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Data Komponen

Komponen Komponen Mr Tb, oC


Aseton C3H6O 58.08 56.2
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02 100
Diaseton Alkohol C6H12O2 116.16 167.9
Asam Sulfat (Katalis 2) H2SO4 98.08 270
Gas Hidrogen H2 2.016 -252.8
Mesitil Oksida (MO) C6H10O 98.14 125
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16 115.9

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George


Kapasitas Pabrik = 65000 ton/tahun

Hasil TH-02 Kating

Feed (Murni)
kg/jam kmol/jam
Urut C3H6O = 14584.5912 251.11210743802
Berdasarkan
H2O = 607.5822 33.717103218646
Titik Didih
C6H10O = 0 0
Ba(OH)2 = 26.8487 0.156698377495
C6H12O2 = 0 0

2 Aseton ---------> 1 DAA


M 1777.23969869146 21.686956783747
R 195.062892561984 97.531446280992
S 1972.30259125344 119.21840306474

Konversi 15 %

Hasil TH-02 Yosua


Asumsi - ayo
Asumsi
H2O = 595.2626625 33.0334440899
Feed (Biasa)
kg/jam kmol/jam
595.2627 C3H6O = 14286.3039 245.97630681818
H2O = 595.2626625 33.0334440899
C6H10O = 0 Gk ada
Ba(OH)2 = 26.2995139865 0.1534931363749
C6H12O2 = 0 0

Input MO 65.2245562216422
Recycle MO Gk ada

2 Aseton ---------> 1 DAA


M 1857.82709077177 20.390785142617
R 185.782709077177 92.891354538588
S 1672.04438169459 113.28213968121

Konversi 10 %

Input Recycle TH
C6H12O = 33.0334440899 12.926130296048
C6H10O = #VALUE! Gk ada

#VALUE!

Feed (Biasa)
kg/jam kmol/jam
H2O = 245.97630681818
C6H10O = 65.224556221642

Mass Balance
I
Bahan
Feed
C3H6O 14286.3039
H2O 595.2626625
C6H10O 0
Ba(OH)2 26.299513986471
C6H12O2 0
SubTotal 14907.866076486
Total 111828
Inpt - Output
Sg, tidak ada satuan
0.79

1
0.9387
1.84
0.0696
0.855
1.94
0.802

rni) Hasil k
Ratio
11.5860527129905 C3H6O =
3.46525361240887 H2O =
0 C6H10O =
9.04526862379597 Ba(OH)2 =
0 C6H12O2 =

Katalis
Ba(OH)2

10.9756096887552

H2O =
sa) Hasil k

Kira Kira --> C3H6O =


Hitungan di Ipad H2O =
C6H10O =
Nembak Ba(OH)2 =
C6H12O2 =

Katalis
Ba(OH)2
0.153493136374875
1.38143822737387 Recycle 1672.0443816946
1.53493136374874

Output
71.8118349780438
Gk ada

71.8118349780438

sa)
Input
Output
Recycle TH-1 Recycle MD-1
17480.2207839879 76136.0727480363 97112.3376888218
232.928867934783 465.857735869566 1294.04926630435
0 0 0
236.695625878238 0 262.995139864709
2368.59360216639 0 13158.8533453688
20318.4388799673 76601.9304839059 111828.23544036
111828.23544036 111828.23544036
0
Hasil ke TH-1 Recycle Masuk dari TH-1
kg/jam kmol/jam kg/jam
114551.3345 1972.302591253 C3H6O = 26047.4658
17533.5565 973.0053551609 H2O = 3189.52
41.4767 0.422627878541 C6H10O = 7.545
296.8259 1.732379479398 Ba(OH)2 = 269.9772
13848.4097 119.2184030647 C6H12O2 = 2519.1569

100
100
100
100
100

0 0 H2O =
Hasil ke TH-1 Recycle Masuk dari TH-1
kg/jam kmol/jam Ratio kg/jam
97112.33768882 1672.044381695 90 C3H6O = 17480.220784
1294.049266304 71.81183497804 100 H2O = 232.928867935
0 Gk ada #VALUE! C6H10O = 0
262.9951398647 1.534931363749 100 Ba(OH)2 = 236.695625878
13158.85334537 113.2821396812 555.55555555556 C6H12O2 = 2368.59360217

MIBK 6944.445
97112.33768882

Cara Hitung Hidrogen masih bingung


- kalau olin perbadningan gitu
Recycle Masuk dari TH-1 Recycle Masuk dari FD-1
kmol/jam Ratio kg/jam
448.475650826446 20.692202315 C3H6O = 82476.9608
176.998890122087 18.19094717 H2O = 6424.2951
0.076879967393519 18.190936116 C6H10O = 0
1.57568110190265 90.954731376 Ba(OH)2 = 0
21.6869567837466 100 C6H12O2 = 0

0 0 H2O =
Recycle Masuk dari TH-1 Recycle Masuk dari MD-1
kmol/jam Ratio kg/jam
300.967988705026 16.2 C3H6O = 76136.0727480363
12.9261302960479 18 H2O = 465.857735869566
Gk ada #VALUE! C6H10O = 0
1.38143822737387 90 Ba(OH)2 = 0
20.390785142617 100 C6H12O2 = 0
Masuk dari FD-1 Recycle Masuk dari MD-1
kmol/jam Ratio kg/jam kmol/jam
1420.05786501 65.5200000008 C3H6O = 2771.5695 47.71986053719
356.509162042 36.6399999909 H2O = 7312.1592 405.78019977802
0 0 C6H10O = 33.9317 0.3457479111473
0 0 Ba(OH)2 = 0 0
0 0 C6H12O2 = 0 0

0 0 H2O = 595.2626625 33.0334440899


asuk dari MD-1 Feed Awal + Recycle
kmol/jam Ratio kg/jam kmol/jam
1310.88279525 70.56 C3H6O = 107902.597432 1857.8270907718
25.8522605921 36 H2O = 1294.049266304 71.811834978044
Gk ada #VALUE! C6H10O = #VALUE!
0 0 Ba(OH)2 = 262.9951398647 1.5349313637487
0 0 C6H12O2 = 2368.593602166 20.390785142617
MD-1 Feed Awal + Recycle
Ratio kg/jam kmol/jam Ratio
2.201744970728 C3H6O = 125880.5873 2167.3654838
41.70379922636 H2O = 17533.5565 973.00535516
81.80906388406 C6H10O = 41.4767 0.4226278785
0 Ba(OH)2 = 296.8259 1.7323794794
0 C6H12O2 = 2519.1569 21.686956784
cle
Perbandingan
Ratio Thickener Bawah Thickener Samping
% 25 75
Recycle Purge
90 10
Aseton
Itungan Coba Coba misal F = 1672.0444

A= 245.9763068
A + R1 + R2 = 1857.827091
Reaksi = 185.7827091
F= 1672.044382

F-F= 0

R2 = 300.9679887
R1 = 1310.882795

Reaksi Aseton
M 1857.827091
Konveri 10% R 185.7827091
S 1672.044382
Air DAA
Itungan Coba Coba misal F = 71.811835 Itungan Coba Coba

A= 33.0334440899001
R1 0,8 x 0,45 x F = 25.8522605920958 R1
R2 0,9 x 0,2 x F = 12.9261302960479 R2
F= 71.8118349780438 Reaksi

F-F= 0
Katalis Ba(OH)2
gan Coba Coba misal F = 113.28213968 Itungan Coba Coba misal F =

A= 20.39078514262 A= 0.1534931364
Gk ada 0 R1 Gk ada 0
0,9 x 0,2 x F = 20.39078514262 R2 0,9 x F = 1.3814382274
Reaksi = 92.89135453859 karena reaksi 1:2 F= 1.5349313637
F= 113.2821396812
F-F= 0
F-F= 0
1.5349314
Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu


Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000

Hasil TH-01 Kating

Feed
kg/jam
Urut H2O = 17533.5565
Berdasarkan C3H6O = 114551.3345
Titik Didih C6H10O = 41.4767
C6H12O2 = 13848.4097
Ba(OH)2 = 296.8259

Hasil TH-01 Yosua


Asumsi - ayo

Komponen F, kmol/jam

Air 71.8118
Aseton 1672.0444
DAA 113.2821
Ba(OH)2 1.5349
1858.6733
Mass Balance

Bahan
Air
Aseton
DAA
Ba(OH)2
SubTotal
Total
Inpt - Output
Tb, oC Sg, tidak ada satuan
56.2 0.79

100 1
167.9 0.9387
270 1.84
-252.8 0.0696
125 0.855
1.94
115.9 0.802

ton/tahun

Feed
kmol/jam
973.005355161
1972.30259125
0.42262787854
119.218403065
1.7323794794

F, kg/jam D, kmol/jam D, kg/jam R + P, kmol/jam

1294.0493 57.449467982435 1035.2394 14.3624


97112.3377 1337.63550535567 77689.8702 334.4089
13158.8533 90.6257117449643 10527.0827 22.6564
262.9951 0 0.0000 1.5349
1485.7107 372.9626 335.6663 37.2963
Mol balance = 1448.414424820

Input Output
Feed Recycle Purge Output ke MD-01
1294.0493 232.9289 25.8810 1035.2394
97112.3377 17480.2208 1942.2468 77689.8702
13158.8533 2368.5936 263.1771 10527.0827
262.9951 236.6956 26.2995 0.0000
111828.23544 20318.4388799673 2257.60431999637 89252.192240396
111828.23544 111828.2354
0
Persamaan Antoine
TEKANAN UAP TE
Komponen A B C Komponen
Aseton 7.31742 1315.6735 240.479 Air
Air 8.05573 1723.6425 233.08 MO
MIBK 7.37701 1527.2068 223.816 MIBK
MO 7.12851 1483.4864 219.745
DAA 8.62593 2568.7558 279.12
Asam Sulfat 8.28538 2976.837 213.95

Hasil ke MD-1
kg/jam kmol/jam Ratio
H2O = 14026.8452 778.4042841287 80
C3H6O = 85913.5009 1479.226943871 80
C6H10O = 33.1813 0.338101691461 80
C6H12O2 = 11078.7278 95.37472279614 80
Ba(OH)2 = 0 0 0

R, kmol/jam R, kg/jam P, kmol/jam P kg/jam

12.9261 232.9289 1.4362 25.8810


300.9680 17480.2208 33.4409 1942.2468
20.3908 2368.5936 2.2656 263.1771
1.3814 236.6956 0.1535 26.2995
TEKANAN UAP
A B C
8.05573 1723.6425 233.08
7.12851 1483.4864 219.745
7.37701 1527.2068 223.816

Hasil Recycle + Purge Hasil Recycle


kg/jam kmol/jam Ratio
H2O = 3506.7113 194.601071032 20 H2O =
C3H6O = 28637.8337 493.075649105 20 C3H6O =
C6H10O = 8.2953 0.08452516813 20 C6H10O =
C6H12O2 = 2769.682 23.8436811295 20 C6H12O2 =
Ba(OH)2 = 296.8259 1.7323794794 100 Ba(OH)2 =
Hasil Recycle Hasil Purging
kg/jam kmol/jam Ratio kg/jam kmol/jam
3189.52 176.9988901 90 H2O = 317.1913 17.6021809101
26047.4658 448.4756508 90 C3H6O = 2590.3679 44.5999982782
7.545 0.076879967 90 C6H10O = 0.7503 0.00764520073
2519.1569 21.68695678 90 C6H12O2 = 250.5251 2.15672434573
269.9772 1.575681102 90 Ba(OH)2 = 26.8487 0.1566983775
ng
Ratio
10
10
10
10
10
Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu


Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000 ton/tahun

Hasil MD-02 Kating

Feed
kg/jam kmol/jam
C3H6O = 85913.5009 1479.226943871
H2O = 14026.8452 778.4042841287
C6H12O2 = 11078.7278 95.37472279614

Hasil MD-02 Yosua


Asumsi -

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.2
T avg = 89.29007691792

Komponen F,kmol/jam

Aseton 1337.6355
Air 57.4495
DAA 90.6257
Total 1485.7107

Kondisi Atas (Distilat)


P= 1.1
T = 58.99200541393

Komponen D,kmol/jam

Aseton 1324.2592
Air 1.1490
DAA 0.0000
Total 1325.4081

Mass Balance

Bahan
Aseton
Air
DAA
SubTotal
Total
Inpt - Output

Komponen A
Aseton 46.878
Air 92.053
DAA 154.081

T= 89.29007691792
Treferensi 25
MR Komp massflow
58.08 Aseton 77689.8702
18.02 Air 1035.2394
116.16 DAA 10527.0827
TOTAL 89252.1922
T= 58.99200541393
Treferensi 25
MR Komp massflow
58.08 Aseton 76912.9714
18.02 Air 20.7048
116.16 DAA 0.0000
TOTAL 76933.6762

T= 119.5881484219
Treferensi 25
MR Komp massflow
58.08 Aseton 776.8987
18.02 Air 1014.5346
116.16 DAA 10527.0827
TOTAL 12318.5160

T= 89.29007691792
Treferensi 25
MR Komp massflow
58.08 Aseton 776.8987
18.02 Air 1014.5346
116.16 DAA 10527.0827
TOTAL 12318.5160
Hbot 649676.0288509
Hin Reboiler 399578.410383
Qrb 250097.6184679

T= 89.29007691792
Treferensi 25
MR Komp massflow
58.08 Aseton 76912.9714
18.02 Air 20.7048
116.16 DAA 0.0000
TOTAL 76933.6762
Htop 2257138.576118
Hin Kondenser 7197798.690339
Qkondenser 4940660.114221
INPUT OUTPUT
Komponen H, kkal/jam Komponen
ASETON 7268889.59245643 TOP
AIR 79899.6903646539 ASETON
DAA 248587.817901073 AIR
Q-RB 250097.618467856 Bottom
Aseton
AIR
DAA
QCD
TOTAL 7847474.71919001 total
SELISIH 0
Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802

Hasil Atas
kg/jam kmol/jam
C3H6O = 82476.9608 1420.05786501377
H2O = 6424.2951 356.509162042175
C6H12O2 = 0 0

HK di D =
LK di B =

Distillat
F, kg/jam Po alfa
D xd
77689.8702 2.79849906952855 4.1571 1324.2592 0.9991
1035.2394 0.673185083140321 1.0000 1.1490 0.0009
10527.0827 0.0592340620093593 0.0880 0.0000 0.0000
1325.4081 1.0000 160.3025

atm
o
C

D, kg/jam Po yd Ki Xi

76912.9714 1.10479387283158 0.9991 1.00435806621052 0.99479771095823


20.7048 0.187709559394902 0.0009 0.17064505399537 0.00508010476154
0.0000 0.014052861443206 0.0000 0.01277532858473 0
1 0.99987781571977

Input Output
Feed Distilat Bottom
77689.8702 76912.9714 776.8987
1035.2394 20.7048 1014.5346
10527.0827 0.0000 10527.0827
89252.192240396 76933.6762378077 12318.51600259
89252.192240396 89252.1922
0

Kapasitas Panas
B C D E Cp @25C
9.6265 -2.08E-03 2.96E-06 0 127.53
-0.04 -2.11E-04 5.35E-07 0 75.55
0.8551 -2.36E-03 2.99E-06 0 233.58
INPUT
C = 362.4400769179 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
3013.7902257581 19894.1922379044 -1.84E+02 1.26E+01 0
5918.0944505249 -82.6642798022311 -1.87E+01 2.28E+00 0
9905.8793415894 1767.1556414722 -2.09E+02 1.28E+01 0
DISTILAT
C = 332.1420054139 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
1593.4772297943 5561.50067161636 -2.72E+01 9.88E-01 0
3129.0660743686 -23.1091286412148 -2.76E+00 1.79E-01 0
5237.522186184 494.01539752757 -3.09E+01 9.98E-01 0

BOTTOM
C = 392.7381484219 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
4434.1032217219 43063.7522061807 -5.87E+02 5.92E+01 0
8707.1228266812 -178.93835643767 -5.95E+01 1.07E+01 0
14574.236496995 3825.25471474629 -6.66E+02 5.98E+01 0

Hin Reboiler
C = 362.4400769179 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
ga diitung mirip inp 0 0.00E+00 0.00E+00 0
0 0 0.00E+00 0.00E+00 0
0 0 0.00E+00 0.00E+00 0

Hin Kondenser
C = 362.4400769179 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
ga diitung mirip inp #VALUE! #VALUE! 7.86E+09 0
2364.7037105475 #VALUE! #VALUE! 5.97E+09 0
#VALUE! #VALUE! #VALUE! #VALUE! 0
OUTPUT
H, kkal/jam
TOP
2256286.3422309
852.23388754292

150165.54968277
114099.68843124
385410.79073684
4940660.1142207
7847474.71919
0
Persamaan Antoine
TEKANAN UAP TEKANAN UAP
B C Komponen A B
1315.674 240.479 Aseton 7.31742 1315.6735
1723.643 233.08 Air 8.05573 1723.6425
1527.207 223.816 MO 7.12851 1483.4864
1483.486 219.745 DAA 8.62593 2568.7558
2568.756 279.12
2976.837 213.95

Hasil Bawah
ratio kg/jam kmol/jam ratio
96 C3H6O = 3436.54 59.16907713499 3.9999999581
45.8 H2O = 7602.5501 421.8951220866 54.2000000114
0 C6H12O2 = 11078.7278 95.37472279614 100

0.01
0.01

Bottom
B xb
13.3764 0.0834
56.3005 0.3512
90.6257 0.5653
1.0000

Kondisi Bawah (Bottom)


P= 1.3 atm
T = 119.588148421901 oC

Komponen B,kmol/jam B. kg/jam Po

Aseton 13.3764 776.8987 6.0623268405337


Air 56.3005 1014.5346 1.9385715670535
DAA 90.6257 10527.0827 0.200640862901
Total 160.3025 1

1 joule 0.239006 cal

Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)


22736.39 1337.63550535567 30413000.4788852 7268889.592456
5819.026 57.449467982435 334299.935418583 79899.69036465
11476.77 90.6257117449643 1040090.28183842 248587.8179011
31787390.6961422 7597377.100722
Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)
7128.734 1324.25915030212 9440291.63381202 2256286.342231
3103.373 1.1489893596487 3565.74264889969 852.2338875429
5701.638 0 0 0
9443857.37646092 2257138.576118

Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)


46970.34 13.3763550535568 628291.966238373 150165.5496828
8479.37 56.3004786227863 477392.569354918 114099.6884312
17793.59 90.6257117449643 1612556.96818007 385410.7907368
2718241.50377336 649676.0288509

Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)


22736.39 13.3763550535568 304130.004788854 72688.89592456
5819.026 56.3004786227863 327613.936710212 78301.69655736
11476.77 90.6257117449643 1040090.28183842 248587.8179011
1671834.22333749 399578.410383

Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)


22736.39 1324.25915030212 30108870.4740963 7196200.696532
5819.026 1.1489893596487 6685.99870837167 1597.993807293
11476.77 0 0 0
30115556.4728047 7197798.690339
C
240.479
233.08
219.745
279.12

REAKSI Yield
C3H6O = 1479.227 C3H6O =
H2O = 778.4043 Total 2353.006 H2O =
C6H12O2 = 95.37472 C6H12O2 =
xb Ki Yi

0.0834 4.663328 0.38912879036402


0.3512 1.491209 0.52373325980757
0.5653 0.154339 0.08725434174744
1.0001163919
0.628654
0.330813
0.040533
Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu


Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000

Hasil TH-02 Kating

Feed
kg/jam
Urut H2O = 7799.74
Berdasarkan
C6H10O = 33.1813
Titik Didih
C6H12O2 = 11078.7278
H3PO4 = 1117.4095

DAA
M 95.3747227961433
R 85.8372580922865
S 9.53746470385675

Konversi 90.0000079431503 %

Hasil TH-02 Yosua


Asumsi - Asumsi reaksi 1:1:1
H2SO4 (98%) =

Feed (Biasa)
kg/jam
H2O Feed + dari Katalis) = 1060.62605983102
C6H10O = 0
C6H12O2 = 10527.0826762951
H2SO4 = 2258.48031737234

Input MO 65.2245562216422

DAA
M 90.6257117449643
R 81.5631405704678
S 9.06257117449643

Konversi 90 %

Hasil MD-02 Yosua


- DAA udah hilang di RD jadi di MD-2
Asumsi gk perlu pisahin

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.300
T avg = 119.588148421901

Komponen F,kmol/jam

Air 140.4214
Aseton 13.3764
Katalis Asam Sulfat 23.0269
MO 81.5631
DAA 9.0626
Total 267.4504

Kondisi Atas (Distilat)


P= 1.2
T= 117.276701011583
Komponen D,kmol/jam

Air 140.4214
Aseton 13.3764
Katalis Asam Sulfat 0.0000
MO 80.7475
DAA 0.0000
Total 234.5453

Mass Balance

Bahan
Air
Aseton
Katalis Asam Sulfat
MO
DAA
SubTotal
Total
Inpt - Output
Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802

ton/tahun

Feed Hasil Atas


kmol/jam kg/jam
432.83795782464 H2O = 9346.9416
0.3381016914612 C6H10O = 8414.5505
95.374722796143 C6H12O2 = 11.0778
11.392837479608 H3PO4 = 0

MO Air H3PO4
0.3381016914612 432.837957824639 0.095367

86.171130018341 518.69820199778 0.095367

mol H2SO4 massa H2SO4 massa air mol air


23.026920038462 2258.48031737234 46.0914350484151 2.557793

eed (Biasa) Hasil Atas


kmol/jam kg/jam
58.858271910712 H2O =
0 Belom ada MO C6H10O =
90.625711744964 C6H12O2 =
23.026920038462 Pake Perbandingan H3PO4 =

Gk ada recycle mo Katalis


MO Air H2SO4
0 58.8582719107117 23.02692
81.563140570468 81.5631405704678 Asumsi Reaksi 1 : 1 : 1
81.563140570468 140.42141248118 23.02692

HK di D = 0.01
LK di B = 0.01

Distillat Bottom
F, kg/jam Po alfa
D xd B
2530.3939 1.93857156705353 6426.0262 140.4214 0.5987 0.0000
776.8987 6.06232684053371 20095.5547 13.3764 0.0570 0.0000
2258.4803 0.000301675018711402 1.0000 0.0000 0.0000 23.0269
8004.6066 0.751495939598578 2491.0778 80.7475 0.3443 0.8156
1052.7083 0.200640862901011 665.0894 0.0000 0.0000 9.0626
234.5453 1.0000 32.9051

atm
o
C
D, kg/jam Po yd Ki Xi

2530.3939 1.79985459233914 0.5987 1.499879 0.399163177649


776.8987 5.74157695511341 0.0570 4.784647 0.011919585476
0.0000 0.000261370479936579 0.0000 0.000218 0
7924.5605 0.701363340475812 0.3443 0.584469 0.589034357074
0.0000 0.184014088138226 0.0000 0.153345 0
1 1.000117120199

Input Output
Feed Distilat Bottom
1060.6261 2530.3939 0.0000
776.8987 776.8987 0.0000
2258.4803 0.0000 2258.4803
0.0000 7924.5605 80.0461
10527.0827 0.0000 1052.7083
14623.087755009 11231.8531 3391.2347
14623.087755009 14623.0878
0.0000

Kapasitas Panas
Komponen A B C D
Aseton 46.878 9.6265 -2.08E-03 2.96E-06
Air 92.053 -0.04 -2.11E-04 5.35E-07
MO 125.316 0.5368 -1.44E-03 2.01E-06
DAA 154.081 0.8551 -2.36E-03 2.99E-06
Asam sulfat 26.004 0.70337 -1.39E-03 1.03E-06
INPUT
T= 119.588148421901 C = 392.73815
Treferensi 25 C = 298.15
MR Komp massflow AT 1/2BT2 1/3CT3
58.08 Aseton 776.8987 4434.103 43063.752206181 -5.87E+02
18.02 Air 1060.6261 8707.123 -178.9383564377 -5.95E+01
98.14 MO 0.0000 11853.41 2401.3527433935 -4.06E+02
116.16 DAA 10527.0827 14574.24 3825.2547147463 -6.66E+02
98.08 SULFAT 2258.4803 2459.67 3146.4967941891 -3.92E+02
TOTAL 14623.0878

DISTILAT
T= 117.276701011583 C = 390.4267
Treferensi 25 C = 298.15
MR Komp massflow AT 1/2BT2 1/3CT3
58.08 Aseton 776.8987 4325.747 40984.773449521 -5.45E+02
18.02 Air 2530.3939 8494.347 -170.2997909916 -5.53E+01
98.14 MO 7924.5605 11563.75 2285.4231951076 -3.77E+02
116.16 DAA 0.0000 14218.09 3640.5837819234 -6.18E+02
98.08 SULFAT 0.0000 2459.67 2994.5940997444 -3.64E+02
TOTAL 11231.8531

BOTTOM
T= 223.12910951382 C = 496.27911
Treferensi 25 C = 298.15
MR Komp massflow AT 1/2BT2 1/3CT3
58.08 Aseton 0.0000 9287.896 188944.82203484 -5.39E+03
18.02 Air 0.0000 18238.38 -785.1028807348 -5.47E+02
98.14 MO 80.0461 24828.75 10536.080659461 -3.73E+03
116.16 DAA 1052.7083 30527.93 16783.536832908 -6.12E+03
98.08 SULFAT 2258.4803 5152.149 13805.445330561 -3.60E+03
TOTAL 3391.2347

Hin Reboiller
T= 119.588148421901 C = 392.73815
Treferensi 25 C = 298.15
MR Komp massflow AT 1/2BT2 1/3CT3
58.08 Aseton 0.0000 4434.103 43063.752206181 -5.87E+02
18.02 Air 0.0000 8707.123 -178.9383564377 -5.95E+01
98.14 MO 80.0461 11853.41 2401.3527433935 -4.06E+02
116.16 DAA 1052.7083 14574.24 3825.2547147463 -6.66E+02
98.08 SULFAT 2258.4803 2459.67 3146.4967941891 -3.92E+02
TOTAL 3391.2347
Hbot 184722.4
Hin rb 70057.97
Qrb 114664.4

Hin kondenser
T= 119.588148421901 C = 392.73815
Treferensi 25 C = 298.15
MR Komp massflow AT 1/2BT2 1/3CT3
58.08 Aseton 776.8987 4434.103 43063.752206181 -5.87E+02
18.02 Air 2530.3939 8707.123 -178.9383564377 -5.95E+01
98.14 MO 7924.5605 11853.41 2401.3527433935 -4.06E+02
116.16 DAA 0.0000 14574.24 3825.2547147463 -6.66E+02
98.08 SULFAT 0.0000 2459.67 3146.4967941891 -3.92E+02
TOTAL 11231.8531
Htop 681829.2
Hin cd 702787.8
Qcd -20958.65

INPUT OUTPUT
Komponen H, kkal/jam KomponenH, kkal/jam
ASETON 150165.549682769 TOP
AIR 119283.364029795 Aseton 143288.92038779
MO 0 Air 277838.7560183
DAA 385410.790736845 MO 260701.4792846
SULFAT 28809.3999494848 Bottom
Qcd MO 6317.2363705816
DAA 91719.586200408
SULFAT 86685.543445932
Qrb 114664.39824538
TOTAL 683669.104398893 TOTAL 981215.919953
SELISIH

NPNYA ADA REAKSINYA GATAU WEH


Persamaan Antoine
TEKANAN UAP TEKANAN UAP
B C Komponen A B C
1315.6735 240.479 Air 8.05573 1723.643 233.08
1723.6425 233.08 MO 7.12851 1483.486 219.745
1527.2068 223.816 DAA 8.62593 2568.756 279.12
1483.4864 219.745 Asam Sulfat 8.28538 2976.837 213.95
2568.7558 279.12 Aseton 7.31742 1315.674 240.479
2976.837 213.95

Hasil Atas Hasil Bawah


kmol/jam Ratio kg/jam kmol/jam
518.698202 119.836579168024 H2O = 0 0
85.7402741 25359.3153372532 C6H10O = 42.2842 0.430856
0.095366736 0.0999916253922224 C6H12O2 = 1096.794 9.442098
0 H3PO4 = 1117.41 11.39284

REAKSI Yield
DAA = 85.8372580922865 DAA =
MO = 85.83302832688 Total 257.5305 MO =
Air = 85.860244173141 Air =

Hasil Bawah MO 0.00500000313


0.50000031336
Hasil Atas Hasil Bawah
kmol/jam Ratio kg/jam kmol/jam
#REF! H2O = 0
#REF! C6H10O = 0
#REF! C6H12O2 =
H3PO4 =

Cara Hitung Hidrogen masih bingung

Hasil atas 97%


Hasil bawah 3%

Bottom
xb
0.0000 1.4042141248118
0.0000
0.6998
0.0248
0.2754 0
1.0000

Kondisi Bawah (Bottom)


P= 1.4 atm
T= 223.12910951382 oC
Komponen B,kmol/jam B, kg/jam Po xb Ki

Air 0.0000 0.0000 24.930513 0.0000 17.80751


Aseton 0.0000 0.0000 39.692304 0.0000 28.35165
Katalis Asam Sulfat 23.0269 2258.4803 0.0392478 0.6998 0.028034
MO 0.8156 80.0461 7.9070911 0.0248 5.647922
DAA 9.0626 1052.7083 4.2718006 0.2754 3.051286
Total 32.9051 1

pasitas Panas
E Cp @25C
0 127.53
0 75.55
0 213.3
0 233.58 1 joule 0.239006 cal
0 139.95 R 1
INPUT
K
1/4DT4 E/2T2 Cp dt molflow (kmol/j H = N Cp dtH(kkal/jam)
5.92E+01 0 46970.3416007418 13.3763550536 628292 150165.5
1.07E+01 0 8479.36964361267 58.8582719107 499081 119283.4
4.02E+01 0 13888.7741910241 0 0 0
5.98E+01 0 17793.5923164727 90.625711745 1612557 385410.8
2.06E+01 0 5234.67298765617 23.0269200385 120538.4 28809.4
2860468 683669.1

DISTILAT
K

1/4DT4 E/2T2 Cp dt molflow (kmol/j H = N Cp dtH(kkal/jam)


5.37E+01 0 44819.3980072943 13.3763550536 599520.2 143288.9
9.70E+00 0 8.28E+03 140.421412481 1162476 277838.8
3.64E+01 0 1.35E+04 80.7475091648 1090774 260701.5
5.42E+01 0 1.73E+04 0 0 0
1.87E+01 0 5.11E+03 0 0 0
2852770 681829.2

BOTTOM
K

1/4DT4 E/2T2 Cp dt molflow (kmol/j H = N Cp dtH(kkal/jam)


1.14E+03 0 193980.573383227 0 0 0
2.06E+02 0 17112.3566842867 0 0 0
7.74E+02 0 3.24E+04 0.8156314057 26431.29 6317.236
1.15E+03 0 4.23E+04 9.0625711745 383754.3 91719.59
3.97E+02 0 1.58E+04 23.0269200385 362691.9 86685.54
772877.5 184722.4

Hin Reboiller
K

1/4DT4 E/2T2 Cp dt molflow (kmol/j H = N Cp dtH(kkal/jam)


5.92E+01 0 46970.3416007418 0 0 0
1.07E+01 0 8.48E+03 0 0 0
4.02E+01 0 13888.7741910241 0.8156314057 11328.12 2707.489
5.98E+01 0 17793.5923164727 9.0625711745 161255.7 38541.08
2.06E+01 0 5234.67298765617 23.0269200385 120538.4 28809.4
293122.2 70057.97
in kondenser
K

1/4DT4 E/2T2 Cp dt molflow (kmol/j H = N Cp dtH(kkal/jam)


5.92E+01 0 46970.3416007418 13.3763550536 628292 150165.5
1.07E+01 0 8479.36964361267 140.421412481 1190685 284580.9
4.02E+01 0 13888.7741910241 80.7475091648 1121484 268041.4
5.98E+01 0 17793.5923164727 0 0 0
2.06E+01 0 5234.67298765617 0 0 0
2940461 702787.8
Bawah Perbandingan Atas Bawah %
Ratio Ratio Bawah Ratio Atas
0 H2O = 0 100
127.4338 C6H10O = 0.5000003134 99.499999687
9.9 C6H12O2 = 99.000082952 0.9999170482
H3PO4 = 100 0

0.333309
0.333293
0.333398
Sementara gk make
Bawah Recycle Masuk dari MD-2
Ratio kg/jam kmol/jam Ratio
#REF! H2O = 0 #DIV/0!
#REF! C6H12O = 35.2293 #DIV/0!
#REF! C6H10O = 655.295 #DIV/0!
Ni = 0 #DIV/0!
Yi

0
0
0.019618
0.139997
0.840371
0.999986
Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu


Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000 ton/tahun

Hasil MD-02 Kating

Feed
kg/jam kmol/jam
C3H6O = 3436.54 59.16907713499
H2O = 9346.9416 518.6982019978
C6H10O = 8414.5505 85.74027409823
C6H12O2 = 11.0778 0.095366735537

Hasil MD-02 Yosua


- DAA udah hilang di RD jadi di MD-2 gk
Asumsi perlu pisahin

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.1
T avg = 115.9465040322

Komponen F,kmol/jam
Komponen F,kmol/jam

Air 140.4214
Aseton 13.3764
MO 80.7475
Total 234.5453

Kondisi Atas (Distilat)


P= 1
T = 96.65315219019

Komponen D,kmol/jam

Air 139.0172
Aseton 13.3764
MO 2.4224
Total 154.8160

Mass Balance

Bahan
Air
Aseton
MO
SubTotal
Total
Inpt - Output

Neraca Panas

Komponen
Aseton
Air
MIBK
MO
DAA
Asam sulfat

T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total

T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total

T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total

T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total
T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total

Htop
Hin cd
Qcd

INPUT
Komponen
ASETON
AIR
MO
Q-RB

TOTAL
SELISIH
Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802

Hasil Atas
kg/jam kmol/jam
C3H6O = 3436.54 59.1690771349862
H2O = 9066.5334 503.137258601554
C6H10O = 42.0728 0.42870185449358
C6H12O2 = 0 0

HK di D =
LK di B =

Distillat
F, kg/jam Po alfa
F, kg/jam Po alfa
D xd
2530.3939 1.7238033517788 2.5585 139.0172 0.8980
776.8987 5.56296469857533 8.2567 13.3764 0.0864
7924.5605 0.673753229772902 1.0000 2.4224 0.0156
154.8160 1.0000

atm
o
C

D, kg/jam Po yd Ki Xi

2505.0899 0.886197043884412 0.8980 0.88619704388441 1.01326362503016


776.8987 3.42027555040257 0.0864 3.42027555040257 0.02526160321963
237.7368 0.362265353158286 0.0156 0.36226535315829 0.04319244672503
1 1.08171767497482

Input Output
Feed Distilat Bottom
2530.3939 2505.0899 25.3039
776.8987 776.8987 0.0000
7924.5605 237.7368 7686.8237
11231.8531 3519.7254 7712.1277
11231.853103851 11231.8531
0

Kapasitas Panas
A B C D E
46.878 9.6265 -2.08E-03 2.96E-06 0
92.053 -0.04 -2.11E-04 5.35E-07 0
126.633 0.5726 -1.63E-03 2.38E-06 0
125.316 0.5368 -1.44E-03 2.01E-06 0
154.081 0.8551 -2.36E-03 2.99E-06 0
26.004 0.70337 -1.39E-03 1.03E-06 0
INPUT
115.94650403222 C = 389.096504032225 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4
776.8987 4263.39021602263 39811.67394167 -5.22E+02 5.06E+01
2530.3939 8371.89853567838 -165.4253319137 -5.29E+01 9.15E+00
7924.5605 11516.8286451127 2368.063626344 -4.09E+02 4.07E+01
11231.8531

DISTILAT
96.653152190194 C = 369.803152190194 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4
776.8987 3358.95646837189 24712.0640586 -2.55E+02 1.95E+01
2505.0899 6595.88761856388 -102.6834843758 -2.59E+01 3.53E+00
237.7368 9073.65362130078 1469.91407884 -2.00E+02 1.57E+01
3519.7254

BOTTOM
135.2399 C = 408.389855874256 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4
0.0000 5167.82396367336 58494.58889341 -9.29E+02 1.09E+02
25.3039 10147.9094527929 -243.0565164635 -9.42E+01 1.98E+01
7686.8237 13960.0036689246 3479.354033175 -7.28E+02 8.79E+01
7712.1277

Hin reboiler
115.9465 C = 389.096504032225 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4
0.0000 278950.253649995 50871112.3567 -7.39E+07 -1.95E+09
25.3039 873602.41283596 69981006.27971 1.06E+09 -1.51E+10
7686.8237 1238197.86736938 0 0.00E+00 0.00E+00
7712.1277 CP MIRIP FEED

Hbot 317785.201380835
Hin rb 255777.757450869
Qrb 62007.4439299657
Hin kondenser
115.9465 C = 389.096504032225 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4
776.8987 388014.024381997 0 0.00E+00 0.00E+00
2505.0899 0 0 0.00E+00 0.00E+00
237.7368 0 0 0.00E+00 0.00E+00
3519.7254 CP MIRIP FEED

309988.88209062
418443.55759556
108454.67550494

INPUT OUTPUT
H, kkal/jam Komponen H, kkal/jam
139403.69048977 TOP
273953.47746781 ASETON 88990.78705171
260864.14708886 AIR 215000.2871004
62007.443929966 MO 5997.807938488
BOTTOM
AIR 3299.228641876
MO 314485.972739
QCD 108454.6755049
736228.75897639 total 736228.7589764
SELISIH 0
Persamaan Antoine
TEKANAN UAP TEKANAN UAP
B C Komponen A B
1315.674 240.479 Aseton 7.31742 1315.6735
1723.643 233.08 Air 8.05573 1723.6425
1527.207 223.816 MO 7.12851 1483.4864
1483.486 219.745
2568.756 279.12
2976.837 213.95

Hasil Bawah
ratio kg/jam kmol/jam ratio
100 C3H6O = 0 0 0
97 H2O = 280.4082 15.56094339623 2.99999948646
0.500001 C6H10O = 8372.4778 85.311573262686 99.5000006239
0 C6H12O2 = 11.0778 0.095366735537 100

0.01 Hasil atas 97%


0.01 Hasil bawah 3%

Bottom
B xb
1.4042 0.0176 1.404214124812
0.0000 0.0000
78.3251 0.9824 45.40292336891
79.7293 1.0000

Kondisi Bawah (Bottom)


P= 1.2 atm
T = 135.239855874256 oC

Komponen B,kmol/jam B, kg/jam Po

Air 1.4042 25.3039 3.1273232664835


Aseton 0.0000 0.0000 8.6070914467624
MO 78.3251 7686.8237 1.171340618344
Total 79.7293

Cp @25C
127.53
75.55
212.42
213.3
233.58 1 joule 0.239006 cal
139.95

E/2T2 Cp dt molflow (kmol/jam) H = N Cp dt (KJ/j H(kkal/jam)


0 43604.1354128225 13.3763550535568 583264.3970853 139403.6904898
0 8162.7158140996 140.42141248118 1146220.084298 273953.4774678
0 13516.8799352937 80.7475091647632 1091454.386454 260864.1470889
Total 65283.7311622159 234.5452766995 2820938.867838 674221.3150464

E/2T2 Cp dt molflow (kmol/jam) H = N Cp dt (KJ/j H(kkal/jam)


0 27835.4634333092 13.3763550535568 372337.0419642 88990.78705171
0 6470.85553981384 139.017198356368 899560.2081137 215000.2871004
0 10359.3704084707 2.4224252749429 25094.80070998 5997.807938488
Total 44665.6893815938 154.815978684867 1296992.050788 309988.8820906

E/2T2 Cp dt molflow (kmol/jam) H = N Cp dt (KJ/j H(kkal/jam)


0 62842.8277950064 0 0 0
0 9830.37925209034 1.4042141248118 13803.95739804 3299.228641876
0 16799.3162846639 78.3250838898203 1315807.857288 314485.972739
Total 89472.5233317607 79.7292980146321 1329611.814686 317785.2013808

E/2T2 Cp dt molflow (kmol/jam) H = N Cp dt (KJ/j H(kkal/jam)


0 43604.1354128225 0 0 0
0 8162.7158140996 1.4042141248118 11462.20084298 2739.534774678
0 13516.8799352937 78.3250838898203 1058710.754861 253038.2226762
Total 65283.7311622159 79.7292980146321 1070172.955703 255777.7574509
E/2T2 Cp dt molflow (kmol/jam) H = N Cp dt (KJ/j H(kkal/jam)
0 43604.1354128225 13.3763550535568 583264.3970853 139403.6904898
0 8162.7158140996 139.017198356368 1134757.883455 271213.9426931
0 13516.8799352937 2.4224252749429 32743.63159362 7825.9244126657
Total 65283.7311622159 154.815978684867 1750765.912134 418443.5575956
UAP
C
240.479
233.08
219.745
xb Ki Yi

0.0176 2.606103 0.045899


0.0000 7.172576 0
0.9824 0.976117 0.958926
1 1.004825
Data Komponen
Komponen Komponen Mr Tb, oC
Aseton C3H6O 58.08 56.2
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02 100
Diaseton Alkohol C6H12O2 116.16 167.9
Asam Sulfat (Katalis 2) H2SO4 98.08 270
Gas Hidrogen H2 2.016 -252.8
Mesitil Oksida (MO) C6H10O 98.14 125
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16 115.9

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George


Kapasitas Pabrik = 65000 ton/tahun

Hasil TH-02 Kating

Feed
kg/jam kmol/jam
Urut H2O = 280.4082 15.560943396226
Berdasarkan C6H12O = 0 0
Titik Didih C6H10O = 8372.4778 85.311573262686
C6H12O2 = 11.0778 0.0953667355372
Ni = 1285.7694 12.837154552716
H2 = 168.8556 83.757738095238

MO H2 MIBK
M 93.6748624414102
R 84.3073761972692 18.9421934912
S 9.36748624414102 103.2495696885

Konversi 90 %

Hasil TH-02 Yosua


Asumsi - ayo
Feed (Biasa)
kg/jam kmol/jam
H2O = 25.3039385291 1.4042141248118
C6H12O = 0 0
C6H10O = 7686.82373295 78.32508388982
Ni = 88.035 1.5
H2 = 145.005094207 71.927130063207

Input MO 65.2245562216422
Recycle MO 1.43569400205373

MO H2 MIBK
M 79.760777891874 71.9271300632 15.757617095712
R 71.7847001026866 71.9271300632 71.784700102687
S 7.9760777891874 87.542317198398

Konversi 90 %

Mass Balance

Input
Bahan
Feed
H2O 25.3039
C6H12O 0.0000
C6H10O 7686.8237
Ni 88.0350
H2 145.0051
SubTotal 7945.1678
Total 10462.2192
Inpt - Output 0
Sg, tidak ada satuan
0.79

1
0.9387
1.84
0.0696
0.855
1.94
0.802

Hasil ke MD-2
kg/jam kmol/jam
H2O = 341.9613 18.97676470588
C6H12O = 10341.4769 103.2495696885
C6H10O = 919.3251 9.367486244141
DAA C6H12O2 = 110.7877 0.953750860882
Ni = 1285.7694 12.83715455272
H2 = 0 0

Cek Jumlah MO
93.6748654982678
sa) Hasil ke TH-2
kg/jam kmol/jam
H2O = 30.85846162086 1.71245624977
C6H12O = 8768.238490592 87.5423171984
C6H10O = 782.7722742309 7.976077789187
Asumsi Ni = 880.35 15
Goal Seek H2 = 0

Cek Jumlah MO Nikel Ratio


0 1.5 0.224599657507
13.5 Asumsi Reaksi 1 : 1 kecuali H2
15

Cara Hitung Hidrogen masih


- kalau olin perbadningan gitu

Tsistem
Output
Recycle TH-2 120 C
5.5545 30.8585 393.15
1578.2829 8768.2385 393.15
140.8990 782.7723 393.15
792.3150 880.3500 393.15
0.0000 0.0000 393.15
2517.0515 10462.2192
10462.2192 10462.2192
0
2 Recycle Masuk dari TH-2
Ratio kg/jam kmol/jam Ratio
121.95124821599 H2O = 61.553 3.41581576 17.999990057
#DIV/0! C6H12O = 1861.4658 18.5849221 17.999999594
10.980322933791 C6H10O = 165.4785 1.68614734 17.999998042
1000.0875625124 C6H12O2 = 19.94 0.17165978 17.998387908
100 Ni = 1157.1925 11.5534395 90.000003111
0
2 Recycle Masuk dari TH-2
Ratio kg/jam kmol/jam Ratio
121.9512195122 H2O = 5.55452309176 0.30824212 100
#DIV/0! C6H12O = 1578.28292831 15.7576171
10.183299389002 C6H10O = 140.899009362 1.435694 100
1000 Ni = 792.315 13.5 100
0 H2 = 0 0

Hitung Hidrogen masih bingung


u olin perbadningan gitu
Recycle Masuk dari MD-2
kg/jam kmol/jam Ratio
H2O = 0 0 0
C6H12O = 35.2293 0.35173023163 0.34066023974
C6H10O = 655.295 6.67714489505 71.280007475
C6H12O2 = 79.7672 0.68670110193 72.0000505471
Ni = 0 0 0

Sementara gk make
Recycle Masuk dari MD-2
kg/jam kmol/jam Ratio
H2O = 0
C6H12O = #REF!
C6H10O = 0
Ni = 0
H2 = 0 0
Feed Awal + Recycle
kg/jam kmol/jam
H2O = 30.8584616209 1.7124562498 555.5556
C6H12O = 1578.28292831 15.757617096
C6H10O = 7827.72274231 79.760777892 5555.556
Ni = 0 0 0
H2 = 0 0
MO
Itungan Coba Coba misal F = 7.9760778

A= 78.3250838898203
Mula-Mula A+R= 79.760777891874
R Reaksi = 71.7847001026866
S F= 7.9760777891874

F-F= 0

R= 1.43569400205373

Reaksi MO
M 79.760777891874
Konveri 90% R 71.7847001026866
S 7.9760777891874
MIBK
Itungan Coba Coba misal F = 87.5423171984

A= 15.7576170957117
R1 Gk ada 0
R2 0,9 x 0,2 x F = 15.7576170957117
Reaksi Reaksi = 71.7847001026866 karena reaksi 1:2
F= 87.5423171983983

F-F= 0
Air Katalis Nikel
Itungan Coba Coba misal F = 1.71245624977 Itungan Coba Coba

A= 1.4042141248118 A=
R1 Gk ada 0 R1 Gk ada
R2 0,9 x 0,2 x F = 0.30824212495869 R2 0,9 x F =
F= 1.71245624977049 F=

F-F= 0 F-F=
misal F = 15

1.5
0
13.5
15

0
Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu


Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000

Hasil TH-02 Kating

Feed
kg/jam
Urut H2O = 341.9631
Berdasarkan C6H12O = 10341.4769
Titik Didih C6H10O = 919.3251
C6H12O2 = 110.7877
Ni = 1285.7694

Hasil TH-02 Yosua


Asumsi - ayo

Komponen F, kmol/jam

Air 1.7125
MO 7.9761
MIBK 87.5423
Nikel 15.0000
Mass Balance

Bahan
Air
MO
MIBK
Nikel
SubTotal
Total
Inpt - Output
Tb, oC Sg, tidak ada satuan TEKANAN U
56.2 0.79 Komponen
Aseton
100 1 Air
167.9 0.9387 MIBK
270 1.84 MO
-252.8 0.0696 DAA
125 0.855 Asam Sulfat
1.94
115.9 0.802

ton/tahun

Feed Hasil ke MD
kmol/jam
18.9768645949 H2O =
103.249569688 C6H12O =
9.36748624414 C6H10O =
0.95375086088 C6H12O2 =
21.9078105299 Ni =

F, kg/jam D, kmol/jam D, kg/jam R + P, kmol/jam R, kmol/jam

30.8585 1.36996499981639 24.6868 0.3425 0.3082


782.7723 6.38086223134992 626.2178 1.5952 1.4357
8768.2385 70.0338537587186 7014.5908 17.5085 15.7576
880.3500 0 0.0000 15.0000 13.5000
Input Output
Feed Recycle Purge Output ke MD-01
30.8585 5.5545 0.6172 24.6868
782.7723 140.8990 15.6554 626.2178
8768.2385 1578.2829 175.3648 7014.5908
880.3500 792.3150 88.0350 0.0000
10462.2192264 2517.05146075979 279.672384528866 7665.495381155
10462.2192264 10462.2192
0
Persamaan Antoine
TEKANAN UAP TEKANAN UAP
A B C KomponenA B
7.31742 1315.6735 240.479 Air 8.05573 1723.6425
8.05573 1723.6425 233.08 MO 7.12851 1483.4864
7.37701 1527.2068 223.816 MIBK 7.37701 1527.2068
7.12851 1483.4864 219.745
8.62593 2568.7558 279.12
8.28538 2976.837 213.95

Hasil ke MD-2 Hasil Recycle + Purge


kg/jam kmol/jam Ratio kg/jam
273.569 15.18140954495 80 H2O = 68.3923
8273.1816 82.59965654952 80 C6H12O = 2068.2954
735.4601 7.493989199103 80 C6H10O = 183.865
88.622 0.762930440771 80 C6H12O2 = 22.1555
0 0 0 Ni = 1285.7694

R, kg/jam P, kmol/jam P, kg/jam

5.5545 0.0342 0.6172


140.8990 0.1595 15.6554
1578.2829 1.7508 175.3648 8768.238 kg/jam yg wajib
792.3150 1.5000 88.0350
UAP
C
233.08
219.745
223.816

il Recycle + Purge Hasil Recycle


kmol/jam Ratio kg/jam kmol/jam
3.79535516093 20 H2O = 61.553 3.41581576
20.6499141374 20 C6H12O = 1861.4658 18.58492212
1.87349704504 20 C6H10O = 165.4785 1.686147341
0.19073261019 20 C6H12O2 = 19.94 0.17165978
21.9078105299 100 Ni = 1157.1925 19.71703016
cle Hasil Purging
Ratio kg/jam kmol/jam Ratio
90 H2O = 6.8393 0.37953940067 10
90 C6H12O = 206.8296 2.06499201278 10
90 C6H10O = 18.3865 0.1873497045 10
90 C6H12O2 = 2.2155 0.01907283058 10
90 Ni = 128.5769 2.19078037144 10
Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu


Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000 ton/tahun

Hasil MD-02 Kating

Feed
kg/jam kmol/jam
H2O = 273.569 15.1814095449501
C6H10O = 735.4601 7.49398919910332
C6H12O = 8273.1816 71.2222933884298
C6H12O2 = 88.622 0.884804313099042

Hasil MD-02 Yosua


- DAA udah hilang di RD jadi di MD-2 gk
Asumsi perlu pisahin

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.2
T avg = 127.924577288968

Komponen F,kmol/jam
Komponen F,kmol/jam

Air 1.3700
MO 6.3809
MIBK 70.0339
Total 77.7847

Kondisi Atas (Distilat)


P= 1.1
T= 118.790829736173

Komponen D,kmol/jam

Air 1.3289
MO 0.0000
MIBK 69.3335
Total 70.6624

Kemurnian MIBK

Mass Balance

Bahan
Air
MO
MIBK
SubTotal
Total
Inpt - Output
HEAT BALANCE

Komponen
Aseton
Air
MIBK
MO
DAA
Asam sulfat
T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total

T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total

T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total

Hreboiler

T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total

T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total

Input OUTPUT
Komponen H, kkal/jam Komponen
AIR 3012.67225577731 TOP
MIBK 260131.834135855 AIR
MO 23294.4690717126 MIBK
Q-RB 2623.41701711823 BOTTOM
Air
MIBK
MO
QCD
TOTAL 289062.392480463 total
SELISIH 0
Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A B
Aseton 7.31742 1315.674
100 1 Air 8.05573 1723.643
167.9 0.9387 MIBK 7.37701 1527.207
270 1.84 MO 7.12851 1483.486
-252.8 0.0696 DAA 8.62593 2568.756
125 0.855 Asam Sulfat 8.28538 2976.837
1.94
115.9 0.802

Hasil Atas
kg/jam kmol/jam ratio
H2O = 273.569 15.1814095449501 100
C6H10O = 7.3546 0.07493988180151 1
C6H12O = 8231.8156 70.8661811294766 99.5
C6H12O2 = 0 0 0

HK di D = 0.01
LK di B = 0.01

Distillat Bottom
F, kg/jam Po alfa
F, kg/jam Po alfa
D xd B
24.6868 2.51387675833351 2.6278 1.3289 0.0188 0.0411
626.2178 0.956649901855592 1.0000 0.0000 0.0000 6.3809
7014.5908 1.42672671785737 1.4914 69.3335 0.9812 0.7003
70.6624 1.0000 7.1223 1.0000

atm
o
C

D, kg/jam Po yd Ki Xi

23.9462 1.88976237627259 0.0188 1.71796579661144 0.0109465792165


0.0000 0.733888796543892 0.0000 0.66717163322172 0
6944.4449 1.09292115194129 0.9812 0.99356468358299 0.98754934382105
1 0.99849592303755
69.3335 6944.44488454853
0.996563602 55000003.48562 55000.0034856243

Input Output
Feed Distilat Bottom
24.6868 23.9462 0.7406
626.2178 0.0000 626.2178
7014.5908 6944.4449 70.1459
7665.495381 6968.3911 697.1043
7665.495381 7665.4954
0

Kapasitas Panas
A B C D E Cp @25C
46.878 9.6265 -2.08E-03 2.96E-06 0 127.53
92.053 -0.04 -2.11E-04 5.35E-07 0 75.55
126.633 0.5726 -1.63E-03 2.38E-06 0 212.42
125.316 0.5368 -1.44E-03 2.01E-06 0 213.3
154.081 0.8551 -2.36E-03 2.99E-06 0 233.58
26.004 0.70337 -1.39E-03 1.03E-06 0 139.95
INPUT
127.9245773 C = 401.074577288968 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
24.6868 9474.51611318139 -211.8693722023 -7.67E+01 1.50E+01 0
7014.5908 13033.6479958339 3032.910063075 -5.92E+02 6.68E+01 0
626.2178 12898.0963275443 2843.286974954 -5.23E+02 5.64E+01 0
7665.4954 Total

DISTILAT
118.7908 C = 391.9408 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
23.9462 8633.72724970391 -175.934394852 -5.80E+01 1.03E+01 0
6944.4449 11877.0141419808 2518.500862306 -4.48E+02 4.60E+01 0
0.0000 11753.4916192182 2361.039578914 -3.96E+02 3.89E+01 0
6968.3911 Total

BOTTOM
137.0583 C = 410.2083 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
0.7406 10315.3049766589 -251.1413633268 -9.90E+01 2.11E+01 0
70.1459 14190.281849687 3595.088616024 -7.65E+02 9.38E+01 0
626.2178 14042.7010358704 3370.317095846 -6.75E+02 7.92E+01 0
697.1043 Total

Hin reboiler
127.9246 C = 401.0746 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
0.7406 70172.9198263094 80981137.40051 1.33E+09 -2.06E+10 0
70.1459 858982.571494464 0 0.00E+00 0.00E+00 0
626.2178 0 0 0.00E+00 0.00E+00 0
697.1043 GAK KUITUNG KARNA CP/Rnya mirip feed Total
Hin reboiler 25986.1675807444
Qreboiler 2623.41701711823

Hin kondense
127.9246 C = 401.0746 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
23.9462 780866.22799121 0 0.00E+00 0.00E+00 0
6944.4449 0 0 0.00E+00 0.00E+00 0
0.0000 0 0 0.00E+00 0.00E+00 0
Hin reboiler GAK KUITUNG KARNA CP/Rnya mirip feed Total

Hin kondenser 260452.8078826


Qkondenser 25897.2990797397

OUTPUT
H, kkal/jam
TOP
2671.110766
231884.398

98.09424116
2864.738061
25646.7523
25897.29908
289062.3925
0
Persamaan Antoine
N UAP TEKANAN UAP
C Komponen A B
240.479 Air 8.05573 1723.6425
233.08 MO 7.12851 1483.4864
223.816 MIBK 7.37701 1527.2068
219.745 DAA
279.12
213.95

Hasil Bawah
kg/jam kmol/jam ratio
H2O = 0 0 0
C6H10O = 728.1055 7.41904931730181 99.000000136
C6H12O = 41.366 0.356112258953168 0.50000111203
C6H12O2 = 88.622 0.884804313099042 100

Bottom
xb
0.0058
0.8959
0.0983

Kondisi Bawah (Bottom)


P= 1.3 atm
T = 137.058324841764 oC

Komponen B,kmol/jam B, kg/jam Po

Air 0.0411 0.7406 3.297342768104


MO 6.3809 626.2178 1.2302171814358
MIBK 0.7003 70.1459 1.8375255270973
Total 7.1223 1

1 joule 0.239006 cal


R 1
Cp dt Cpdt (kJ/kmol) molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)
9200.96995465879 9200.96995465879 1.36996499981639 12605.0068022448 3012.67225578
15540.9181992349 15540.9181992349 70.0338537587186 1088390.39244142 260131.834136
15274.4170712528 15274.4170712528 6.38086223134992 97463.9509958435 23294.4690717
40016.3052251465 40016.3052251465 77.784680989885 1198459.35023951 286438.975463

Cp dt Cpdt (kJ/kmol) molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)


8410.11410229757 8410.11410229757 1.3288660498219 11175.9151056716 2671.11076575
13993.2794001364 13993.2794001364 69.3335152211315 970203.250282899 231884.398037
13757.3910040073 13757.3910040073 0 0 0
36160.7845064412 36160.7845064412 70.6623812709534 981379.165388571 234555.508803

Cp dt Cpdt (kJ/kmol) molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)


9986.28558511066 9986.28558511066 0.041098949994492 410.425851893177 98.0942411576
17114.6526562867 17114.6526562867 0.700338537587186 11986.0508126164 2864.73806052
16816.8327807369 16816.8327807369 6.38086223134992 107305.893141531 25646.7522962
43917.7710221342 43917.7710221342 7.1222997189316 119702.369806041 28609.5845979

Cp dt Cpdt (kJ/kmol) molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)


9200.96995465879 9200.96995465879 0.041098949994492 378.150204067343 90.3801676733
15540.9181992349 15540.9181992349 0.700338537587186 10883.9039244142 2601.31834136
15274.4170712528 15274.4170712528 6.38086223134992 97463.9509958435 23294.4690717
40016.3052251465 40016.3052251465 7.1222997189316 108726.005124325 25986.1675807
Cp dt Cpdt (kJ/kmol) molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)
9200.96995465879 9200.96995465879 1.3288660498219 12226.8565981774 2922.2920881
15540.9181992349 15540.9181992349 69.3335152211315 1077506.48851701 257530.515794
15274.4170712528 15274.4170712528 0 0 0
40016.3052251465 40016.3052251465 70.6623812709534 1089733.34511519 260452.807883
C
233.08
219.745
223.816
xb Ki Yi

0.0058 2.536418 0.014636


0.8959 0.946321 0.847808
0.0983 1.413481 0.138988
1.0014325516
Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu


Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000 ton/tahun

Hasil MD-02 Kating

Feed
kg/jam kmol/jam
H2O = 0
C6H12O = 0

Hasil MD-04 Yosua


- DAA udah hilang di RD jadi di MD-2 gk
Asumsi perlu pisahin

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.1
T avg = 118.7908297362

Komponen F,kmol/jam

Air 1.3289
MIBK 69.3335
Total 70.6624

Kondisi Atas (Distilat)


P= 1
T = 99.99861302985

Komponen D,kmol/jam

Air 1.3289
MIBK 0.0000
Total 1.3289

Mass Balance

Bahan
Air
MIBK
SubTotal
Total
Inpt - Output
Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A B
Aseton 7.31742 1315.674
100 1 Air 8.05573 1723.643
167.9 0.9387 MIBK 7.37701 1527.207
270 1.84 MO 7.12851 1483.486
-252.8 0.0696 DAA 8.62593 2568.756
125 0.855 Asam Sulfat 8.28538 2976.837
1.94
115.9 0.802

Hasil Atas
kg/jam kmol/jam ratio
H2O = 0 #DIV/0!
C6H12O = 0 #DIV/0!

HK di D = 0.01
LK di B = 0.01

Distillat Bottom
F, kg/jam Po alfa
D xd B
23.9462 1.88976237627259 1.7291 1.3289 1.0000 0.0000
6944.4449 1.09292115194129 1.0000 0.0000 0.0000 69.3335
1.3289 1.0000 69.3335 1.0000

atm
o
C

D, kg/jam Po yd Ki Xi

23.9462 1.00007936225664 1.0000 1.00007936225664 0.99992064404123


0.0000 0.602416129241516 0.0000 0.60241612924152 0
1 0.99992064404123

Input Output
Feed Distilat Bottom
23.9462 23.9462 0.0000
6944.4449 0.0000 6944.4449
6968.391051 23.9462 6944.4449
6968.391051 6968.3911
0
Persamaan Antoine
N UAP TEKANAN UAP
C Komponen A B C
240.479 Air 8.05573 1723.6425 233.08
233.08 MO 7.12851 1483.4864 219.745
223.816 MIBK 7.37701 1527.2068 223.816
219.745 DAA
279.12
213.95

Hasil Bawah
kg/jam kmol/jam ratio
H2O = 0 #DIV/0!
C6H12O = 0 #DIV/0!

Bottom
xb
0.0000
1.0000

Kondisi Bawah (Bottom)


P= 1.2 atm
T = 121.941382857938 oC

Komponen B,kmol/jam B, kg/jam Po xb

Air 0.0000 0.0000 2.0887086115368 0.0000


MIBK 69.3335 6944.4449 1.2000703455305 1.0000
Total 69.3335 kmol/jam 1

6944.44488454853 kg/jam
166666.677229165 kg/hari
55000003.4856243 kg/tahun 330 hari
55000.0034856243 ton/tahun
Ki Yi

1.740591 0
1.000059 0.999941

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