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DEPARTMENT OF APPLID CHEMISTRY & CHEMICAL TECHNOLOGY

UNIVERSITY OF KARACHI.

B.Sc. (HONS) COURSE TITLE

B.Sc. (Hons) 1St. year (1st. Semester)

Course No. TOPIC CR. HRS REMARKS

AC-301 General Chemistry 2+1 Passing Head


AC-303 Engineering Drawing & Workshop Practice 0+3 50 Marks

B.Sc. (Hons) 1st. year (2nd. Semester)

AC-302 Chemical Engineering –I (Stochiometry) 3+0 50 Marks


AC-304 Chemical Engineering – II (Unit Operation) 2+1

B.Sc. (Hons) 2nd. year (1st. Semester)

AC-401 Chemical Process Industries Inorganic-1 2+1


AC-403 Chemical Process Principles-I (Thermodynamic) 2+1
AC-405 Computer Science - I 2+1 Passing Head

B.Sc. (Hons) 2nd. year (2nd. Semester)

AC-402 Chemical Process Industries Organic-1 2+1


AC-404 Chemical Process Principles-II (Equilibrium) 2+1
AC-406 Computer Science - II 2+1

B.Sc. (Hons) 3rd. year (1st. Semester)

AC-501 Chemical Process Industries Inorganic-II 2+1


AC-503 Polymer Science 2+1
AC-505 Chemical Process Industries Organic-II 2+1
AC-507 Chemical Engineering – III (Fluid Mechanics) 2+1
AC-509 Analytical Techniques 2+1

B.Sc. (Hons) 3rd. year (2nd. Semester)

AC-502 Chemical Process Industries Inorganic-III 2+1


AC-504 Textile Processing 2+1
AC-506 Chemical Process Industries Organic-III 2+1
AC-508 Industrial Economics & Business Management 3+0
AC-510 Chemical Process Principles-III (Dynamics) 2+1
DEPARTMENT OF APPLID CHEMISTRY & CHEMICAL TECHNOLOGY
UNIVERSITY OF KARACHI.
M.Sc. (FINAL) COURSE TITLE

(1ST. SEMESTER)
COMPULSORY COURSES

Course No. TOPIC CR. HRS REMARKS

AC-601 Chemical Engineering –I (Heat and Mass Transfer) 2+1


AC-603 Chemical Engineering -II (Chemical Reaction Engg.) 2+1
AC-605 Analytical Techniques & Qual. Control-I (Spectroscopy) 2+1

SPECIALIZATION COURSES

AC-607 Chemical Process Principles-I (Equilibrium Process) 3+0


AC-609 Chemical Process Industries Inorganic-1 2+1
AC-611 Petroleum & Petrochemicals –I (Petroleum Tech.) 2+1
AC-613 Pharmaceutical Industries –I 2+1
AC-615 Polymer Technology –I 2+1
AC-617 Textile Processing –I 2+1
AC-619 Food Science & Technology –I 2+1
AC-621 Metallurgy & Materials Technology –I 2+1

OPTIONAL COURSES

AC-623 Research Project 0+3


AC-625 Electro Chemical Industries 2+1
AC-627 Polymer Rheology 2+1
AC-629 Leather Technology 2+1
Ac-631 Fuel Technology & energy Resources 2+1
Ac-633 Engineering Materials 2+1

(2nd. SEMESTER)
COMPULSORY COURSES

Course No. TOPIC CR. HRS REMARKS

AC-602 Chemical Engineering –III (Plant Design) 3+0


AC-604 Industrial Pollution 2+1
AC-606 Analytical Techniq.& Qual. Control-II (Chromatography) 2+1

SPECIALIZATION COURSES

AC-608 Chemical Process Principles-II (Flow Process) 3+0


AC-610 Chemical Process Industries Inorganic-II 2+1
AC-612 Petroleum & Petrochemicals –II (Petrochemicals) 2+1
AC-614 Pharmaceutical Industries –II 2+1
AC-616 Polymer Technology –II 2+1
AC-618 Textile Processing –II 2+1
AC-620 Food Science & Technology –II 2+1
AC-622 Metallurgy & Materials Technology –II 2+1
AC-624 Industrial Training 0+3
DEPARTMENT OF APPLID CHEMISTRY & CHEMICAL TECHNOLOGY
UNIVERSITY OF KARACHI.

MPROPOSED COURSE PLAN FOR B.S. (ACH) MORNING

(1ST. SEMESTER)

FIRST YEAR

C. No.AC-301 (General Chemistry) 2+1 (passing Head)

INORGANIC CHEMISTRY

Types of bonding, co-ordination compounds, Source of metals, Ore preparation.

ORGANIC CHEMISTRY

Nomerclature, Inter-conversion of functional groups.

PHYSICAL CHEMISTRY

Kinetic molecular theory of gases, Dilute solutions.

PRACTICALS ARE BASE ON FOLLOWING TOPICS:

1. Preparation of alum, Sizing & screening of ores, Calcinations of calcareous


materials.
2. Element detection, Functional group determination.
3. Preparation of solutions Basic volumetric anlysis.

BOOKS

1. J.E. Brady, General Chemistry: Principles & Structures, John Wiley& Sons, New
York, 1990.
2. S.Z. Haider, Introduction to Modern Inorganic Chemistry, Friends International,
1994.
3. Brescit, Arents, Meislich, Turk, General Chemistry, 5th. Ed., Harcourt Brace
Jovanovich Publishers, New York, 1988.
4. M.J. Winter, Chemical Bonding, Oxford Science Publications, Ozford, 1994.

5. I.L.Finar, Organic Chemistry: The Fundamental Principles, Vo. 1, 6th. Ed.,


ELBS,Longman, Essex, 1986.

6. P.W.Atkins, Physical Chemistry, 4th. Ed., ELBS,Oxford University Press, Oxford,


1990.

C. No.AC-303 (Engg. Drawing & Workshop) 0+3 (50 marks)

ENGINEERING DRAWING

Basic drawing techniques, projection of simple solids, lettering and dimensioning,


isometric & pictorial projection, freehand sketching.

WORKSHOP PRACTICE

Working tools, lathe machine, shaper machine, carpenter work.


BOOKS

1. T. E. French, C. J. Vierck, R. J. Foster, Engineering Drawing & Graphic


Technology, McGraw Hill, New York, 1993.
2. O.Ostrowsy, Enginnering Drawing for Technicians, Vol.1 & 2, ELBS 1985.

3. R.R.Kibbg, Machine Toll practice, John Wiley & Sons.

(2ND. SEMESTER)

FIRST YEAR

C. No.AC-302 Chemical Engineering-I(Stoichiometry(3+0) (50 Marks)

General Principles, Conservation of mass, Liquefaction & vaporization, Humidification,


Equilibrium Distribution Curve, Material & energy balance with and without chemical
reactions, Recycle combustion processes, Energy balance.

BOOKS

1. E.V.Thompson, W.H. Ceckler, Introduction to Chemical Enginering, Internation


Student Edition, McGraw-Hill 1982.

2. O.A.Hougan, K.M.Watson, R.A. Ragatz, Chemical Process Principles: Material


and Energy Balancaes, Part-1, 2n. ed., John Wiley &Sons, New York, 1973.

3. J.M.Smith, H.C. Van Ness, and M.M.Abbott, Introduction to Chemical


Engineering Thermodynamics, 5th. Ed., McGraw_hill New York, 1996.

C. No.AC-304 Chemical Engineering-II(Unit Operations(2+1)

SIZE REDUCTION OF SOLIDS

Mechanisms of size reduction, Energy and power requirements, Rittinger's law, Bond's
crushing law work index, Size reduction requirement.

MECHANICAL SEPARATIONS

Screen analysis, Material Balance over screen, Capacity and Effectiveness of screens.

MIXING (LIQUIDS AND SOLIDS)

Mixing of liquid systems, propellers and agitators, velocity in agitated vessel (Reynolds
number) Power consumption in agitated wessel, equipment for solid & paste missing.

DRYING

Principles of drying, Rate of drying, Mechanism of moistre movement, drying


equipment.
DISTILLATION

Various types of distillation, Continuous and batch distillation, Constant reflux and
constant composition, HETP and lower (McCabe-Thiele's diagram), Efficiencies of
different packing.
PRACTICALS ARE BASE ON FOLLOWING TOPICS:

1. Size separation
2. Size reduction
3. Mixing of liquids
4. Drying
5. Distillation

BOOKS

1. j.m.Colulson, J.F. Richardson, J.H. Backhurst, J.H. Harker, Chemical


Engineering, Vol. 2, Pergamon Press. 1990.

2. W.L. McCabe, J.C. Smith, P. Harriott, Unit operations of Chemical Enginering,


5th. Ed., McGraw Hill, New Yourk, 1993.

SECOND YEAR
(1ST. SEMESTER)

C. No.AC-401 (Chemical Process Industries In-Organic-I) 2+1

SULFUR & SULFURIC ACID

Sources of sulfur, Recovery of sulfur from flue and fuel gasses, Burners for sulfur and
sulfides, Contact process, Kinetics of the oxidation of SO2 to SO3 Role of catalyst,
Burification of sulfuric Acid.

CAUSTIC SODA & CHLORINE

Purification of brine, Production of caustic soda from diaphragm & mercury cell, Merits
and demerits of electrolytic cells in the production of caustic soda, Purification &
handling of caustic soda, By-products of chlorine & related industries.

PHOSPHORIC ACID & RELATED PRODUCTS

Production of H3PO4 by dry & wet Processes, Merits & demerits of these processes
Match industry, Baking powders.

FERTILIZERS

Minor & major nutrients, Nitrogen, phosphorus & mixed fertilizers.

INORGANIC PIGMENTS

Production, properties & applications of white & coloured pigments

PRACTICALS ARE BASE ON FOLLOWING TOPICS:

1. Determination of the strength of strong acid by titration


2. Determination of the sodium content in washing soda
3. Estimation of available chlorine in bleaching powder / liquid bleach.
4. Determination of sulphate as barium sulphate gravimetrically
5. Standardization of sodium thiosulfate against potassium dichromate
6. Estimation of phosphate in phosphate fertilizer.
7. Estimation of nitrogen in urea.
8. Preparation of coloured pigments (iron oxide / lead chromate)
9. Estimation of Fe/Pb in coloured pigments
10. Estimation of separate amount of NaOH & Na2Co3 in a given mixture
11. Standardization of permanganate.

BOOKS

1. G. T. Austin, Chemical Process Industrties, 6th. Ed., McGraw-Hill, New York,


1997.
2. J.A. Kent, Riegel's Handbook of Industrial Chemistry, 8th. Ed.m Van Nostrand
Reinhold company, New York, 1983.
3. K. Othmer, Encyclopedia of Chemical Technology, A Wiley Interscience
Publication, 1997.

C. No.AC-403 Chemical Process Principles –I (Thermodynamics) 2+1

FIRST LAW OF THERMODYNAMICS AND OTHER BASIC CONCEPT

The concept of internal energy, Formulation of the first law of thermodynamics, The
concept of enthalpy, the steady-state-flow process, Equilibrium and the phase rule, The
reversible process, Heat capacity, Constant-volume constant-pressure constant-
temperature adiabatic and polytrophic process.

VOLUMETRIC PROPERTIES OF PURE FLUIDS

The pressure-volume-temperature behavior of pure substance, The virial equation,


cubic equations of state (van der waais, Redlich-kweng, soave, reng-robinsons),
Generalized correlations for gases with emphasis to lee-Kessler equation, pvt properties
of liquids.

HEAT EFFECTS

Hansible heat effects, Heat effects accompanying phase changes, heat effects of
chemical reactions.

SECOND LAW OF THERMODYNAMICS

The second law of thermodynamics, The heat engine, Thermodynamic temperature


scale, Carnot cycle for an ideal gases, The concept of entropy, Entropy changes for an
ideal gases, Principle of increase of entropy.

THERMODYNAMIC PROPERTIES OF PURE FLUIDS

Relationships among thermodynamic properties for a homogeneous phase of constant


composition, Residual properties, Two-phases systems, Generalized correlations of
thermodynamic properties for gases.

PRACTICALS ARE BASE ON FOLLOWING TOPICS:

1. Ratio of heat capacities of gases


2. Heat of neutralization of strong acids and strong bases by calorimetric methods.
3. Heat of formations by combustion techniques.
4. Integral heat of solutions
5. Entropy and Gibbs energy changes of solutions
6. Partial molar volumes in binary mixtures.
BOOKS

1. j.m.Smith, H.c. Van Neess, M.M.Abbott, Introduction to Chemical Engineering


Thermodynamics, 5th. Ed., McGraw-Hill, New York, 1996.
2. K.S. Pitzer, Thermodynamics, 3rd. ed., McGraw_hill, New York, 1995.

3. T.D. Eastop, A. McConkey, Applied Thermodynamics for


Engineering.Thechnologists, 5th. Ed., ELBS, Longman, Essex, 1998.

4. R.C.Reid, J.M. Prausnitz, B.E. Foling, The properties of Gases and liquids, 4 th.
Ed., Mc.Graw-Hill, New York, 1988.
5. P.Benedek, Olti, Computer Aided Chemical Thermodynamics of Gases and
liquids: Theory, Models, Programs, John Wiley & Sons, New York, 1985.

C. No.AC-405 (Computer Science –I ( 2+1) (Passing Head)

INTRODUCTION TO COMPUTER

Introduction to computers, Hardware basics, Peripherais devices, Software basics,


Working with words, Caliculation, Visualization and simulation, Graphics, Hypermedia
and multimedia, Database applications and implications, Networking and
telecommunication.

CONCEPTS OF PASCAL AND C LANGUAGE (BEGINNERS LEVELS)

Variables, Constants, Operators, Data types (chair, word, ral, integer, Boolean, floating,
string, arrays), Program reading and declaration, Input / Output, Basic baranching and
looping, simple functions.

PRACTICALS ARE BASE ON FOLLOWING TOPICS:

1. Simple programming exercises in Pascal and C language.

BOOKS

1. C.S. French, Computer studies, 4th. Ed., ELBS, 1993.


2. B.W. Kernighan, D.M.Ritchie, The C Programming language (ANSIC) Pertie hall
Softwere series
3. R.Kemp, Pascal for students, 2nd. Ed., ELBS 1988.
4. B.S.Gotfried, Programming with Pascal, 2nd. Ed., Schaum's outline series,
McGraw Hill International Edition 1994.

SECOND YEAR
(2ND. SEMESTER)

C. No.AC-402 (Chemical Process Industries Organic-I) 2+1

UNIT PROCESSES

Introduction, Agents, Thermodynamics, Kinetics and mechanisms with industrial


examples of Nitration, Halogenation, Sulphonation and sulphation, Amination,
Oxidation, Hydrolysis, Esterification.
PRACTICALS ARE BASE ON FOLLOWING TOPICS:

1. Determination of optimum conditions for nitration


2. Pilot plant nitration
3. Extraction and hydrogenation of oil
4. Sulphonation of naphthalene

BOOKS

1. p.h. Greggins, Unit Processes in Organic synthesis, 5th. Ed., McGraw Hill, New
York.
2. K.Othmer, Encyclopedia of Chemical Technology, A Wiley Intesrscience
Publication, 1997.

C. No.AC-404 (Chemical Process Principles –II (Equilibrium) 2+1

PHASE EQUILIBRIUM

Solution thermodynamics of ideal systems, Surface phenomena, Colloids and


surfactants.

CHEMICAL REACTION EQUILIBRIUM

Application of equilibrium criteria to chemical reactions, The standard Gibbs energy


change and the equilibrium constant, Effect of temperature on equilibrium constant,
Evaluation of equilibrium constant, Relation between equilibrium constant and
compositions, Calculation of equilibrium conversions for single reactions.

ELECTROCHEMICAL EQUILIBRIUM

Electrochemical potential, Electrode potential, Electrochemical series, Galvanic cells.

PRACTICALS ARE BASE ON FOLLOWING TOPICS:

1. Critical solution temperature of binary mistures


2. Mutual solubility of three component systems
3. Equilibrium constants
4. Partition coefficients
5. Surface area by adsorption isotherms
6. Dissociation constant by conductmetric and e.m.f. methods
7. Electrode potentials

BOOKS

1. j.m. Smith, H.C. Van Ness, and M.M.Abbott, Introduction to Chemical


Engineering Thermodynamics, 5th. Ed., McGraw-Hill New York, 1996.

2. H.C.Van. Ness, and M.M.Abbott, Classical Thermodynamics of Non-electrolyte


solutions: With Applications to phase equilibria, McGraw_hill, New York, 1982.

3. W.R. Smith, R.W. Missen, Chemical Reaction Equilibrium Analysis, John Wiley &
Sons, New York, 1982.

4. R.C.Reid, J.M.Prausnitz, and B.E. Poling, The Preperties of Gases and liquids,
4th. Ed., McGraw-Hill Now York 1988.

5. J.M.Smith, Chemical Engineering Kinatics, 3rd. ed. McGraw_hill New York 1987.
6. P.W.Atkins, Physical Chemistry, 4th. Ed., Oxford University Press, Oxford, 1990.

7. J. Koryta, and J.Dvorak, Principles of Elecatrochemistry, Wiley, Chichester,


1987.

C. No.AC-406 (Computer Science –II ( 2+1)

OPERATING SYSTEMS

Operating systems with and without GUI (Graphic User Interface), concept of UNIX<
Concept of LAN and WAN.

APPLICATION PROGRAMS

----xt Editor, Presentation, Mathematical modeling, simulation, database, worksheets,


Utilities.

COMPUTER PROGRAMMING LANGUAGES (PASCAL & C)

Language constructs, structured programming, Branching and looping, Recursion,


Functions and subroutines, Pointers, Files, Records.

NUMERICAL ANALYSIS

Linear equations, and matrix analysis, Error analysis and Taylor expansion,
Interpolation, Least squares analysis, Root finding techniques and non linear
Equations, Optimization and linear programming, Numerical integration, Numerical
differentiation.

SOFTWARE DESIGNING

Software specification, Software design, software conding, Software testing.

PRACTICALS ARE BASE ON FOLLOWING TOPICS:

1. Developments of programs for numerical techniques.


2. Application of numerical techniques to the problems of chemistry and chemical
engineering.
3. Software development in connection to Chemical Engineering.

BOOKS

1. B. W. Kernighan, D.M.Ritchie, The C Programming Language (ANSIC), Prentice


Hall Software Series.
2. R.Kemp, Pascal for Students, 2nd ed., ELBS I993.
3. B.S.Gotried, programming with hpascal, 2nd. Ed. Schaum's outline series,
Mc.Graw Hill Internationa edition, 1994
4. K.Atkinson, ElementaryNumerical Analysis, 2nd. Ed., john Wiley, 1992.
5. F.Schelid, Numerical Analysis, 2nd. Ed., Schaum's Outline series, McGraw Hill
International Edition, 19989.
6. O.T. Hunna, O.C. Sandall, computational methods in chemical engineering,
prentice Hall, 1995.
7. D.Kananr, C. Moler, S. Nash, Numerical Mathods and software, Prentice Hall,
1989.
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PRACTICALS:

01. Tensile test, Ferrous, Nonferrous, Polymers, Composites, Specimen preparation


and testing.

02. Compression test, Cements, Composites.

03. Hardness test, Ferrous, Nonferrous, Polymers, Composites.

04. Photosensitivity tests of thin films.

05. Resistance testing of super conducting materials.

06. Microscopy of materials.

BOOKS:

1. ENGINEERING Materials, Kenneth G. Budinski K., Preentie Hall Publisher,


1998.
2. Material Science and Enginerin, William D. Callister, Wiley John & Sons, Inc.,
1999.
3. Modern Physical Metallurgy and Materials Engineering, R.E. Smallman, R.J.
Bishop, Butterworth- Heinemann, 2000.
THIRD YEAR

FIRST SEMESTER
Course No. AC-501
Chemical Process Industries Inorganic-II
2+1 Credit Hours

Phase Diagram & Applications:

Crystal structures, solid solutions, Interstitial & substitutional solid solutions, Rules for
formation of solid solutions, Binary system of alloys, complete solid soluble system,
Eutectic transformations with and without terminal solid solubility, Peritectic
transformation, Eutectic transformation, Lever rule, Calculation for composition of
phases, Binary systems of Cu-Ni, Cu-Zn, Al – Si, Ca – Mg, Fb – Sn & Fe – C.

Cement:

Type of cements, Manufacturer of ordinary Portland Cement, Equipment & Chemical


reactions, Merits & demerits of wet & dry processes, setting & hardening of Portland
Cement, Different type of special cements and their composition & applications, Ternary
Phase diagram of the system.

Glass:

Type of Glasses, Raw materials & their sources, Chemical reactions during
manufacture, Furnaces used, Finishing operations, Special glasses and their
composition & applications, Ternary phases diagram of the system.

Ceramics:

Production of white-wares, ceramic tiles, pottery, enamels & enameled metal-wares.

Practicals are Based on Following Topics:

1. Detailed Portland Cement analysis i.e. loss on ignition, estimation of total silica,
determination of CaO, determination of sesqui oxides (Al2O3 / Fe2O2)

2. Analysis of copper in an alloy

3. Analysis of nickel in an alloy.

4. Estimation of Zinc as Zinc pyrophosphate.


5. Electroplating on a metallic surface.

6. Electroplating on a non-metallic surface

7. Compression testing of cement blocks

8. Estimation of magnesium by complexometric titration.

9. Estimation of aluminium by complexemetric titration.


Books:

1. Dinsdale, Pottery Science: Materials, Processes & Products, Ellis Horwood Ltd.,
1986.

2. G. T. Austin, Chemical Process Industries, 6th ed., McGraw Hill, New York, 1997.

3. K. Othmer, Encyclopedia of Chemical Technology, A Wiley Interscience


Publication, 1997.

4. H. G. Pfaneder, H. Schroeded, Schott’s Guide to Glass, Van Nostrand Reinhold


Company, New York, 1990.

Course No. AC-503


Polymer Science
2+1 Credit Hours

Fundamentals of Polymer Science:

Fundamental definitions, Classification an types of polymers, Configuration and


conformation isomery, Bonding, Single molecules, Network molecules, Cohesive energy
density, Thermodynamics of binary solutions.

Synthesis of Polymers & Polymerization Processes:

Chain (Free radical and ionic), Condensation and Ring scission polymerization, Co-
polymerization, catalyzed and heterogeneous polymerization, Polymerization of
heterocyclic monomers, Polymerization in structured systems, Bulk, solution,
suspension and emulsion polymerization processes.

Polymer Chains and Their Characterization:

Molecular weigh and its distribution, measurement of molecular weight and size of
polymer, End, group analysis, Colligative properties measurement, Light scattering,
solution viscosity and molecular size, Ultra centrifugation, Poly-electrolytes.

Structure and Properties of Polymers:

1. Structure of crystals, Crystallization and melting, Glass transition

Chemical Transformation of Polymers

Degradation, Cross linking reaction

Practicals are based on following topics.

1. Synthesis of high Polymers (free radical polymerization of methyl methacrylate,


solution polymerization of vinyl acetate, emulsion polymerization of styrene,
condensation polymerization amides and imides)

2. Determination of rate of polymerization.

3. Determination of rate of initiation.

4. Eng group analysis.


5. Determination of molecular weight of polymers by viscometery.

6. Determination of molecular weight of polymers by gel permeation


chromatography.

7. Hardness and Fatigue tests of rubbery polymers.

8. Tensile and creep tests of thermoplasts and thermosets.

9. Determination of moisture content of polymers.

Books:

1. Arora, Singh, Polymer Chemistry, Anmol Publications Pvt. Ltd., New Delhi, 1994.

2. P. Munk, Introduction to Macromolecular Science, Wiley Interscience, 1989.

3. J. M. G. Gowie, Polymer Chemistry and Physics, Chapman, London, 1994.

4. R. J. Young, Introduction to Polymers, Chapman and Hall, 1997.

5. Y. Grosberg, A. R. Khokhlov, Giant Molecules, Academic Press, New York,


1997.

6. F. Rodriguez, Frinciples of Polymer Systems, 4th ed., Taylor and Francis, 1996.

7. N. G. McCrum, C. P. Bucley, C. B. Bucknell, Principles of Polymer Engineering,


2nd ed., Oxford, 1997.

8. D. W. Van Krevelen, Properties of Polymer, 3rd ed., Elsevier. Science, 1994.

9. G. Moad, D.H. Solomon, The Chemistry of Free Radical Polymerization, Elsevier


Science, 1994.

10. Odian, George, Principles of Polymerization, 3rd ed., John Wiley & Sons, New
York, 1991.

11. S. L. Rosen, Fundamental Principles of Polymeric Materials, 2 nd ed., John Wiley


& Sons, New York, 1993.

12. J. Brandrup, E. H. Immergut, Polymer Handbook, 3 rd ed., John Wiley & Sons,
New York, 1989.
Course No. AC-505
Chemical Process Industries Organic-II
2+1 Credit Hours

Paper & Pulp:

Kinds & manufacture of pulp, Manufacture of paper, Equipment employed.

Oils & Fats:

Sources, Properties, Processing, Industrial application.

Paints & Surface Coating Materials:

Pigment details, Varnishes, Industrial Coatings, Manufacture of paints sugar.

Sugar:

Sources, uses & economics, Manufacturing & refining.

Soap:

Uses & economics, Raw materials, Manufacture, By product.

Dyes & Dyestuffs:

Classification, Properties, Manufacture, Dye Intermediates.

Pharmaceuticals:

Classification, Alkylation, Acrylation, Complex chemical conversions, Fermentation for


antibiotics, Vitamins.

Practicals are based on Following Topics:

1. Determination of moisture and Rosin content of paper.

2. Determination of peroxide value of oil.

3. Determination of fatty acid value.

4. Determination of saponification value of oil

5. Preparation of fluorecene and Rosin dye.

6. Preparation and analysis of liquid soap i.e., matter insoluble in alcohol, free alkali
or free acid, Volatile matter.

7. Extraction of Mustard oil by soxhellet apparatus.

8. Qualitative and quantitative analysis of sugar.

9. Preparation and analysis of mild tincture of Iodine.


Books:

1. Natural Products Chemistry, Vol. 2 Academic Press, New York & London, 1987.

2. V. H. HuBaliys, Industrial oil & Fat Products, Vol. 4, 5th ed., 1996.

3. P. J. Hamilton, A. Bhati, Fats and Oils: Chemistry & Technology, Applied Science
Publishers, 1980.

4. The Pharmacological Basis of Therapeutics, Vol. 2, 5th ed., 1975.

5. G. T. Austin, Chemical Process Industries, 6th ed., McGraw Hill, New York, 1997.

6. A. Burger, Medicinal Chemistry, 5th ed., 1995.

7. K. Othmer, Encyclopedia of Chemical Technology, A Wiley Interscience


Publication, 1997.

8. J. P. Casey, Paper and pulp, Vol. 2, 3rd ed., Interscience Publications, 1983.

Course No. AC-507


Chemical Engineering-III (Fluid Mechanics)
2+1 Credit Hours

Introduction to Transfer Processes, Fluid Mechanics

Density, viscosity. Pressure and head, Uniform and steady flow, Laminar and turbulent
flow

Concepts of Ideal Fluid Flow

Fluid flow rate, Continuity equation, Commercial pipes and tubes, Bernoulli’s equation,
Momentum equation, Angular motion, Velocity and flow measurement (Pitot tube,
Venturi meter, Orifice meter), Elementary theory of notches and wires, Padial flow and
vortex motion, Two dimensional ideal flow, Flow past cylinders with circulation.

Behaviour of Real Fluids

1. Laminar and turbulent flow in bounded systems


(a) Flow in circular pipes, velocity profiles and Hagen-Poiseulle’s equation
(b) Steady and uniform turbulent flow in circular pipes
(c) Friction factors
(d) Losses in expansion / contraction
(e) Velocity distribution in fully developed turbulent flow in pipes.
(f) Fluid machines and pumps

2. Drag, Flow through beds


3. Fluidisation

Boundary Layers

Pipe flow at entrances, Polhausen’s analysis for laminar boundary layers, properties of
laminar and turbulent boundary layers, Power law for turbulent flow.
Introduction to Computational Fluid Mechanics

Fluid difference representation, Couette flow with viscosity distribution, two dimensional
inviscid invicid incompressible flow

Dimensional Analysis and Similitude

Dimensions and equations, Buckingham theorem, Dimensional analysis methods,


vortex shedding and bubble rise, Approximate similitude methods.

Practicals are based on following topics:-

1. Discharge coefficients of nozzles and valves


2. Reynolds experiment and tube flow
3. Measurement of friction loss due to fittings and valves in pumping systems
4. Measurement of pressure head in pipes of varying construction materials.
5. Vortex flow and calculation of motor speed
6. Calibration of capillary viscometers and measurements of Newtonian and non-
Newtonian fluid viscosity

7. Net pump suction head calculation


8. Pressure drop and viscosity measurements of non-Newtonian fluids by piston
viscometer.

9. Determination of discharge coefficient for venturi


10. Determination of discharge coefficient for orifice.
11. Boundary layer velocity profile and thickness.
12. Verification of Stokes law

Books:-

1. J. Smiths, A Physical Introduction to Fluid Mechanics, John Wiley & Sons, New
York, 1999.

2. J. M., Kay, R. M. Nedderman, Fluid Mechanics and Transfer Processes,


Cambridge University Press, 1985.

3. J. M. Coulson, J. F. Richardson, J. H. Backhurst, J. H. Harker, Chemical


Engineering, Vol. 1, Pergamon Press, 1990.

4. W. L. McCabe, J. C. Smith, P. Harriott, Unit Operation, 1994 Engineering, 5 th ed.,


McGraw Hill, New York, 1993.

5. R. L. Mott, Applied Fluid Mechanics, 4th ed., Merrill Publication, 1994.


6. F. M. White, Fluid Mechanics, 3rd ed., McGraw Hill International Edition, 1994.
7. J. F. Douglas. J. M. Caiorek. J. A. Swaffield Mechanics, 2nd ed. ELBS Edition,
1990.
Course No. AC-509
Analytical Techniques
2+1 Credit Hours

Potentiometry

Modern and classical method of potentiometry, Differential potentiometric titration,


Automation in potentiometry, Graphical methods for selection of and point, Application
in quality control.

Conductometry

Instruments used for measurement of conductivity, Conductometric titration, Low and


high frequency titration, Applications of conducmetric titration.

Electrogravimetry

Theory of electrogravimetric analysis. Over potential, Completeness of deposition,


Electrolytic separation of metals, Electrolytic determinations at constant current,
Electrolytic determinations with controlled cathodes potential.

Coulmetry

General discussions, Coulmetry at controlled potential, coulmetry at constant current,


Instrumentation, External generation of titrant.

Amperometry

Apmerometric titration, Techniques of amperometric titration with dropping mercury


electrode, Titration with rotating platinum electrode, Bi-amperometric titration.

Voltametry

Introduction, Polarography, Direct current polarography, Alternating current


polarography, Anodic stripping, Use in quality and environmental control.

Practicals are based on following topics:-

1. Potentiometric location of end point


2. Conductometric location of end point
3. Analysis of super alkalis
4. Determination of alcohol content in cough syrup
5. Estimation of hydrogen peroxide in solution.
6. Determination of copper in brass plating solution.
7. Amperometric titration of thiosulfate with iodine (dead stop end point).
8. Fast sweep DC polarography with dropping mercury electrode
9. Draw the polarographic spectrum of manganese, zinc, nickel and copper ions.
10. Determination of environmentally poisonous cadmium ion by standard addition
methods.
11. Determination of environmentally poisonous cadmium ion by calibration curve
method.
Books:-

1. L. G. Hargis, Analytical Chemistry, Prentice-Hall, New Jersey, 1988.


2. R.D. Braun, Introduction to Chemical Analysis, McGraw Hill, New York 1983.
3. R. A. Day Jr. A. L. Underwood, Quantitative Analysis, 6 th ed., Prentice-Hall, New
Jersey, 1991.

4. C. T. Kenner, Quantitative Analysis, Macmillan Publishing Co. Inc. New York,


1979.

5. J. S. Fritz, G. H. Schenks, Quantitative Analytical Chemistry, 4 th ed., Allyn and


Bacon Inc., Boston, 1979.

6. D. A. Skoog, D. M. West, Principles of Instrumental Analysis, Holt-Sauder Ltd.,


Japan, 1981.

7. R. L. Pecsok, L. D. Shields, T. Catrns, I. G. Mewillian, Modern Methods of


Chemical Analysis, John Wiley & Sons, New York, 1976.

8. H. H. Bauer, G. D. Christian, J. E. O’Reilly, Instrumental Analysis, Allyn and


Bacon Inc., Boston, 1978.
THIRD YEAR

SECOND SEMESTER
Course No. AC-502
Chemical Process Industries Inorganic-III
2+1 Credit Hours

Ellingham Diagrams & Applications in Extractive Metallurgy:-

Ellingham diagram of oxides, sulfides & chlorides, Role of carbon in metal extraction.

Production of Pig Iron:-

Reducing agents, Preparation of metallurgical Coke, Blast furnace reactions.

Mild Steel and Special Steels:-

Basic oxygen steel making, Electric steel making, HSLA steels, Stainless steel (ferritic,
austenitic, martensitic), Tool steel, Maraging Steel.

Production of Nickel:-

Source of nickel, Commercial processes for sulfide & oxide ores, Electrolytic nickel
refining.

Production of Titanium:-

Source of titanium, Treatment of Ilmenite concentrate, Production of titanium.

Production of Magnesium:-

Source of magnesium, Electrolytic production, Magnesium reduction process.

Important Ferrous & Non-Ferrous Alloys & their Applications:-

Fe-Ni, Fe-Cr Alloys, Ni-based Alloys, Ti-based Alloys, Mg-based Alloys

Practicals are based on following topics:-

1. Preparation metallurgical specimen for microscopic examination.


2. Microscopic examination of microstructure in ferrous alloys (determination of
grain size and volume fraction of pearlite & ferrite phases in a low carbon steel).

3. Microscopic examination of non-ferrous alloys.


4. Determination of hardness of metal by Brinell hardness tester.
5. Dissolution of iron ores & preparation of stock solutions.
6. Estimation of iron in ores.
7. Estimation of sulfur content in iron pyrite by ion exchange technique
8. Determination potassium by ion exchange technique.
9. Spectrophotometric determination of strength of KMnO4 solution.
10. Determination of magnesium as Mg-pyrophosphate.
Books:-

1. K. Othmer, Encyclopedia of Chemical Technology, A Wiley Interscience


Publication, 1997.

2. R. E. Smallman, R. J. Biship, Metal and Materials, Butterworth-Heinemann Inc.,


1995.

3. W. F. Smith, Principle of Material Science and Engineering, 3 rd ed., McGraw Hill,


New York, 1996.

4. P. H. Rieger, Electrochemistry, 2nd ed., Chapman and Hall Inc., New York, 1994.

Course No. AC-504


Textile Processing
2+1 Credit Hours

Introduction:-

Textile raw material, Yarn preparation, Procedures and machinery.

Textile Pre-treatment:-

Chemistry and technology of desizing, scouring and bleaching in relation to cotton, wool
and synthetic fibres.

Dyeing:-

Dyes and dyeing phenomenon, Classification of dyes in relation to cotton, wool and
synthetic fibres, Physical chemistry of dyeing.

Finishing:-

Finishing of fabrics with important stabilization procedures.

Practicals are based on following topics:-

1. Determination and establishing relationship of various yarn count systems of


synthetic and natural fibers.

2. Determination of construction of cloths.


3. Desizing of cloths.
4. Scouring of cloths and fluidity measurement.
5. Dyeing of synthetic fibres using different classes of dye stuffs (3 exercises).
6. Resin finishing treatment of cotton cloths.

Books:-

1. A. Ormered, Modern Preparation and Weaving Machinery, Butterworth, London,


1983.

2. A. L. Jakobi, Detergents and Terminate washing: Principle and Practice, VCH,


1987.
3. M. Lowin, S. B. Sellow, Chemical Processing of Fibres and Fabrics:
Fundamentals and Preparation, Part A & B, Chemical Publishing, New York,
1984.

4. E. R. Trotman, Dyeing and Chemical Technology of Textile Fibres, 4 th ed., Griffin,


London, 1986.

5. D. M. Nun, Dyeing of Synthetic Polymers: Acetate Fibres, SDC, Bradford, 1980.

Course No. AC-506


Chemical Process Industries Organic-III
2+1 Credit Hours

Fermentation:-

Industrial alcohol, Absolute alcohol, Butyl alcohol preparations, Vinegar & acetic acid.

Fuels (Solid, Liquid & Gases):-

Energy, Fossil fuels, Coal, Natural gas, Synthetic gas, Petroleum.

Rubbers:-

Natural rubbers, Properties, Synthetic rubbers, Manufacture, Specialties, Rubber


compounding.

Food & Nutrition:-

Food composition, Food ingredients, Energy concepts, Food processing.

Perfumes and Flavors:-

Constituents of perfumes & flavors, Synthetic & Semi Synthetic perfumes & flavors.

Leather:-

Sources, Tanning, Processing.

Practicals are based on following topics:-

1. Preparation and analysis of glyptal.


2. Preparation and analysis of Thiokol.
3. Extraction of perfumes from flowers using soxhellet apparatus.
4. Distillation of crude oil.
5. Distillation of coal.
6. Isolation of lactose and casein from milk.
7. Preparation and analysis of lotions.
8. Analysis of waxes.
9. Preparation of disinfectants.
10. Preparation of phthalic anhydride.
Books:-

1. Morton, Rubber Technology, 2nd ed., Litton Educational Publishers, 1973.


2. J. E. Mark, Science & Technology of Rubber, 2nd ed., Academic Press 1994.
3. P. M. Gaman, An Introduction of Food Science: Nutrition and Microbiology, 1989.
4. Martin, Geoffrey, Industrial & Manufacturing Chemistry, Part I, 8th ed., Organic
Technical Press Ltd., 1974.

5. H. A. Witt, C. Bryan, G. Ruben, Industrial Organic Chemicals in Perspectives:


Raw Material & manufacture, Part I, Wiley Interscience Publication, 1980.

6. G. T. Austin, Chemical Process Industries, 6th ed., McGraw-Hill, New York, 1997.

Course No. AC-508


Industrial Economics & Business Management
3+0 Credit Hours

Industrial Economics:-

Local Chemical and Other Industries:

Characteristics of local industry, Magnitude and growth.

Cost Estimation:

Capital and production cost, Cost index, Capital investment, Methods for estimating
capital investment, Estimation of product cost, Break even point and cash break even.

Interest and Investment Costs:

Type of interests, Present worth and discount, Annuities.

Depreciation:

Type of depreciation, Service, salvage and present value, Methods for determining
depreciation.

Project Evaluation:

Basis for evaluating project profitability, Discounted cash flow, capitalized cost, Pay out
period, Rate of return.

Business Management:

Industrial Management:

Essentials of industrial management, Organization, Market survey & marketing.

Analysis and Planning:

Network models PERT (Program evaluation and review technique) and CPM (Critical
Path method), Philosophical Foundation of PERT and CPM, Basic concepts of PERT
and CPM, Probabilistic analysis in PERT, Mechanics of PERT, PERT / Cost networks.
Books:

1. M. S. Peter, K. D. Timmerhous, Plant Design & Economics for Chemical


Engineers, 4th ed., McGraw Hill, 1991.

2. F. A. Holland, F. A. Wastson, Introduction to Process Economics, 2nd ed., John


Wiley & Sons, 1983.

3. H. Kerzner, Project Management: A System Approach to Planning, Scheduling,


and Controlling, 3rd ed., Van Nostrand Reinhold, New York, 1989.
Course No. AC-510
Chemical Process Principles – III (Dynamics)
2+1 Credit Hours

Chemical Kinetics:-

Chemical kinetic fundamentals, Evaluation of rate equations from laboratory data,


Simultaneous reactions, Theories of reaction rates.

Catalysis:-

Homogeneous acid-base catalysis, Heterogeneous catalysis, Solid catalysts and their


characterization, Rate equations for fluid-solid catalytic reactions.

Electrode Kinetics:-

Butler-Volmer equation, Total slopes, Effect of adsorption, Sherwood & Schmidt


numbers.

Practicals are based on following topics:-

1. Determination of Order of reactions by various techniques (integration,


differential and fractional life methods).

2. Activation energies and rate constants.


3. Tafel slopes.
4. Mobility and transport number of ions.

Books:-

1. J. M. Smith, Chemical Engineering Kinetics, 3rd ed., McGraw-Hill, New York,


1987.

2. K. J. Laidler, Chemical Kinetics, 2nd ed., McGraw-Hill, New York, 1965.


3. P. W. Atkins, Physical Chemistry, 4th ed., Oxford University Press, Oxford, 1990.
4. D. Pletcher, F. C. Walsh, Industrial Electrochemistry, 2 nd ed., Chapman and Hall,
London, 1990.

5. P. H. Rieger, Electrochemistry, 2nd ed., Chapman and Hall, New York, 1994.
DEPARTMENT OF APPLIED
CHEMISTRY AND
CHEMICAL TECHNOLOGY
UNIVERSITY OF KARACHI
PROPOSED COURSE PLAN FOR M. Sc.
FIRST SEMESTER
COMPULSORY COURSES

Course No. AC-601


Chemical Engineering – I
2+1 Credit Hours

Course NO. AC-603


Chemical Engineering – II (Chemical Reaction Engineering)
3+0 Credit Hours

Course No. AC-605


Analytical Techniques & Quality Control – I (Spectroscopy)
2+1 Credit Hours

SPECIALIZATION COURSES

Course No. AC – 607


Chemical Process Principles – I (Equilibrium Processes)
3+0 Credit Hours

Course No. AC – 609


Chemical Process Industries Inorganic – I
2+1 Credit Hours

Course No. AC – 611


Petroleum & Petrochemicals – I (Petroleum Technology)
2+1 Credit Hours
Course No. AC – 613
Pharmaceutical Industries – I
2+1 Credit Hours

Course No. AC – 615


Polymer Technology – I
2+1 Credit Hours

Course No. AC – 617


Textile Processing – I
2+1 Credit Hours

Course No. AC – 619


Food Science & Technology – I
2+1 Credit Hours

Course No. AC – 621


Metallurgy & Materials Technology – I
2+1 Credit Hours

OPTIONAL COURSES
Course No. AC – 623
Research Project
0+3 Credit Hours

Course No. AC – 625


Electrochemical Industries
2+1 Credit Hours

Course No. AC – 627


Polymer Rheology
2+1 Credit Hours

Course No. AC – 629


Leather Technology
2+1 Credit Hours

Course No. AC – 631


Fuel Technology & Energy Resources
2+1 Credit Hours

Course No. AC – 633


Engineering Materials
2+1 Credit Hours
PROPOSED COURSE PLAN FOR M. Sc.
SECOND SEMESTER
COMPULSORY COURSES

Course No. AC-602


Chemical Engineering – III (Plant Design)
2+1 Credit Hours

Course NO. AC-604


Industrial Pollution
2+1 Credit Hours

Course No. AC-606


Analytical Techniques & Quality Control – II (Chromatography)
2+1 Credit Hours
SPECIALIZATION COURSES

Course No. AC – 608


Chemical Process Principles – II (Flow Processes)
3+0 Credit Hours

Course No. AC – 610


Chemical Process Industries Inorganic – II
2+1 Credit Hours

Course No. AC – 612


Petroleum & Petrochemicals – II (Petrochemicals)
2+1 Credit Hours

Course No. AC – 614


Pharmaceutical Industries – II
2+1 Credit Hours

Course No. AC – 616


Polymer and Technology – II
2+1 Credit Hours

Course No. AC – 618


Textile Processing – II
2+1 Credit Hours

Course No. AC – 620


Food Science & Technology – II
2+1 Credit Hours

Course No. AC – 622


Metallurgy & Materials Technology – II
2+1 Credit Hours

Course No. AC – 624


Industrial Training
0+3 Credit Hours

OPTIONAL COURSES
Course No. AC – 623
Research Project
0+3 Credit Hours

Course No. AC – 625


Electrochemical Industries
2+1 Credit Hours

Course No. AC – 627


Polymer Rheology
2+1 Credit Hours

Course No. AC – 629


Leather Technology
2+1 Credit Hours

Course No. AC – 631


Fuel Technology & Energy Resources
2+1 Credit Hours

Course No. AC – 633


Engineering Materials
2+1 Credit Hours
DEPARTMENT OF APPLIED CHEMISTRY AND
CHEMICAL TECHNOLOGY
UNIVERSITY OF KARACHI

PROPOSED COURSE PLAN FOR M. Sc.

FIRST SEMESTER

COMPULSORY COURSES

Course No. AC – 601


CHEMICAL ENGINEERING – I (HEAT & MASS TRANSFER)
2+1 Credit Hours

INTRODUCTION:

Mechanism, Conduction, Resistance in series, Convention, Dimensional analysis, Radiation,


Heat transfer to fluid with or without phase change, CO and Counter heat exchange Shell and
tube types. Evaporation, extended surfaces, Cooling towers

INTRODUCTION TO MASS TRANSFER:

Diffusion: Inter – phase mass transfer. Gas – Liquid and liquid – liquid operation

PRACTICALS:

1. 1 – 2 heat exchange
2. Heating and Cooling in vessels
3. Cooling Towers
4. Diffusion
5. Extraction

BOOKS:

1. Kern. D. Q. Process Heat transfer Mc Graw Hill, 1988.


2. Coulson, J. M. & Richardson J. F. Chemical Engg. Vol – I Pergamon Press, 1994.
3. Treybal R. E. Mass Transfer Operations, Mc Graw Hill, 1986
Course No. AC – 603
CHEMICAL ENGINEERING – II CHEMICAL REACTION ENGINEERING)
3+0 Credit Hours

INTRODUCTION:

Classification of Chemical reactors, Fundamentals of Chemical reactor design, Mass balance


equation for ideal reactors.

DESIGN OF HOMOGENOUS REACTORS:

1. Isothermal Reactors:

Design procedures for stirred tank, and tubular flow reactors.

2. Non-isothermal Reactors

Energy balance equations, Design procedures for stirred tank, and tubular flow reactors.

Transport Processes in Heterogeneous Catalytic Reactions:

External transport process in the fixed – bed and the fluidized – bed catalytic reactors, Internal
transport process in porous catalytic i.e. Intrapellet mass transfer, Intrapellet heat transfer, Mass
transfer with reaction. Mass and heat transfer with reaction, Effect of internal transport on
selectivity and poisoning.

Interpretation of Experimental Kinetics Data:

Interpretation of laboratory kinetic data from homogeneous and heterogeneous laboratory


reactors, Calculation of the global rate.

Design of Heterogeneous Catalytic Reactors:

1. Fixed – bed Reactors

Design of isothermal and adiabatic fixed – bed reactors, Design of non isothermal – non
adiabatic fixed – bed reactors.

2. Fluidised – bed Reactors

BOOKS:

1. O. Levensreal, Chemical Reaction Engineering, John Wiley & Sons, 1992.


2. H. Scott Foglar, Elements of Chemical Reaction Engineering, Practice Hall, USA, 1992.
Course No. AC-605
ANALYTICAL TECHNIQUES & QUALITY CONTROL – I (SPECTROSCOPY)
2+1 Credit Hours
ELECTROMAGNETIC RADIATION:
Electromagnetic radiation; Nature of Electromagnetic radiation, Adsorption and emission
radiation; Luminescence phenomena; Reaction & refractive index; Interference and diffraction;
Light scattering; Rotation of polarized light.

INSTRUMENTS OF SPECTROMETRY:
Infrared spectroscopy: Theory, Sample preparation
Spectra: Interpretation of spectra.
Ultraviolet spectroscopy: Introduction, Theory, Salvation and substitution.
Flame Photometry: Emission and adsorption in flame, Atomic Emission spectrophotometry,
Atomic adsorption
Spectrophotometry: Atomic fluorescene spectrophotometry, Atomization, Flames and Burners,
Non-flame atomization.
PLASMA SPECTROPHOTOMETRY:
Introduction, Instrumentation, Plasma, appearance and spectra, Analytical application.

X-RAY SPECTROSCOPY:
Introduction & Instrumentation application, Emission, Dispersion and detection of x-rays,
Absorption and Diffraction of x-rays, Preparation of Samples, Quantitative X-ray fluorescence
analysis.

ELECTRONMICROBE:

Introduction, Instrumentation, Applications.

PRACTICALS:

1. Separation of Calcium by Ion-exchanger and its determination by Flame photometry in


baking powder.
2. Determination of trace amount of copper by Spectrophotometry.
3. Separation and estimation of Food dyes by Spectrophotometry.
4. Water Analysis.
5. Semi quantitative separation of Copper, Cobalt and Nickel on Slotted paper strips.
6. Analysis of dye mixtures by TLC and Spectrophotometry.
7. Determination of Phosphate in baking powder.
8. Determination of Plasticisers in Plastic product.
9. Analysis of super alkalies.
10. Determination of the adsorption curve and concentration of a substance by ultraviolet
spectrophotometers.
BOOKS:

1. Hargis, G. L. Analytical Chemistry, Prentice – Hall, Inc, New Jersey, 1988.


2. Kenner, C. T. Quantitative Analysis, Mecmillan Publishing Co., Inc. New York, 1979.
3. Fritz J. S., George H. Schenks; quantitative Analytical Chemistry, Fourth Ed., Allyn and
Bacon Inc. Bostan, 1979
4. Skoog D. A. & D. M. West; Principles of Instrumental Analysis, Holt – Saunder (Japan)
Ltd., 1981.
5. Pecsok, R. L.; Robert, L., Donald Shields, Thomas Cairns, Ian G. Mewilliam, Modern
methods of Chemical Analysis; John Wiley & Sons New York, 1976.
6. Vogel. A. I. Text book of Quantitative Inorganic Analysis, Ed.III, Longmans, 1961.
7. Dick, J. G. Analytical Chemistry McGraw Hill, 1973.
8. Willard, H. H.; L. L, Merritte & J. A. Dean; Instrumental Method of analysis 5 th Ed. D. Van
Inc 1978.
9. Bauer, H. H; Gary D. Christian and James E. O’Reiley; Instrumental Analysis, Allyn and
Bacon, Inc 1978.
10. Walton H. F. and Jorge Rayes; Modern Chemical Analysis and instrumentation Mercel
Dekker, Inc. New York, 1973.
SPECIALIZATION COURSES

Course No. AC – 607


CHEMICAL PROCESS PRINCIPLES – I (EQUILIBRIUM PROCESSES)
3+0 Credit Hours

THEORETICAL SOLUTION THERMODYNAMICS:

Partial properties, Fugacity and fugacity coefficient of a pure species fugacity and fugacity
coefficient for species in solution, Generalized correlations for the fugacity coefficient, Excess
properties, Bahavior of excess properties of liquid mixtures.

APPLIED SOLUTION THERMODYNAMICS:

Liquid phase properties from Vapour / Liquid equilibrium (VLE) data, Models for the excess
Gibbs energy, Property changes of mixing Heat effects of mixing processes.

VLE CALCULATIONS:

Dew Point and Bubble Point Calculation, Flash Calculations.

APPLICATION OF EQUATIONS OF STATE TO MULTI COMPONENT SYSTEMS:

Properties of fluid mixtures from Virtual and Cubic Equations of state, Properties of fluid
mixtures from generalized correlations.

PHASE EQUILIBRIA:

Equilibrium and stability, Liquid / Liquid equilibrium (LLE), Vapour / Liquid / Liquid equilibrium
(VLE), Solid / Liquid equilibrium (SLE), Solid / Vapour equilibrium (SVE).

CHEMICAL REACTION EQUILIBRIA:

Reactions in heterogeneous systems, Phase rule and Duhem’s theorem for reacting systems,
Multi reaction equilibria.

PRACTICALS:

1. Measurement of heat of mixing of binary mixtures at different temperature.

2. Measurement of volumes of mixing of liquid mixtures.

3. Determination of free energy changes.

4. Phase Equilibria study (liquid-vapour, liquid-liquid).

5. Determination of partial molar quantities.

6. Measurement of Equilibrium Constants.


7. Study of Phase rule.
BOOKS:

1. J. M. Smith, H. C. Van Ness, and M. M. Abbot, Introduction to Chemical Engineering


Thermodynamics, 5th Ed., McGraw Hill, New York, 1996.
2. H. C. Van Ness, and M. M. Abbot, Classical Thermodynamics of Non-electrolyte
Solution: With Applications to Phase Equilibria, McGraw Hill, New York, 1982.
3. J. M. Prausnitz, R. N. Lichtenthaler, and E. g. be Azevedo, Molecular Thermodynamics
of Fluid Phase Equilibria, 2nd ed., Prentice Hall, Englewood Cliffs, NJ, 1986.
4. P. Benedek, F. Olti, Computer Aided Chemical Thermodynamics of Gasses and Liquids:
Theory, Models. Programs, John Wiley & Sons, New York, 1985.

5. R. C. Reid. J. M. Prausnitz, and B. E. Poling, The Properties of Gasses and Liquids, 4 th


ed., McGraw Hill, New York, 1988.
Course No. AC – 609
CHEMICAL PROCESS INDUSTRIES INORGANIC – I
2+1 Credit Hours

SPECIAL CERAMICS:

Technical & Chemical Ceramics, Ceramics in the electrical industry, The ceramics for the new
technologies.

COMPOSITE MATERIALS:

Properties, Types & different materials

EXPLOSIVES & PROPELLANTS:

Characteristics, Types & applications of explosive & propellants.

FERTILIZER TECHNOLOGY:

Recent advancements and process control in the introduction of fertilizers, super & triple super
phosphate fertilizer, Role of fertilizer in agricultural soil.

SUPER CONDUCING MATERIALS:

Theory, types & application of super – conducting materials.

PRACTICALS: Practicals to be based on the following

1. Fertilizer analysis (Qualitative & Quantitative)


2. Material Testings to be performed different industries.

BOOKS:

1. The Science & Engineering of materials Donals R. AsReland PWS Published 1985.
2. Industrial Ceramics Felix Singer & Sonja S. Singer, Oxford & IBH Publishing Co PVY-
1963.
3. G. T. Austin “Shreve’s Chemical Process Industries” 5th edition 1988. McGraw Hill.
4. Kirk-Othmer Encyclopedia of Chemical Technology Joh Viley & Sons. 1984.
5. Materials & Technology Vol 1, 2, 3, Barnes & Noble Incorporation Longman Group Ltd.
1970.
6. Chemistry of Explosives Akkhavan, J. John Wiley & Sons; Incorp 1998.
7. Fertilizer Manufacture M. E. Pozin, Mir Publication 1986.
Course No. AC – 611
PETROLEUM & PETROCHEMICALS – I (PETROLEUM TECHNOLOGY)
2+1 Credit Hours

PETROLEUM PRODUCTION:

Introduction to Petroleum, Origin, geological survey, Drilling types of drilling equipment. Drilling
mud, completion.

PETROLEUM REFINING:

Chemistry, Desulphurization, Evaluation of oil stocks. Tube still heaters, Distillation towers.
Atmospheric and vacuum distillation, Stabilization. Thermal and catalytic cracking and
reforming. Chemical treatment, Transportation. Refinery gases. Testing of Petroleum Products.

PRACTICALS:

1. Factional distillation of local crudes.


2. Vacuum distillation of topped crude.
3. Stabilization of straight run gasoline.
4. Air blowing of asphalt.
5. Quality control of oil products.

(i) Percentage of water in oil.


(ii) Flash Point
(iii) Carbon residues
(iv) API Gravity
(v) Pour Point
(vi) Smoke Point
(vii) Freezing Point of wax

BOOKS:

1. Nelson, W. L. Petroleum Refinery Engineering McGraw Hill Ed. IV. 1991.


2. Hobson, G. D. & Modern, W. P. Petroleum Technology, Applied Science Publishers,
1984.
3. Mc Ketter J. J. (Ed.) Advances in Petroleum Che. And Refining Inter Science Publishers,
1964.
Course No. AC – 613
PHARMACEUTICAL INDUSTRIES – I
2+1 Credit Hours

CHEMOTHERAPY:

Thesis of drugs development.

ANTIBIOTICS:

General methods of preparation, testing and product maintenance.

VITAMINS:

Classification production and quality control.

SULFA DRUGS:

Characters, production with special reference to structure, activity detail.

ANALGESICS:

Characters and synthesis:


Structure activity relationship in drug.

PRACTICALS:

Practicals of this course are based on the preparation of drugs.

BOOKS:

1. Burger, Alfred drugs and people Virginin 1986.


2. Greedomnew people’s pharmacy, Avon 1976, Bantam, 1985, updated remedies, generic
drugs, natural substitutes.

3. Griffth H. Winter, complete guide to prescription and non-prescription drugs HP, 1983,
1985, information reference for public on 400 drugs arrange by generic names.

4. Physician’s Desk Reference Medical Economics 1967. Annual complete information on


prescription drugs.
Course No. AC – 615
POLYMER TECHNOLOGY – I
2+1 Credit Hours

POLYMER SYNTHESIS:

The thermodynamics aspects of polymerization and polycondensation. Thermodynamics of the


monomer-polymer conversion. The radical polymerization and co-polymerization. T he reactivity
of monomers and radicals. Stereo chemical aspects of radical polymerization. Anionic and
cationic polymerization. The coordinated ionic polymerization. Polymerization by using of C=O,
C=N, C=S bounds. Polymerization of hetercyclic monomers. Polymerization in structured
systems. Polycondensation and Poyaddition. The preparation of high – modulus and thermo
resistant polymers. The matrix synthesis of macromolecules. Molar mass and molar – mass
distribution and the correlation with mechanism of reaction.

PRACTICALS:

1. Bulk polymerization of -aminodecanoic acid and estimation of kinetics of


polymerization by end group analysis.

2. Polymerization of methyl methacrylate in the presence and absence of chain transfer


agent and observation of time dependence of reaction.

3. Copolymerization of styrene and methyl methacrylate with azoisobutyronitrile and


estimation of reactivity ratios by infrared – absorption spectroscopy.

4. Emulsion polymerization of cross-linked polymers by radical polymerization using


difunctional monomers added to vinyl monomers and estimation of solubility properties.

5. Anionic polymerization of styrene using sodium napthalide catalyst and tetrahyrofuron as


a solvent.

BOOKS:

1. A. Y. Grosberg and A. R. Khokhlov, Giant Molecules, Academic Press, NY 1997.


2. Ward I. M. Structure and Properties of Oriented Polymers, 2 nd Ed. Chapman and Hall,
1997.
3. Moore J. A. Ed. Macromolecular Synthesis, Vol 1, Wiley, 1977.
4. Sandler S. R. and Karo W, Polymer Synthesis, Vol. 1 & 2, Academic Press 1996.
5. Campbell D and White DR “Polymer Characterisation: Physical Techniques”, Chapman
and Hall 1989.

6. Odian G. Principles of Polymerization, 3rd Ed. Wiley, 1991.


7. Cowie J. M. G, Polymers: Chemistry and Physics of Modern Materials, 2nd edition, 1991.
Course No. AC – 617
TEXTILE PROCESSING – I
2+1 Credit Hours

DATA COLOUR MEASUREMENT:

System and numerical measurement of colour and quantity, colour mixing difference.

FABRIC HANDLE MEASUREMENT:

Objective parameters of fabric handle, objective and subjective assessment of fabric handle
KES of fabric handle.

PRACTICALS:

1. Data Colour prediction


2. Colour difference measurements
3. Fabric handle measurements

BOOKS:

1. Tyron, L. Vigo, Textile Processing and Properties, Elsewer Amestradem, 1994.


2. Colour & Coloumetry Alain Chrisment 3c Canonical France 1999.
3. Objective Parameters of Fabric handle, S. Kawabata Textile Machinery Society Japan
Kyoto 1996.
Course No. AC – 619
FOOD SCIENCE & TECHNOLOGY – I
2+1 Credit Hours

FOOD PROCESSING:

Composition of food, Molecular structure and functions of Nutrients.


The Chemistry and biochemistry & methods of Food Processing.
Toxicity of Food.

PRACTICALS:

1. Extraction of oil by soxhelt apparatus and to check the following properties of oil.
Saponification value, Peroxide value, color, rancidity, Iodine value, total fatty matter.

2. Determination of bulk density of sugar.


3. Determination of Oxalates of Citric acid.
4. Manufacture of Citric acid by fermentation.
5. Determination of moisture content of wheat flour.
6. Solvent extraction of oil from orange peel.

BOOKS:

1. Baley’s Industrial oil and fat products, Y. H. Hui, 5th Edi., Vol. IV, 1989.
2. Thornton’s meat Hygiene, J. F. Gracey, 7th Edi, 1983.
3. Meat, D. Ja Cole, 2nd Edi., 1982.
4. Shreve’s Chemical Process Industries, George T. Austen, 5th Edi. McGraw Hill, 1995.
5. Food Science, Norman N. Pathr, 2nd Edi. 1983.
6. Modern Food Microbiology, James M. Jay, 4th Edi. 1987.
Course No. AC – 621
Metallurgy & Materials Technology – I
2+1 Credit Hours

MATERIAL TESTING:

Tensile test, Hardness test, Impact test, Fatigue and Creep properties.

METAL WORKING:

Rolling, Forging, Deep drawing & extrusion.

FOUNDRY PRACTICE:

Pattern and Core making, Runner & Feeder system. Continuous casting. Relationship between
cast structure and properties.

POWDER METALLURGY:

Production, Compaction and Sintering of powder metal into solid shapes. Application of powder
metallurgy.

WELDING, BRAZING AND SOLDERING:

Types of welding and defects in weld structure, Brazing & Soldering.

FRACTURE ANALYSIS:

Mechanism and characteristics of fractures, Fracture – toughness criteria, Deformation and


Dislocation theories.

PRACTICALS:

1. Tensile test – Ferrous & Non Ferrous


2. Hardness & Impact test
3. Casting of low melting alloy
4. Welding, Brazing and Soldering
5. Ductile and Brittle fracture study

BOOKS:

1. Dharmendar Kumar, S. K. Jain, Foundry Technology, CBS Publishers, Delhi, 1994.


2. L. M. Ground, Principle of Welding Technology, English Language Book Society,
1980.
3. George E. Dieter, Mechanical Metallurgy, Mc Graw Hill Company, 1988.
4. V. J. Colengelo, Analysis of Metallurgical Failure, John Willy & Sons, 1987.
OPTIONAL COURSES

Course No. AC – 623


RESEARCH PROJECT
0+3 Credit Hours

RESEARCH PROJECT:

A study may opt to take Research Project instead of an optional course. He / She has to be
attached with a Faculty member. After completion of his / her project, a report has to be
submitted. A viva voce examination would be conducted.
Course No. AC – 625
ELECTROCHEMICAL INDUSTRIES
2+1 Credit Hours
FUNDAMENTAL CONCEPTS:
Electron Transfer, Mass Transfer, Adsorption, Electro catalysis, Properties of electrolyte
solution, Phase formation in electrode reactions, Basic Electrochemical Engineering.

CHLOR-ALKALI INDUSTRIES:
Brine Electrolysis, Chlorine Cell Technologies, Production of KOH.

INORGANIC ELECTROLYTIC PROCESSES:


Fluorine, Potassium Permanganate, Potassium dichromate & Chromic acid, Hydrogen peroxide,
Peracids and their salts, Synthesis of metal salts via anodic dissolution.

ORGANIC ELECTRO SYNTHESIS:

The hydrodimerization of acrylonitrile other commercial electro synthetic process, Indirect


electro synthesis.

TREATMENT OF WATER AND EFFLUENTS:

Metal ion removal and metal recovery, Electro dialysis, Electrolytic methods of phase
separation, Flue gas desulphurization, other electrochemical processes.

METAL FINISHING:
Electroplating, Electro less plating, Electrophoretic painting, Conversion coatings, other surface
finishing technique.

BATTERIES AND FUEL CELLS:


Battery characteristics, Battery specification, Battery components, Fuel cells.

PRACTICALS:

1. Laboratory scale electrochemical synthesis of inorganic and organic compounds.


2. Metal Finishing: Electroplating
3. The practical study of Anodic behavior of metal
4. Differential potentiometer titrations.

BOOKS:

1. Pletcher, D. and Walsh, F. C. Industrial electrochemistry, second edition, Chapman and


Hall, 1990.

2. Crow, D. R. Principles and applications of electrochemistry. Chapman & Hall 1988.

3. Lowenheim, F. A. Ed. Modern Electroplating 3rd edition, Wiley New York, 1974.

4. Vincent, C. A. Bonino, F., Lazzari, M and B. Scrosati, Modern Batteries. Edward Arnold,
London, 1984.

5. Linden, D, (Ed.) Handbook of batteries and Fuel Cell. McGraw Hill, New York, 1983.

6. Bard, A. J. and Faulkner, L. R. Electrochemical methods. Fundamentals and application.


Wiley, Calchester 1980.

7. Selly, N. J. Experimental approach to electrochemistry. Edward Arnold, London, 1977.

8. Heltz, E. & Kreysa, G., Principles of Electrochemical Engineering, VCH Publishers,


1986.
Course No. AC – 627
POLYMER RHEOLOGY
2+1 Credit Hours
Introduction to elastic solids and viscous liquids. Flow of polymeric liquids, Material functions.
Generalized Newtonian fluid Linear viscoelastic constitutive equations. Non-linear viscoelastic
constitutive equations. Single integral Doi – Edwards, KBKZ and Larson – Bell constitutive
equations. Fluid dynamics of rheometry, shear and extensional rheometry, rheometer design,
rheo – optics.

PRACTICALS:

1. Birefringence in 1-2 plane measurement of orientation angle in a cone-plate geometry.


2. Birefringence in 1-3 plane using a slit geometry in a flow cell.
3. Flow velocity measurement in v1, v2, v3 direction through a slit die using laser
velocimetry.
4. Birefringence in 2-3 plane using a capillary apparatus.
5. Linear viscoelastic oscillatory shear measurement in a parallel plat geometry at low
strains.
6. Measurement of relaxation spectrum by linear regression, singular value and non-linear
regression techniques.

7. Non-linear viscoelastic step strain measurements in a parallel plate geometry


8. Non-linear viscoelastic steady measurement in a parallel plat geometry.
9. Numerical solution of Lodge, Maxwell and Wagner’s constitutive equation for the 1-3
plane centre line streamline and its comparison with experimental results.

BOOKS:

1. Larson R. G. Constitutive equation for Polymeric Melts and Solutions, Buttorworths,


1989.
2. Macosko C. W. Rheology Principles, Measurements and Applications, VCH Publishers,
New York, 1999.
3. Bird R. B. Armstrong R. C., Hassager O, Dynamics of Polymeric Liquids Vol. 1 & 2,
McGraw Hill, New York, 1987.

4. Roberts, Royston M; Raymond B, and Carraher, Charies E; Giant Molecules; John Wiley
and Sons Inc., New York 1990.

5. Piau. J. M and Agassant J. F. Rheology for Polymer Melt Processing, Elsevier


Amsterdam, 1996.
6. A. W. Birley, B Haworth and J Batchelor, Physics of plastics – processing properties and
materials engineering Carl Hanser Verlag (Munich), 1992.
Course No. AC – 629
LEATHER TECHNOLOGY
2+1 Credit Hours
LEATHER TECHNOLOGY:

Chemical Composition, Pretreatment of raw materials.

TANNERY:

Introduction & Processing.

MANUFACTURE / PRODUCTIONS:

Utilities, Curing Soaking, Limiting Fleshing Beam house Operations, Deliming, Bating Picking,
Tannings.

NEUTRALIZATION:

Retaining Leather dyeing methods & equipment, Fat liquoring.

DRY MOISTURE OPERATIONS:

Stacking, storage, sizing.

FINISHING OPERATIONS:

Bye Products:

Powder Consumption:

PRACTICALS:

1. Microscopic study of leather.


2. Tanning Chrome & vegetable techniques
3. Dyeing of leather
4. Quality control analysis and test of leather

BOOKS:

1. Encyclopedia of Chemical Technology 3rd Edition, Wiley Inter Science, New York 1982.
2. The Chemistry & Technology of leather by Fred. O. Flaherty, William T. Roddy, 3 rd
Edition, 1987.

3. Chemical Process Industries by R. Norris Shreve. 5th Edition 1995.


Course No. AC – 631
FUEL TECHNOLOGY & RENEWABLE ENERGY RESOURCES
2+1 Credit Hours

INTRODUCTION:

Sources of Fuel and Energy

SOLID FUELS:

Coal and other solid fuel

LIQUID FUELS:

Petroleum and other liquid fuels

GASEOUS FUELS:

Natural gas producer gas, Water gas, Bio gas and others.

SOURCES OF RENEWABLE ENERGY:

Solar energy, Geothermal energy, Water & Wind energy resources.

PRACTICALS:

1. Analysis of Coal
2. Practicals on Petroleum
3. Practicals on gaseous fuels
4. Practicals on solar energy

BOOKS:

1. Solar Energy, Bob Brooke, Russell E. Train (Introduction), Chelsea House Publishers,
1993.
2. Wind Energy Resources Atlas of the United States, D. L. Elliot, C.G. Holladay. W. R.
Barchet, H.P Foote, Wind Books Inc. 1992.

3. Advances in Solar Energy, Vol. 11, Karl W. Boer American Solar Energy Society, 1996.
4. Fuels and Fuel Technology, Wilfrid Francis Martin C. Peters, Franklin Book Company,
Inc., 1980.

5. Fuels for the year 2000 and beyond, American Chemical Society Division of Fuel
Chemis, 1988.
Course No. AC – 633
ENGINEERING MATERIALS
2+1 Credit Hours

Materials for 21st Century:

Comparision of Conventional and Emerging Engineering Materials:

Composite Materials & Nano Composites:

Polymer based, Metal based, Ceramic based, Properties, Uses and Economics.

Metallic glasses:

Super conducting materials:

Semi-conductory:

Photo sensitive materials:

PRACTICALS:

1. Tensile test, Ferrous, Nonferrous, Polymers, Composites, Specimen preparation and


testing.
2. Compression test, Cements, Composites.
3. Hardness test. Ferrous, Nonferrous, Polymers, Composites.
4. Photosensitivity tests of thin films.
5. Resistance testing of super conducting materials.
6. Microscopy of materials.

BOOKS:

1. Engineering Materials, Kenneth G. Budinski K., Prentice Hall Publisher 1998.


2. Material Science and Engineering Willaium D. Callister, Wiley John & Sons, Inc. 1999.
3. Modern Physical Metallurgy and Materials Engineering R. E. Smallman, R. J. Bishop,
Butterworth-Heincmann, 2000.
SECOND SEMESTER
COMPULSORY COURSES

Course No. AC – 602


Chemical Engineering – III (Plant Designing)
3+0 Credit Hours

MATERIAL AND ENERGY BALANCE:

Stiochiometry, Choice of system boundary, Choice of basic calculation.

FLOW SHEETING:

Flow sheet presentation, Graphic symbols for per piping systems and plants.

PIPING AND INSTRUMENTATION:

Piping and Instrumentation diagram, Pipe size selection, Control and Instrumentation, Typical
control system.

Equipment selection specification and design:

Separations Process, Solid – Solid separation, liquid – Solid separation, Liquid – Liquid
separation Gas- Solid separation.

DESIGN PROJECT:

A DESIGN PROJECT BASED ON THEORETICAL Principles and data collected is to submitted


by each student convening the following:

Market survey, Manufacturing cost, Cost of Product, Breakeven analysis, Pay Back period,
Process details of each unit; Materials and energy balance; process flow sheet.

Material of construction; Instrumentation; Mechanical drawng of one main equipment, Safety


and Hazards.

Books:

1. Coulson. J. M., & Richardson, J.F., Sinnott, R.K., Chemical Engineering Vol., 6,
Pergamon press, 1998.
2. Peter M.S.& Timmerhaus, K.D., Plant Design & Economics for chemical Engineers,
McGraw Hill 1991.
Course No. AC-604
Industrial Pollution
2+1 Credit Hours

INTRODUCTION:

Environmental pollution and sources.

WATER QUALITY:

Physical, Chemical & Biological parameters.

WATER PURIFICATION:

Processes, Waste water treatment methods and applications. Primary, Secondary and Tertiary
Treatments. Disposal and reuse.

AIR-POLLUTION:

Sources, Air-Pollution control methods in industries.

NOISE POLLUTION:

Health impact, Measurement and control in industries. Environmental Impact assessment.

PRACTICALS:

1. Waster-quality Assessment for 32 NEQS parameters.


2. Air-Pollution Measurement (CO2, CO3, H2S3, NH3, SO3, NO )
3. Noise-Level Measurements in industrial units.
4. Study of Waste-Treatment and disposal methods.

BOOKS:

1. Environmental Engineering by H.S.Peary, D.R.Rowe , and G Techobtanoglus Mc Law


Hill Book Company 1995.
2. Air Pollution by J. H.Seintild, John wiley and Sons Inter Science Publisher 1985.
3. Noise Pollution by Anotony Milne, Daved and Charles, 1979.
4. Environmental Engineering by G. N. Pandey & G. C. Gamey Tata, McGraw Hill 1989.

5. Industrial Pollution Control handbook by H.F.Lund, Mc.Graw Hil,1979.


6. Industrial Water Pollution, Origin Characteristics and treatment Nemerow, Addison-Wiley
Public Co. 1978-89.
7. ASTM-1739.
Course No.AC-606
Analytical Techniques & Quality Control-II (Chromatography)
2+1 Credit Hours
CHROMATOGRAPHY:
Introduction and types of chromatography, theoretical treatment of chromatography.
Liquid column chromatography, liquid-solid chromatography, liquid-liquid chromatography,
high performance liquid chromatography, gel permeation chromatography, ion-exchange
chromatography and its application.

Gas chromatography: Instrumentation, Gas liquid chromatography; Gas solid chromatography;


Packed and capillary column, Packing and handling of these column, Detection and
interpretation of chromatograms. Plane chromatography: paper chromatography, Thin Layer
chromatography.

RADIOCHEMICAL METHODS:
Neutron activation Analysis Principles of neutron activation analysis, Source of neutron,
Capabilities and limitation of neutron activation, Practical consideration in neutron activation.

AUTOMATIC AND PROCESS ANALYZER:


Introduction, Sample handling system. Analyzer calibration, Process gas chromatography,
Oxigen Analyzers, Moisture analyzers, Calorimetric Analyzers.

PRACTICALS:

1. To prepare standard solution of KOH by Ion exchange Chromatography.


2. Examination of dyes in ink by ascending paper chromatography.
3. To separate the mixture of methyl orange and methylene blue by column
chromatography.
4. Determination of Ion exchange conditioning and capacity.
5. Separation of Vitamin 'A' compounds by TLC.
6. Determination of Phosphate by electro analytical method.
7. Quantitative analysis of a mixture of BTX by Gas Chromatography.
8. Separation and concentration of traces of copper by Ion chromatography.
9. Determination of total ions of tap water by Ion exchange chromatography.
10. Examination of indicators and inks by two dimensional paper chromatography.

BOOKS:

1. Hargis G.L., Analytical Chemistry, Prentice-Hall Inc. New Jsersey, 1988.

2. Kener C.T. Quantitative Analysis, Mac Millan Publishing Co., Inc. New Yourk 1979.

3. Fritz. J.S., George H. Schenks, Quantitative analytical Chemistry, 4th. Edi., Allyn and
Bacon Inc., Bostan, 1979.

4. Skog D. A. and D.M. West, principles of Instrumental Analysis Holt Saunder Ltd., Japan,
1981

5. Pecsok R.L, Robert L., Donald Shield, Thomas Cairns, Modern Methods of Chemical
Analysis, John Willey & Sons, New Yourk, 1976.

6. Bauer. H.H. Gray D. Christian and James E.m Instrumental Analysis Allyn and Bacon
Inc. 1978.
SPECIALIZATION COURSES

Course No.AC-608
Chemical Process Principles – II (Flow Process)
3+0 Credit Hours

THERMODYNAMIC OF FLOW PROCESSES:

Mass, energy, and entropy balances, Duct flow of compressible fluids. Expression processes.

POWER GENERATION:

The steam power plant, The Otto engine, The Desel engine, The Gas-Turbine power plant.

REFRIGERATION, HEAT PUMPS, AIR-CONDITIONING AND LIQUEFACATION:

The Carnot refrigerator, The Vapour – Compression cycle, Comparison of refrigeration cycles,
The choice of refrigerant, Absorption refrigeration, The Heat Pump, Air-conditioning systems,
Cooling towers. Liquefaction Processes.

THERMODYNAMIC ANALYSIS OF PROCESSES:

Sources of energy supply and energy demands, Combined cycles, Combined heat and power
co-generation, Energy management and energy audits, The technology of energy saving,
Alternative energy sources.

BOOKS:

1. J.M.Smith H.C.,Van Ness, and M.M. Abbot, Introduction to Chemical Engineering


Thermodynamics, 5th. Ed., McGraw Hill, New York, 1996.
2. E.B.Woodruff, H.B.Lammers, and T.S. Lammers, Steam Plant Operation 6 th. Ed.
McGraw-Hill New York 1992.
3. C.F.Taylor, The Internal Combustion Engine in Theory and Practice: Thermodynamics,
Fluid Flow, performance, MIT press, Boston, 1984.
4. T.D. Eastop A. Mc Conkey, Applied Thermodynamics for Engineering Techlologists 5 th.
Ed., ELBS Longman, Essex, 1993.
Course No.AC-610
Chemical Process Industries Inorganic – II
2+1 Credit Hours

REFRACTORIES & ALLIED PRODUCTS:

Physical forms of a refractory, Manufacture. Properties & application of refractories. Refractory


coatings & special refractories.

INORGANIC FIBERS:

Glass Fiber, Refractory Fiber

MEASUREMENT & CONTROL OF HIGH TEMPERATURE:


METALLIC CORROSION:

Corrosion in general, Reaction mechanism of corrosion, Types & prevention of corrosion .

ELECTRO THERMAL INDUSTRIES:

Electro thermal products, Manufacture & Applications, Artificial abrasives, Furnaces used for
manufacturing electro – thermal products.

PRACTICALS:

Practicals to be based on the following:

01- Qualitative & Quantitative analysis of refractories.


02- Physical testing to be performed in the concerned industries.
BOOKS:

01- Industrial Ceramics, Felix Singer & Sonja S. Singer, Oxford & IBH Publishing Co PVT,
1963.
02- Refractions Technology, C. Storey, ELLIS HORWOOD.
03- Fiber Glass, J.Gilbert Mohr & William, P. Rowe, Van Nostrand Reinhold Company, 1978.
04- Schott Guide to glass, Heinz G. Preander, Van Nostrand Reinhold Company,1983
05- Industrial Inorganic Chemistry by Dr. W. Buchner, Dr. R Schlibs. Dr. G. winter & Dr. K.
H. Buchel, VCH Publisher, New York, 1989.
06- Industrial Chemistry Vol. 1 & 2 E.Stocchiellis Horwood ltd, 1990.
07- Refractory Materials; Their manafacture & uses Alfered B.Searle Charles Griffin &
Company Ltd.
08- Refractories, F. H. Norton, McGraw Hill Book Company.
09- Glass; J. Wong & C.A.Angsell Mercel Dekker. Inc. 1976.
10- Kirk-Other, Encyclopedia of Chemical Technology, Jon Wiley & Sons, 1984.
Course No.AC-612
Petroleum & Petrochemicals –II (Petro-Chemical Technology)
2+1 Credit Hours

GENERAL PETROCHEMICAL INDUSTRIES:

Manufacture and purification of acetone, Olefins and BTX Petroleum derived products.
Lubricants.

AMMONIA:

Natural gas, desulphurization. Reforming, Shift conversion separation and purification of gas
streams Ammonia synthesis.

PRACTICALS:

01- Separation and purification of BTX by fractional distillation.


02. Separation of various isomers of xylene.
03- Manufacture and testing of lubricating oils.
04- Carbon dioxide separation using various solvents.

BOOKS:

01- Waddams A. L. Chemicals from petroleums. John Murrcy, 1978.


02- Stack, A. V. & James, G.R. Ammonia Mercel Dekker Inc. 1973.
03- Strelzolf, S. Ammoia Kirk- Othmer Encyclopedia Chemical Technology (Ed.) III Wiley-
Interscience Publishers, 1982.
Course No.AC-614
Pharmaceutical Industries – II
2+1 Credit Hours

TABLETS:

Types, Manufacture, Ingredients, Coating and evaluation of tablets.

LIQUID:

Raw Materials, Preparation, equipment employed.

SYRUPS:

Types, Preparation and preservation.

OINTMENTS:

Classification, Raw material, Properties based on raw material, Manufacture, Devices for
ointment filling.

STERLIZATION;

Introduction Conditions and methods of sterilization, Factors affecting sterilization.

QUALITY CONTRL:

Chemical safety, Microbiological safety and environmental safety, Environmental and product
monitoring labs, product safety test and packaging inspection units.

PRACTICALS:

Practicals are based on the quality control test of different pharmaceutical product.

BOOKS:

01. A test book of pharmaceutical and medical Chemistry by William and Griswold J.B.,
Lippin cot co 7th. Edi. 1992.
02. Medical Chemistry by Aflerd Burger Vol. I & II and IIIrd. Edi., wiley inter science New
York, 1976.
3. Encyclopedia of Chemical Technology, 3rd. edi.m Wiley Inter Science New York 1982.
4. Austin G. Shrves, Chemical Process Industries, 5th. Edi. McGraw Hill 1995.

5. The Pharmaceutical basis of therapeutics by Good man & Gilman, 5 th. Edi. Macmillan
publishing Co. 1982.

6. Dispensing of medication by Hoover, Mac publishing Co. 1976.

7. Fundamentals of packaging by Paine . F.A.


Course No.AC-616
Polymer Technology – II (Polymer Physics)
2+1 Credit Hours

VICOELASTICITY OF POLYMERS:

Integral representation, conventional stsres strain curves, relations between static and dynamic
properties.

TRANSITIONS:

Free volume theory, thermodynamic theory.

POLYMER CHAINSTATICS:

End-to-end distance, random chains, distributions at large extensions.

THEORY OF RUBBER ELASTICITY:

Phenomeological approach, statistical treatment, non Gaussaian network theory, strain energy
functions. Non-linear viscoelasticity; single integral and differential constitutive equations, fluid
dynamics of

PRACTICALS:

01. Falling cylinder and falling ball viscometry to establish terminal velocity in Newtonian and
viscoelastic fluids.
02. Concsertric cylinder rheometry to establish relationship between shear stress and torque
and shear rate and angular velocity for a viscoelastic fluid.
03. Measurement of normal stresss and effects on secondary flow instabilities for a
polymeric fluid in couettee geometry.
04. Measurement of wall shear stress in a capillary rheometer and estimation of apparent
viscosity.
05. Wall slip and melt fracture in capillary flow with capillaries of similar length to radius
ratios but different radii.
06. Measurement of normal streses and exit pressure in a slit rheometer and estimation of
pressure pofile.
07. Planar elongation flow of polyethylenes of varying levels of branching at constant flow
rate in a slit die.

BOOKS:

1. Macosko C. W, rheology Principles, Measurements and Applications, VCH publishers,


New York. 1987.

2. Bird R. B, Amstrong R., C, Hassager O, Dynamics of Polymeric Liquids Vol I & 2,


McGraw Hill, New York, 1999.

3. Ward I M, Sturcture and Properties of Oriented Polymers, 2 nd. ed. Chamman and Hall,
1997.

4. Ward I.M, Mechanical properties of Solid Polymers, 2nd ed. Wiley, Chiichester 1983.

5. Roberts, Royston M; Raymond B. and Caraher, Charles E; Gaint Molecules John Wiley
and Sons, Inc, New York, 1990.

6. Pain J M. and Agassant J F, Rheology for Polymer Melt Procesing, Elsevier Amsterdam,
1996.
7. A.W.Birley B. Haworth and J. Bathelor, Physics of Plastics-Processing Properties and
materials engineering, carl Hanser Verlag (Munich), 1992
Course No.AC-618
Textile Processing – II
2+1 Credit Hours

SURFACTANTS:

Preparation and end uses as softners, detergents, emulsifirs and other auxiliaries of textile
processing.

SYNTHESIS OF TEXTILE CHEMICALS:

Polymer synthesis of textile chemicals including suspension, dispersion, and emulsion


polymerizatzion.

PRACTICALS:

1. Surfactant synthesis
2. Surfactant characterization
3. Synthesis of various emusltion polymers.

BOOKS:

1. Textile Procesing and Properties, Tyron L., Vigo Elsewer Amestradem, 1994.

2. Emulsion and emulsion and emulsion technology, Kenneth J. Lissant. Merceldecker inc.
New York. 1994.
Course No.AC-620
Food Science & Technology – II (Food Engineering)
2+1 Credit Hours

Techniques of drying.
Food preservation
Evaporator in food industry
Fermenter, its design and functioning
Carbonated and non-carbonated drinks
Rheology of food utilization of various agricultural and food industries wastes.
Food packaging, bottling, plant, various machines in packaging.

PRACTICALS:

1. To compare the Managanese content in different samples of tea.


2. Isolation of Casein and Lactose from milk.
3. Determination of Protien content of food.
4. Preparation of food products by Lyophilization.
5. Determination of Amino acid content of Mysin (meat Protien.)
6. Protein precipitation tests by heavy metals.
7. Determination of Bensoic acid in orange drinks.

BOOKS:

1. Chemical Enginering,J.M.Coulson, vol 1, 3rd. ed. 1982.


2. Unit Operation of Chemical Engineering, Warren, L.McCabe, 3rd. eid. 1983.
3. Animal by products, Mann, Food & agricultural Organization of the United Nation, Italy,
1986.
4. Shreve's Chemical Process Industries, George T. Austen, 5th. Ed. McGraw Hill 1995.
5. Food Science, Norman N. Parhr, 2nd. ed. Mc.Graw Hill, 1995.
6. Modern Food Microbiology, James M. Jay, 4th. Ed. 1987.
Course No.AC-622
Metallurgy and Materials Technology-II
2+1 Credit Hours

X – RAY DIFFRACTION:

Principles of X-ray diffraction. Single crystal and powder methods, Interperetation of diffraction
data.

ELECTRON MICROSCOPPY:

Scanning electron Microscopes, Transmission electron microcopes, Specimen preparation –


Replica & thin toil.

HEAT TREATMENT OF METALS AND ALLOYS:

Annealing, spherodizing and Tempering, Isothermal & Continous cooling, Phase formation
products in steel, Hardenability, Case hardening methods, Age hardening of Al alloys,
Commercial practice in heat treatment of ferrous and non ferrous alloys.

STRUCTURE PROPERTY RELATION SHIP:

Effect of alloy elements in steel, effect of grairi size & practicle on properties.

COMPOSITE MATERIALS:

Classification of composites, Polymer based Metal based. Refractory based composites, Nano
Composites.

PRACTICALS:

1. X-ray diffraction pattern of single crystal and powder specimen.


2. Scanning electron microscopy.
3. Transmission electron microscopy
4. Continuous cooling structure Harden ability test.
5. Effect of grain size and precipitate particles.
6. Composite methods.
Course No. AC-624
Industrial Training
0+3 Credit Hours

INDUSTRIAL TRAINING:

Every student of M.Sc.( Final) has to complete at least 6-8 weeks of industrial training in a
particular industry as suggested by the teacher incharge. After completing the training he/she
has to submit a report and deliver a seminar.
SECOND SEMESTER
COMPULSORY COURSES

C. No.AC-602 Chemical Engg. – III (Plant Designing ( 3+0)

MATERIAL AND ENERGY BALANCE:

Stiochiometry, Choice of system boundary, Choice of basic calculation.

FLOW SHEETING:

Flow sheet presentation, Graphic symbols for per piping systems and plants.

PIPING AND INSTRUMENTATION:

Piping and Instrumentation diagram, Pipe size selection, Control and Instrumentation,
Typical control system.

Equipment selection specification and design:

Separations Process, Solid – Solid separation, liquid – Solid separation, Liquid – Liquid
separation Gas- Solid separation.

DESIGN PROJECT:

A DESIGN PROJECT BASED ON THEORETICAL Principles and data collected is to


submitted by each student convening the following:

Market survey, Manufacturing cost, Cost of Product, Breakeven analysis, Pay Back
period, Process details of each unit; Materials and energy balance; process flow sheet.

Material of construction; Instrumentation; Mechanical drawng of one main equipment,


Safety and Hazards.

Books:

1. Coulson. J. M., & Richardson, J.F., Sinnott, R.K., Chemical Engineering Vol., 6,
Pergamon press, 1998.
2. Peter M.S.& Timmerhaus, K.D., Plant Design & Economics for chemical
Engineers, McGraw Hill 1991.

C. No.AC-604 Industrial Pollution ( 2+1)

INTRODUCTION:

Environmental pollution and sources.

WATER QUALITY:

Physical, Chemical & Biological parameters.

WATER PURIFICATION:

Processes, Waste water treatment methods and applications. Primary, Secondary and
Tertiary Treatments. Disposal and reuse.
AIR-POLLUTION:

Sources, Air-Pollution control methods in industries.

NOISE POLLUTION:

Health impact, Measurement and control in industries. Environmental Impact


assessment.

PRACTICALS:

1. Waster-quality Assessment for 32 NEQS parameters.


2. Air-Pollution Measurement (CO2, CO3, H2S3, NH3, SO3, NO )
3. Noise-Level Measurements in industrial units.
4. Study of Waste-Treatment and disposal methods.

BOOKS:

1. Environmental Engineering by H.S.Peary, D.R.Rowe , and G Techobtanoglus Mc


Law Hill Book Company 1995.
2. Air Pollution by J. H.Seintild, John wiley and Sons Inter Science Publisher 1985.
3. Noise Pollution by Anotony Milne, Daved and Charles, 1979.
4. Environmental Engineering by G. N. Pandey & G. C. Gamey Tata, McGraw Hill
1989.

5. Industrial Pollution Control handbook by H.F.Lund, Mc.Graw Hil,1979.


6. Industrial Water Pollution, Origin Characteristics and treatment Nemerow,
Addison-Wiley Public Co. 1978-89.
7. ASTM-1739.

C. No.AC-606 Analytical Techniques & Quality Control-II


(Chromatography) ( 2+1)

CHROMATOGRAPHY:

introduction and types of chromatography, theoretical treatment of chromatography.


liqid column chromatography, liquid-solid chromatography, liquid-liquid chromatography,
high performance liquid chromatography, gel permeation chromatography, ion-
exchange chromatography and its application.
Gas chromatography: Instrumentation, Gas liquid chromatography; Gas solid
chromatography; Packed and capillary column, Packing and handling of these column,
Detection and interpretation of chromatograms. Plane chromatography: paper
chromatography, Thin Layer chromatography.

RADIOCHEMICAL METHODS:

Neutron activation Analysis Principles of neutron activation analysis, Source of neutron,


Capabilities and limitation of neutron activation, Practical consideration in neutron
activation.

AUTOMATIC AND PROCESS ANALYZER:

Introduction, Sample handling system. Analyzer calibration, Process gas


chromatography, Oxigen Analyzers, Moisture analyzers, Calorimetric Analyzers.

PRACTICALS:

1. To prepare standard solution of KOH by Ion exchange Chromatography.


2. Examination of dyes in ink by ascending paper chromatography.

3. To separate the mixture of methyl orange and methylene blue by column


chromatography.

4. Determination of Ion exchange conditioning and capacity.

5. Separation of Vitamin 'A' compounds by TLC.

6. Determination of Phosphate by electro analytical method.

7. Quantitative analysis of a mixture of BTX by Gas Chromatography.

8. Separation and concentration of traces of copper by Ion chromatography.

9. Determination of total ions of tap water by Ion exchange chromatography.

10. Examination of indicators and inks by two dimensional paper chromatography.

BOOKS:

1. Hargis G.L., Analytical Chemistry, Prentice-Hall Inc. New Jsersey, 1988.

2. Kener C.T. Quantitative Analysis, Mac Millan Publishing Co., Inc. New Yourk
1979.

3. Fritz. J.S., George H. Schenks, Quantitative analytical Chemistry, 4th. Edi., Allyn
and Bacon Inc., Bostan, 1979.

4. Skog D. A. and D.M. West, principles of Instrumental Analysis Holt Saunder Ltd.,
Japan, 1981

5. Pecsok R.L, Robert L., Donald Shield, Thomas Cairns, Modern Methods of
Chemical Analysis, John Willey & Sons, New Yourk, 1976.

6. Bauer. H.H. Gray D. Christian and James E.m Instrumental Analysis Allyn and
Bacon Inc. 1978.

SPECIALIZATION COURSES

C. No.AC-608 Chemical Process Principles – II (Flow Process) ( 3+0)

THERMODYNAMIC OF FLOW PROCESSES:

Mass, energy, and entropy balances, Duct flow of compressible fluids. Expression
processes.

POWER GENERATION:

The steam power plant, The Otto engine, The Desel engine, The Gas-Turbine power
plant.

REFRIGERATION, HEAT PUMPS, AIR-CONDITIONING AND LIQUEFACATION:


The Carnot refrigerator, The Vapour – Compression cycle, Comparison of refrigeration
cycles, The choice of refrigerant, Absorption refrigeration, The Heat Pump, Air-
conditioning systems, Cooling towers. Liquefaction Processes.

THERMODYNAMIC ANALYSIS OF PROCESSES:

Sources of energy supply and energy demands, Combined cycles, Combined heat and
power co-generation, Energy management and energy audits, The technology of
energy saving, Alternative energy sources.

BOOKS:

1. J.M.Smith H.C.,Van Ness, and M.M. Abbot, Introduction to Chemical Engineering


Thermodynamics, 5th. Ed., McGraw Hill, New York, 1996.
2. E.B.Woodruff, H.B.Lammers, and T.S. Lammers, Steam Plant Operation 6 th. Ed.
McGraw-Hill New York 1992.
3. C.F.Taylor, The Internal Combustion Engine in Theory and Practice:
Thermodynamics, Fluid Flow, performance, MIT press, Boston, 1984.
4. T.D. Eastop A. Mc Conkey, Applied Thermodynamics for Engineering
Techlologists 5th. Ed., ELBS Longman, Essex, 1993.

C. No.AC-610 Chemical Process Industries Inorganic – II ( 2+1)

REFRACTIORIES & ALLIED PRODUCTS:

Physical forms of a refractory, Manufacture. Properties & application of refractories.


Refractory coatings & special refractories.

INORGANIC FIBERS:

Glass Fiber, Refractory Fiber

MEASUREMENT & CONTROL OF HIGH TEMPERATURE:


METALLIC CORROSION:

Corrosion in general, Reaction mechanism of corrosion, Types & prevention of


corrosion .

ELECTRO THERMAL INDUSTRIES:

Electro thermal products, Manufacture & Applications, Artificial abrasives, Furnaces


used for manufacturing electro – thermal products.

PRACTICALS:

Practicals to be based on the following:

01- Qualitative & Quantitative analysis of refractories.


02- Physical testing to be performed in the concerned industries.

BOOKS:

01- Industrial Ceramics, Felix Singer & Sonja S. Singer, Oxford & IBH Publishing Co
PVT, 1963.
02- Refractions Technology, C. Storey, ELLIS HORWOOD.
03- Fiber Glass, J.Gilbert Mohr & William, P. Rowe, Van Nostrand Reinhold
Company, 1978.
04- Schott Guide to glass, Heinz G. Preander, Van Nostrand Reinhold
Company,1983
05- Industrial Inorganic Chemistry by Dr. W. Buchner, Dr. R Schlibs. Dr. G. winter &
Dr. K. H. Buchel, VCH Publisher, New York, 1989.
06- Industrial Chemistry Vol. 1 & 2 E.Stocchiellis Horwood ltd, 1990.
07- Refractory Materials; Their manafacture & uses Alfered B.Searle Charles Griffin
& Company Ltd.
08- Refractories, F. H. Norton, McGraw Hill Book Company.
09- Glass; J. Wong & C.A.Angsell Mercel Dekker. Inc. 1976.
10- Kirk-Other, Encyclopedia of Chemical Technology, Jon Wiley & Sons, 1984.

C. No.AC-612 Petroleum & Petrochemicals –II


(Petro-Chemical Technology) ( 2+1)

GENERAL PETROCHEMICAL INDUSTSIRES:

Manufacture and purification of acetone, Olefins and BTX Petroleum derived products.
Lubricants.

AMMONIA:

Natural gas, desulphurization. Reforming, Shift conversion separation and purification of


gas streams Ammonia synthesis.

PRACTICALS:

01- Separation and purification of BTX by fractional distillation.


02. Separation of various isomers of xylene.
03- Manufacture and testing of lubricating oils.
04- Carbon dioxide separation using various solvents.

BOOKS:

01- Waddams A. L. Chemicals from petroleums. John Murrcy, 1978.


02- Stack, A. V. & James, G.R. Ammonia Mercel Dekker Inc. 1973.
03- Strelzolf, S. Ammoia Kirk- Othmer Encyclopedia Chemical Technology (Ed.) III
Wiley-Interscience Publishers, 1982.

C. No.AC-614 Pharmaceutical Industries - II ( 2+1)

TABLETS:

Types, Manufacture, Ingredients, Coating and evaluation of tablets.

LIQUID:

Raw Materials, Preparation, equipment employed.

SYRUPS:

Types, Preparation and preservation.

OINTMENTS:

Classification, Raw material, Properties based on raw material, Manufacture, Devices


for ointment filling.
STERLIZATION;

Introduction Conditions and methods of sterilization, Factors affecting sterilization.

QUALITY CONTRL:

Chemical safety, Microbiological safety and environmental safety, Environmental and


product monitoring labs, product safety test and packaging inspection units.

PRACTICALS:

Practicals are based on the quality control test of different pharmaceutical product.

BOOKS:

01. A test book of pharmaceutical and medical Chemistry by William and Griswold
J.B., Lippin cot co 7th. Edi. 1992.
02. Medical Chemistry by Aflerd Burger Vol. I & II and IIIrd. Edi., wiley inter science
New York, 1976.
3. Encyclopedia of Chemical Technology, 3rd. edi.m Wiley Inter Science New York
1982.
4. Austin G. Shrves, Chemical Process Industries, 5th. Edi. McGraw Hill 1995.

5. The Pharmaceutical basis of therapeutics by Good man & Gilman, 5th. Edi.
Macmillan publishing Co. 1982.

6. Dispensing of medication by Hoover, Mac publishing Co. 1976.

7. Fundamentals of packaging by Paine . F.A.

C. No.AC-616 Polymer Technology – II (Polymer Physics) ( 2+1)

VICOELASTICITY OF POLYMERS:

Integral representation, conventional stsres strain curves, relations between static and
dynamic properties.

TRANSITIONS:

Free volume theory, thermodynamic theory.

POLYMER CHAINSTATICS:

End-to-end distance, random chains, distributions at large extensions.

THEORY OF RUBBER ELASTICITY:

Phenomeological approach, statistical treatment, non Gaussaian network theory, strain


energy functions. Non-linear viscoelasticity; single integral and differential constitutive
equations, fluid dynamics of

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PRACTICALS:
01. Falling cylinder and falling ball viscometry to establish terminal velocity in
Newtonian and viscoelastic fluids.
02. Concsertric cylinder rheometry to establish relationship between shear stress
and torque and shear rate and angular velocity for a viscoelastic fluid.
03. Measurement of normal stresss and effects on secondary flow instabilities for a
polymeric fluid in couettee geometry.
04. Measurement of wall shear stress in a capillary rheometer and estimation of
apparent viscosity.
05. Wall slip and melt fracture in capillary flow with capillaries of similar length to
radius ratios but different radii.
06. Measurement of normal streses and exit pressure in a slit rheometer and
estimation of pressure pofile.
07. Planar elongation flow of polyethylenes of varying levels of branching at constant
flow rate in a slit die.

BOOKS:

1. Macosko C. W, rheology Principles, Measurements and Applications, VCH


publishers, New York. 1987.

2. Bird R. B, Amstrong R., C, Hassager O, Dynamics of Polymeric Liquids Vol I & 2,


McGraw Hill, New York, 1999.

3. Ward I M, Sturcture and Properties of Oriented Polymers, 2nd. ed. Chamman and
Hall, 1997.

4. Ward I.M, Mechanical properties of Solid Polymers, 2nd ed. Wiley, Chiichester
1983.

5. Roberts, Royston M; Raymond B. and Caraher, Charles E; Gaint Molecules John


Wiley and Sons, Inc, New York, 1990.

6. Pain J M. and Agassant J F, Rheology for Polymer Melt Procesing, Elsevier


Amsterdam, 1996.

7. A.W.Birley B. Haworth and J. Bathelor, Physics of Plastics-Processing Properties


and materials engineering, carl Hanser Verlag (Munich), 1992

C. No.AC-618 Textile Processing – II ( 2+1)

SURFACTANTS:

Preparation and end uses as softners, detergents, emulsifirs and other


auxiliaries of textile processing.

SYNTHESIS OF TEXTILE CHEMICALS:

Polymer synthesis of textile chemicals including suspension, dispersion,


and emulsion polymerizatzion.

PRACTICALS:

1. Surfactant synthesis
2. Surfactant characterization
3. Synthesis of various emusltion polymers.
BOOKS:

1. Textile Procesing and Properties, Tyron L., Vigo Elsewer


Amestradem, 1994.

2. Emulsion and emulsion and emulsion technology, Kenneth J. Lissant.


Merceldecker inc. New York. 1994.

C. No.AC-620 Food Science & Technology – II (Food Engineering)


( 2+1)

Techniques of drying.
Food preservation
Evaporator in food industry
Fermenter, its design and functioning
Carbonated and non-carbonated drinks
Rheology of food utilization of various agricultural and food industries
wastes.
Food packaging, bottling, plant, various machines in packaging.

PRACTICALS:

1. To compare the Managanese content in different samples of tea.


2. Isolation of Casein and Lactose from milk.
3. Determination of Protien content of food.
4. Preparation of food products by Lyophilization.
5. Determination of Amino acid content of Mysin (meat Protien.)
6. Protein precipitation tests by heavy metals.
7. Determination of Bensoic acid in orange drinks.

BOOKS:

1. Chemical Enginering,J.M.Coulson, vol 1, 3rd. ed. 1982.


2. Unit Operation of Chemical Engineering, Warren, L.McCabe, 3rd. eid. 1983.
3. Animal by products, Mann, Food & agricultural Organization of the United Nation,
Italy, 1986.
4. Shreve's Chemical Process Industries, George T. Austen, 5th. Ed. McGraw Hill
1995.
5. Food Science, Norman N. Parhr, 2nd. ed. Mc.Graw Hill, 1995.
6. Modern Food Microbiology, James M. Jay, 4th. Ed. 1987.

C. No.AC-622 Metallurgy and Materials Technology-II ( 2+1)

X – RAY DIFFRACTION:

Principles of X-ray diffraction. Single crystal and powder methods, Interperetation of


diffraction data.

ELECTRON MICROSCOPPY:

Scanning electron Microscopes, Transmission electron microcopes, Specimen


preparation – Replica & thin toil.

HEAT TREATMENT OF METALS AND ALLOYS:


Annealing, spherodizing and Tempering, Isdothermal & Continous cooling, Phase
formation products in steel, Hardenability, Case hardening methods, Age hardening of
Al alloys, Comeercial practice in heat treatment of ferrous and non ferrous alloys.

STRUCTURE PROPERTY RELATION SHIP:

Effect of alloy elements in steel, effect of grairi size & practicle onproperties.

COMPOSITE MATERIALS:

Classification of composites, Polymer based Metal based. Refractory based


composites, Nano Composites.

PRACTICALS:

1. X-ray diffraction pattern of single crystal and powder specimen.


2. Scanning electron microscopy.
3. Transmission electron microscopy
4. Continuous cooling structure Harden ability test.
5. Effect of grain size and precipitate particles.
6. Composite methods.

C. No.AC-624 Industrial Training ( 0+3)

INDUSTRIAL TRAINING:

Every student of M.Sc.( Final) has to complete at least 6-8 weeks of industrial training in
a particular industry as suggested by the teacher incharge. After completing the training
he/she has to submit a report and deliver a seminar.

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