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Simulation of Heat Treatment and Materials with the Use of the Abaqus
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SIMULATION
UDC 621.785.545:621.001.57
Translated from Metallovedenie i Termicheskaya Obrabotka Metallov, No. 7, pp. 41 – 48, July, 2013.
A module supplementing the ABAQUS software is developed for solving a joint heat and diffusion problem
with allowance for the phase transformations in materials in the process of induction quenching. The approach
provides a deeper study of the structure and properties of materials and makes it possible to develop a method
for computing the number of phase components, the size of austenite grains, the hardness, the thermophysical
characteristics, and the latent heat of induction quenching. Such computations are impossible on the basis of
standard softwares. The adequacy of the simulation tool suggested by the authors is confirmed by matching
between simulated and experimental data.
386
0026-0673/13/0708-0386 © 2013 Springer Science + Business Media New York
Simulation of Heat Treatment and Materials with the Use of the ABAQUS Software 387
with the Dirichlet boundary condition with the help of the puted at all points of the elements of the analyzed material by
ABAQUS software, i.e., the algorithm of the user.
Upon heating above the temperature Ac1 the initial fer-
¶T
r Cp = div(l grad(T )) + q&; (1) rite-pearlite structure of a steel is transformed into austenite.
¶t This transformation finishes when the temperature Ac3 is at-
tained. During cooling the austenite decomposes into ferrite,
Ts = f (t ), (2)
pearlite, bainite or martensite depending on the cooling rate.
where T is the temperature, l is the thermal conductivity, r is The austenization and the diffusion kinetics are computed by
the density, Cp is the specific heat, q& is the thermal power re- the algorithm of D. Farias [13] that has been educed from the
leased or absorbed during the phase transformation, t is the modeling of F. Fernandes [14]. This modeling is based on ex-
time, and Ts is the surface temperature. The initial condition panding the JMAK isothermal kinetics to the law of
for t = 0 at each point of the specimen is anisothermal transformation. For this purpose a continuous
temperature curve is replaced by a sequence of elementary
T = T0 , (3) isothermal transformation steps, and the proportion of the
new phase is computed using the concept of fictitious time
where T0 is the initial temperature of the specimen. The [15, 16]. An exception is the case of diffusion transforma-
boundary condition is represented by Eq. (2), where Ts is a tions, when the growth of phases is preceded by a stage of
variable surface temperature that describes the thermal cycle nucleation modeled with the help of Scheil’s sum [8]. The
on the surface and is obtained experimentally. distribution of the proportion of carbon in the formed austen-
Functional possibilities of the ABAQUS in simulation ite depends on the kinetics of the phase transformation dur-
of the behavior of materials in heat treatment. We have de- ing cooling. This distribution is modeled in accordance with
veloped subroutine interfaces that permit determination of
the variation of the temperature DT = Tmax – Ac1, where Tmax
important characteristics of materials, which cannot be esti-
is the heating temperature. For example, when the proportion
mated with the help of the standard version of the ABAQUS.
of carbon in the austenite is equal to the proportion of carbon
In addition, the user subroutines make it possible to deter-
in the steel, the austenite becomes homogeneous. The tem-
mine solution-dependent state variables SDV, user-defined
perature of the start of martensitic transformation Ms de-
fields FIELD(n ), where n is the number of the field, and the
pends on the austenite grain size (AGS); in this case the com-
heat flux FLUX due to the internal source of heat, which can
putation is performed by the Leblond relation [17]. The tem-
be connected, for example, with the phase transformations in
perature Ms is estimated from empirical formulas that in-
the material modeled in the solution [12]. The user subrou-
volve the proportion of carbon and the austenite grain size as
tines are commonly written in the FORTRAN programming
variables [18 – 20]. A martensitic transformation is com-
language and are included into the model when an analysis is
monly modeled by the Koistinen – Marburguer equations
executed. The subroutines should be created with great care.
[11]. The distribution of hardness over the thickness of a
Specifically, the first statement after the argument list should
specimen is estimated in accordance with the following con-
be “include ‘aba param.inc’ ” in order to provide linkage
cepts [14, 21, 22]:
with the standard ABAQUS solver. The file ‘aba param.inc’
– the hardness of a multiphase material is determined by
is installed by the ABAQUS installation procedure and con-
a linear dependence on the set of hardnesses of the compo-
tains important installation parameters. This statement tells
nents;
the ABAQUS execution procedure, which complies and
– the hardness of the ferrite, pearlite and bainite formed
links the user subroutine with the rest of the ABAQUS, to in-
in the process of cooling is determined by the temperature of
clude the ‘aba param.inc’ file automatically. There is no
their formation;
need to search for the file and to copy it to any particular di-
– the hardness of the martensite depends only on the
rectory; the ABAQUS will know where to find it.
content of carbon in the austenite, from which the martensite
“UMAT” User Subroutine has been formed.
The leading role in modeling a phase transformation dur- “HETVAL” User Subroutine
ing quenching belongs to the evolution of the temperature This user subroutine is used to determine the internal
and of the time. For example, the user subroutine “UMAT” source of heat (FLUX) connected with the phase transforma-
involves several variables for storing of data characterizing tion and is represented by the value of the heat power in the
nonstationary analysis such as the running time, the time in- heat transfer equation, i.e.,
crement, the initial temperature increment, the number of
DZ i
step, the number of increment, etc. Therefore, such variables q& = å H i .
as the proportion of a phase, the transformation temperature, i Dt i
the relative content of carbon, the size of austenite grains,
etc. are defined as SDV. At each time increment the UMAT To estimate the distribution of temperature at any mo-
subroutine is addressed and the values of the SDV are com- ment of time this equation is solved with the help of the stan-
388 M. Yaakoubi et al.
T(t), T(r), z(k), %C(r,t) Notations: th is the duration of heating, taus is the austenization
D(r, t), Ms(r), HV(r), ...
temperature, vh is the heating rate, and vc is the cooling rate.
l, W/(m × K) t, °C
55 Surface
Ferrite 1000 à
50 1.5 mm
Austenite
45 800 Center
40
35 600
30
400
25
20 200
15 à
10 0 3 6 9 12 t, sec
0 200 400 600 800 1000 1200 t, °C
t, °C Surface
960
b
1.5 mm
r, kg/m3
800 Center
7900
7850 640
7800 480
7750
320
7700
7650 160
7600
0 3 6 9 12 t, sec
7550 t, °C
7500 b
c
7450 Surface 1.5 mm
0 200 400 600 800 1000 1200 800
t, °C
Center
600
Cp , J/(kg × K)
900 400
800 200
700
0 3 6 9 12 t, sec
600 Fig. 3. Heating and cooling curves for specimens 1 (a), 2 (b ) and
3 (c) on the surface, at a distance of 1.5 mm from the surface, and in
500
the center: solid lines) computed data; dash and dash-and-dot lines)
c
experimental results.
400
0 200 400 600 800 1000 1200
t, °C
0.6 0.4
0.5
0.3
0.4 à
0.3 Pearlite ® austenite 0.2
0 2 4 6 8
0.2 h, mm
0.1
C, %
0 1 2 t, sec 0.7
0.6
Fig. 4. Kinetic curves of formation of austenite due to heating of
specimen 2 (Vaus is the volume fraction of austenite): :) computed 0.5
data; N, *, ^, =) experimental results. 0.4
0.3
0.2
0.1 b
tures correspond to 3 and 97% of the formed austenite. Ta-
ble 2 presents the values of computed and experimental criti- 0 2 4 6 8
h, mm
cal temperatures for the case of heating of three specimens. It
can be seen that the computed and experimental data match Fig. 5. Distribution of carbon in austenite over the thickness of
well. specimens 1 (a) and 2 (b ) in the end of heating to the austenization
Note that the grain size on the surface of a specimen is temperature (h is the distance from the surface): solid, dash, and
dash-and-dot lines) homogeneous, enriched and depleted austenite,
determined with scattering of from ± 0.5 mm to ± 2,5 mm,
respectively.
i.e., the scattering is on order of the error of the computation
(Table 2). Thus, we may conclude that the chosen law for
computing the grain size is satisfactory.
The results of the determination of the proportion of car- Cooling
bon in austenite, which depends on the austenization temper- The data of Table 4 allow us to compare the computed
ature, are presented in Table 3. The surface of the first two and experimental values of the temperature of the start of
specimens contains homogeneous austenite, i.e., the propor- martensitic transformation for three specimens. In specimens
tion of carbon in the austenite is equal to that in the steel 1 and 2 near the surface the austenite is homogeneous. The
(0.43%). In the third specimen the austenization temperature temperature Ms in this region depends on the size of the aus-
has been insufficient for homogenization of the austenite. tenite grains. The coincidence of the computed and experi-
Therefore, the specimen contains two types of austenite, i.e., mental data implies that M shom increases upon growth of the
(1 ) saturated one, with carbon concentration exceeding its
austenite grains. In specimen 3 the depleted and enriched
concentration in the matrix, and (2 ) depleted one, where the
austenites containing different amounts of carbons have
carbon content is lower than in the steel (Fig. 5). In this stage
transformed successively into dark and light martensite at
the experimental and computed data were not compared.
two different temperatures Ms . The highest of these tempera-
This will be done below when discussing the temperature Ms
tures (M sdark ) coincides with the experimental value of Ms .
and the hardness.
Figure 6 presents the dependence of the proportion of
4 300
0.2
b
200
0 2 4 6 8
0 50 100 150 200 250 300 350 h, mm
t, °C
Fig. 7. Distribution of phases in the surface layer (a), variation of
Fig. 6. Dependence of the volume fraction of martensite M on the the computed (the solid line) and experimental (the marks) hardness
temperature in the process of cooling of specimens 1 (a) and 2 (b ): HV over the thickness of specimen 1 (b ) after surface quenching
1 ) homogeneous martensite (computation); 3 and 4 ) light and dark (h is the distance from the center): Mhom , Mlight , Mdark ) homoge-
martensite (computation); 5 ) total content of martensite (computa- neous, light and dark martensite, respectively; B ) bainite; P ) pear-
tion); 2 and 6 ) experimental curves. lite; F ) ferrite; Aret ) retained austenite.
martensite on the temperature for specimens 2 and 3. It can Figure 7 presents the distribution of the phases and of the
be seen that the cooling curves obtained by computation and hardness over the thickness of specimen 1 after heat treat-
experimentally coincide. ment. The hardness was measured in sections perpendicular
Similar results were obtained for specimen 1 when we to its axis. In the direction from the center to the surface of
measured the hardness over its thickness after quenching the specimen the initial pearlite partially transforms into en-
(Fig. 7). The hardness of the other specimens was measured riched austenite, because the transformation of pearlite into
only on the surface at a load of 10 kg; the scattering of the enriched austenite precedes the transformation of ferrite into
measured results was ± 20 HV (Table 4). We may conclude depleted austenite. Due to the relatively low rate of cooling
that the computed values of the proportion of carbon in the in this zone (A ) the bainite-martensite transformation does
austenite are adequate. not occur, and the hardness increases inconsiderably (from
300 to 350 HV ), because the austenization is not complete.
In zone B the initial pearlite transforms fully into enriched
TABLE 4. Temperature of the Start of Martensitic Transformation austenite, but this is accompanied by partial austenization of
and Hardness of Specimens after Quenching the ferrite. Thus, the growth in the fraction of martensite
Computation Experiment leads the growth in the hardness. The temperature in zone C
Speci- is higher than Ac3, which reflects the end of the auste-
men M light , °C M dark, °C M hom , °C HV, Ms , °C HV,
s s s
kgf/mm2 kgf/mm2 nization. The growth in the fraction of bainite in the cooling
process leads the growth in the hardness. In zone D the con-
1 – – 329 764 331 746
tent of bainite decreases somewhat, and that of martensite in-
2 – – 343 747 345 735
creases due to the high rate of cooling of this part of the spec-
3 294 323 – 752 320 736
imen. Since the hardness of martensite exceeds that of bai-
Notations: M slight , M sdark, and M shom ) computed values of the tem- nite, the total hardness increases until so does the fraction of
perature of the start of martensitic transformation (for light, dark and
martensite. Near the surface, the high temperature (1060°C)
homogeneous martensite, respectively); Ms ) experimental tempera- and the dissolution of alloying elements in the austenite dur-
ture of the start of martensitic transformation; HV ) hardness of the ing heating result in homogenization. For this reason, the
steel after quenching. carbon concentration in the thin surface layer of homoge-
392 M. Yaakoubi et al.
neous martensite (zone E ) formed due to fast cooling is con- induction d’un acier XC42,” in: Thesis INPL, Nancy (1985),
stant and equals its content in the steel. The hardness of the p. 105.
6. J. W. Christian, The Theory of Phase Transformations in Metals
surface layer of martensite is about 746 HV.
and Alloys. Part 1, Pergamon Press, New York (1981),
pp. 525 – 548.
CONCLUSIONS 7. J. Orlich, “Les processus d’austenitisation au cours de l’échauf-
fement rapide et l’échauffement par impulsion de l’acier,”
Thermal and diffusion computations used for analyzing Traitement Thermique, 90, 69 – 75 (1974).
8. Caner Simsir and C. Hakan Gur, “3D FEM simulation of steel
dilatometric curves describing fast heating and cooling of a
quenching and investigation of the effect of asymmetric geome-
material make it possible to check the evolution laws chosen try on residual stress distribution,” J. Mater. Proc. Technol.,
for describing various phenomena that characterize fast 207, 211, 221 (2008).
austenization and their effect on the structure of martensite. 9. A. M. Habraken and M. Bourdouxhe, “Coupled thermo-me-
The ABAQUS software used for the computation is linked to chanical-metallurgical analysis during cooling process of steel
user subroutines. pieces,” Eur. J. Mechan. A. Solids, 11(3), 381 – 402 (1992).
The user subroutines simulate phase transformations 10. W. P. Oleivera, M. A. Savi, P. M. C. L. Pacheco, and L. F. G. Sou-
with allowance for the temperature fields and make it possi- za, “Thermo mechanical analysis of steel cylinders quenching
using a constitutive model with diffusional and non-diffusional
ble to predict the hardness. This means of thermo-diffusion phase transformations,” Mechan. Mater., 42, 31 – 43 (2010).
simulation has three advantages over the standard method, 11. D. P. Koistinen and R. E. Marburguer, “A general equation pre-
namely, (1 ) improvement of the algorithm of computation of scribing extent of the austenite-martensite transformation in
phase transformations and hardness, (2 ) possibility to pure Fe – C alloys and plain carbon steels,” Acta Metall., 7,
change the algorithm and compare various models in order to 59 – 60 (1959).
choose the most suitable of them, and (3 ) no need for other 12. “ABAQUS documentation,” in: ABAQUS Analysis User’s
softwares for simulation but the ABAQUS, which is an Manual.
13. D. Farias, S. Denis, and A. Simon, “Les transformations de
available means for simulating phase transformations and phases en cycle thermique rapide et leur modélisation. Cas d’un
this lowers the expenses. acier XC42,” Traitement Thermique, 237, 63 – 70 (1990).
The performed simulation of the process of surface 14. F. M. B. Fernandes, “Modélisation et calcul de l’évolution de la
quenching has shown only inconsiderable differences be- température et de la microstructure au cours du refroidissement
tween computational and experimental results. This implies continu des aciers,” in: Thesis INPL, Nancy (1985), p. 177.
that the suggested simulation tool is adequate for solving 15. M. Melander, “A computational and experimental investigation
problems of surface heat treatment and makes it possible to of induction and laser hardening,” in: Thesis Linkoping, Suede
(1985), p. 124.
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thermal metallurgical transformations in steels including effect
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