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Wear 255 (2003) 556–568

Communication
Detailed surface roughness characterization of engineering surfaces
undergoing tribological testing leading to scuffing
Allison Y. Suh a , Andreas A. Polycarpou a,∗ , Thomas F. Conry b
a Department of Mechanical and Industrial Engineering, 1206 West Green Street, University of Illinois at Urbana, Champaign, Urbana, IL 61801, USA
b Department of General Engineering, 104 South Mathews Avenue, University of Illinois at Urbana, Champaign, Urbana, IL 61801, USA

Abstract
Controlled tribological scuffing experiments were conducted on typical engineering surfaces (Al390-T6 discs and 52100 steel pins)
under starved lubrication conditions (a mixture of R410A refrigerant combined with a polyolester (POE) lubricant) to simulate the contact
conditions in an automotive air conditioning compressor. The time-to-scuff was established and was repeatable using a test protocol with
increasing load increments. Test were then conducted for periods of 25, 50, and 75% of the time-to-scuff to investigate the progression of
surface change preparatory to scuffing. Detailed studies of the surface topography were conducted using line and areal (usually referred as
one dimensional (1D) and two dimensional (2D), respectively) analyses. Simple amplitude roughness parameters as well as more detailed
spatial, hybrid, and functional parameters were calculated and used to track detailed roughness changes as the Al390-T6 samples undergo
progressive wear until scuffing occurs. One-dimensional amplitude descriptors, such as the root-mean-square value, were not reliable in
tracking surface topographic changes. However, 2D functional parameters, such as the surface bearing index and the fluid retention index,
clearly showed progressive changes as the surfaces wear and reach scuffing.
© 2003 Published by Elsevier Science B.V.
Keywords: Surface roughness; Engineering rough surfaces; Al390-T6; Scuffing; Compressor surfaces

1. Introduction the case of scuffing under starved lubricated contact condi-


tions. Ludema [9] showed the significance of surface rough-
In many engineering applications, surfaces in prolonged ness as it affects the magnitudes of the real area of contact
contact may experience abrupt catastrophic failure in the and the local contact pressures and temperatures. However,
form of scuffing. Scuffing is typically preceded by a mild commonly used roughness parameters are generally limited
wear process after which friction, noise, vibration, and in- to one dimensional (1D) profiling line amplitude properties,
terface temperature increase abruptly in the sliding contact e.g. center-line average (CLA) and root-mean-square (rms),
region, indicating a catastrophic failure [1]. Types of wear which lack information about other roughness characteris-
processes known to have a precursor role leading to scuffing tics. Since mild wear processes usually alter the top surface
include adhesive wear [2], abrasive wear [3], fatigue wear and the contained topographic features, decreasing trends
[4], and corrosive wear [5]. Under operational test condi- in the CLA or rms may not provide any new and signifi-
tions, scuffing is signaled by a drop in electrical contact re- cant insights into how scuffing-induced damage induces to-
sistance in a critically worn area, indicating a breakdown pographic change that can contribute to catastrophic failure.
in the boundary films and the resulting contact of the base In terms of topographic analysis, the initial surface finish,
materials [6]. Factors influencing scuffing include pressure, whether polished or textured, may also influence the path
velocity, temperature, lubrication, surface topography, ma- leading to different mild wear–scuffing related failures. For
terials and metallurgical composition, and film coatings on instance, depending on the types of virgin surface finish and
the surfaces in contact [6–8]. how the surface is progressively worn for the duration of
The characterization of surface topography and roughness performance, the newly changed surface may accommodate
are important factors in describing the wear and damage lubricant differently, which may either help retard or accel-
to surfaces in engineering tribological applications. Surface erate the scuffing process. Although the 1D line roughness
roughness in particular is known to play an important role in characterization has been useful to date, the resulting param-
eters do not contain information on detailed spatial variation,
∗ Corresponding author. Tel.: +1-217-244-1970; fax: +1-217-244-6534. areal and volumetric aspects of lubricant retention capabil-
E-mail address: polycarp@uiuc.edu (A.A. Polycarpou). ities. However, the roughness characterization of an area

0043-1648/03/$ – see front matter © 2003 Published by Elsevier Science B.V.


doi:10.1016/S0043-1648(03)00224-2
A.Y. Suh et al. / Wear 255 (2003) 556–568 557

Nomenclature y sampling interval in y-direction


z(x, y) 2D surface roughness as a function of
Fr force of friction calculated from the
x and y orthogonal coordinates
absolute of the resultant of Fx and Fy
Fx , F y ,
Greek letters
Fz forces in the three orthogonal directions
θ texture direction (0 < θ < 179◦ )
in the high pressure tribometer
τx phase shift in x (areal autocorrelation
h surface height normalized with respect to Sq
function), τx = i x
h0.05 surface height at 5% bearing area
τy phase shift in y (areal autocorrelation
normalized with respect to Sq
function), τj = j y
h0.8 surface height at 80% bearing area
ωx surface frequency in x-direction
normalized with respect to Sq
(areal power spectrum density)
Lx sampling length in x-direction,
ωy surface frequency in y-direction
Lx = (N–1) x
(areal power spectrum density)
Ly sampling length in y-direction,
Ly = (M–1) y
m maximum value of the autocorrelation
lengths in the x-direction of the surface (two dimensional (2D)), can account for the
M size of sampling matrix in y-direction mapping of the geometric features over an area and provide
(number of rows) insight into the physical and functional behavior of surface.
n maximum value of the autocorrelation To gain more insight into the scuffing process, a series
lengths in the y-direction of controlled experimental and analytical studies were con-
N size of sampling matrix in x-direction ducted on the evolution of the contact interface as it pro-
(number of columns) gresses from virgin to run-in, to mildly-worn, to worn, and
R radius of spherical summits ultimately to the scuffed state. The fundamental investigation
Sa arithmetic mean deviation of the surface of the tribological failure mechanisms was carried out on
Sbi surface bearing index or the ratio between Al390-T6 discs and 52100 steel pins as the exemplary con-
the Sq and the surface height at 5% of tacting surfaces (representative of the contact surface pairs
bearing area usually found in automotive air conditioning swash-plate
Sci core fluid retention index compressors) that eventually succumbed to scuffing [10,11].
Sdr developed interfacial area ratio One result from this work is that the most critical changes
Sds density of summits of the surface in material, chemical, and micro-structural properties occur
(based on eight nearest neighbor in the first 50–100 nm below the surface [11].
summit definition) The objective of this paper is to examine and quantify
Sku kurtosis of topography height changes in roughness occurring at surfaces during mild wear
distribution of the surface that ultimately lead to scuffing damage. Surface roughness is
Sq root-mean-square deviation of the surface a geometrical property of the surface and several standards
S q root-mean-square slope of the surface have been proposed to quantify it [12–15]. The surface finish
Ssc arithmetic mean summit curvature of or texturing chosen during the surface manufacturing pro-
the surface cess and the types of wear conditions that a surface has with-
Ssk skewness of topography height distribution stood over time are all visibly indicated in the topography
of the surface and roughness of the surface. The underlying assumption is
Std texture direction (−90 ≤ Std < 90◦ ) that surface topography characteristics can be useful precur-
Str texture aspect ratio (between 0 and 1; sors for predicting other changes that may occur in internal
0 = anisotropic, 1 = isotropic) sub-layers as well, features like hardness, elastic–plastic de-
Svi valley fluid retention index formation, chemical composition, and micro-structure [16].
Sz 10-point heights of the surface To quantify the changes on the roughness at various stages
Tscuff time to full-scuff prior to scuffing, pre-established 2D areal surface rough-
V(h0.05 ) void volume at the surface heights at ness parameters, namely the Birmingham-14 are used in this
5% bearing area study [16]. The Birmingham-14 parameters are a set of 14
V(h0.8 ) void volume at the surface heights at distinguishing roughness parameters for characterizing areal
80% bearing area surface topography, which quantify the geometric and func-
x x-coordinate of a 2D surface z(x, y) tional properties of a surface. By evaluating the amplitude,
x sampling interval in x-direction spatial, hybrid, and functional properties of actual engineer-
y y-coordinate of a 2D surface z(x, y) ing rough surfaces, the Birmingham-14, in principle, can
provide comprehensive parameters needed to characterize
558 A.Y. Suh et al. / Wear 255 (2003) 556–568

the 2D surface. The functional roughness parameters were


found to capture most accurately certain prominent charac-
teristics in the worn topography of the disc surfaces. This
paper is based on the experimental findings of surface rough-
ness characterization, which will aid in the understanding of
the wear conditions and the resulting evolution of surface
topography leading up to scuffing.

2. Background

2.1. Controlled tribological scuffing experiments

The materials used to simulate the compressor surfaces


are Al390-T6 discs (cast aluminum with 16.0–18.0% sili-
con content) and 52100 steel pins under a starved lubricated Fig. 1. Typical scuffing experiment data obtained from HPT: (a) applied
condition. With a pin-on-disc geometry, a versatile high normal load; (b) friction coefficient; and (c) electrical contact resistance.
pressure tribometer (HPT) is used to simulate the plate–pin
(usually referred to as plate–shoe) contacts in an automotive As the hardness of the steel pin is much higher than that
air conditioning swash-plate compressor [10,11]. The HPT of the disc (i.e. macro hardness of the Al390-T6 discs is 72
has a capability to measure the forces in the three orthogonal HRB while that of the 52100 steel pins is 62 HRC), wear
directions (Fx , Fy , and Fz ). From these forces, the force of due to sliding contact at the interface is most visible on the
friction (Fr ) and the coefficient of friction can be calculated. aluminum disc itself [6]. Thus, in this work, the detailed
The HPT is also capable of testing with ambient pressures roughness analysis was performed on the Al390-T6 discs.
up to 250 psig and temperatures from −12 to 120 ◦ C. The Furthermore, detailed roughness measurements on the steel
maximum applied load for the HPT is 1000 lbs [11]. To en- pins did not show any significant changes with tribological
able mild-wear contact between the material pair, the lower testing leading to scuffing. Fig. 2 shows the primary wear
sample (steel pin) is stationary and in contact with the up- track within the overall wear track of a scuffed sample exam-
per rotating sample (Al390-T6 disc) in the test chamber at ined by a scanning electron microscope (SEM). Though the
the linear sliding velocity of 2.4 m/s. In order to simulate width of a wear scar can be approximately 2 mm, the width
typical air conditioning compressor environments, the ex- of the primary wear track (the region of material transfer)
periments were performed in a refrigerant atmosphere under is <1 mm. Also, notice that the initial surfaces possess ma-
a 50 psi ambient pressure at 121 ◦ C near the contact inter- chining marks that are approximately perpendicular to the
face. To simulate a starved lubricated condition, a mixture of sliding direction, as depicted in Fig. 2(b).
R410A refrigerant combined with a polyolester (POE) lubri-
cant was sprayed on the disc surface at a rate of 40 mg/min. 2.2. Surface topography measurements
For more details on the HPT and scuffing experiments refer
to [6–8,17]. In general, engineering contact-related problems cannot
The test protocol leading to scuffing between the steel be simplified into line-profile geometries due to the complex-
pins and aluminum discs employs a method of incremen- ity in their contact conditions and given environments. The
tal loading. By increasing the normal load in increments of surface is best represented as an “area with height deviation
89 N at an interval of every 15 s, scuffing occurs after ap- rather than a line with height deviation” [18]. Therefore, a
proximately 6 min and 15 s, denoted as Tscuff , at a maximum surface profiler system that can acquire the 2D (usually re-
mean contact pressure of 20 MPa. This result is based on the ferred as 3D) height description of the disc topography over
repeatable scuffing results after executing a number of ex- an area is necessary. Also, in this study, the apparent contact
periments. A typical scuffing experiment is shown in Fig. 1, area dimensions between the Al390-T6 disc and the steel
where Fig. 1(a) shows the applied normal load; Fig. 1(b) the pin area is on the order of several mm. Therefore, an optical
friction coefficient; and Fig. 1(c) the electrical contact resis- surface profiler is used as the imaging instrument due to its
tance. Scuffing of the sample is signaled by both a sudden in- built-in capability to detect large range of vertical (surface
crease in friction coefficient, and a sudden drop in electrical height) variation and to accommodate a large imaging area.
contact resistance, which implies that direct metal-to-metal The advantages of using an optical profiler to measure
contact occurs without a protective lubricant film. Keeping surface topography are its quick data accumulation response
the same test protocol conditions and parameters, additional and that it is a non-contacting method. However, because
tests at three other intermediate conditions were performed this instrument relies on imaging techniques, as opposed
on the samples in which the test protocols were halted at to contact scanning techniques, it may lack accuracy in
1/4, 1/2, and 3/4 times of the total scuffing time Tscuff [11]. comparison to other alternative roughness measurement
A.Y. Suh et al. / Wear 255 (2003) 556–568 559

Fig. 2. The SEM surface images of Al390-T6 disc sample showing primary wear track magnification: (a) 20×; and (b) 50×.

instruments, such as contact profilometers [12]. The ver- observed, designated as Ra and Rq in Fig. 3. When compar-
tical scales of optical profile systems are based on the ing a virgin part to mildly-worn part at (3/4)Tscuff as shown
reflective coefficients over the sample surface; depending in Fig. 3(a) and (b), the surface is smoothened out signif-
on the reflectivity of the region, the vertical and lateral res- icantly from the previous stages. Because the disc at this
olution may also suffer due to optical noise (i.e. artifacts) stage is near scuffing in which destroyed protective surface
originating from wave interference. Despite these potential films can no longer “protect” the surfaces from damage, the
drawbacks, in this work the optical profiler has proven to induced surface damage is expected to be much greater than
be a sufficiently accurate method when the roughness data just change in vertical distribution of the asperities. Other
are correlated with data previously obtained using a line topographic changes, however, cannot be inferred from vi-
contact profilometer [11]. The details on the sampling con- sual analyses based on simple roughness profiling.
ditions of the obtained optical data are given in Table 1. When the sample is scuffed, different regions on the
Refer to Fig. 3 for the coordinate orientation of the data. disc exhibit different topographical features, as expected.
Fig. 3 displays typical roughness images of the virgin, Fig. 3(c) shows one of the most severely scuffed regions,
(3/4)Tscuff , and Tscuff samples in both top and isometric referred asprimary wear scar, which was also shown in the
views. As seen in all the images, both the virgin and worn SEM image of Fig. 2(b). In this region, faint scuffing tracks
samples seem to be highly anisotropic with traces of the in the sliding direction (perpendicular to the machining
original texture from machining. Notice how the roughness marks) are visible. At Tscuff , the scuffing is presented as
image of the fully-scuffed region (Fig. 3(c)) displays mild material transfer in small, defined regions between the steel
wear tracks due to scuffing damage. For all the samples, the pin and aluminum disc sample along the “wear track,” in
sliding direction is in the direction perpendicular to the ma- which the surface is extremely smooth. In essence, the disc
chining marks, as indicated by arrows. sample has already failed at this stage, thus comprehensive
According to the roughness images obtained in this study, analysis at this stage will probably not provide any insight
all the virgin discs have a predominant directionality in their into the surface changes leading up to scuffing. However,
topography due to the original machining process. These Fig. 3(c) shows the importance of 2D (versus 1D profiling)
discs were prepared from the identical blanks and machined roughness analysis since measuring in different areas will
using the same methods as the actual discs in swash-plate give different results.
automotive air-conditioning compressors. Although the ma- From observation of the optical images of the discs at
chining textures on the discs after (1/4)Tscuff and (1/2)Tscuff various wear stages, the lack of gross visual topographical
have become less dominant, no significant visual change changes seems to reinforce the hypothesis that mild progres-
other than small decrease in the CLA and rms values are sive wear may accompany other geometric and functional
topographical changes that become apparent only upon de-
Table 1 tailed surface characterization.
Sampling conditions of the optical profiler
x-direction y-direction 3. Areal roughness characterization using the
Number of sampling points 368 240 Birmingham-14 parameters
Image aspect ratio 1 1.167
Image size/length (mm) 1.1964 0.9093 As a standard procedure prior to areal roughness analy-
Sampling interval (␮m) 3.260 3.804
sis, all the topographical images are filtered under exactly
560 A.Y. Suh et al. / Wear 255 (2003) 556–568

Fig. 3. 2D surface roughness images of Al390-T6 discs: (a) virgin; (b) (3/4)Tscuff ; and (c) scuffed.

the same filtering conditions. Specifically, low-pass filtering surface roughness parameters may be used as the indicator
with cutoff wavelength of 8.5 ␮m is applied to remove the for quantifying the physical changes occurring at the surface.
high frequency noise. Due to the inherent method of opti- With the filtered roughness data, all parameters specified in
cal measurements, there is no need for high-pass filtering to the 2D Birmingham-14 [16] are used to describe the distin-
remove low frequency components (waviness). By keeping guishing aspects of the surface roughness of the Al390-T6
the same filtering conditions in all the topographical data, it discs undergoing mild progressive wear. Specifically, the to-
enables fair and consistent “roughness” comparison, avoid- pographic evolution during wear leading to scuffing can be
ing the issues and complexities associated with filtering and described through the characterization of amplitude, spatial,
its effect on roughness parameters [19]. and hybrid properties of the disc surfaces. More importantly,
In order to characterize the geometric properties of a sur- the evolution of functional properties, i.e. bearing, sealing,
face at various stages prior to scuffing, pre-established 2D lubrication retention capabilities at each tribological stage
A.Y. Suh et al. / Wear 255 (2003) 556–568 561

that lead to scuffing, can be characterized in reference to


how the changes in surface topography influence its intended
functional performance potential.
An important part of the 2D roughness characterization
is the distinction of summits and valleys within the digi-
tized sampling area. In this work, the “eight nearest neighbor
summit–valley” definition is adopted throughout the digital
calculation of summits and valleys, owing to its common
usage and its statistically superior behavior compared to the
“four nearest neighbor” definition [20]. The results are tab-
ulated and categorized in the following sections by different
roughness properties.

3.1. Areal amplitude parameters

The amplitude roughness parameters of the Al390-T6


discs at various tribological stages are summarized in
Table 2. The definition and method of calculation for each
parameter are explained in [21,22], and are also summa-
rized in the Appendix A. V and W stand for virgin (original
untested) and mildly-worn (tribologically tested) states,
respectively.
The CLA (Sa ) and rms (Sq ) parameters are the simplest
and most widely used amplitude parameters. As summa-
rized in Table 2, the results of these simple amplitude de-
scriptors are similar in their wear trends as well as virgin to
mildly-worn states within each disc. Fig. 4(a) helps visual-
ize the wear trends of the rms values, such that the surface
is mildly worn-out progressively with longer tribological
testing. Three important observations can be made from the
CLA and rms values with tribological testing. First and fore-
most, there exists a large sample-to-sample variability of
up to 76% difference between their virgin states. Next, re-
duction in the CLA and rms values persist with progressive
tribological testing, with the largest decrease of 50–60% ap-
pearing at (3/4)Tscuff stage. Finally, no severe wear occurs
due to the presence of boundary and mixed lubrication. De-

Table 2
Amplitude parameters as samples undergo tribological scuffing testing
Amplitude property (1/4)Tscuff (1/2)Tscuff (3/4)Tscuff Tscuff

CLA (␮m) Sa V 0.211 0.357 0.448 0.239


W 0.110 0.334 0.260 0.136
Rms (␮m)a Sq V 0.263 0.454 0.566 0.306
W 0.151 0.406 0.354 0.189
Ten-point height Sz V 2.552 3.514 3.668 3.669
Fig. 4. Amplitude parameter variation with different levels of tribologi-
(␮m)b
cal testing: (a) root-mean-square (Sq ); (b) 10-point height (Sz ); and (c)
W 1.694 2.811 3.078 1.810
skewness (Ssk ).
Skewnessc Ssk V −0.19 −0.16 −0.30 −0.35
W −0.61 −0.43 −1.74 −1.07 spite the clear reduction in the CLA and rms values with
Kurtosis Sku V 3.03 3.09 2.96 3.98 tribological testing, these parameters do not behave in a sys-
W 5.15 2.70 5.77 5.62 tematic way in which they can be used as precursors to
a See Fig. 4(a). scuffing.
b See Fig. 4(b). After averaging the 10 extreme peaks and valleys using
c See Fig. 4(c).
the “eight-nearest summit–valley” definition, the 10-point
562 A.Y. Suh et al. / Wear 255 (2003) 556–568

height variation (Sz ) of the surface is plotted in Fig. 4(b). 3.2. Areal spatial parameters
Interestingly, the disc-to-disc variation in the virgin discs is
smaller in the Sz analysis compared to the amplitude pa- In addition to the amplitude parameters examined in the
rameter (Sq ). Within a sample, the mildly-worn Sz is al- previous section, spatial parameters are then utilized to char-
ways smaller than the virgin Sz as with CLA and rms. How- acterize roughness information in the planar directions. Spa-
ever, the amount of the drop between the virgin Sz and the tial parameters include the density of summits (Sds ), measure
mildly-worn Sz in each stage is nearly identical for all the of isotropy–anisotropy of the surface (Str ), and directionality
wear stages. Due to its insensitive disc-to-disc variation in of surface texture (Std ). The areal autocorrelation function
the virgin states, 10-point height variation can be a more ap- (AACF), areal power spectrum density (APSD), and angu-
propriate amplitude parameter for determining the surface lar spectrum of the APSD are used to obtain the anisotropy
wear evolution, resulting in more steady, progressive wear of the surfaces and direction of the lay [16,23,24], also sum-
behavior. marized as Eqs. (A.1), (A.3) and (A.4), respectively, in the
Referring to Table 2 and Fig. 4(c), the skewness value Appendix A. Eqs. (A.2) and (A.5) in the Appendix A sum-
(Ssk ) at each tribological stage behaves relatively well. Not marize the mathematical definitions for calculating Str and
only is disc-to-disc variation in the initial virgin states neg- Std , respectively, in continuous integral forms. Table 3 sum-
ligible, but the skewness value also progressively decrease marizes the areal spatial parameters calculated in this study
from −0.25 at the virgin stages to −1.7 at (3/4)Tscuff . The for the samples undergoing tribological testing.
skewness decreases between virgin and mildly-worn states Using the “eight nearest neighbor summit–valley” defi-
for all the samples. The highly negative skewness values in nition, the density of summits (Sds ) is calculated for all the
the mildly-worn states support the theory that mildly-worn disc samples. As shown in Table 3, despite minor variation
asperities result in the surface being more negatively from disc-to-disc in their initial virgin states, it is clear
skewed by revealing more pits and valleys than peaks. The that the density of summits in the mildly-worn states is
most change is observed when moving from (1/2)Tscuff to always higher than the virgin states, albeit not by much.
(3/4)Tscuff . At this worn stage just before full scuffing, con- Most change occurs at (3/4)Tscuff , which explains that as
dition of the surface seems to be characterized by losing the the surface smoothens out, it reveals more minor asperities
spikiness of the top asperities by significant amounts. Not in the lower zones. The increase in the number of summits
only does the skewness show a clear trend with progressive in the “valley” in turn causes the total density of summits.
tribological testing but the lack of sample-to-sample vari- Other than a general increase from virgin to mildly-worn
ability in the virgin state seems to indicate a potential for states, no conclusive trend can be seen from the Sds
its use as precursor to scuffing. analysis.
The kurtosis (Sku ) values for all the virgin states are near A useful spatial parameter is the texture aspect ratio (Str ),
Gaussian, varying between 3 and 4. After the progressive sometimes referred to as the isotropy index, which describes
tribological testing, the kurtosis values seem to increase up the degree of isotropy of the surface roughness. The texture
to around 5 at all stages except (1/2)Tscuff . Unlike in the aspect ratio is based on the calculation of the areal autocor-
skewness analysis, no conclusive trend can be deduced from relation function (AACF) over the surface of interest. For
the kurtosis analysis other than its generally increasing ten- strongly anisotropic surfaces exhibiting a lay direction, the
dency towards being centrally distributed (Sku > 3). Str for a surface is typically <0.3. Indeed, this seems to be the
In the amplitude roughness analysis of Al390-T6 discs, case in Table 3 for all of the virgin and mildly-worn disc sam-
the CLA and rms parameters that are used extensively to ples, mainly due to the highly directional originally present
quantify surface roughness and changes do not show any machining marks. In a traditional wear test, the initial ma-
systematic trends that can be used as precursors to scuffing. chining marks are obliterated significantly, thereby chang-
On the other hand, the skewness seems to present clearly ing the surface from highly anisotropic to isotropic. In this
a well-behaved progressive trend with tribological testing, case, however, Str does not change much, indicating that the
suggesting its use as a precursor to scuffing. “wear” does not significantly affect the original machining

Table 3
Spatial parameters as samples undergo tribological scuffing testing
Spatial property (1/4)Tscuff (1/2)Tscuff (3/4)Tscuff Tscuff

Density of summits (mm−2 ) Sds V 5.089 × 103 4.777 × 103 4.690 × 103 5.587 × 103
W 5.657 × 103 4.969 × 103 5.769 × 103 5.157 × 103
Texture aspect ratio (0–1) Str V 0.28 0.094 0.28 0.036
W 0.12 0.041 0.28 0.070
Texture direction (◦ ) Std V −88.32 −89.16 88.32 −88.05
W −85.01 83.15 89.37 −89.27
A.Y. Suh et al. / Wear 255 (2003) 556–568 563

Fig. 5. Texture direction defined by the areal power spectrum density.

marks of the top surface, which was highly anisotropic be- ing on the relative influence of either the amplitude or
fore the tribological scuffing testing. the spacing or both, hybrid parameters will represent the
In order to determine the texture direction of the surface, combined aspects of roughness. Table 4 summarizes the hy-
first the areal power spectrum density (APSD) analysis, im- brid parameters, extracted from the virgin and mildly-worn
mediately followed by the angular spectrum analysis, must samples.
be performed [16]. The lay directions are found to be the an- The hybrid slope S q is the scalar magnitude of the
gle at which the maximum peak occurs in the angular spec- continuous surface slope at any point. Between virgin and
trum matrix, as illustrated in Fig. 5. Due to the pronounced mildly-worn states of each tribological testing stage, the
directionality in the Al390-T6 discs, each disc, whether vir- S q value of the mildly-worn state is always smaller as
gin or worn, has a distinctive maximum peak in its respec- summarized in Table 4. The reason for this reduction may
tive angular spectrum plot (i.e. anisotropic). be that the top asperities are being polished with tribological
From the spatial parameter characterization of the testing. Despite the large virgin sample variability, the dif-
Al390-T6, it is found that the Sds does not yield a signifi- ference between worn S q and virgin S q seems to increase
cant trend with tribological scuffing testing. Similarly, not for more severely worn stages, especially at (3/4)Tscuff .
much change is observed in Str and Std either, though they This indicates that the S q decreases steadily as the surface
are unique 2D spatial parameters not found in 1D analysis. approaches scuffing. This result seems to agree with the
From a practical point of view, knowledge of the degree of previously regarded observation on the reduction of asper-
anisotropy and its direction are very important, especially ity heights, in which the slope of a summit is expected to
in cases where there is no severe wear to completely alter reduce when the top asperity is worn off. However, because
the surface roughness and lay direction. the sample-to-sample variability is relatively large in the
S q , wear evolution through different stages of tribological
3.3. Areal hybrid parameters testing is difficult to substantiate.

Hybrid parameters explain relative characteristics be- Table 4


tween amplitude and spatial properties. For instance, what Hybrid parameters as samples undergo tribological scuffing testing
is simply considered as the summit radius R or curvature
Hybrid property (1/4)Tscuff (1/2)Tscuff (3/4)Tscuff Tscuff
by 1D line profile definition can be expanded into the true
2D perspective radius or curvature Ssc (Eq. (A.6) in the Rms slope S q V 0.078 0.14 0.16 0.12
W 0.058 0.12 0.10 0.065
Appendix A). The parameter Sdr (Eq. (A.7)), or developed
interfacial area ratio, is a unique 2D hybrid parameter that Mean summit 1/Ssc V 35.21 20.92 20.24 24.27
is indicative of the total surface area over a given sam- radius (␮m) W 50.16 25.04 42.35 54.44
pling area. The rms of summit curvature S q (Eq. (A.8)) Developed area Sdr V 0.30 1.00 1.19 0.67
is the magnitude of the surface slope similar to the rms ratio (%)a W 0.17 0.75 0.49 0.21
of height variation in amplitude property [22]. Depend- a See Fig. 6.
564 A.Y. Suh et al. / Wear 255 (2003) 556–568

The mean summit curvature (Ssc ) and summit radius (R)


are inversely related according to the spectral moment rough-
ness characterization [25]. Within an individual sample, mild
wear increases the summit radius or decreases its curvature.
The difference between the virgin and mildly-worn summit
radii from sample-to-sample also increases progressively as
the surface approaches scuffing. This seems to indicate that
the summit radius and rms slope of the surface (S q ) are
in a cause-and-effect relationship; the larger the summit ra-
dius, the larger the rms slope, and vice versa. Overall, the
disc-to-disc variation in the virgin summit radii is compa-
rably small (within 20%) except in the initial virgin state
of (1/4)Tscuff (70%). As with the previous S q analysis, no
clear trend between each state of tribological testing is ob-
served in the Ssc analysis.
The trend in the developed area ratio Sdr can further en-
hance the understanding of the tribological testing effects on Fig. 6. Hybrid parameter variation with different levels of tribological
roughness. Sdr stands for the unique areal measure of how testing—developed area ratio (Sdr ).
much the true area of the surface exceeds that of the nominal
reference surface or sampling area [16]. The general trend the surfaces go through wear–scuffing under various con-
of the Sdr shown in Fig. 6 is that as the surface goes from ditions [21]. In order to better understand the actual per-
virgin to mildly-worn states, Sdr decreases, indicating that formance of 2D surfaces and their lifecycle under various
the total real surface area decreases after tribological testing. processes, investigations on area and volume properties of
This is due to the diminishing true surface area above the the surface features are further required. In the 1930’s, Ab-
mean plane with mild wear. As with the other hybrid param- bott and Firestone [26] introduced the “bearing area curve,”
eters, no clear trend is observed with Sdr , with the existence which is defined by percentage length obtained intersect-
of large sample-to-sample variability. ing a line at different heights with the 1D profile. It is still
Observing clear trends in hybrid parameters between pro- widely used today for characterizing in fluid retention prop-
gressive tribological testing stages is complicated by the fact erties, mechanical resistance and load carrying capacity [14].
that a hybrid property is influenced by both amplitude and One drawback in using the bearing area curve is that it is a
spatial properties of the surface. Although hybrid parame- “qualitative” measure. To alleviate this disadvantage, func-
ters may not be used as precursors to scuffing, values before tional parameters defined in the Birmingham-14 are used as
and after tribological testing exhibit consistent patterns de- the “quantitative” measures directly derived from the bear-
spite sample-to-sample variability. ing area curve analyzed over 2D surface as opposed to con-
ventional 1D Abbott–Firestone bearing area curve. Table 5
3.4. Areal functional parameters summarizes the functional parameters of the Al390-T6 disc
samples in simple index form. Surface bearing area ratio
The geometrical properties, i.e. amplitude, spatial, and curves from which the functional parameters are derived,
hybrid of a given areal surface topography change with are provided in Fig. 6 for (1/4)Tscuff and (3/4)Tscuff cases.
wear, friction, and lubrication states, which in turn affect Truncation plane marks at 5 and 80% of the bearing area are
performance and reliability of the component. The geo- also included in Fig. 6 to categorize the bearing area curve
metric roughness, influences not only the “mechanical and into three functional zones, namely, material volume in peak
physical” properties of contacting interfaces, but also the zone (0–5%), void volume in core zone (5–80%), and void
functional properties in actual tribological applications as volume in valley zone (80–100%) [16].

Table 5
Functional parameters as samples undergo tribological scuffing testing
Functional propertya (1/4)Tscuff (1/2)Tscuff (3/4)Tscuff Tscuff Gaussian reference

Surface bearing index Sbi V 0.640 0.624 0.649 0.652 0.608


W 0.703 0.715 1.104 0.724
Core fluid retention index Sci V 1.46 1.492 1.422 1.422 1.56
W 1.285 1.286 0.681 1.214
Valley fluid retention index Svi V 0.119 0.130 0.140 0.133 0.11
W 0.166 0.126 0.238 0.186
a See Fig. 8.
A.Y. Suh et al. / Wear 255 (2003) 556–568 565

Fig. 8. Functional parameter variation with different levels of tribological


testing: (a) bearing index (Sbi ); and (b) core fluid retention index (Sci ).
Fig. 7. Bearing area ratio curves: (a) virgin and (1/4)Tscuff states; and (b)
virgin and (3/4)Tscuff states.
the horizontal intersections at 5 and 80% levels in the bear-
ing area curve.
When virgin and mildly-worn states are overlaid together By definition, Sbi is the ratio of the Sq over the surface
in the bearing area ratio curves, a definite wear trend can height at 5% bearing area, or h0.05 , given by Eq. (A.9) in
be observed. Although the difference between virgin and the Appendix A. Although the bearing area ratio curve for
mildly-worn parts is hardly recognizable at (1/2)Tscuff stage each tribological stage does not show much physical differ-
as shown in Fig. 7(a), a dramatic difference is observed ence, marked differences are shown when analyzed in terms
at (3/4)Tscuff stage as delineated in Fig. 7(b). This may be of Sbi . One novel advantage in performing this analysis is
due to increasingly detrimental plastic deformation in the that the Sbi values for virgin parts are nearly constant and
asperities as the contact surface approaches the fully-scuffed close to Gaussian (≈0.608) as seen in Fig. 8(a). Invariabil-
stage. ity in the virgin states immediately eliminates the issues
Rather than analyzing the functional characteristics of the concerning with the disc-to-disc variation. As for individ-
discs in terms of absolute physical quantities presented in ual tribological stages, mildly-worn Sbi values are always
the bearing area ratio curve, which is not only qualitative higher than virgin Sbi values. An increase in Sbi is expected
but also can get easily complicated, a simpler and better when undergoing tribological testing, as it was reported that
method is to use a series of simple indexes. As summa- as the surface is worn out, the Sbi value grows from Gaus-
rized in Table 5, three functional indexes derived from the sian ≈0.608 [16]. As for the global trend, the Sbi increases
bearing area curves describe the functional evolution of the as well. Ignoring the fully-scuffed stage, the mildly-worn
Al390-T6 discs with wear. The mathematical formulae for Sbi graph steadily increases up to 1.104, about 1.7 times
these indices are given in the Appendix A and are, surface larger than that of the virgin state. Generally, the higher the
bearing index (Sbi ), core fluid retention index (Sci ), and val- Sbi , the better the bearing property of the surface. If only
ley fluid retention index (Svi ), all of which are derived from the Sbi is considered ignoring other roughness properties,
566 A.Y. Suh et al. / Wear 255 (2003) 556–568

chemical and micro-structural properties, the bearing area 4. Conclusions


of the Al390-T6 disc increases as the surface undergoes
wear. The surface roughness characterization technique is an
Sci is the ratio of the void volume at the core zone (defined important analytical method by which one can understand
by 5–80% bearing area) over Sq , as seen in Eq. (A.10) of the the conditions of mild wear to scuffing. In this work the
Appendix A. The void area trapped in this zone is integrated study of the roughness evolution of Al390-T6 engineering
and normalized with respect to the sampling area and Sq . rough surfaces prior to scuffing involved the use of the
Similar to the Sbi trend, all virgin parts are approximately well-established areal surface topography characterization
constant and near Gaussian (≈1.56) as shown in Fig. 8(b). tools, namely the Birmingham-14 parameters. Based on such
Invariability in the virgin Sci trend, despite manufacturing areal data, various geometric and functional properties of
irregularities, makes this parameter not only unique but also the disc roughness were analyzed as the discs underwent
reliable. In general, as a surface experiences wear, the Sci controlled tribological testing. The Birmingham-14 param-
decreases. For all the Al390-T6 samples, mildly-worn Sci eters in this study yielded numerically distinctive and statis-
values are smaller than virgin Sci values, indicating an exis- tically sound parameters. Also, the roughness parameters at
tence of mild wear. The trend in the Sci is decreasing as the the different tribological stages prior to scuffing can be sum-
surfaces progress toward the scuffed state. The decreasing marized simultaneously for practical comparison and trend
trend of the Sci implies the deterioration of the fluid retention analyses.
property in the core zone. This is a justifiable conclusion, One important conclusion from the analyses of amplitude
since reduction of the top asperities inevitably decreases the parameters is that the CLA and rms values, commonly used
void volume once formed by the existing asperities. There- in tribological tests, may not yield reliable and consistent
fore, at scuffing fluid can not be retained. By referring to results, when determining parameters that can be used as
Fig. 8(b) that shows the Sci trends, it becomes clear that the precursors to scuffing. The large sample-to-sample variabil-
lubricant–refrigerant retention capability within the disc sur- ity seems to lessen in the skewness analysis, which shows a
face degenerates as the surface approaches the scuffed state. clear evolutionary trend to scuffing. The analyses of spatial
Similar to Sbi , Svi is the ratio of the void volume at the parameters and hybrid parameters further support the hy-
valley zone (entrapped within 80–100% bearing area) over pothesis that as virgin surfaces undergo controlled tribolog-
Sq , and is given by Eq. (A.11) of the Appendix A. The void ical testing, the top asperities are smoothened or decrease
volume at this zone is calculated by integrating the bear- in height until the onset of scuffing. However, large sample
ing area within this range, whose result is normalized by variability in their virgin states complicates the observation
the sampling area and Sq . Unlike the previous indices, the of evolutionary trends towards scuffing.
Svi is relatively constant for all cases. If a value is signifi- A sound conclusion in the tribological progression of
cantly larger than 0.11, this indicates a flat top, a deviated roughness can be drawn from the functional parameters or
shape from a standard Gaussian distribution. For all tribo- indices derived from the bearing area curve, namely the sur-
logical stages except at (1/2)Tscuff , mildly-worn Svi values face bearing index and fluid retention index. Unlike the pre-
are larger, indicating its tendency towards a flatter surface vious geometric parameters, the functional indices remain
geometry. Overall, the trend in the Svi may be perceived as fairly constant on the virgin surfaces, making the inherent
increasing, the opposite of the Sci . A reasonable explanation disc-to-disc variation minimal. As the surface approaches
for this behavior is that as the surface approaches scuffing scuffing, the effects of progressive wear are translated into
the core void volume decreases while the valley void vol- a decreased fluid retention capability and an increased bear-
ume increases in turn to compensate for the loss. However, ing index, which both indicate that lubricant can no longer
the increase in the valley zone is usually not sufficient to be retained sufficiently. The loss of lubricant retention capa-
fully compensate for the loss of the core void volume. bility means an increase of the real area of contact, leading
Though strictly speaking, functional parameters are cal- to eventual direct metal-to-metal contact without any films
culated by geometrical aspects of roughness, the ramifica- at scuffing. It is shown that the functional parameters can
tions of their use are much more than simple references to be used to correlate the topographical changes to the mean-
geometric properties of a surface. Given that tribological ingful physical changes occurring during progressive wear
wear leads to scuffing under boundary and mixed lubrica- leading to scuffing.
tion conditions, functional parameters imply how the sur-
face changes to exhibit different bearing and fluid retention
properties. The most prominent advantage of using func- Acknowledgements
tional parameters in analyzing Al390-T6 discs is the lack of
sample-to-sample variability in their virgin states, thereby This research was supported in part by the National
enabling a sound comparison between tribological stages. Science Foundation and the 30 member companies of the
Furthermore, all functional parameters exhibit clear system- Air Conditioning and Refrigeration Center, and Industry–
atic progressive trends, indicating a potential use of these University Cooperative Research Center at the University
parameters as precursors to scuffing. of Illinois at Urbana, Champaign. The tribological testing
A.Y. Suh et al. / Wear 255 (2003) 556–568 567

was performed by Mr. J.J. Patel in the Tribology Labora- A.2. Hybrid parameters
tory of the University of Illinois. The surface roughness
measurements were performed at Professor C. Liu’s Micro • Mean summit curvature, Ssc
Actuators, Sensors, and Systems Group at the University 
t
of Illinois. The scanning electron microscope images were 11 ∂z2 (x, y) ∂z2 (x, y) 
Ssc = − + 
taken at the Center for Microanalysis of Materials at the 2t ∂x2 ∂y2 for any summit
k=1
University of Illinois, which is supported by the US De-
(A.6a)
partment of Energy under Grant DEFG02-96-ER45439.
where t is number of summits and
1
Appendix A. Formulae for calculating the 2D R= (A.6b)
Ssc
roughness parameters
• Developed area ratio, Sdr
A.1. Spatial parameters
total interfacial area − sampling area
Sdr (%) = × 100
sampling area
• Areal autocorrelation function, r(τ x , τ y )
(A.7)
r(τx , τy ) = E[z(x, y) z(x + τx , y + τy )]
 Ly  Lx or
1
= lim z(x, y) total interfacial area − (M − 1)(N − 1) x y
Lx ,Ly →∞ 4Lx Ly −Ly −Lx Sdr (%) =
(M − 1)(N − 1) x y
× z(x + τx , y + τy ) dx dy (A.1) × 100
• Texture aspect ratio, Str See [16,22] for calculating the “total interfacial area”.
   • Root-mean-square slope, S q
min τi 2 + τ j 2 
0 < Str = 

  ≤ 1,  Lx  Ly 
1 ∂z(x, y) 2
max τi 2 + τj 2  S q=
Lx Ly 0 0 ∂x
r(τi , τj )  1/2
where ≤ 0.2 (A.2) ∂z(x, y) 2
r(0, 0) + ∂x ∂y (A.8)
∂y
where i = 0, 1, ..., m < M; j = 0, 1, ..., n < N; τi =
i x; τj = j y
• Discrete Fourier transform, F(ωx , ωy ) A.3. Functional parameters
 ∞ ∞
F(ωx , ωy ) = z(x, y) • Surface bearing index, Sbi
−∞ −∞
× exp[−j2π(ωx x + ωy y)] dx dy (A.3) Sq 1
Sbi = = (A.9)
(z)Stp =5% h0.05
• Areal power spectrum density, G(ωx , ωy ), and angular
spectrum Ga (θ) • Core fluid retention index, Sci
G(ωx , ωy ) = F(ωx , ωy ) F ∗ (ωx , ωy ) (A.4a) ((Vv (h0.05 )−Vv (h0.8 ))/((M−1)(N−1) x y))
Sci =
Sq
 rr(θ) (A.10)
Ga (θ) = G(θ, r) dr
0 • Valley fluid retention index, Svi
2 −1/2
rr(θ) = 1
2 [( x cosθ) + ( y sinθ) ]
2
(Vv (h0.8 ))/((M − 1)(N − 1) x y)
◦ Svi = (A.11)
where 0 ≤ θ ≤ 179 . (A.4b) Sq
• Texture direction, Std
 π

 −θ, θ≤ References
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