I2OCR

Glassware and reagents: porcelain evaporation dish, 100 ml

in volume; a glass stick with a rubber point; funnel 10-12 cm in

diameter; conical 500-750 ml flask, measuring 500 and 200 ml

flask, 50 ml pipette, two conical 250 ml flasks. Ammonium acetate

solution: 1N CH3;COONH,. H2O2 solution (30%), HNO; solution

(10%), HCl solution (10%). Distilled water, purified from the

admixtures of Ca?*, Mg?*, Cu?*, and Mn?*, 0.05N Trilon B, 5%

NH2OHxHCI, sodium sulfide or sodium ethylditiocarbonate salt

(CsHioNS2Nax3H20), chloride-ammoniacal buffer solution, 10%

NaOH, indicators : chromogen Black and Murexide.

6.1.6. Determination of Exchangeable Potassium and

Sodium on the Flame Photometer

Exchangeable potassium and sodium are determined in 1N

ammonium acetate extract from the soil on the flame photometer.

If the soil contains soluble salts it needs proper treatment with

distilled water. In water extract, the sodium and potassium cations

are also determined on the flame photometer (blank determination),

which will allow to make corrections on the content of soluble salts.

The difference between the results obtained in two extracts -

ammonium acetate and water, will show an actual content of

exchangeable potassium and sodium in the soil.

After preparation of a flame photometer for working regime, it

should be calibrated by the scale of standard solutions. To prepare

the scale, the following volumes of the initial standard solution

should be put into measuring 200-ml flasks:

Number of standard solution: 12345

Volume (ml) of initial standard solution: 01 2 5 10 15 20

Content of potassium K* (Na*), mg/ml: 05102550 75 100

OCR.Space

Glassware and reagents: porcelain evaporation dish, 100 ml

in volume; a glass stick with a rubber point; funnel 10-12 cm in

diameter; conical 500-750 ml flask, measuring 500 and 200 ml

flask, 50 ml pipette, two conical 250 ml flasks. Ammonium acetate

solution: IN CH3COONH4. H202 solution (30%), HN03 solution

(10%), HCI solution (10%). Distilled water, purified from the

admixtures of Ca2+, Mg cu2+ and Mn2+ O.05N Trilon B, 50/0

NH20HxHCl, sodium sulfide or sodium ethylditiocarbonate salt

(CsH10NS2Nax3H20), chloride-ammoniacal buffer solution, 100/0

NaOH, indicators : chromogen Black and Murexide.

6.1.6. Determination of Exchangeable Potassium and

Sodium on the Flame Photometer

Exchangeable potassium and sodium are determined in IN

ammonium acetate extract from the soil on the flame photometer.

If the soil contains soluble salts it needs proper treatment with

distilled water. In water extract, the sodium and potassium cations

are also determined on the flame photometer (blank determination),

which will allow to make corrections on the content of soluble salts.

The difference between the results obtained in two extracts

ammonium acetate and water, will show an actual content of

exchangeable potassium and sodium in the soil.

After preparation of a flame photometer for working regime, it

should be calibrated by the scale of standard solutions. To prepare

the scale, the following volumes of the initial standard solution

should be put into measuring 200-ml flasks:

Number of standard solution: 12345

Volume (ml) of initial standard solution: 012 510 15 20

Content of potassium K + (Na+), mg/ml: 0 5 10 25 50 75 100

Online ocr

Glassware and reagents: porcelain evaporation dish, 100 ml in volume; a glass stick with a rubber point; funnel 10-12
cm in diameter; conical 500-750 ml flask, measuring 500 and 200 ml flask, 50 ml pipette, two conical 250 ml flasks.
Ammonium acetate solution: 1N CH3COONH4. H202 solution (30%), HNO3 solution (10%), HCI solution (100/0).
Distilled water, purified from the admixtures of Ca', Mg', Cu', and Mn', 0.05N Trilon B, 5% NH2OHxHCI, sodium sulfide
or sodium ethylditiocarbonate salt (Cshl10NS2Nax3H20), chloride-ammoniacal buffer solution, 10% NaOH, indicators :
chromogen Black and Murexide.

6.1.6. Determination of Exchangeable Potassium and Sodium on the Flame Photometer

Exchangeable potassium and sodium are determined in 1N ammonium acetate extract from the soil on the flame
photometer. If the soil contains soluble salts it needs proper treatment with distilled water. In water extract, the
sodium and potassium cations are also determined on the flame photometer (blank determination), which will allow to
make corrections on the content of soluble salts. The difference between the results obtained in two extracts -
ammonium acetate and water, will show an actual content of exchangeable potassium and sodium in the soil. After
preparation of a flame photometer for working regime, it should be calibrated by the scale of standard solutions. To
prepare the scale, the following volumes of the initial standard solution should be put into measuring 200-m1 flasks:

Number of standard solution: 1 2 3 4 5 6 7 Volume (ml) of initial standard solution: 0 1 2 5 10 15 20 Content of

potassium K+ (Na+), mg/ml: 0 5 10 25 50 75 100
NewOCR

Glassware and reagents: porcelain evaporation dish, 100 ml

in volume; a glass stick with a rubber point; funnel 10-12 cm in

diameter; conical 500-750 ml flask, measuring 500 and 200 ml

flask, 50 ml pipette, two conical 250 ml flasks. Ammonium acetate

solution: 1N CH3;COONH,. H.0. solution (30%), HNO; solution

(10%), HCl solution (10%). Distilled water, purified from the

admixtures of Ca?*, Mg?*, Cu®*, and Mn?*, 0.05N Trilon B, 5%

NH2,OHxHCI, sodium sulfide or sodium ethylditiocarbonate salt

(C3HygpNS2Nax3H,20), chloride-ammoniacal buffer solution, 10%

NaOH, indicators : chromogen Black and Murexide.

6.1.6. Determination of Exchangeable Potassium and

Sodium on the Flame Photometer

Exchangeable potassium and sodium are determined in 1N

ammonium acetate extract from the soil on the flame photometer.

If the soil contains soluble salts it needs proper treatment with

distilled water. In water extract, the sodium and potassium cations

are also determined on the flame photometer (blank determination),

which will allow to make corrections on the content of soluble salts.

The difference between the results obtained in two extracts -

ammonium acetate and water, will show an actual content of

exchangeable potassium and sodium in the soil.

After preparation of a flame photometer for working regime, it

should be calibrated by the scale of standard solutions. To prepare

the scale, the following volumes of the initial standard solution

should be put into measuring 200-ml flasks:

Number of standard solution: 123 45 6/7

Volume (ml) of initial standard solution: 01 2 5 10 15 20

Content of potassium K* (Na*), mg/ml: 05102550 75 100