4z 7° coNosTay, IN STAN ‘Adision of SCP SCIENCE 21800 Clark-Graham Avenve Oil Analysis Standards Seca cciiaaes January 1, 2008 Certificate of Analysis Catalogue Number: 150-021-003 / 150-021-019 Description CONOSTAN Multi-Element Standard S-21:100 ppm Lot Number: 21398100 ELEMENTS ~ CONCENTRATION, ppm (ug/g) Ag 1020.1 Al 1000.2 B 100802 Ba 0020.1 ca 1000.1 ca 1000.2 Cr 1000.2 cu 1020.3, Fe 0020.2 Mg 1080.2 Mn 100802 Mo 100201 Na 10020.1 Ni 1020.2 P 100802 Po 1020.3 Si 10080.1 sn 1080.3 Ti 10080:1 v 1040.3 2n 1080.1 QUALITY ASSURANCE ‘This standard was prepared by weight measurements originating fom assayed element Concentrates. A precursor blend was vei by alomic emission or absorption spectroscopy. Element concentrations for thie standard are based on the Concentrate 12980" vakes and were prepared fo win the unceainty values listed above al the 95% Confidence Interval. a8 determined by ‘weigh! measurements of blend components conducted on balances calxated and verified with NIST tracaabla weighs “Each element Concentrate was assayed by classical wet chemical methods. Precision of assay measurement is 405 percenl ‘maxinum, bul ypcaly +03 percen. oF ss. Assay accuracy 1s wihin one percent of measured vawe, bul typically much les, 6s etemmined by co-measurement of, and laceabily to, NIST Standards, of Ceriiad Anaiyical Reagent Grade Chemicals, no ‘sulable NIST standards exels. a shot information Pras wes i Ryman Wassat CONOSTAN ‘Telephone: 1-800-361-6820 (tollree) or +4 (514) 457-0701 wwrw.conostan.com Fex: 1-800-259-5549 ((lliree) or +1 (514) 487-4499 onostan@scpscience.com4A ye ConosTaN ONO. STAN Aduison of SCP SCIENCE 21800 CiarkGraham Avenue Oil Analysis Standards January 19, 2009 Certificate of Analysis Reference: CONOSTAN Custom Blend Multi-Element Standard $-21:25 ppm; Lot No. 080430-2 ati: 150-021-006 / 150-021-024 ag 5 AES 8 25 Ba 25 fo 5 5 cr cs Fe 25 Mg 25 Mn 25 Mo 25 Na 2s No 25 P 25 Pho 25 si 25 su 25 Ti 25 v 25 mn 25 QUALITY ASSURANCE This standard was prepared by weight measurements originating from assayed element Cancentrales, Element Concentrations for this standard are based on the Concentrate assay” values and ware prepared to within #2.0 percent relative or better as determined by weight measurements of blend components conducted on balances calibrated and verified with NIST traceable weights. “Each element Concentrate was assayed by classical wel chemical methods, Precision of assay measurement is 20.5 percent maximum, but typically +0.3 percent, or less. Assay accuracy is within one percent of measured value, but typically much less, as determined by co-measurement of, and traceability to, NIST Standards, or Cerified Anaiylical Reagent Grade Chemicals, i no suitable NIST Standard exists, ‘See other side for shelf life and warranty information, Ry mis wssef Ayman Wassef CONOSTAN ‘Telephone: 1-800-361-6620 (tall-ree) or +1 (514) 457-0701 ww.conostan.com Fax: 1-800-253-5549 (tollfrea) or +1 (S14) 457-4499, conostan@sepscience.comre ® CONOSTAN, CONOSTAN era Oil Analysis Standards SRA eee January 19, 2009 Certificate of Analysis Reference: CONOSTAN Custom Blend Multi-Element Standard $-21:25 ppm; Lot No. 080401-6 Cat: 150-021-006 / 150-021-024 Ag 25 AL 25 B 25 Ba 25 Ca 25 Cd 25 Cr 25 cu 25 Fe 5 Me 25 Nn 25 Mo 25 Na 25 Ni 25 Pp a Pb 25 Si 25 ‘sn 25 Tt a v 25 In 25 QUALITY ASSURANCE ‘This standard was prepared by weight measurements originating from assayed element Concentrates. Element concentrations for this standard are based on the Concentrate assay" values and were prepared to within +2.0 percent relive or better as determined by weight measurements of blend components conducted on balances Calibrated and verified with NIST traceable weights “Each element Concentrate was assayed by classical wel chemical methods. Precision of assay measurement is 40.5 percent maximum, but typically +0.3 percent, or less. Assay accuracy is within one percent of measured value, but typically much less, as determined by co- measurement of, and traceability to, NIST Standards, of Certified Analytical Reagent Grade Chemicals, ifno suitable NIST Standard exis, ‘See other side for shelf fe and warranty information Afroman wessif ‘Ayman Wassef CONOSTAN ‘Telephone: 1-800-361-6820 (tolfee) or +1 (514) 457-0701 wwww.conostan.com Fax: 1-800-253-6549 (toll-ree) or +1 (514) 457-4499 conosian@sepscience.com4a ye ‘CONOSTAN. 4 | A division of SCP SCIENCE 21800 Clark-Graham Avenue ; ‘ Bueou og nex aes Oil Analysis Standards Gavan January 19, 2009 Certificate of Analysis Reference: CONOSTAN Custom Blend Multi-Element Standard $-21:25 ppm; Lot No. 081202-1 Catt: 150-021-006 / 150-021-024 Ag 5 Al 5 B 25 Ba 25 ca 25 ca 25 cr 25 cu 25 Fe 25 Mg 25 Mn 25 Mo 25 Na 25 Ni 25 P 25 Pb 25 si 25 sn 25 Ti 25 v 25 Zn 25 QUALITY ASSURANCE ‘This standard was prepared by weight measurements originating from assayed element Concentrates: Element ‘concentrations for this standard are based on the Concentrate assay" values and were prepared to within #2 0 Percent relative or better as determined by weight measurements of blend components conducted an balances calibrated and verified with NIST traceable weights. “Each oloment Concentrate was assayed by classical wet chemical methods. Precision of assay measurement is 20.5 percent maximum, but typically £0.3 percent, or ess, Assay accuracy is wilhin one percent of measured Value, but typically much less, as determined by co-measurement of, and traceabilly to, NIST Standards, of Cortified Anaiytical Reagent Grade Chemicals, ifna suitable NIST Standard exists See other side for shelf life and warranty information. Pri roan whee ‘Ayman Wassef CONOSTAN ‘Telephone: 1-800-961-6820 (tolfee) or +1 (614) 457-0701 yrww.canastan.com Fax: 1-800-258-5549 (tol-ree) or +1 (Sid) 487-4499 conostan@scpscience.comSHELF LIFE OF CONOSTAN STANDARDS ‘Sholf life: Standards should not be used beyond 12 months* from the date of receipt (see date of shipment on botte). Stabiity varies withthe element or element combination and the concentration. Higher Concentrations contioute to longer shelf life. Contamination introduced wien transfers are mace with ‘droppers and pinetes is a common problem. For unopened product containers, Conostan warrants stably Up to 12 months" from the date of shipment ‘Moisture: Moisture sensitivity varies with tne element but all -based standards should be protected from exposure to moisture. Keep container caps tchtened during storage, If high humidity is a normal operating Coneition, minimize exposure and consider replacing standards more frequently. ‘Storage: Store standards in thei original Conostan containers at ambient laboratory temperatures, keep Containers tightly sealed, and avoid drect exposure to sunlight. Do not refrigerate, Dilutions: Dilutions to lower concentrations contribute to shorer stable if. Use care, As stated above, Contarnination introduced when transfers are made with droppers and pipettes is a common problem. She life in solvents may range from one day to several weeks. Solvent qualty (moisture content and purity) can have @ significant effect on stabilty. We recommend: 1. using a high-quality, analtical-grade solvent 2. determining shel ife of your clutions by preparing a batch of solvent-dluted standard. Run tests over time comparing your aged diution against a freshly prepared dilution to learn how long your dilution may remain stable, Remember, when you change to another lot number (or even another botte) of solvent, shelf life may be affected, For mut-slement standards, be aware that shel Ife may vary among individual elements, DUREE DE VIE DES ETALONS CONOSTAN Durée de vie : Les éiaions ne doivent pas étre utlisés aprés 12 mois” de la date de réception (voir a cate expedition sur la boutetle). La stabillé varie selon |'slemant ou la combinaison éléments ainsi que leur concentration. Les concentrations plus élevées contriouent a une durée de vie pls longue. La Contemination introdute los de transfers fits avec des tubes comptes-gouttes ou pipettes est un probléme ‘courant. Conostan garantie les contenants non-ouvers pendant une période de 12 mois" de la data expedition Humidité : La sensipite due a rhumisité varle selon Iélément, par contra, les étalons & base d'huile ne \devraient pas eire gardés dans des enaroits hummides. Garder les contenants bien fermés pendant "entreposege. Si humidité est un probleme courant, minimisar le eontact et prévoir le emplacement plus frequent des étalons, Stockage ; Stocker les alons dans leur contenant dorigine et conserver dans des concitions normales de ‘aboratoie, gerder les contenanis bien fermes et éviter le contact crect avec les rayons de sole, Ne pas resrigerer. Dilutions : Les dilutions a des concentrations infériaures contribuent& une durée de vie plus court, Uiliser de la arécaution. Tel que mentionné ci-dessus, la contamination inttoduite los de transfers avec des tubss comptes-gouttes ou pipettes est un probleme courant, La durée de vie dans des solvants peut varier dune journée jusqu'a plusieurs semaines. La qualité du solvant (contenu d*humicite st pursta) Peuvent avoir un effet significa sur la stabilte. Nous recommandons 1. Tuttisation d'un solvant anaiytique de haute qualité 2 determiner la durée de vie selon en preparant un lot dételon diué par solvant. Effectuer des analyses Sur une periede de temps en comparant un étalon fais ain de déterminer la durée de vie de [a lution Noubliez pas que lorsque le ot de solvant change ou une autre boulelle de solvant est utlisée, la durée de. ie Peut ere aectee, Pour des éiaions mut-eiements, veuilez noter que a durée de vie peut vaner dun element 3 rau,