FIX BANGET NM SAMA NP 4 Desember 2022 21.20

Data Komponen
Komponen Komponen Mr Tb, oC

Aseton C3H6O 58.08 56.2
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02 100
Diaseton Alkohol C6H12O2 116.16 167.9
Asam Sulfat (Katalis 2) H2SO4 98.08 270
Gas Hidrogen H2 2.016 -252.8
Mesitil Oksida (MO) C6H10O 98.14 125
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16 115.9
Punya Kating Dulu
Asumsi Punya Pak Sarto, Mas George

Kapasitas Pabrik = 65000 ton/tahun
Hasil TH-02 Kating
Feed (Murni)
kg/jam kmol/jam
Urut C3H6O = 14584.5912 251.11210743802
Berdasarkan
H2O = 607.5822 33.717103218646
Titik Didih
C6H10O = 0 0
Ba(OH)2 = 26.8487 0.156698377495
C6H12O2 = 0 0
2 Aseton ---------> 1 DAA

M 1777.23969869146 21.686956783747
R 195.062892561984 97.531446280992
S 1972.30259125344 119.21840306474
Konversi 15 %
Hasil TH-02 Yosua

Asumsi - ayo
Asumsi
H2O = 562.891847917 31.237061482612
Feed (Biasa)
kg/jam kmol/jam
562.8918 C3H6O = 13509.40435 232.59993715565
H2O = 562.891847917 31.237061482612
C6H10O = 0 Gk ada
Ba(OH)2 = 24.8693273739 0.145146068483
C6H12O2 = 0 0
Input MO 65.2245562216422
Recycle MO Gk ada
2 Aseton ---------> 1 DAA

M 1857.82697408664 20.390783861927
R 185.782697408664 92.891348704332
S 1672.04427667798 113.28213256626
Konversi 10 %
Mass Balance
I
Bahan
Hf, kj/mol Hf,kj/kmol Feed
-217.1 -217100 C3H6O 13509.40435
-241.8 -241800 H2O 562.89184791667
0 0 Ba(OH)2 24.869327373872
-545.8 -545800 C6H12O2 0
SubTotal 14097.165525291
Total 111219
Inpt - Output
Cp (J/mol.K) =A+B*T+C*T^2
A B C
Ni 26 -1,34,E-02 4,77,E-05
Cp (J/mol.K) = A + B*T + C*T^2 + D*T^3 + E*T^4
A B C
H2 25 2,02,E-02 -3,85,E-05
Komponen A B C
Aseton 46.878 9.6265 -2.08E-03
Air 92.053 -0.04 -2.11E-04
DAA 154.081 0.8551 -2.36E-03
NERAC
Tinput 15 288.15
Toutput 30 303.15
Mr Komponen massflow (kg/jam) molflow (kmol/j AT
58.08 Aseton 107902.590654952 1857.82697409 468.78
18.02 Air 700.114238702322 38.8520665207 920.53
116.16 DAA 2368.59345340139 20.3907838619 1540.81
NERAC
Tinput 15 288.15
Toutput 30 303.15
58.08 Aseton 97112.3315894569 1672.04427668 234.39
18.02 Air 700.114238702322 38.8520665207 460.265
116.16 DAA 13158.8525188966 113.282132566 770.405
NERACA P
15 288.15
Toutput 30 303.15
58.08 Aseton 107902.590654952 1857.82697409 -234.39
18.02 Air 700.114238702322 38.8520665207 -460.265
116.16 DAA 2368.59345340139 20.3907838619 -770.405
Hr,298
392204946.24237
H1 Tref-Tout
H2 Tout-Treact
Sg, tidak ada satuan
0.79
1
0.9387
1.84
0.0696
0.855
1.94
0.802
rni) Hasil k
Ratio
11.5860527129905 C3H6O =
3.46525361240887 H2O =
0 C6H10O =
9.04526862379597 Ba(OH)2 =
0 C6H12O2 =
Katalis
Ba(OH)2
10.9756096887552
H2O =
sa) Hasil k
Kira Kira --> C3H6O =

Hitungan di Ipad H2O =
C6H10O =
Nembak Ba(OH)2 =
C6H12O2 =
Katalis
Ba(OH)2
0.145146068482967
1.3063146163467 Recycle 1672.044276678
1.45146068482967
Input
Output
Recycle TH-1 Recycle MD-1 TOTAL INPUT
17480.2196861023 76912.9666188499 97112.3315894569 107902.59065495
126.020562966418 11.2018278192371 700.114238702322 700.11423870232
223.823946364844 0 248.693273738715 248.69327373872
2368.59345340139 0 13158.8525188966 2368.5934534014
20198.6576488349 76924.1684466691 111219.991620795
111219.991620795 111219.991620795
0
Tmin Tmax Cp 25°C Cp Tmin

275 624 25.913 25.588
T (K)
3 + E*T^4
D E Tmin Tmax
3.19E-08 -8.76E-12 250 1500
D E Cp @25C
2.96E-06 0 127.53
5.35E-07 0 75.55
2.99E-06 0 233.58 1 joule
NERACA PANAS MASUK
Tref 298.15
Treacted 303.15
1/2BT2 1/3BT3 1/4BT4 Cp dt
481.325 -6.93E-01 7.40E-03 949.41906666667
-2 -7.03E-02 1.34E-03 918.46100416667
42.755 -7.87E-01 7.48E-03 1582.7858083333
TOTAL 3450.6658791667
NERACA PANAS KELUAR

Tref 298.15
Treacted 303.15
1/2BT2 1/3BT3 1/4BT4 Cp dt
120.33125 -8.67E-02 4.63E-04 354.63504583333
-0.5 -8.79E-03 8.36E-05 459.75629192708
10.68875 -9.83E-02 4.67E-04 780.99588385417
TOTAL 1595.3872216146
NERACA PANAS REAKSI, Cp H1

Tref 298.15
Treacted 303.15
1/2BT2 1/3BT3 1/4BT4 Cp dt
120.33125 8.67E-02 4.63E-04 -113.9716208333
-0.5 8.79E-03 8.36E-05 -460.7561247396
10.68875 9.83E-02 4.67E-04 -759.6174494792
TOTAL -1334.345195052
Hasil ke TH-1 Recycle Masuk dari TH-1
kg/jam kmol/jam kg/jam
114551.3345 1972.302591253 C3H6O = 26047.4658
17533.5565 973.0053551609 H2O = 3189.52
41.4767 0.422627878541 C6H10O = 7.545
296.8259 1.732379479398 Ba(OH)2 = 269.9772
13848.4097 119.2184030647 C6H12O2 = 2519.1569
100
100
100
100
100
0 0 H2O =
Hasil ke TH-1 Recycle Masuk dari TH-1
kg/jam kmol/jam Ratio kg/jam
97112.33158946 1672.044276678 90 C3H6O = 17480.2196861
700.1142387023 38.85206652066 100 H2O = 126.020562966
0 Gk ada #VALUE! C6H10O = 0
248.6932737387 1.45146068483 100 Ba(OH)2 = 223.823946365
13158.8525189 113.2821325663 555.55555555556 C6H12O2 = 2368.5934534
MIBK 6944.444
97112.33158946
Cara Hitung Hidrogen masih bingung
Cp Tmax
35.906
0.239006 cal
H= m cp dt (kJ/jamH(kkal/jam)
1763856.351765 421572.2512101
35684.10803052 8528.715923942
32274.24331745 7713.73779833
1831814.703113 437814.7049323
592965.4986951 141722.3119811
17862.48203724 4269.240381793
88472.87924847 21145.54897766
699300.8599808 167137.1013406
-211739.5514645 -50607.0232373
-17901.32760818 -4278.52470632
-15489.19523008 -3702.01059516
-245130.0743028 -58587.5585388
Recycle Masuk dari TH-1 Recycle Masuk dari FD-1
kmol/jam Ratio kg/jam
448.475650826446 20.692202315 C3H6O = 82476.9608
176.998890122087 18.19094717 H2O = 6424.2951
0.076879967393519 18.190936116 C6H10O = 0
1.57568110190265 90.954731376 Ba(OH)2 = 0
21.6869567837466 100 C6H12O2 = 0
0 0 H2O =
Recycle Masuk dari TH-1 Recycle Masuk dari MD-1
kmol/jam Ratio kg/jam
300.967969802036 16.2 C3H6O = 76912.9666188499
6.99337197371909 18 H2O = 11.2018278192371
Gk ada #VALUE! C6H10O = 0
1.3063146163467 90 Ba(OH)2 = 0
20.3907838619266 100 C6H12O2 = 0
Masuk dari FD-1 Recycle Masuk dari MD-1
kmol/jam Ratio kg/jam kmol/jam
1420.05786501 65.5200000008 C3H6O = 2771.5695 47.71986053719
356.509162042 36.6399999909 H2O = 7312.1592 405.78019977802
0 0 C6H10O = 33.9317 0.3457479111473
0 0 Ba(OH)2 = 0 0
0 0 C6H12O2 = 0 0
0 0 H2O = 562.8918479167 31.237061482612

asuk dari MD-1 Feed Awal + Recycle
1324.25906713 71.28 C3H6O = 107902.590655 1857.8269740866
0.62163306433 1.6 H2O = 700.1142387023 38.852066520662
Gk ada #VALUE! C6H10O = #VALUE!
0 0 Ba(OH)2 = 248.6932737387 1.4514606848297
0 0 C6H12O2 = 2368.593453401 20.390783861927
MD-1 Feed Awal + Recycle
Ratio kg/jam kmol/jam Ratio
2.201744970728 C3H6O = 125880.5873 2167.3654838
41.70379922636 H2O = 17533.5565 973.00535516
81.80906388406 C6H10O = 41.4767 0.4226278785
0 Ba(OH)2 = 296.8259 1.7323794794
0 C6H12O2 = 2519.1569 21.686956784
cle
Perbandingan
Ratio Thickener Bawah Thickener Samping
% 25 75
Recycle Purge
90 10
Aseton
Itungan Coba Coba misal F = 1672.04427668
A= 232.5999372
A + R1 + R2 = 1857.826974
Reaksi = 185.7826974
F= 1672.044277
F-F= 0
R2 = 300.9679698
R1 = 1324.259067
Reaksi Aseton
M 1857.826974
Konveri 10% R 185.7826974
S 1672.044277
Air
A= 31.2370614826119
R1 0,8 x 0,02 x F = 0.621633064330585
R2 0,9 x 0,2 x F = 6.99337197371909
F= 38.8520665206616
F-F= 0
DAA Katalis Ba(OH)2
Itungan Coba Coba misal F = 113.28213257 Itungan Coba Coba
A= 20.39078386193 A=
R1 Gk ada 0 R1 Gk ada
R2 0,9 x 0,2 x F = 20.39078386193 R2 0,9 x F =
Reaksi Reaksi = 92.89134870433 karena reaksi 1:2 F=
F= 113.2821325663
F-F=
F-F= 0
misal F = 1.4514607
0.1451460685
0
1.3063146163
1.4514606848
0
Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16
Punya Kating Dulu

Kapasitas Pabrik = 65000
Hasil TH-01 Kating
Feed
kg/jam
Urut H2O = 17533.5565
Berdasarkan C3H6O = 114551.3345
Titik Didih C6H10O = 41.4767
C6H12O2 = 13848.4097
Ba(OH)2 = 296.8259
Hasil TH-01 Yosua

Asumsi - ayo
Komponen F, kmol/jam
Air 38.8521
Aseton 1672.0443
DAA 113.2821
Ba(OH)2 1.4515
1825.6299
Mass Balance
Bahan
Air
Aseton
DAA
Ba(OH)2
SubTotal
Total
Inpt - Output
Tb, oC Sg, tidak ada satuan
56.2 0.79
100 1
167.9 0.9387
270 1.84
-252.8 0.0696
125 0.855
1.94
115.9 0.802
ton/tahun
Feed
kmol/jam
973.005355161
1972.30259125
0.42262787854
119.218403065
1.7323794794
F, kg/jam D, kmol/jam D, kg/jam R + P, kmol/jam
700.1142 31.0816532165293 560.0914 7.7704

97112.3316 1337.63542134238 77689.8653 334.4089
13158.8525 90.6257060530069 10527.0820 22.6564
248.6933 0 0.0000 1.4515
1459.3428 366.2872 329.6584 36.6287
Mol balance = 1422.714065028
Input Output
Feed Recycle Purge Output ke MD-01
700.1142 126.0206 14.0023 560.0914
97112.3316 17480.2197 1942.2466 77689.8653
13158.8525 2368.5935 263.1771 10527.0820
248.6933 223.8239 24.8693 0.0000
111219.991621 20198.6576488349 2244.29529431499 88777.0386776447
111219.991621 111219.9916
0
R+P
Air 140.0228
Aseton 19422.4663
DAA 2631.7705
Ba(OH)2 248.6933
22442.9529
111219.9916
0.0000
Persamaan Antoine
TEKANAN UAP TE
Komponen A B C Komponen
Aseton 7.31742 1315.6735 240.479 Air
Air 8.05573 1723.6425 233.08 MO
MIBK 7.37701 1527.2068 223.816 MIBK
MO 7.12851 1483.4864 219.745
DAA 8.62593 2568.7558 279.12
Asam Sulfat 8.28538 2976.837 213.95
Hasil ke MD-1
kg/jam kmol/jam Ratio
H2O = 14026.8452 778.4042841287 80
C3H6O = 85913.5009 1479.226943871 80
C6H10O = 33.1813 0.338101691461 80
C6H12O2 = 11078.7278 95.37472279614 80
Ba(OH)2 = 0 0 0
R, kmol/jam R, kg/jam P, kmol/jam P kg/jam
6.9934 126.0206 0.7770 14.0023

300.9680 17480.2197 33.4409 1942.2466
20.3908 2368.5935 2.2656 263.1771
1.3063 223.8239 0.1451 24.8693
TEKANAN UAP
A B C
8.05573 1723.6425 233.08
7.12851 1483.4864 219.745
7.37701 1527.2068 223.816
Hasil Recycle + Purge Hasil Recycle

H2O = 3506.7113 194.601071032 20 H2O =
C3H6O = 28637.8337 493.075649105 20 C3H6O =
C6H10O = 8.2953 0.08452516813 20 C6H10O =
C6H12O2 = 2769.682 23.8436811295 20 C6H12O2 =
Ba(OH)2 = 296.8259 1.7323794794 100 Ba(OH)2 =
Hasil Recycle Hasil Purging
kg/jam kmol/jam Ratio kg/jam kmol/jam
3189.52 176.9988901 90 H2O = 317.1913 17.6021809101
26047.4658 448.4756508 90 C3H6O = 2590.3679 44.5999982782
7.545 0.076879967 90 C6H10O = 0.7503 0.00764520073
2519.1569 21.68695678 90 C6H12O2 = 250.5251 2.15672434573
269.9772 1.575681102 90 Ba(OH)2 = 26.8487 0.1566983775
ng
Ratio
10
10
10
10
10
Data Komponen
Aseton C3H6O 58.08
Air H2O 18.02
Nikel Ni 58.69
Punya Kating Dulu

Hasil MD-02 Kating
Feed
kg/jam kmol/jam
C3H6O = 85913.5009 1479.226943871
H2O = 14026.8452 778.4042841287
C6H12O2 = 11078.7278 95.37472279614
Hasil MD-02 Yosua

Asumsi -
1. Asumsi awal distribusi awal komponen di Distilat dan Bottom
P avg = 1.2
T avg = 89.29007691792
Komponen F,kmol/jam
Aseton 1337.6354
Air 31.0817
DAA 90.6257
Total 1459.3428
Kondisi Atas (Distilat)

P= 1.1
T = 58.99200541393
Komponen D,kmol/jam
Aseton 1324.2591
Air 0.6216
DAA 0.0000
Total 1324.8807
Mass Balance
Bahan
Aseton
Air
DAA
SubTotal
Total
Inpt - Output
Komponen A
Aseton 46.878
Air 92.053
DAA 154.081
T= 89.29007691792
Treferensi 25
MR Komp massflow
58.08 Aseton 77689.8653
18.02 Air 560.0914
116.16 DAA 10527.0820
TOTAL 88777.0387
T= 58.99200541393
Treferensi 25
MR Komp massflow
58.08 Aseton 76912.9666
18.02 Air 11.2018
116.16 DAA 0.0000
TOTAL 76924.1684
T= 119.5881484219
Treferensi 25
MR Komp massflow
58.08 Aseton 776.8987
18.02 Air 548.8896
116.16 DAA 10527.0820
TOTAL 11852.8702
T= 89.29007691792
Treferensi 25
MR Komp massflow
58.08 Aseton 776.8987
18.02 Air 548.8896
116.16 DAA 10527.0820
TOTAL 11852.8702
Hbot 597307.1995553
Hin Reboiler 363639.9437194
Qrb 233667.2558358
T= 89.29007691792
Treferensi 25
MR Komp massflow
58.08 Aseton 76912.9666
18.02 Air 11.2018
116.16 DAA 0.0000
TOTAL 76924.1684
Htop 2256747.281172
Hin Kondenser 7197064.800682
Qkondenser 4940317.51951
INPUT OUTPUT
Komponen H, kkal/jam Komponen
ASETON 7268889.13591701 TOP
AIR 43227.8061962477 ASETON
DAA 248587.802287941 AIR
Q-RB 233667.25583584 Bottom
Aseton
AIR
DAA
QCD
TOTAL 7794372.00023704 total
SELISIH 0
Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802
Hasil Atas
kg/jam kmol/jam
C3H6O = 82476.9608 1420.05786501377
H2O = 6424.2951 356.509162042175
C6H12O2 = 0 0
HK di D =
LK di B =
Distillat
F, kg/jam Po alfa
D xd
77689.8653 2.79849906952855 4.1571 1324.2591 0.9995
560.0914 0.673185083140321 1.0000 0.6216 0.0005
10527.0820 0.0592340620093593 0.0880 0.0000 0.0000
1324.8807 1.0000 134.4621
atm
o
C
D, kg/jam Po yd Ki Xi
76912.9666 1.10479387283158 0.9995 1.00435806621052 0.99519368077165

11.2018 0.187709559394902 0.0005 0.17064505399537 0.00274956269912
0.0000 0.014052861443206 0.0000 0.01277532858473 0
1 0.99794324347077
Input Output
Feed Distilat Bottom
77689.8653 76912.9666 776.8987
560.0914 11.2018 548.8896
10527.0820 0.0000 10527.0820
88777.038677645 76924.1684466691 11852.87023098
88777.038677645 88777.0387
0
Kapasitas Panas
B C D E Cp @25C
9.6265 -2.08E-03 2.96E-06 0 127.53
-0.04 -2.11E-04 5.35E-07 0 75.55
0.8551 -2.36E-03 2.99E-06 0 233.58
INPUT
C = 362.4400769179 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
3013.7902257581 19894.1922379044 -1.84E+02 1.26E+01 0
5918.0944505249 -82.6642798022311 -1.87E+01 2.28E+00 0
9905.8793415894 1767.1556414722 -2.09E+02 1.28E+01 0
DISTILAT
C = 332.1420054139 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
1593.4772297943 5561.50067161636 -2.72E+01 9.88E-01 0
3129.0660743686 -23.1091286412148 -2.76E+00 1.79E-01 0
5237.522186184 494.01539752757 -3.09E+01 9.98E-01 0
BOTTOM
C = 392.7381484219 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
4434.1032217219 43063.7522061807 -5.87E+02 5.92E+01 0
8707.1228266812 -178.93835643767 -5.95E+01 1.07E+01 0
14574.236496995 3825.25471474629 -6.66E+02 5.98E+01 0
Hin Reboiler
C = 362.4400769179 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
ga diitung mirip inp 0 0.00E+00 0.00E+00 0
0 0 0.00E+00 0.00E+00 0
0 0 0.00E+00 0.00E+00 0
Hin Kondenser
C = 362.4400769179 K
C = 298.15
AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
ga diitung mirip inp #VALUE! #VALUE! 7.86E+09 0
2364.7037105475 #VALUE! #VALUE! 5.97E+09 0
#VALUE! #VALUE! #VALUE! #VALUE! 0
OUTPUT
H, kkal/jam
TOP
2256286.2005196
461.08065195804
150165.54025127
61730.892773771
385410.76653023
4940317.5195102
7794372.000237
0
Persamaan Antoine
TEKANAN UAP TEKANAN UAP
B C Komponen A B
1315.674 240.479 Aseton 7.31742 1315.6735
1723.643 233.08 Air 8.05573 1723.6425
1527.207 223.816 MO 7.12851 1483.4864
1483.486 219.745 DAA 8.62593 2568.7558
2568.756 279.12
2976.837 213.95
Hasil Bawah
ratio kg/jam kmol/jam ratio
96 C3H6O = 3436.54 59.16907713499 3.9999999581
45.8 H2O = 7602.5501 421.8951220866 54.2000000114
0 C6H12O2 = 11078.7278 95.37472279614 100
0.01
0.01
Bottom
B xb
13.3764 0.0995
30.4600 0.2265
90.6257 0.6740
1.0000
Kondisi Bawah (Bottom)

P= 1.3 atm
T = 119.588148421901 oC
Komponen B,kmol/jam B. kg/jam Po
Aseton 13.3764 776.8987 6.0623268405337

Air 30.4600 548.8896 1.9385715670535
DAA 90.6257 10527.0820 0.200640862901
Total 134.4621 1
1 joule 0.239006 cal
Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)

22736.39 1337.63542134238 30412998.5687264 7268889.135917
5819.026 31.0816532165293 180864.941450205 43227.80619625
11476.77 90.6257060530069 1040090.21651314 248587.8022879
31633953.7266897 7560704.744401
7128.734 1324.25906712896 9440291.04089267 2256286.20052
3103.373 0.621633064330585 1929.15931800055 461.080651958
5701.638 0 0 0
9442220.20021067 2256747.281172

46970.34 13.3763542134238 628291.926777039 150165.5402513
8479.37 30.4600201521987 258281.770222384 61730.89277377
17793.59 90.6257060530069 1612556.8668997 385410.7665302
2499130.56389912 597307.1995553

22736.39 13.3763542134238 304129.985687264 72688.89135917
5819.026 30.4600201521987 177247.642621201 42363.25007232
11476.77 90.6257060530069 1040090.21651314 248587.8022879
1521467.84482161 363639.9437194

22736.39 1324.25906712896 30108868.5830391 7196200.244558
5819.026 0.621633064330585 3617.2988290041 864.556123925
11476.77 0 0 0
30112485.8818681 7197064.800682
C
240.479
233.08
219.745
279.12
REAKSI Yield
C3H6O = 1479.227 C3H6O =
H2O = 778.4043 Total 2353.006 H2O =
C6H12O2 = 95.37472 C6H12O2 =
xb Ki Yi
0.0995 4.663328 0.4639102078448

0.2265 1.491209 0.337807156744
0.6740 0.154339 0.10402257766009
0.9057399422
0.628654
0.330813
0.040533
Data Komponen
Aseton C3H6O 58.08
Air H2O 18.02
Nikel Ni 58.69
Punya Kating Dulu

Hasil TH-02 Kating
Feed
kg/jam
Urut H2O = 7799.74
Berdasarkan
C6H10O = 33.1813
Titik Didih
C6H12O2 = 11078.7278
H3PO4 = 1117.4095
DAA
M 95.3747227961433
R 85.8372580922865
S 9.53746470385675
Konversi 90.0000079431503 %
Hasil TH-02 Yosua

Asumsi - Asumsi reaksi 1:1:1
H2SO4 (98%) =
Feed (Biasa)
kg/jam
H2O Feed + dari Katalis) = 594.980995296156
C6H10O = 0
C6H12O2 = 10527.0820151173
H2SO4 = 2258.48017552326
Input MO 65.2245562216422
DAA
M 90.6257060530069
R 81.5631354477062
S 9.06257060530069
Konversi 90 %
Hasil MD-02 Yosua

- DAA udah hilang di RD jadi di MD-2
Asumsi gk perlu pisahin
P avg = 1.300
T avg = 119.588148421901
Komponen F,kmol/jam
Air 114.5809
Aseton 13.3764
Katalis Asam Sulfat 23.0269
MO 81.5631
DAA 9.0626
Total 241.6099

P= 1.2
T= 117.276701011583
Komponen D,kmol/jam
Air 114.5809
Aseton 13.3764
Katalis Asam Sulfat 0.0000
MO 80.7475
DAA 0.0000
Total 208.7048
Mass Balance
Bahan
Air
Aseton
Katalis Asam Sulfat
MO
DAA
SubTotal
Total
Inpt - Output
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802
ton/tahun
Feed Hasil Atas

kmol/jam kg/jam
432.83795782464 H2O = 9346.9416
0.3381016914612 C6H10O = 8414.5505
95.374722796143 C6H12O2 = 11.0778
11.392837479608 H3PO4 = 0
MO Air H3PO4
0.3381016914612 432.837957824639 0.095367
86.171130018341 518.69820199778 0.095367
mol H2SO4 massa H2SO4 massa air mol air

23.026918592203 2258.48017552326 46.091432153536 2.557793
eed (Biasa) Hasil Atas

kmol/jam kg/jam
33.017813279476 H2O =
0 Belom ada MO C6H10O =
90.625706053007 C6H12O2 =
23.026918592203 Pake Perbandingan H3PO4 =
Gk ada recycle mo Katalis

MO Air H2SO4
0 33.0178132794759 23.02692
81.563135447706 81.5631354477062 Asumsi Reaksi 1 : 1 : 1
81.563135447706 114.580948727182 23.02692
HK di D = 0.01
LK di B = 0.01
Distillat Bottom
F, kg/jam Po alfa
D xd B
2064.7487 1.93857156705353 6426.0262 114.5809 0.5490 0.0000
776.8987 6.06232684053371 20095.5547 13.3764 0.0641 0.0000
2258.4802 0.000301675018711402 1.0000 0.0000 0.0000 23.0269
8004.6061 0.751495939598578 2491.0778 80.7475 0.3869 0.8156
1052.7082 0.200640862901011 665.0894 0.0000 0.0000 9.0626
208.7048 1.0000 32.9051
atm
o
C
2064.7487 1.79985459233914 0.5490 1.499879 0.3660359886151

776.8987 5.74157695511341 0.0641 4.784647 0.0133953900619
0.0000 0.000261370479936579 0.0000 0.000218 0
7924.5601 0.701363340475812 0.3869 0.584469 0.6619647125132
0.0000 0.184014088138226 0.0000 0.153345 0
1 1.0413960911903
Input Output
594.9810 2064.7487 0.0000
776.8987 776.8987 0.0000
2258.4802 0.0000 2258.4802
0.0000 7924.5601 80.0461
10527.0820 0.0000 1052.7082
14157.441838652 10766.2074 3391.2344
14157.441838652 14157.4418
0.0000
Kapasitas Panas
Komponen A B C D
Aseton 46.878 9.6265 -2.08E-03 2.96E-06
Air 92.053 -0.04 -2.11E-04 5.35E-07
MO 125.316 0.5368 -1.44E-03 2.01E-06
DAA 154.081 0.8551 -2.36E-03 2.99E-06
Asam sulfat 26.004 0.70337 -1.39E-03 1.03E-06
INPUT
T= 119.588148421901 C = 392.73815
Treferensi 25 C = 298.15
MR Komp massflow AT 1/2BT2 1/3CT3
58.08 Aseton 776.8987 4434.103 43063.752206181 -5.87E+02
18.02 Air 594.9810 8707.123 -178.9383564377 -5.95E+01
98.14 MO 0.0000 11853.41 2401.3527433935 -4.06E+02
116.16 DAA 10527.0820 14574.24 3825.2547147463 -6.66E+02
98.08 SULFAT 2258.4802 2459.67 3146.4967941891 -3.92E+02
TOTAL 14157.4418
DISTILAT
T= 117.276701011583 C = 390.4267
58.08 Aseton 776.8987 4325.747 40984.773449521 -5.45E+02
18.02 Air 2064.7487 8494.347 -170.2997909916 -5.53E+01
98.14 MO 7924.5601 11563.75 2285.4231951076 -3.77E+02
116.16 DAA 0.0000 14218.09 3640.5837819234 -6.18E+02
98.08 SULFAT 0.0000 2459.67 2994.5940997444 -3.64E+02
TOTAL 10766.2074
BOTTOM
T= 223.12910951382 C = 496.27911
58.08 Aseton 0.0000 9287.896 188944.82203484 -5.39E+03
18.02 Air 0.0000 18238.38 -785.1028807348 -5.47E+02
98.14 MO 80.0461 24828.75 10536.080659461 -3.73E+03
116.16 DAA 1052.7082 30527.93 16783.536832908 -6.12E+03
98.08 SULFAT 2258.4802 5152.149 13805.445330561 -3.60E+03
TOTAL 3391.2344
Hin Reboiller
T= 119.588148421901 C = 392.73815
58.08 Aseton 0.0000 4434.103 43063.752206181 -5.87E+02
18.02 Air 0.0000 8707.123 -178.9383564377 -5.95E+01
98.14 MO 80.0461 11853.41 2401.3527433935 -4.06E+02
116.16 DAA 1052.7082 14574.24 3825.2547147463 -6.66E+02
98.08 SULFAT 2258.4802 2459.67 3146.4967941891 -3.92E+02
TOTAL 3391.2344
Hbot 184722.4
Hin rb 70057.96
Qrb 114664.4
Hin kondenser
T= 119.588148421901 C = 392.73815
58.08 Aseton 776.8987 4434.103 43063.752206181 -5.87E+02
18.02 Air 2064.7487 8707.123 -178.9383564377 -5.95E+01
98.14 MO 7924.5601 11853.41 2401.3527433935 -4.06E+02
116.16 DAA 0.0000 14574.24 3825.2547147463 -6.66E+02
98.08 SULFAT 0.0000 2459.67 3146.4967941891 -3.92E+02
TOTAL 10766.2074
Htop 630701
Hin cd 650419
Qcd -19718
INPUT OUTPUT
Komponen H, kkal/jam KomponenH, kkal/jam
ASETON 150165.540251273 TOP
AIR 66914.5680467516 Aseton 143288.9113882
MO 0 Air 226710.6397468
DAA 385410.766530229 MO 260701.46291064
SULFAT 28809.3981400438 Bottom
Qcd MO 6317.235973813
DAA 91719.580439748
SULFAT 86685.538001446
Qrb 114664.39104362
TOTAL 631300.272968298 TOTAL 930087.75950426
SELISIH
NPNYA ADA REAKSINYA GATAU WEH

Persamaan Antoine
B C Komponen A B C
1315.6735 240.479 Air 8.05573 1723.643 233.08
1723.6425 233.08 MO 7.12851 1483.486 219.745
1527.2068 223.816 DAA 8.62593 2568.756 279.12
1483.4864 219.745 Asam Sulfat 8.28538 2976.837 213.95
2568.7558 279.12 Aseton 7.31742 1315.674 240.479
2976.837 213.95
Hasil Atas Hasil Bawah

518.698202 119.836579168024 H2O = 0 0
85.7402741 25359.3153372532 C6H10O = 42.2842 0.430856
0.095366736 0.0999916253922224 C6H12O2 = 1096.794 9.442098
0 H3PO4 = 1117.41 11.39284
REAKSI Yield
DAA = 85.8372580922865 DAA =
MO = 85.83302832688 Total 257.5305 MO =
Air = 85.860244173141 Air =
Hasil Bawah MO 0.00500000313

0.50000031336
Hasil Atas Hasil Bawah
#REF! H2O = 0
#REF! C6H10O = 0
#REF! C6H12O2 =
H3PO4 =
Cara Hitung Hidrogen masih bingung
Hasil atas 97%

Hasil bawah 3%
Bottom
xb
0.0000 1.14580948727182
0.0000
0.6998
0.0248
0.2754 0
1.0000

P= 1.4 atm
T= 223.12910951382 oC
Komponen B,kmol/jam B, kg/jam Po xb Ki
Air 0.0000 0.0000 24.930513 0.0000 17.80751

Aseton 0.0000 0.0000 39.692304 0.0000 28.35165
Katalis Asam Sulfat 23.0269 2258.4802 0.0392478 0.6998 0.028034
MO 0.8156 80.0461 7.9070911 0.0248 5.647922
DAA 9.0626 1052.7082 4.2718006 0.2754 3.051286
Total 32.9051 1
pasitas Panas
E Cp @25C
0 127.53
0 75.55
0 213.3
0 233.58 1 joule 0.239006 cal
0 139.95 R 1
INPUT
K
1/4DT4 E/2T2 Cp dt molflow (kmol/jaH = N Cp dtH(kkal/jam)
5.92E+01 0 46970.3416007418 13.3763542134 628291.9 150165.5
1.07E+01 0 8479.36964361267 33.0178132795 279970.2 66914.57
4.02E+01 0 13888.7741910241 0 0 0
5.98E+01 0 17793.5923164727 90.625706053 1612557 385410.8
2.06E+01 0 5234.67298765617 23.0269185922 120538.4 28809.4
2641357 631300.3
DISTILAT
K

5.37E+01 0 44819.3980072943 13.3763542134 599520.1 143288.9
9.70E+00 0 8.28E+03 114.580948727 948556.3 226710.6
3.64E+01 0 1.35E+04 80.7475040932 1090774 260701.5
5.42E+01 0 1.73E+04 0 0 0
1.87E+01 0 5.11E+03 0 0 0
2638850 630701
BOTTOM
K

1.14E+03 0 193980.573383227 0 0 0
2.06E+02 0 17112.3566842867 0 0 0
7.74E+02 0 3.24E+04 0.81563135448 26431.29 6317.236
1.15E+03 0 4.23E+04 9.0625706053 383754.3 91719.58
3.97E+02 0 1.58E+04 23.0269185922 362691.9 86685.54
772877.5 184722.4
Hin Reboiller
K

5.92E+01 0 46970.3416007418 0 0 0
1.07E+01 0 8.48E+03 0 0 0
4.02E+01 0 13888.7741910241 0.81563135448 11328.12 2707.489
5.98E+01 0 17793.5923164727 9.0625706053 161255.7 38541.08
2.06E+01 0 5234.67298765617 23.0269185922 120538.4 28809.4
293122.2 70057.96
in kondenser
K

5.92E+01 0 46970.3416007418 13.3763542134 628291.9 150165.5
1.07E+01 0 8479.36964361267 114.580948727 971574.2 232212.1
4.02E+01 0 13888.7741910241 80.7475040932 1121484 268041.4
5.98E+01 0 17793.5923164727 0 0 0
2.06E+01 0 5234.67298765617 0 0 0
2721350 650419
Bawah Perbandingan Atas Bawah %
Ratio Ratio Bawah Ratio Atas
0 H2O = 0 100
127.4338 C6H10O = 0.5000003134 99.499999687
9.9 C6H12O2 = 99.000082952 0.9999170482
H3PO4 = 100 0
0.333309
0.333293
0.333398
Sementara gk make
Bawah Recycle Masuk dari MD-2
#REF! H2O = 0 #DIV/0!
#REF! C6H12O = 35.2293 #DIV/0!
#REF! C6H10O = 655.295 #DIV/0!
Ni = 0 #DIV/0!
Yi
0
0
0.019618
0.139997
0.840371
0.999986
Data Komponen
Aseton C3H6O 58.08
Air H2O 18.02
Nikel Ni 58.69
Punya Kating Dulu

Hasil MD-02 Kating
Feed
kg/jam kmol/jam
C3H6O = 3436.54 59.16907713499
H2O = 9346.9416 518.6982019978
C6H10O = 8414.5505 85.74027409823
C6H12O2 = 11.0778 0.095366735537
Hasil MD-02 Yosua

- DAA udah hilang di RD jadi di MD-2 gk
Asumsi perlu pisahin
P avg = 1.1
T avg = 115.9465040322
Komponen F,kmol/jam
Komponen F,kmol/jam
Air 114.5809
Aseton 13.3764
MO 80.7475
Total 208.7048

P= 1
T = 96.65315219019
Komponen D,kmol/jam
Air 113.4351
Aseton 13.3764
MO 2.4224
Total 129.2339
Mass Balance
Bahan
Air
Aseton
MO
SubTotal
Total
Inpt - Output
Neraca Panas
Komponen
Aseton
Air
MIBK
MO
DAA
Asam sulfat
T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total
T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total
T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total
T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total
T=
Treferensi
MR Komp
58.08 Aseton
18.02 Air
98.14 MO
Total
Htop
Hin cd
Qcd
INPUT
Komponen
ASETON
AIR
MO
Q-RB
TOTAL
SELISIH
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802
Hasil Atas
kg/jam kmol/jam
C3H6O = 3436.54 59.1690771349862
H2O = 9066.5334 503.137258601554
C6H10O = 42.0728 0.42870185449358
C6H12O2 = 0 0
HK di D =
LK di B =
Distillat
F, kg/jam Po alfa
F, kg/jam Po alfa
D xd
2064.7487 1.7238033517788 2.5585 113.4351 0.8778
776.8987 5.56296469857533 8.2567 13.3764 0.1035
7924.5601 0.673753229772902 1.0000 2.4224 0.0187
129.2339 1.0000
atm
o
C
2044.1012 0.886197043884412 0.8778 0.88619704388441 0.99046879711434

776.8987 3.42027555040257 0.1035 3.42027555040257 0.03026217592913
237.7368 0.362265353158286 0.0187 0.36226535315829 0.05174245712905
1 1.07247343017252
Input Output
2064.7487 2044.1012 20.6475
776.8987 776.8987 0.0000
7924.5601 237.7368 7686.8233
10766.2074 3058.7367 7707.4707
10766.207400489 10766.2074
0
Kapasitas Panas
A B C D E
46.878 9.6265 -2.08E-03 2.96E-06 0
92.053 -0.04 -2.11E-04 5.35E-07 0
126.633 0.5726 -1.63E-03 2.38E-06 0
125.316 0.5368 -1.44E-03 2.01E-06 0
154.081 0.8551 -2.36E-03 2.99E-06 0
26.004 0.70337 -1.39E-03 1.03E-06 0
INPUT
115.94650403222 C = 389.096504032225 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4
776.8987 4263.39021602263 39811.67394167 -5.22E+02 5.06E+01
2064.7487 8371.89853567838 -165.4253319137 -5.29E+01 9.15E+00
7924.5601 11516.8286451127 2368.063626344 -4.09E+02 4.07E+01
10766.2074
DISTILAT
96.653152190194 C = 369.803152190194 K
25 C = 298.15
776.8987 3358.95646837189 24712.0640586 -2.55E+02 1.95E+01
2044.1012 6595.88761856388 -102.6834843758 -2.59E+01 3.53E+00
237.7368 9073.65362130078 1469.91407884 -2.00E+02 1.57E+01
3058.7367
BOTTOM
135.2399 C = 408.389855874256 K
25 C = 298.15
0.0000 5167.82396367336 58494.58889341 -9.29E+02 1.09E+02
20.6475 10147.9094527929 -243.0565164635 -9.42E+01 1.98E+01
7686.8233 13960.0036689246 3479.354033175 -7.28E+02 8.79E+01
7707.4707
Hin reboiler
115.9465 C = 389.096504032225 K
25 C = 298.15
0.0000 227617.598670633 50871112.3567 -7.39E+07 -1.95E+09
20.6475 873602.357967341 69981006.27971 1.06E+09 -1.51E+10
7686.8233 1186865.15214225 0 0.00E+00 0.00E+00
7707.4707 CP MIRIP FEED
Hbot 317178.054862106
Hin rb 255273.61011703
Qrb 61904.4447450761
Hin kondenser
115.9465 C = 389.096504032225 K
25 C = 298.15
776.8987 337194.688927225 0 0.00E+00 0.00E+00
2044.1012 0 0 0.00E+00 0.00E+00
237.7368 0 0 0.00E+00 0.00E+00
3058.7367 CP MIRIP FEED
270424.34655788
368534.53567078
98110.189112904
INPUT OUTPUT
H, kkal/jam Komponen H, kkal/jam
139403.68173419 TOP
223540.33334894 ASETON 88990.78146243
260864.13070468 AIR 175435.7575337
61904.444745076 MO 5997.807561782
BOTTOM
AIR 2692.101875166
MO 314485.9529869
QCD 98110.1891129
685712.59053289 total 685712.5905329
SELISIH 0
Persamaan Antoine
B C Komponen A B
1315.674 240.479 Aseton 7.31742 1315.6735
1723.643 233.08 Air 8.05573 1723.6425
1527.207 223.816 MO 7.12851 1483.4864
1483.486 219.745
2568.756 279.12
2976.837 213.95
Hasil Bawah
ratio kg/jam kmol/jam ratio
100 C3H6O = 0 0 0
97 H2O = 280.4082 15.56094339623 2.99999948646
0.500001 C6H10O = 8372.4778 85.311573262686 99.5000006239
0 C6H12O2 = 11.0778 0.095366735537 100
0.01 Hasil atas 97%

0.01 Hasil bawah 3%
Bottom
B xb
1.1458 0.0144 1.145809487272
0.0000 0.0000
78.3251 0.9856 37.04784008846
79.4709 1.0000

P= 1.2 atm
T = 135.239855874256 oC
Komponen B,kmol/jam B, kg/jam Po
Air 1.1458 20.6475 3.1273232664835

Aseton 0.0000 0.0000 8.6070914467624
MO 78.3251 7686.8233 1.171340618344
Total 79.4709
Cp @25C
127.53
75.55
212.42
213.3
233.58 1 joule 0.239006 cal
139.95
E/2T2 Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jaH(kkal/jam)

0 43604.1354128225 13.3763542134238 583264.360452 139403.6817342
0 8162.7158140996 114.580948727182 935291.7221699 223540.33334894
0 13516.8799352937 80.7475040932292 1091454.317903 260864.1307047
Total 65283.7311622159 208.704807033835 2610010.400525 623808.1457878

0 27835.4634333092 13.3763542134238 372337.0185788 88990.78146243
0 6470.85553981384 113.43513923991 734022.3991601 175435.7575337
0 10359.3704084707 2.42242512279688 25094.79913384 5997.807561782
Total 44665.6893815938 129.233918576131 1131454.216873 270424.3465579

0 62842.8277950064 0 0 0
0 9830.37925209034 1.14580948727182 11263.74181053 2692.101875166
0 16799.3162846639 78.3250789704323 1315807.774646 314485.9529869
Total 89472.5233317607 79.4708884577041 1327071.516456 317178.0548621

0 43604.1354128225 0 0 0
0 8162.7158140996 1.14580948727182 9352.917221699 2235.4033334894
0 13516.8799352937 78.3250789704323 1058710.688366 253038.20678354
Total 65283.7311622159 79.4708884577041 1068063.605587 255273.61011703
0 43604.1354128225 13.3763542134238 583264.360452 139403.6817342
0 8162.7158140996 113.43513923991 925938.8049482 221304.9300155
0 13516.8799352937 2.42242512279688 32743.62953708 7825.92392114
Total 65283.7311622159 129.233918576131 1541946.794937 368534.5356708
UAP
C
240.479
233.08
219.745
xb Ki Yi
0.0144 2.606103 0.037575

0.0000 7.172576 0
0.9856 0.976117 0.962044
1 0.999618
Data Komponen
Komponen Komponen Mr Tb, oC
Aseton C3H6O 58.08 56.2
Air H2O 18.02 100
Diaseton Alkohol C6H12O2 116.16 167.9
Asam Sulfat (Katalis 2) H2SO4 98.08 270
Gas Hidrogen H2 2.016 -252.8
Mesitil Oksida (MO) C6H10O 98.14 125
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16 115.9
Punya Kating Dulu

Hasil TH-02 Kating
Feed
kg/jam kmol/jam
Urut H2O = 280.4082 15.560943396226
Berdasarkan C6H12O = 0 0
Titik Didih C6H10O = 8372.4778 85.311573262686
C6H12O2 = 11.0778 0.0953667355372
Ni = 1285.7694 12.837154552716
H2 = 168.8556 83.757738095238
MO H2 MIBK
M 93.6748624414102
R 84.3073761972692 18.9421934912
S 9.36748624414102 103.2495696885
Konversi 90 %
Hasil TH-02 Yosua

Asumsi - ayo
Feed (Biasa)
kg/jam kmol/jam
H2O = 20.6474869606 1.1458094872718
C6H12O = 0 0
C6H10O = 7686.82325016 78.325078970432
Ni = 88.035 1.5
H2 = 145.0050851 71.927125545659
Input MO 65.2245562216422
Recycle MO 1.43569391188165
MO H2 MIBK
M 79.7607728823139 71.9271255457 15.757616106018
R 71.7846955940825 71.9271255457 71.784695594083
S 7.97607728823139 87.542311700101
Konversi 90 %
Mass Balance
Input
Bahan
Feed
H2O 20.6475
C6H12O 0.0000
C6H10O 7686.8233
Ni 88.0350
H2 145.0051
SubTotal 7940.5108
Total 10456.5400
Inpt - Output 0
Sg, tidak ada satuan
0.79
1
0.9387
1.84
0.0696
0.855
1.94
0.802
Hasil ke MD-2
kg/jam kmol/jam
H2O = 341.9613 18.97676470588
C6H12O = 10341.4769 103.2495696885
C6H10O = 919.3251 9.367486244141
DAA C6H12O2 = 110.7877 0.953750860882
Ni = 1285.7694 12.83715455272
H2 = 0 0
Cek Jumlah MO
93.6748654982678
sa) Hasil ke TH-2
kg/jam kmol/jam
H2O = 25.17986214712 1.397328643014
C6H12O = 8768.237939882 87.5423117001
C6H10O = 782.772225067 7.976077288231
Asumsi Ni = 880.35 15
Goal Seek H2 = 0
Cek Jumlah MO Nikel Ratio

0 1.5 0.224599657507
13.5 Asumsi Reaksi 1 : 1 kecuali H2
15
Cara Hitung Hidrogen masih

- kalau olin perbadningan gitu
Input Tsistem
Output
Recycle TH-2 120 C
4.5324 25.1799 393.15
1578.2828 8768.2379 393.15
140.8990 782.7722 393.15
792.3150 880.3500 393.15
0.0000 0.0000 393.15
2516.0292 10456.5400
10456.5400 10456.5400
0
2 Recycle Masuk dari TH-2
121.95124821599 H2O = 61.553 3.41581576 17.999990057
#DIV/0! C6H12O = 1861.4658 18.5849221 17.999999594
10.980322933791 C6H10O = 165.4785 1.68614734 17.999998042
1000.0875625124 C6H12O2 = 19.94 0.17165978 17.998387908
100 Ni = 1157.1925 11.5534395 90.000003111
0
2 Recycle Masuk dari TH-2
121.9512195122 H2O = 4.53237518648 0.25151916 100
#DIV/0! C6H12O = 1578.28282918 15.7576161
10.183299389002 C6H10O = 140.899000512 1.43569391 100
1000 Ni = 792.315 13.5 100
0 H2 = 0 0
Hitung Hidrogen masih bingung

u olin perbadningan gitu
Recycle Masuk dari MD-2
H2O = 0 0 0
C6H12O = 35.2293 0.35173023163 0.34066023974
C6H10O = 655.295 6.67714489505 71.280007475
C6H12O2 = 79.7672 0.68670110193 72.0000505471
Ni = 0 0 0
Sementara gk make
Recycle Masuk dari MD-2
H2O = 0
C6H12O = #REF!
C6H10O = 0
Ni = 0
H2 = 0 0
Feed Awal + Recycle
kg/jam kmol/jam
H2O = 25.1798621471 1.397328643 555.5556
C6H12O = 1578.28282918 15.757616106
C6H10O = 7827.72225067 79.760772882 5555.556
Ni = 0 0 0
H2 = 0 0
MO
A= 78.3250789704323
Mula-Mula A+R= 79.7607728823139
R Reaksi = 71.7846955940825
S F= 7.97607728823139
F-F= 0
R= 1.43569391188165
Reaksi MO
M 79.7607728823139
Konveri 90% R 71.7846955940825
S 7.97607728823139
MIBK
A= 15.7576161060181
R1 Gk ada 0
R2 0,9 x 0,2 x F = 15.7576161060181
Reaksi Reaksi = 71.7846955940825 karena reaksi 1:2
F= 87.5423117001007
F-F= 0
Air Katalis Nikel
Itungan Coba Coba misal F = 1.397328643014 Itungan Coba Coba
A= 1.14580948727182 A=
R1 Gk ada 0 R1 Gk ada
R2 0,9 x 0,2 x F = 0.25151915574259 R2 0,9 x F =
F= 1.39732864301441 F=
F-F= 0 F-F=
misal F = 15
1.5
0
13.5
15
0
Data Komponen
Aseton C3H6O 58.08
Air H2O 18.02
Nikel Ni 58.69
Punya Kating Dulu

Hasil TH-02 Kating
Feed
kg/jam
Urut H2O = 341.9631
Berdasarkan C6H12O = 10341.4769
Titik Didih C6H10O = 919.3251
C6H12O2 = 110.7877
Ni = 1285.7694
Hasil TH-02 Yosua

Asumsi - ayo
Komponen F, kmol/jam
Air 1.3973
MO 7.9761
MIBK 87.5423
Nikel 15.0000
Mass Balance
Bahan
Air
MO
MIBK
Nikel
SubTotal
Total
Inpt - Output
Tb, oC Sg, tidak ada satuan TEKANAN U
56.2 0.79 Komponen
Aseton
100 1 Air
167.9 0.9387 MIBK
270 1.84 MO
-252.8 0.0696 DAA
125 0.855 Asam Sulfat
1.94
115.9 0.802
ton/tahun
Feed Hasil ke MD
kmol/jam
18.9768645949 H2O =
103.249569688 C6H12O =
9.36748624414 C6H10O =
0.95375086088 C6H12O2 =
21.9078105299 Ni =
F, kg/jam D, kmol/jam D, kg/jam R + P, kmol/jam R, kmol/jam
25.1799 1.11786291441153 20.1439 0.2795 0.2515

782.7722 6.38086183058512 626.2178 1.5952 1.4357
8768.2379 70.0338493600805 7014.5904 17.5085 15.7576
880.3500 0 0.0000 15.0000 13.5000
Input Output
Feed Recycle Purge Output ke MD-01
25.1799 4.5324 0.5036 20.1439
782.7722 140.8990 15.6554 626.2178
8768.2379 1578.2828 175.3648 7014.5904
880.3500 792.3150 88.0350 0.0000
10456.5400271 2516.02920487732 279.558800541925 7660.952021677
10456.5400271 10456.5400
0
R+P
Air 5.0360
MO 156.5544
MIBK 1753.6476
Nikel 880.3500
Persamaan Antoine
A B C KomponenA B
7.31742 1315.6735 240.479 Air 8.05573 1723.6425
8.05573 1723.6425 233.08 MO 7.12851 1483.4864
7.37701 1527.2068 223.816 MIBK 7.37701 1527.2068
7.12851 1483.4864 219.745
8.62593 2568.7558 279.12
8.28538 2976.837 213.95
Hasil ke MD-2 Hasil Recycle + Purge

kg/jam kmol/jam Ratio kg/jam
273.569 15.18140954495 80 H2O = 68.3923
8273.1816 82.59965654952 80 C6H12O = 2068.2954
735.4601 7.493989199103 80 C6H10O = 183.865
88.622 0.762930440771 80 C6H12O2 = 22.1555
0 0 0 Ni = 1285.7694
R, kg/jam P, kmol/jam P, kg/jam
4.5324 0.0279 0.5036

140.8990 0.1595 15.6554
1578.2828 1.7508 175.3648 8768.238 kg/jam yg wajib
792.3150 1.5000 88.0350
UAP
C
233.08
219.745
223.816
il Recycle + Purge Hasil Recycle

3.79535516093 20 H2O = 61.553 3.41581576
20.6499141374 20 C6H12O = 1861.4658 18.58492212
1.87349704504 20 C6H10O = 165.4785 1.686147341
0.19073261019 20 C6H12O2 = 19.94 0.17165978
21.9078105299 100 Ni = 1157.1925 19.71703016
cle Hasil Purging
90 H2O = 6.8393 0.37953940067 10
90 C6H12O = 206.8296 2.06499201278 10
90 C6H10O = 18.3865 0.1873497045 10
90 C6H12O2 = 2.2155 0.01907283058 10
90 Ni = 128.5769 2.19078037144 10
Data Komponen
Aseton C3H6O 58.08
Air H2O 18.02
Nikel Ni 58.69
Punya Kating Dulu

Hasil MD-02 Kating
Feed
kg/jam kmol/jam
H2O = 273.569 15.1814095449501
C6H10O = 735.4601 7.49398919910332
C6H12O = 8273.1816 71.2222933884298
C6H12O2 = 88.622 0.884804313099042
Hasil MD-02 Yosua

P avg = 1.2
T avg = 122.4497
Komponen F,kmol/jam
Komponen F,kmol/jam
Air 1.1179
MO 6.3809
MIBK 70.0338
Total 77.5326

P= 1.1
T= 118.790829736173
Komponen D,kmol/jam
Air 1.0843
MO 0.0000
MIBK 69.3335
Total 70.4178
Kemurnian MIBK
Mass Balance
Bahan
Air
MO
MIBK
SubTotal
Total
Inpt - Output
HEAT BALANCE
Komponen
Aseton
Air
MIBK
MO
DAA
Asam sulfat
T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total
T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total
T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total
Hreboiler
T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total
T=
Treferensi
MR Komp
18.02 Air
100.16 MIBK
98.14 MO
Total
Input OUTPUT
Komponen H, kkal/jam Komponen
AIR 2331.79995387938 TOP
MIBK 244550.031653514 AIR
MO 21902.9189001894 MIBK
Q-RB 4173.15820889839 BOTTOM
Air
MIBK
MO
QCD
TOTAL 272957.908716481 total
SELISIH 0
56.2 0.79 Komponen A B
Aseton 7.31742 1315.674
100 1 Air 8.05573 1723.643
167.9 0.9387 MIBK 7.37701 1527.207
270 1.84 MO 7.12851 1483.486
-252.8 0.0696 DAA 8.62593 2568.756
125 0.855 Asam Sulfat 8.28538 2976.837
1.94
115.9 0.802
Hasil Atas
kg/jam kmol/jam ratio
H2O = 273.569 15.1814095449501 100
C6H10O = 7.3546 0.07493988180151 1
C6H12O = 8231.8156 70.8661811294766 99.5
C6H12O2 = 0 0 0
HK di D = 0.01
LK di B = 0.01
Excel Olin
Distillat Bottom
F, kg/jam Po alfa
F, kg/jam Po alfa
D xd B
20.1439 2.12236135358838 2.5962 1.0843 0.0154 0.0335
626.2178 0.817494621214704 1.0000 0.0000 0.0000 6.3809
7014.5904 1.21812213085154 1.4901 69.3335 0.9846 0.7003
70.4178 1.0000 7.1147 1.0000
atm
o
C
19.5396 1.88976237627259 0.0154 1.71796579661144 0.00896319991989

0.0000 0.733888796543892 0.0000 0.66717163322172 0
6944.4444 1.09292115194129 0.9846 0.99356468358299 0.99097879119331
1 0.9999419911132
69.3335 6944.44444838661
0.997194196 55000000.03122 55000.0000312219
Input Output
20.1439 19.5396 0.6043
626.2178 0.0000 626.2178
7014.5904 6944.4444 70.1459
7660.952022 6963.9840 696.9680
7660.952022 7660.9520
0
Kapasitas Panas
A B C D E Cp @25C
46.878 9.6265 -2.08E-03 2.96E-06 0 127.53
92.053 -0.04 -2.11E-04 5.35E-07 0 75.55
126.633 0.5726 -1.63E-03 2.38E-06 0 212.42
125.316 0.5368 -1.44E-03 2.01E-06 0 213.3
154.081 0.8551 -2.36E-03 2.99E-06 0 233.58
26.004 0.70337 -1.39E-03 1.03E-06 0 139.95
INPUT
122.4497 C = 395.5997 K
25 C = 298.15
massflow AT 1/2BT2 1/3CT3 1/4DT4 E/2T2
20.1439 8970.5372341 -189.9288806018 -6.51E+01 1.21E+01 0
7014.5904 12340.3478601 2718.831925815 -5.03E+02 5.37E+01 0
626.2178 12212.0066052 2548.845577676 -4.44E+02 4.53E+01 0
7660.9520 Total
DISTILAT
118.7908 C = 391.9408 K
25 C = 298.15
19.5396 8633.72724970391 -175.934394852 -5.80E+01 1.03E+01 0
6944.4444 11877.0141419808 2518.500862306 -4.48E+02 4.60E+01 0
0.0000 11753.4916192182 2361.039578914 -3.96E+02 3.89E+01 0
6963.9840 Total
BOTTOM
137.0583 C = 410.2083 K
25 C = 298.15
0.6043 10315.3049766589 -251.1413633268 -9.90E+01 2.11E+01 0
70.1459 14190.281849687 3595.088616024 -7.65E+02 9.38E+01 0
626.2178 14042.7010358704 3370.317095846 -6.75E+02 7.92E+01 0
696.9680 Total
Hin reboiler
122.4497 C = 395.5997 K
25 C = 298.15
0.6043 70172.915418937 76673499.69466 1.20E+09 -1.75E+10 0
70.1459 858473.450242245 0 0.00E+00 0.00E+00 0
626.2178 0 0 0.00E+00 0.00E+00 0
696.9680 GAK KUITUNG KARNA CP/Rnya mirip feed Total
Hin reboiler 24418.373215341
Qreboiler 4173.15820889839
Hin kondense
122.4497 C = 395.5997 K
25 C = 298.15
19.5396 780372.383664324 0 0.00E+00 0.00E+00 0
6944.4444 0 0 0.00E+00 0.00E+00 0
0.0000 0 0 0.00E+00 0.00E+00 0
Hin reboiler GAK KUITUNG KARNA CP/Rnya mirip feed Total
Hin kondenser 244366.377292242

Qkondenser 10302.4230522363
OUTPUT
H, kkal/jam
TOP
2179.570767
231884.3835
80.04285826
2864.737881
25646.75069
10302.42305
272957.9087
0
Persamaan Antoine
N UAP TEKANAN UAP
C Komponen A B
240.479 Air 8.05573 1723.6425
233.08 MO 7.12851 1483.4864
223.816 MIBK 7.37701 1527.2068
219.745 DAA
279.12
213.95
Hasil Bawah
H2O = 0 0 0
C6H10O = 728.1055 7.41904931730181 99.000000136
C6H12O = 41.366 0.356112258953168 0.50000111203
C6H12O2 = 88.622 0.884804313099042 100
Bottom
xb
0.0047
0.8969
0.0984

P= 1.3 atm
T = 137.058324841764 oC
Komponen B,kmol/jam B, kg/jam Po
Air 0.0335 0.6043 3.297342768104

MO 6.3809 626.2178 1.2302171814358
MIBK 0.7003 70.1459 1.8375255270973
Total 7.1147 1
1 joule 0.239006 cal

R 1
Cp dt Cpdt (kJ/kmol) molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)
8727.58198734772 8727.58198734772 1.11786291441153 9756.24023614211 2331.79995388
14610.0237553545 14610.0237553545 70.0338493600805 1023196.2028297 244550.031654
14361.964565144 14361.964565144 6.38086183058512 91641.7115059431 21902.9189002
37699.5703078462 37699.5703078462 77.5325741050772 1124594.15457178 268784.750508

8410.11410229757 8410.11410229757 1.08432702697919 9119.31402110004 2179.57076693
13993.2794001364 13993.2794001364 69.3335108664797 970203.18934704 231884.383473
13757.3910040073 13757.3910040073 0 0 0
36160.7845064412 36160.7845064412 70.4178378934589 979322.50336814 234063.95424

9986.28558511066 9986.28558511066 0.033535887432346 334.89894924953 80.0428582643
17114.6526562867 17114.6526562867 0.70033849360081 11986.0500598049 2864.73788059
16816.8327807369 16816.8327807369 6.38086183058512 107305.886401937 25646.7506854
43917.7710221342 43917.7710221342 7.11473621161827 119626.835410991 28591.5314242

8727.58198734772 8727.58198734772 0.033535887432346 292.687207084263 69.9539986164
14610.0237553545 14610.0237553545 0.70033849360081 10231.962028297 2445.50031654
14361.964565144 14361.964565144 6.38086183058512 91641.7115059431 21902.9189002
37699.5703078462 37699.5703078462 7.11473621161827 102166.360741324 24418.3732153
8727.58198734772 8727.58198734772 1.08432702697919 9463.55302905784 2261.84595526
14610.0237553545 14610.0237553545 69.3335108664797 1012964.2408014 242104.531337
14361.964565144 14361.964565144 0 0 0
37699.5703078462 37699.5703078462 70.4178378934589 1022427.79383046 244366.377292
C
233.08
219.745
223.816
xb Ki Yi
0.0047 2.536418 0.011956

0.8969 0.946321 0.848709
0.0984 1.413481 0.139136
0.999800842
Data Komponen
Aseton C3H6O 58.08
Air H2O 18.02
Nikel Ni 58.69
Punya Kating Dulu

Hasil MD-02 Kating
Feed
kg/jam kmol/jam
H2O = 0
C6H12O = 0
Hasil MD-04 Yosua

P avg = 1.1
T avg = 118.7908297362
Komponen F,kmol/jam
Air 1.0843
MIBK 69.3335
Total 70.4178

P= 1
T = 99.99861302985
Komponen D,kmol/jam
Air 1.0843
MIBK 0.0000
Total 1.0843
Mass Balance
Bahan
Air
MIBK
SubTotal
Total
Inpt - Output
56.2 0.79 Komponen A B
Aseton 7.31742 1315.674
100 1 Air 8.05573 1723.643
167.9 0.9387 MIBK 7.37701 1527.207
270 1.84 MO 7.12851 1483.486
-252.8 0.0696 DAA 8.62593 2568.756
125 0.855 Asam Sulfat 8.28538 2976.837
1.94
115.9 0.802
Hasil Atas
H2O = 0 #DIV/0!
C6H12O = 0 #DIV/0!
HK di D = 0.01
LK di B = 0.01
Distillat Bottom
F, kg/jam Po alfa
D xd B
19.5396 1.88976237627259 1.7291 1.0843 1.0000 0.0000
6944.4444 1.09292115194129 1.0000 0.0000 0.0000 69.3335
1.0843 1.0000 69.3335 1.0000
atm
o
C
19.5396 1.00007936225664 1.0000 1.00007936225664 0.99992064404123

0.0000 0.602416129241516 0.0000 0.60241612924152 0
1 0.99992064404123
Input Output
19.5396 19.5396 0.0000
6944.4444 0.0000 6944.4444
6963.984021 19.5396 6944.4444
6963.984021 6963.9840
0
Persamaan Antoine
N UAP TEKANAN UAP
C Komponen A B C
240.479 Air 8.05573 1723.6425 233.08
233.08 MO 7.12851 1483.4864 219.745
223.816 MIBK 7.37701 1527.2068 223.816
219.745 DAA
279.12
213.95
Hasil Bawah
H2O = 0 #DIV/0!
C6H12O = 0 #DIV/0!
Bottom
xb
0.0000
1.0000

P= 1.2 atm
T = 121.941382857938 oC
Komponen B,kmol/jam B, kg/jam Po xb
Air 0.0000 0.0000 2.0887086115368 0.0000

MIBK 69.3335 6944.4444 1.2000703455305 1.0000
Total 69.3335 kmol/jam 1
6944.44444838661 kg/jam
166666.666761279 kg/hari
55000000.0312219 kg/tahun 330 hari
55000.0000312219 ton/tahun
Ki Yi
1.740591 0
1.000059 0.999941

FIX BANGET NM SAMA NP 4 Desember 2022 21.20

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FIX BANGET NM SAMA NP 4 Desember 2022 21.20

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Data Komponen

Komponen Komponen Mr Tb, oC

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George

Hasil TH-02 Kating

2 Aseton ---------> 1 DAA

Hasil TH-02 Yosua

2 Aseton ---------> 1 DAA

Kira Kira --> C3H6O =

Tmin Tmax Cp 25°C Cp Tmin

NERACA PANAS KELUAR

NERACA PANAS REAKSI, Cp H1

Cara Hitung Hidrogen masih bingung

0 0 H2O = 562.8918479167 31.237061482612

Punya Kating Dulu

Hasil TH-01 Kating

Hasil TH-01 Yosua

F, kg/jam D, kmol/jam D, kg/jam R + P, kmol/jam

700.1142 31.0816532165293 560.0914 7.7704

R, kmol/jam R, kg/jam P, kmol/jam P kg/jam

6.9934 126.0206 0.7770 14.0023

Hasil Recycle + Purge Hasil Recycle

Punya Kating Dulu

Hasil MD-02 Kating

Hasil MD-02 Yosua

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

Kondisi Atas (Distilat)

76912.9666 1.10479387283158 0.9995 1.00435806621052 0.99519368077165

Kondisi Bawah (Bottom)

Komponen B,kmol/jam B. kg/jam Po

Aseton 13.3764 776.8987 6.0623268405337

1 joule 0.239006 cal

Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)

Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)

Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)

Cp dt molflow (kmol/jam) H = N Cp dt (KJ/jam) H(kkal/jam)

0.0995 4.663328 0.4639102078448

Punya Kating Dulu

Hasil TH-02 Kating

Hasil TH-02 Yosua

Hasil MD-02 Yosua

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

Kondisi Atas (Distilat)

Feed Hasil Atas

86.171130018341 518.69820199778 0.095367

mol H2SO4 massa H2SO4 massa air mol air

eed (Biasa) Hasil Atas

Gk ada recycle mo Katalis

2064.7487 1.79985459233914 0.5490 1.499879 0.3660359886151

NPNYA ADA REAKSINYA GATAU WEH

Hasil Atas Hasil Bawah

Hasil Bawah MO 0.00500000313

Cara Hitung Hidrogen masih bingung

Hasil atas 97%

Kondisi Bawah (Bottom)

Air 0.0000 0.0000 24.930513 0.0000 17.80751

1/4DT4 E/2T2 Cp dt molflow (kmol/jaH = N Cp dtH(kkal/jam)

1/4DT4 E/2T2 Cp dt molflow (kmol/jaH = N Cp dtH(kkal/jam)

1/4DT4 E/2T2 Cp dt molflow (kmol/jaH = N Cp dtH(kkal/jam)

1/4DT4 E/2T2 Cp dt molflow (kmol/jaH = N Cp dtH(kkal/jam)

Punya Kating Dulu

Hasil MD-02 Kating

Hasil MD-02 Yosua