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compositional gradients in hydrocarbon reservoirs is well introduction to these subjects and their application, and Figure
known, and a number of field cases and experiences of 1 displays examples of crude oil spectra in the NIR region.
compositional grading in oil and gas-condensate reservoirs During the pumpout and drawdown periods for formation
have been described in the literature10, 11. cleanup prior to fluid sampling or during downhole fluid
Modern wireline formation testing and sampling tools have analysis stations, the pumpout module of the tool segregates
begun to provide new measurements which can be used to fluid within the displacement unit and the tool flow line
determine in-situ fluid type, and used to characterize according to its density. This effect tends be more pronounced
hydrocarbon fluid properties and composition12-15. These when the fluid density contrast is large. In many situations this
methods of in-situ hydrocarbon analysis or downhole fluid fluid segregation and downhole separation within the tool can
analysis (DFA) are principally made using visible and near- be exploited and combined with optical monitoring to provide
infrared spectroscopy (NIR) and fluorescence15-17. The fluid improved fluid analysis and sample capture. The relative
composition analyzer built on these measurement principles position of the optical fluid analyzers in the flowline is an
currently provides the concentration of C1, C2-C5, C6+ and important consideration since gravity segregation and pressure
CO2 of the fluid in the flowline and the gas-oil-ratio (GOR). differential will affect the spectrometer response. For our
The fluorescence intensity and spectra measurements are applications described here, optical fluid analyzers were
sensitive to hydrocarbon type and may be used for detection of positioned on both the inlet and outlet side of the pumpout
dew formation and any phase transitions17. A measurement of module. Such dual optical fluid analyzer combinations allow
index of refraction also provides gas detection. monitoring of gas separation or condensate dropout on the
Using this DFA measurement technique and methodology, inlet or low pressure side of the flowline, and compositional
sampling and fluid analysis can be performed in real-time at monitoring at the nearest entry point of the sample bottle prior
various depths across the reservoir interval to analyze to sample capture.
formation fluids and optimize the logging operation18-19. In the sections which follow we briefly review selected
Factors such as depth accuracy, number of stations, bed examples where a modular wireline formation tester equipped
thickness and supercharging can impact formation pressure with dual packer and/or probe modules, and latest generation
measurements – this is not the case for downhole fluid optical fluid analyzers was utilized to measure formation
analysis which is a direct method for measuring fluid pressures, perform fluid analysis and collect samples. The
properties in-situ. An integrated analysis of the openhole well MDT (Modular Dynamics Formation Tester)* tool provides
logs, seismic and geological data in combination with this capability12. The tool is wireline conveyed and can be run
formation pressure measurements and fluid properties aids in various configurations, set repeatedly, and positioned at
reservoir characterization and provides valuable input to different locations along the wellbore in a single trip. The
reservoir management20. MDT has been described in detail elsewhere and can be
configured for a variety of applications depending on the
logging objectives, e.g. formation pressure measurements,
Formation Testing with Downhole Fluid Analysis fluid sampling and downhole fluid analysis. In this context
For successful execution of wireline testing and sampling MDT-like tools are more generally known as wireline
operations, in-situ contamination monitoring and quantitative formation testers.
fluid characterization is vital13-15. Availability of real time
variances of fluid compositions, and information about the
phases and contamination levels13,14 which are present during a Application Examples
testing and sampling operation can be used for optimization of Wireline formation testing in combination with downhole
sample acquisition and data for input in the identification of fluid analysis and sampling has been conducted in multiple
hydraulic flow units and characterization of reservoir wells (18 wells surveyed over 2002-2006) during the appraisal
architecture. and development of an oilfield in Oman. The surveyed wells
Optical fluid analysis is the most widely accepted and were drilled into the Gharif and Al Khlata Formations which
advanced technique for fluid identification and quantitative form significant reservoirs in north-central Oman. The
compositional analysis. The near-infrared (NIR) adsorption reservoirs are multilayered, heterogeneous and highly variable
spectra and optical properties of hydrocarbons has been in terms of geometry, connectivity, permeability and fluid
extensively studied and used in many industries for a variety properties. Newly drilled wells often show differential
of monitoring and analysis purposes. Colouration of crude oils pressure depletion between layers, which helps assess lateral
varies over a wide range. The low-energy electronic and vertical reservoir continuity. However such complexity
adsorption tail can occur in the UV for gas-condensates, the and reservoir heterogeneity means that conventional pressure-
visible for medium crude oils, and the near-infrared for heavy depth plot and pressure gradient analysis of wireline pressure
oils and tars. Petroleum hydrocarbons have two types of data is not easy, and identification of in-situ fluid density
adsorptions: colour adsorption and molecular vibration changes can be difficult. Downhole fluid identification and
adsorption. Measurements of these properties and molecular analysis is used to help address important fluid and reservoir
interactions can be used to distinguish oils of different evaluation and management issues, and provide input to well
compositions and to measure GOR during openhole sample completion and selection of intervals for perforation.
acquisition15,16. In this paper we limit our discussion of the
experimental and theoretical background of optical fluid Field Example A
analysis and NIR. References 15 to 20 provide a good
SPE 102571 3
This was a vertical appraisal well drilled using WBM to assess indicates the variation of fluid type, and differences in GOR
the hydrocarbon accumulations and pressure depletion within and C6+ values between the oils and hydrocarbon gases with
the Upper, Middle and Lower Gharif Formations and the Al depth. The GOR and C6+ values for the oils encountered at
Khlata Formation. Conventional wireline logging suites were stations 1 and 3 are different, e.g. GOR of the oil at the
first run after drilling, followed by a combinable wireline deepest point (station 1) is higher than the GOR of the oil
formation tester. The toolstring was configured with multiple encountered at station 3. Similarly, the hydrocarbon gases
probe modules, a pump, multiple sample chamber modules, display some differences in their GOR and C6+ content with
and optical fluid and compositional fluid analyzers. depth, e.g. a general trend of increasing C6+ values with
Forty-four pressure measurements were made across the decreasing depth between stations 4 to 6. For this well the
reservoir interval plus six downhole fluid analysis and combination of openhole logs and formation pressures with
sampling stations. Figure 2 shows a composite display of the the optical composition fluid analyzer data, enabled a proper
openhole logs, together with the formation pressure and assessment of the hydrocarbon fluids and their spatial
mobility measurements against depth. The depths of the variation within the reservoir intervals. This information
sampling and downhole fluid analysis stations are shown by provided valuable input for reservoir engineering studies,
the coloured bars which show the fluid fractions and completion design and selection of optimum intervals for
compositional measurements from the optical fluid analyzers. perforating the well. The well was completed in the oil bearing
In Figure 2 the downhole fluid analysis and sampling stations intervals as a single selective completion with dual perforation
are labeled 1 to 6, and the fluid type and GOR values from the zones.
fluid analyzer are displayed on figure 2. From inspection of
the pressure measurements it is apparent there is considerable
differential pressure depletion and vertical reservoir Field Example C
compartmentalization and significant variation in fluid type Example C is a DFA station from the Example B well. It is
and GOR value. Because of this differential pressure depletion included to illustrate the use of optical fluid analyzers on the
it would be difficult to recognize and define accurate pressure inlet (low pressure) and outlet (high pressure) side of the pump
gradients for estimating in-situ fluid densities; especially during sampling and downhole fluid analysis. In this particular
across the middle (e.g. 2550 - 2600m MD) and uppermost case a composition fluid analyzer was positioned on the outlet
sections (e.g. 2350 -2400m MD) of the reservoir. side (above) of the pump, so we could exploit the residence
Compartmentalization here is probably due to the presence of time of fluids in the pump and gravity segregation of the
several barriers between stations 3 and 4 and between 4 and 5. fluids. Figure 4 shows data from a DFA station where a
There are abrupt pressure changes across the intervals between multirate drawdown was performed after the fluid
stations 3 and 4, and also stations 5 and 6. It is interesting to composition, phase and GOR had been established. In this
note the C6+ and GOR values are different between the oils at case, at about 7300 seconds elapsed time the flow rate and
stations 4, 5 and 6. Oil from the lowest depth (station 3) has a drawdown pressure was progressively and deliberately
lower GOR value and more C6+ than the oils from shallower increased to evaluate fluid and phase behavior, and also
depths (stations 4 and 5). Such variations in fluid composition provide a crude estimate of the bubble-point pressure. Free gas
and heterogeneity within the hydrocarbon column would not broke out when the drawdown pressure was increased (fig. 4)
be evident from conventional pressure gradient analysis. and there is clear mass fraction segregation and increased
fluorescence vibration (FLD0 and FLDR in fig. 4). This
demonstrates the utility of dual fluid analyzers, and the
Field Example B sensitivity of fluorescence intensity measurements to detect
This example is from a vertical development well drilled using phase transitions.
OBM to assess the pressure depletion and fluid type
distributions within the Upper, Middle and Lower Gharif
Formations. Conventional logging suites were first run after Summary and Conclusions
drilling, followed by a combinable wireline formation tester. Downhole fluid analysis is a technique and methodology
The toolstring was configured with a probe module, a pump, which is finding widespread application for in-situ
multiple sample chamber modules, and optical fluid and characterization of reservoir fluids and improved sampling. In
compositional fluid analyzers. combination with other log data it can be used as a new tool to
In total, twenty-five pressure measurements were made better characterize the reservoir, and provide data for input for
across the reservoir interval plus six downhole fluid analysis both reservoir management purposes and in optimizing the
and sampling stations. The oil-based mud contamination well completion and production strategy. The field examples
analysis13,14 showed that low contamination levels were briefly reviewed in this contribution show the utilization of
achieved. Figure 3 shows a composite display of the openhole data from wireline downhole formation fluid analysis and
logs, together with the formation pressure and mobility formation tests, and their practical application in formation
measurements against measured depth. Analysis of the evaluation and reservoir management.
pressure measurements and the depletion profile indicate there
is some level of vertical reservoir compartmentalization, and
the likely presence of permeability barriers and several distinct
flow units. This level of compartmentalization is also
confirmed by the optical fluid analyzer data (Figure 3) which
4 SPE 102571
1. Smolen, J. J., and Litsey, L. R: ‘Formation Evaluation 13. Hashem, M. N., Thomas, E. C., McNeil, R. I., and Mullins,
Using Wireline Formation Tester Pressure Data,’ paper O. C: ‘Determination of Producible Hydrocarbon Type and
SPE 6822 prepared for presentation at the SPE Annual Oil Quality in Wells Drilled with Synthetic Oil-Based
Technical Conference and Exhibition, held in Denver, Muds,’ SPE Reservoir Evaluation and Engineering, 2, 125-
USA, 9-12 October 1977. 133, 1999.
2. Stewart, G., and Wittman, M: ‘Interpretation of the 14. Mullins, O. C., and Schroer, J: ‘Real-Time Determination
Pressure Response of the Repeat Formation Tester,’ paper of Filtrate Contamination During Openhole Wireline
SPE 8362 presented at the SPE Annual Technical Sampling by Optical Spectroscopy,’ paper SPE 63071
Conference and Exhibition, Las Vegas, USA, 23-26 prepared for presentation at the SPE Annual Technical
September 1979. Conference and Exhibition, Dallas, USA, 1-4 October
2000.
3. Dake, L. P: ‘Application of the Repeat Formation Tests in
Vertical and Horizontal Pulse Testing in the Middle 15. Dong, C., Mullins, O. C., Hegeman, P. S., Teague, R.,
Jurassic Brent Sands, ‘ paper EUR 270 presented at the Kurkjian, A., and Elshahawi, H: ‘In-situ Contamination
1982 SPE European Petroleum Conference Monitoring and GOR Measurement of Formation Fluid
Samples,’ paper SPE 77899 prepared for presentation at the
4. Stewart, G., and Ayestaran, L: ‘The Interpretation of SPE Asia Pacific Oil and Gas Conference and Exhibition
Vertical Pressure Gradients Measured at Observation Wells held in Melbourne, Australia, 8-10 October 2002.
in Development Reservoirs,’ paper SPE 11132 prepared for
presentation at the SPE Annual Technical Conference and 16. Fujisawa, G., van Agthoven, M. A., Jenet, F., Rabbito, P.
Exhibition, New Orleans, USA, 26-29 September 1982. A., and Mullins, O. C: ‘Near-infrared compositional
analysis of gas and condensate reservoir fluids at elevated
5. Pelissier-Combescure, J., Pollock, D., and Wittman, M : pressures and temperatures,’ Applied Spectroscopy, 56,
‘Application of Repeat Formation Tester Measurements in 1615, 2002.
the Middle East,’ paper SPE 7775 prepared for presentation
at the Middle East Oil Technical Conference held in 17. Betancourt, S. S., Fujisawa, G., Mullins, O. C., Eriksen, K.
Manama, Bahrain, 25-29 March 1979. O., Dong, C., and Pop, J: ‘Exploration Applications of
Downhole Measurement of Crude Oil Composition and
6. Reignier, P.J., and Joseph, J. A: Management of a North Fluorescence,’ paper SPE 87011 prepared for presentation
Sea Reservoir Containing Near-Critical Fluids Using New at the SPE Asia Pacific Conference on Integrated Modeling
Generation Sampling and Pressure Technology for for Asset Management held in Kuala Lumpur, Malaysia,
Wireline Formation Testers, paper SPE 25014 prepared for 29-30 March 2004.
presentation at the European Petroleum Conference held in
Cannes, France, 16-18 November 1992. 18. Elshahawi, H., Hashem, M., Dong, C., Hegeman, P.,
Mullins, O. C., Fujisawa, G., and Betancourt, S: ‘In-Situ
7. Schlumberger Educational Services: RFT Essentials of Characterization of Formation Fluid Samples – Case
Pressure Test Interpretation, Paris, France, 1981. Studies,’ paper SPE 90932 prepared for presentation at the
SPE Annual Technical Conference and Exhibition,
8. Phelps, G. D., Stewart, G., and Peden, J. M: ‘The Analysis Houston, USA, 26-29 September 2004.
of the Invaded Zone Characteristics and Their Influence on
Wireline Log and Well-Test Interpretation,’ paper SPE 19. Fujisawa, G., Betancourt, S. S., Mullins, O. C., Torgersen,
13287 prepared for presentation at the SPE Annual T., O’Keefe, M., Terabayshi, T., Dong, C., and Eriksen, K.
Technical Conference and Exhibition, Houston, USA, 16- O: ‘Large Compositional Gradient Revealed by In-Situ
19 September 1984. Optical Spectroscopy,’ paper SPE 89704 prepared for
presentation at the SPE Annual Technical Conference and
9. Elshahawi, H., Fathy, K., and Heikal, S: ‘Capillary Pressure Exhibition, Houston, USA, 26-29 September 2004.
and Rock Wettability Effects on Wireline Formation Tester
Measurements,’ paper SPE 56712 prepared for presentation 20. Venkataramanan, L., Weinheber, P., Mullins, O. C., Ballard
at the SPE Annual Technical Conference and Exhibition, Andrews, A., and Gustavason, G: ‘Pressure Gradients and
held in Houston, USA, 3-6 October 1999. Fluid Analysis As An Aid to Determining Reservoir
Compartmentalization,’ Transactions of the 47th Annual
10. Montel, F., Bickert, J., Hy-Billiot, J., and Royer, M: SPWLA Logging Symposium 2006.
‘Pressure and Compositional Gradients in Reservoirs,’
paper SPE 85668 prepared for presentation at the 27th
SPE 102571 5
3.0
2.5
Heavy Oil Water
OD (pathlength = 2mm)
2.0
Black Oil
1.5
Volatile Oil
1.0
Condensate
0.5
0.0
500 1000 1500 2000 2500
Wavelength (nm)
Figure 1: Absorption spectra of crude oils, hydrocarbon gases, and water display distinctive features, which
enable the computation of composition, gas-oil-ratio (GOR), contamination and water fraction.
6 SPE 102571
Middle Gharif
Lower Gharif
GOR 49.2 m3/m3
3 C1 3.6%, C2-C5 1.6%,
C6+ 94.8%
2
Al Khlata
Figure 2: Example Well A - Composite display of openhole logs, formation pressure measurements, and downhole fluid
analysis (DFA) station data. The downhole fluid analysis stations are labelled 1 to 6. The coloured histogram bars in each track
reflect indicate fluid type fractions, and measurements in weight percent for four group compositions (C1, C2-C5, C6+ and CO2).
Gas-oil-ratio (GOR) is also displayed for comparison.
SPE 102571 7
Upper Gharif
Middle Gharif 6
5 Gas
Lower Gharif
Gas
2
Figure 3: Example Well B - Composite display of openhole logs, formation pressure measurements, and downhole fluid
analysis (DFA) stations against measured depth. The downhole fluid analysis stations are labelled 1 to 6, with fluid type and
oil GOR values shown for comparison.
8 SPE 102571
A B
C D
1 1
0.9 0.9
0.8 0.8
LFA Oil Fraction and CFA Mass Fractions
0.7 0.7
0.6 0.6
CFA Fluorescence
0.5 0.5
0.4 0.4
0.3 0.3
0.2 0.2
0.1 0.1
E F 0
10000 10020 10040 10060 10080 10100 10120 10140 10160 10180
0
10200
ETIM (sec)
Figure 4: Example C is optical composition fluid analyzer data from a station in example well B where a multirate drawdown
experiment was performed. [A] display of optical composition fluid analyzer data with pressure and temperature vs. elapsed time, [B]
fluid composition, phase and GOR values prior to multirate drawdown test, [C] phase segregation and slugging behaviour on outlet
side of the pump due to the presence of free gas, [D] fluorescence intensity response measurements (FLD0 and FLDR), [E] schematic
of showing phase segregation and detection downstream of the pump; and [F] expanded scale plot showing the segregation of mass
fractions and the slugging behaviour of fluorescence (FLD0 – red line and FLDR – black line).