following
window opens:
2
3
4
The supervisor has to decide on supervisor access rights or user access rights.
Important: Mark the selected user (visible with the * before the name) by means of the “MARK“ key.
Then confirm with the RET key.
3+4: A numerical keyboard opens. Enter the new password twice (as described under the “Change
password” chapter) and confirm with the RET key. Then complete the procedure by pressing the RET
key. A green bar with the “New user created” message appears on the panel. Now, it is possible to login
with the new user name or password on the panel.
Advantages:
- The supervisor can create user data for each member of staff.
- The supervisor can create a second supervisor with extended rights.
Passwords:
The end user is responsible for passing on the corresponding passwords to authorised
persons.
Warning
By clicking the date/time display on the lower left of the main screen (see page 20), the date and time
can be set and the following screen appears:
By clicking the individual sensor values on the main screen (see page 20) the sensor settings for the
corresponding sensor is called. The screen shows an example of the SO2 sensor settings:
Current measured
value
By pressing
this key, the
measured values of
the last
measurements
appear in the lower
field
Sensor information:
Here, the residual lifetime of the electrochemical sensor (SO2; optionally: HF, CO, H2S) is indicated in days
(see red marking).
90 days before the expiry date a warning message indicates the end of the
lifetime allowing sufficient time to provide a new sensor. After expiry of the
lifetime, which is also displayed, the electrochemical sensor(s) is/are still fully
functional, but the sensors should be replaced by re-calibrated sensors as soon
as possible since the measured values might not fulfil the specifications any
more and might cause functional failure.
Trend analysis:
The trend analysis displays the last measured values (max. values of the last 10 min) in a diagram. With
the ruler it is possible to approach individual values. The corresponding value is shown at the top right of
the display field. The trend analysis is particularly helpful and useful for continuous measurements on a
gas compartment.
For starting a measurement, the “measurement” function has to be selected in the function
selection (see page 20). (After switching on the device it is selected automatically). The corresponding
symbol is then displayed in the function bar on the right side. The selected gas path is shown as broken
line (e. g. to the external bag).
Correct measurement:
The correct measurement and determination of the gas quality to achieve a
useful correct measuring results is described in detail in the “SF6 Measurement
Guide“ of Cigré (document number 723; Download under https://e-cigre.org
(free of charge for Cigré members)).
Correct measurement:
In order to achieve stable measured values, only carry out measurements at constant inlet
pressure. This means that the gas volume of the gas compartment to be measured or the
available quantity of SF6 gas must be sufficient. A fluctuating or constantly decreasing
inlet pressure can lead to deviations in the measuring accuracy.
In the standard settings, the internal depressurised storage vessel (storage capacity of at least two
measurements, depending on the duration of measurement) is selected for storing the measured gas
The selected depressurised storage vessel appears in a green frame and the gas path is shown as line.
If the measured gas is to be collected in an externally connected, depressurised storage vessel, the
latter can be easily selected with a click. In this case, the external storage vessel appears in a green
frame and the gas path has changed correspondingly. (For switching from the external to the internal
storage tank, click on the internal storage vessel.)
Ensure that, in the event the external storage tank has been selected, the latter
is connected to the outlet coupling 103.
If the external vessel has been selected but not connected or if it is already filled,
a started measurement is automatically switched off due to the overpressure in
the device.
If the internal vessel is selected and, additionally, an external depressurised
vessel is connected, both vessels are filled during measurement.
1. When coupling the hose under high pressure, more gas may escape. Danger
exists with decomposed gas. It is recommended to couple the hose at
pressures > 5 bar pa (depressurised).
Danger 2. Be careful when uncoupling the hose at high pressures.
Recoiling of the hose could cause injuries.
Upon selection of the “measurement” function and the storage tank, the measurement is started by
pressing the start key. After starting the measurement, the stop key instead of the start key
appears. The connected measured gas hose is purged automatically prior to the actual measurement.
The timely process of the hose purging has been selected in a way that even with two
connected hoses (max. 12 m) the gas inside the hoses is purged out.
The measured values are displayed and the active gas path flashes green.
The function carried out (purging of hose, measurement) is displayed above the device illustrated.
As long as the measured values are not yet stable, the bar in front of the corresponding measured value
flashes (green inside and red outside the adjusted limits). If the value of a sensor has reached its final
value, which is automatically determined by an algorithm, the bar is displayed statically.
If the measured values are out of the adjusted limits (See settings page 32), the corresponding value will
be marked with a red bar. If it is within the limit values, the bar is green. The elapsed measuring time is
displayed below the stop key.
The input can be made before, during and after a measurement before it is saved.
Once the measurement has been saved, it is no longer possible to make changes.
The end of the measurement is obtained when all sensors have reached a stable final value.
In this case the stop key disappears and it is possible to save or reject the measurement:
The values are saved by pressing the yellow save key. When saving, the entered name, type of gas
compartment and notes are accepted. It is no longer possible to make any changes after saving.
Successful saving is shown on the display and must be confirmed with “OK”.
Then the values can be read in the measurement data archive (see chapter 4.2.3) and the display shows
the main screen again.
The data will be stored with a consecutive number. Overwriting data with the same name
or without name is impossible in this respect.
The maximum storage capacity is 500 Measurements. After saving data of 500
measurements, a warning message indicates that the maximum capacity has been
reached. It is not possible to save the data of further measurements (after the
following measurement the save key will not be shown) until old data has been
deleted.
Significant exceeding of the measuring range final value can cause damage to the sensor
(3-fold overload).
Warning
1). 500ppm sensor:
If the device is equipped with a 500ppm sensor, the device should either be purged
immediately with pure gas for a longer period of time or recovered externally (see special
functions chapter 4.3).
It is recommended to purge the device with pure gas (to near 0 ppm) from a concentration
of half of the measuring range final value; especially prior to storing the device and to
ensure reliable measuring values in subsequent measurements.
If you press the reject key, the measured values are not saved and the main screen is displayed
directly.
If a measurement is interrupted with the stop key, it is possible to both save and reject
the measurement. Unstable measured values are marked with a grey bar in front of the
measured value.
If the automatic function is not selected (see chapter 4.2.6), the gas used for the measurement remains
in the selected depressurised vessel. After the measurement, the gas used can be pumped back
manually either into the gas compartment (connection 101) or into another vessel (connection 102), up
to a pressure of 10 bar pe (see chapter 4.2.5).
In the event that the automatic function is switched on, for each setting (see chapter 4.2.6) the
intermediate stored measured gas is automatically pumped back into the gas compartment (connection
101) after the termination of the measurement or pumped back into a vessel connected to connection
102. Here, the maximum pressure of 10 bar pe is to be observed.
If, during the measurement, the automatic operation key has not been activated, the gas used for
the measurement remains in the internal storage vessel or in the connected depressurised storage
vessel (connection 103) in the event that the latter was connected during the measurement.
For manually pumping back the measured gas, there is an option of pumping the gas either directly back
into the gas compartment (connection 101) or into a tank connected to connection 102.
With both options, the maximum admissible total pressure of 10 bar pe is to be observed.
In order to carry out the functions, select the “Manual pumping back” function.
Select the tank the gas should be pumped into before starting the manual pumping back function by
pressing the corresponding symbol. The selected symbol is framed in green.
By pressing the key, the gas is pumped back into the gas compartment connected to connection
101, by pressing the key, the gas is pumped back into a tank connected to connection 102.
The tank to be emptied has to be selected additionally, either the internal vessel or a depressurised
storage vessel connected to connection 103. The selection is made by clicking on the vessel on the
screen. The selected vessel is framed in green.
If the internal storage vessel has been selected for emptying and if, at the same time a
depressurised storage vessel is connected to connection 103, both storage tanks are
emptied when pumping back. If the external storage vessel has been selected, only this
tank is emptied when pumping back.
After selecting the function it can be started with the start key. During the function, the active gas
paths flash in green and the stop key appears.
The function stops automatically if the selected storage tank has been completely emptied but can be
interrupted with the stop key at any time. After completion or interruption, the start key is
displayed again and other functions can be selected.
Besides the normal measurement (chapter 4.2.4) where the measured gas remains in the internal or
external storage vessel after the measurement and subsequently has to be pumped back manually
(chapter 4.2.5), it is also possible to operate the MultiAnalyserSF6 in automatic mode. Two versions of
automatic operation are possible:
1. Carrying out a measurement with automatic pumping back of the measured gas into the gas
compartment (connection 101) after the measurement.
2. Carrying out a measurement with automatic pumping back of the measured gas into a vessel
connected to connection 102.
The automatic mode can only be activated if “Measurement” has been selected in the function selection
before.
With the automatic operation key the corresponding automatic function can be activated.
As with manual pumping back, before starting the "automatic" measurement, the tank to which the gas
used is pumped back after the measurement must be selected. Either back into the gas compartment by
pressing the gas compartment symbol or into a tank connected to connection 102 by pressing the
gas cylinder symbol. According to the selection (symbol framed in green) the gas path is shown on
the screen as a continuous line and the activated automatic function is indicated by the orange colour of
the automatic key. The measurement can now be started with the start key.
After the measurement, according to the selection, the gas used for the measurement is pumped back
automatically into the gas compartment (connection 101) or into a vessel connected to connection 102.
Observe the maximum pressure of 10 bar pe.
When activating the automatic function, the device can be used in continuous operation.
For this purpose, please refer to chapter 4.2.7.
For monitoring the gas quality over a longer period of time, it is possible to operate the MultiAnalyserSF6
in “continuous operation”. Precondition for continuous operation is that the measurement function
key has been pressed in the function selection menu and that the automatic operation has been
activated.
The continuous operation can then be activated by pressing the continuous operation key.
Example: Activated continuous operation with pumping back via outlet 102.
Once the continuous operation has been activated the gas paths are displayed on the screen as
continuous line and the time period between the measurements can be set below the continuous
operation key. Pressing the time input key, a keyboard opens which enables setting the interval
between measurement within a range of 15 minutes to 200 hours. Then the continuous measurement
can be started with the start key. The number of measuring cycles implemented is indicated above
the continuous operation key.
Between the measurements (in waiting state), "Waiting time continuous operation" is displayed as the
status indication instead of "Measurement".
The continuous measurement can be stopped manually via the stop key at any time.
After the measuring process the measuring data of each measurement are automatically saved under an
additional consecutive number or if a name has been created prior to the measurement it is stored under
this name with an additional consecutive number.
The vessel for storing the measured gas at the connection 102
should correspond to the expected number of measurements. Once
the maximum admissible pressure of 10 bar pe is reached, the
measurement is interrupted automatically.
Before the device can be remotely controlled from an external device (computer, notebook, tablet,
smartphone), establish either a LAN connection or a WLAN connection.
Establish the connection via the RJ45 socket (see page 18) on the MultiAnalyserSF6 with a network cable
to the mobile device (computer, notebook,...).
To establish a WLAN connection with a mobile device, make sure that the integrated WLAN router is
switched on and that the country code is selected accordingly (see chapter 4.2.3). It is then possible to
connect the mobile device to the WLAN, which is marked as
In the WLAN settings it is possible to change both the WLAN name and the WPA key (logged in as
"supervisor"; see chapter 4.2.3).
If one of these connections exists, the screen of the Multi-AnalyserSF6 can be mirrored on the external
device with a suitable viewer (e. g. VNC-Viewer).
On the mirrored screen, the device can be controlled and set with the appropriate input devices
(depending on the external device, mouse or touchpad) as if the operator is directly in front of the device.
Only the hose connections have to be installed in advance.
The transmission of the measuring data as CSV file (comma separated values) to a storage medium
connected to an USB connection - (see page 18) can be carried out via the archive of measuring
data key on the settings page (see chapter 4.2.3).
Before exporting the data the desired units and decimal separators for the data fields should be set and
verified. The selected decimal separators should correspond to the settings in the processing program. A
comma as decimal separator and a semicolon are pre-set as CSV separator (separation of the data
fields). Alternatively, it is possible to choose a point as decimal separator and a comma a CSV separator
(See page 23).
For the transmission of the measuring data as CSV file press the export key and the following
window opens:
The memory location can be selected and the file name can be edited here. It is either possible to save
the CSV file on a storage device connected to the USB connection, in an internal storage, or on the
internal storage (access to the internal storage is possible via LAN/WLAN or via the FTP server). The
selected memory location is framed in orange. When pressing the “file name” field a keyboard opens to
edit the proposed file name.
When exporting the CSV file to the storage medium make sure that it is connected to the USB
connection. Otherwise the export is interrupted and the “Writing error CSV file“ message
appears after pressing the save key.
To access to the internal storage of the device an existing LAN or WLAN connection to a computer,
notebook or mobile device (tablet, smartphone) is necessary (see 4.2.8).
The internal storage of the MultiAnalyserSF6 can be accessed directly with a suitable FTP client on the
mobile device. The installed Windows©-Explorer can be used directly on a Windows© PC or notebook.
Establish the access to the device by entering “ftp://192.168.0.1” in the command line of the FTP server
browser.
The measurement reports are stored directly in the "StorageCard" directory which can be copied, but not
deleted or moved (read only).
The CSV file with the measurement data is stored under "InternalStorage/DATA":
For switching off the MultiAnalyserSF6 press the ON/OFF key on the housing (see page 18) until the
indication on the display extinguishes.
The special functions are selected analogously to the measurement via the function selection key (see
page 20).
The individual special functions (framed in red) can be chosen and started by pressing the start key
and stopped with the stop key. The following special functions can be carried out:
internal gas volume can be recovered after pressing the start key and with the external recovery unit
(compressor unit or service cart) being switched on. The recovered gas should be stored in suitable
vessel according to its gas quality (vessels for new or reuse gas). It is absolutely necessary to avoid
emissions due to the high GWP value of SF6 and toxicity! After completion of the recovery process
the function has to be stopped manually be pressing the stop key and the device has to be vented
with pure SF6 afterwards. Therefore, a cylinder with pure SF6 has to be connected to Inlet 101 and a
measurement has to be started.
internal gas volume is evacuated after pressing the start key and with external evacuation device
being switched on (vacuum pump or service cart).The recovered air/nitrogen can be released into the
atmosphere without hesitation. After completion of the evacuation process the function has to be
stopped manually by pressing the stop key and the device has to be vented with pure SF6
afterwards. Therefore, a cylinder with pure SF6 has to be connected to Inlet 101 and a measurement has
to be started.
this special function and pressing the start key the compressor starts running and an internal
pressure is generated. In accordance with the max. pressure and the time required for generating the
pressure the result of this verification is displayed. In case the max. pressure and the required time do
not correspond to the specification the device should be sent to the manufacturer for verification of the
compressor.
connection of the measuring hose and activation of the special function by pressing the start key the
hose is purged automatically. However, the time sequence is selected so that the gas in the hoses are
purged even with two connected hose (max. 12m). The function stops automatically.
start key. Analogous to the automatic purging process the SO2 sensor is purged until a SO2 value
<1ppm is reached or after a maximum of 5 minutes.
“Drying the device” special function is started with the start key and stopped automatically after a
running time of 5 minutes. First, disconnect the existing gas connections at the connections of the device
in order to avoid possible damage to the device at higher pressures and unnecessary gas consumption.
It t is possible to interrupt the drying function by pressing the stop key at any time. After a drying time
of 5 minutes it is possible to restarted the drying process, if necessary.
Warning
The MultiAnalyserSF6 is equipped with a 4.0 AH ion battery, which enables at least 5 measurements with
pumping back. The battery is charged via an integrated electronic charging system which enables a
simultaneous charging and line operation of the device with 85 – 264 VAC, 47 – 63 Hz. The charging
status is displayed at the left bottom on the display (see page 20) and via the LED (see page 18).
The following status are displayed via the LED:
The battery charging status is continuously monitored during the operation of the MultiAnalyserSF6 and, in
order to avoid deep discharging and thus damage of the battery, the device is shuts down automatically
after a prior warning message if a defined voltage is undercut.
Malfunction and warning messages and information are displayed on the MultiAnalyserSF6.
Malfunction messages are indicated in “red” and avoid the starting of the device.
Warning messages are displayed in “orange” and inform the user on maintenance intervals or critical
operating conditions. Information is displayed in white.
The currently present messages are displayed in the left menu bar of the main screen by the red
message symbol (warning messages are highlighted in yellow). The number of messages is indicated at
the top left of the display.
The error status, the error number, the time of occurrence and the error text are displayed here.
The errors appear in “red”, warning messages in orange and information in “white”.
‘1‘ (first digit) of error status means that there is an active error and ‘0‘ that the error has been eliminated,
but has not yet been confirmed.
After having eliminated the cause of error the marked error can be confirmed with the key and
disappears from the list.
All eliminated errors can be deleted from the list by pressing the key.
Error history:
(View – History)
In case an error occurs, the active function is stopped and cannot be re-started until the error is
eliminated.
In the event of a failure the function switches off and it is not possible
to start a new function. The cause of failure must be eliminated
beforehand.
The following error and warning messages (highlighted in green) can appear on the display of the
MultiAnalyserSF6:
External storage pressure too External storage vessel is full Empty the external storage
high vessel
Inlet pressure too low Pressure of the vessel Connect a vessel with a
connected to the coupling pressure > 0.2 bar pe
pos. 101 is < 0.2 bar pe or no
vessel is connected
Inlet pressure too high Inlet pressure at coupling pos.
Connect a vessel with a
101 is > 35 bar pe pressure of < 35 bar pe
Outlet pressure too high Outlet pressure of the Make sure that vessels with
compressor is >10 bar pe pressures < 10 bar pe are
connected to the couplings
pos. 101 or 102; verify the
valves pos. 139 and 140 in
manual operation (login as
“supervisor”) otherwise return
the device to the manufacturer
Error when switching over to Percentage module does not Check whether the outlet pos.
CF4 switch over 13 of the K04 SPS control
lights up
Bus error charging electronics Interrupted bus connection Check the connection in the
from the panel to the charging “Sensor information“ menu
electronics (supervisor must be logged
in); also check the cable
connections, otherwise return
the device to the
manufacturer.
Attention: expiry of sensor The two year sensor lifetime Note for providing new
lifetime in 90 days will expire in 90 days electrochemical sensors in
time
Attention: sensor lifetime The two year sensor lifetime The electrochemical sensors
expired expired must be exchanged for
compliance with technical
specification
Verification of the compressor Preventive maintenance Carry out a pressure test of
the compressor every 500
hours, otherwise return the
device to the manufacturer for
inspection / maintenance
Defective percentage sensor Interrupted connection to the Check the electrical
percentage module (bus error connection, otherwise return
or cable break) the device to the manufacturer
Defective moisture sensor Interrupted connection to the Check the electrical
moisture sensor (bus error or connection, otherwise return
cable break) the device to the manufacturer
Defective SO2 sensor Interrupted connection to the Check the electrical
module of the electrochemical connection, otherwise return
sensors (SO2 sensor) (bus the device to the manufacturer
error or cable break)
Service Hotline
Our technical after-sales-service is available:
Monday – Thursday: from 7:00 h – 16:00 h CET
Friday: from 7:00 h – 12:00 h CET
Phone: +49 83 33 – 302-94
E-Mail: service@dilo-gmbh.com
https://www.dilo-gmbh.com/en/sf6-service.html
The type of devices, serial number and order number/commission number of measuring devices are very
important for our service team to support you immediately.
6.1 Maintenance
Maintenance of the Multi-AnalyserSF6 must only be carried out by qualified and authorised DILO personnel
or by personnel or companies authorised by DILO.
Only personnel trained by DILO is allowed to replace the modules. If the modules are not replaced
correctly, the guarantee for the components or the entire unit will expire.
The replacement of the modules must be carried out in a dry and dust-free place (not a clean room) with
the appropriate tools, paying particular attention to the EMD protection measures.
The steps listed below only show the work sequence and do not represent comprehensive work
instructions. The technical knowledge to carry out the work steps must be available.
Before the individual measuring modules can be replaced, switch off the device via the main switch on the
front plate and open it as follows:
Loosen
screws
2) Before the percentage sensor can be removed, unscrew the SO2 sensor
module (if available). For this purpose, loosen both screws (1).
3) Loosen the quick couplings (2)
4) Disconnect the electrical connection (3).
5) Loosen the four (4) screws on the bottom plate and the side panel of the
device
6) Remove the module.
(4)
(1)
(2)
(3)
(4)
(Installed percentage module)
7) Insert the re-calibrated percentage module and fasten the module with
the four screws (4).
8) Establish the electrical connection of the percentage module (3).
9) Establish the gas connection (2).
10) Fasten the SO2 module with two screws (1) (if available).
11) Place the front plate on the housing frame without screwing it. Connect
the device or batterie) to make the device work.
12) Switch on the device with the button on the housing.
(1)
(2)
(3)
(2)
(1)
(3)
(Installed SO2 module)
15) Remove the front plate and check the internal piping of the replaced
sensor for leaks using a suitable leak detector.
16) If the piping is tight place the front panel on the housing frame and
fasten it with the four screws. Connect the device or battery to make
the device is ready for operation.
17) Switch on the device with the button on the housing and wait until the
device is ready for operation.
18) The MultiAnalyserSF6 is again ready for use.
Attention: For operation of the device without SO2 module the quick
couplings must be plugged together in order to realise the gas flow
through the device.
Warning
(2)
(1)
3) Disconnect the gas connection of the SO2 sensor module (if available,
chapter 6.2.3 item 5) and the electrical connection of the moisture sensor
(chapter 6.2.2 item 2).
4) Loosen the gas connection (inlet and outlet) (1).
5) Loosen the clamping plate at the four screws (2).
6) Remove and replace the dry filter.
7) Fasten the dry filter with the clamping plate by tightening the four screws.
(2).
8) Connect the gas connection (inlet and outlet) (1).
9) Establish the electrical connection to the moisture sensor (see chapter
6.2.2 item 6) and the gas connection to the SO2 sensor module (if
available; see chapter 6.2.3 item 8).
10) Place the front plate on the housing frame without screwing it. Connect
the device or batterie) to make the device work.
11) Switch on the device with the button on the housing.
12) Then select the “Evacuation of device“ special function and recover the
air inside the Multi-AnalyserSF6 by means of an external vacuum pump or
a service cart.
13) After the recovery carry out a SF6 gas measurement.
14) After the measurement proceed as follows:
a. Switch off the device
b. Disconnect the devices from the mains
c. Disconnect the battery
15) Remove the front plate and check the internal piping of the replaced
sensor for leaks using a suitable leak detector.
16) If the piping is tight place the front panel on the housing frame and fasten
it with the four screws.
17) Connect the device or battery to make the device is ready for operation.
18) Switch on the device with the button on the housing.
19) The MultiAnalyserSF6 is again ready for use.
If it is necessary to remove or replace the battery (e.g. to transport the battery separately from the
device), proceed as follows:
6.4 Purification
6.5 Calibration
The MultiAnalyserSF6 is based on a modular construction and it is therefore possible to replace each
sensor / sensor module by a calibrated module / sensor (see chapter 6.2). For complying with the technical
specification it is recommended to calibrate the sensors every 2 years (under normal application). The
lifetime of the electrochemical sensors (SO2; optionally HF, CO, H2S) is two years and must be
replaced by recalibrated sensors after the date of expiry independent of the use.
The scope of supply of the MultiAnalyserSF6 as well as of the replacement modules includes a certificate
guaranteeing the traceability to the corresponding standards.
CE Certificate: