MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : Technip FMC TC No. : EC0442 Date : 24.08.2022

Invoice No.: WIF/EX/22-23/ Date :
P.O. No.: 4500639058 Line Item: 00010 PO Date : 21.04.2022 Spec. Ref.: M25070 Rev. : F (16.07.2021)

Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. PSL Level Ratio Sr.No. Mill
DETACHABLE NUT F/
1433 3245916 Rev R 33.40 : 1 125 Nos. AISI 4140 BF-EAF-LRF-VD-CCP
FORGING UNION 4 FIG NQT/SB
1502 - TATA Steel Long Products Ltd.
Heat Code: MMO DU500001419 Rev G
CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Mo Grain Size
C67346 0.40 0.93 0.27 0.006 0.013 1.05 0.22 7.5
Specn. Min. 0.38 0.75 0.15 - - 0.80 0.15 6
Max. 0.43 1.00 0.35 0.025 0.025 1.10 0.25 -
HEAT TREATMENT
Procedure :- Q00025 Rev S
Side Thermocouples in the Working Zone ( Method
Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:-
A)
HT Batch No. of N:- AE-527 HT Batch No. of Q&T:- AE-530 Qty :- 125 Nos.
Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. 1st Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs.
QTC 33.40 : 1 900⁰C 3.20 870⁰C 3.20 OIL 30°C 53°C 570°C 5 (Air Cool)
Forging 33.40 : 1 900⁰C 3.20 870⁰C 3.20 OIL 30°C 53°C 570°C 5 (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 540⁰C
Max. 925⁰C 900⁰C --- 80⁰C 700⁰C
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Refer annexure for testing details

Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch
Test Piece Size :- 8.75 mm Dia, 35 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) Dimensional Report

Note :- We hereby guarantee no weld repairs performed.

. We hereby certify that the above figures are correct as contained in the records of the company
For Heat Treatment batch traceability point, "A" stamped near to Heat code. Letter 'A' denotes the heat treatment batch number AE-530
Above material meets the requirements of ASTM A788-22

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorized Signatory

F-MQC-10 / Rev. 00 / 01-Apr-2016

Works & Registered Office Tel : +91-02137-679819

Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) customerservice@westernindiaforgings.com
www.westernindiaforgings.com CIN : U28910PN1981PTC024155
 HARDNESS TEST REPORT

Customer:- Technip FMC TC No: EC0442

P.O. No.:- 4500639058 Line Item: 00010 PO Date : 21.04.2022 Date : 24.08.2022
DETACHABLE NUT FORGING UNION 4
Item : Material : AISI 4140
FIG 1502
Part No.: 3245916 Rev R Heat No. : C67346
Drawing No.: DU500001419 Rev G Ambient Temp : 30°C
Die No.: 1433 Hardness Range:- 277-331 HBW
Qty.: 125 Nos. Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Brinell Hardness Tester
HT Load No.: N: AE-527 QT: AE-530 Sr No. 2017/09
Reference Standard: ASTM E10 Machine Make: Fine Spavy Associates
Load Applied: 3000 Kgs Calibration Agency: MM Engineers
Type of Penetrator: Dia 10 mm Carbide Ball Certificate No.: MME/CAL/072/22-23
Std Block Details: SH-0314/22 (Hardness value -295.8 HBW) Calibrated On: 14.02.2022
Entity Performing Test: WIF Sanaswadi Calibration Due On:13.08.2022
Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 04, 05 & 06.07.2022
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.

QTY. Hardness in HBW Sr. No. Hardness in HBW Sr. No. Hardness in HBW Sr. No. Hardness in HBW
125 Nos. 285 - 321 HBW

Test Performed By Reviewed By Approved By :

Atul Jedhe Satish Gadgil (Sr.Manager HT) Ajay Joshi (HEAD-MQC, HT & NDT)

F-HT-10 / Rev. 00 / 01-Apr-2016

 MAGNETIC PARTICLE EXAMINATION REPORT

Customer : Technip FMC

PO No. : 4500639058 Line Item : 00010 Report No : EC0442 Date : 24.08.2022

PO Date : 21.04.2022 Test Date : 09 to 10.07.2022

DETACHABLE NUT FORGING UNION 4 FIG

Description : Die No. : 1433 Heat Code MMO
1502

Part No. : 3245916 Rev R Qty. : 125 Nos.

Material : AISI 4140 Sr. No. : -

Heat No. : C67346 Heat Load No : N AE-527 QT AE-530

Drg. No. : DU500001419 Rev G Stage of Examination Forged, Normalized, Quenched & Tempered, Shot Blasted

Standard : Q00207 Rev D , ASTM E709-2021 Ed. Acceptance Criteria API 6A Cl no: 10.4.2.10.3 PSL 3

Magnetic Particle Equipment - AC / FWDC : Make: Vector NDT Technologies Model : V6000C

Calibration Date: 01.07.2022 : Calibration Due Date: 31.01.2023

Machine Sr. No : 30040419

Bath Temp.
Bath Concentration - 0.1 to 0.4 ml / 100 ml Bath : 0.30 ml/ 100 ml Bath 48°C Max Observed 32°C
Required:
UV-A Lamp irradiance Intensity - 1000 µWatt / cm² Minimum : 2800µWatt / cm² Make: NDT Consultant (UK) Sr no: 2137
(UV-A + LUX Meter) Calibrated on:
Ambient Visible illumination Intensity - 21.5 LUX Max. : 01 LUX 10.01.2022 Due on: 10.07.2022
Type Of Magnetic Particle Material : Wet fluroscent

Magnetic Particle Used : MG 410 Magnaflux Make Batch no: 22E24 May-22
Bath Medium : LTM 105 Carrier oil Batch no: VO4P0151 Apr-22
Surface Temp.
Surface Condition : As Shot Blasted 48°C Max Observed 29°C
Required:
Area to be examined : 100 % of accessible Surfaces

Magnetizing Process / Method : Wet Continuous Method

Means Of Establishing Magnetization : Internal Conductor (Dia 50 x 600 mm L) + Longitudinal on FWDC Mode
: 52 Gauss - Digital Hall Effect Probe Sr no:6050 Make: NDT Consultant (UK)
Observed Field Strength (Tangential)
Calibrated on:10.01.2022 Due on: 10.07.2022

Magnetization Field : Circular + Longitudinal MT Technique Sheet - MT/TS/234

Applied Current : Circular : 2800 Amp , Longitudinal : 2000 AMP

Sensitivity ensured By : Ketos Ring & QQI SHIMS CX-230

: Within (± 3 Gauss) - Make: GNAT, DRFI Digital Gauss Meter

Residual field ensured after Demagnetization
Sr no:218001 Calibrated on: 08.03.2022 Due on: 08.09.2022

Result : No Linear or rounded indication observed.

Remark : Material is accepted

Examined By Reviewed & Accepted By

Sign Sign
Name : Anil Thorat Name : Hemant Takawale
WIFPL NDT Level II UT,MT,PT,VT.
WIFPL NDT Level II MT - As per SNT-TC-1A
As per SNT-TC-1A
Doc. No:- F-NDT-03 Rev-02 /09-July- 2018
 Certificate of Compliance
Customer : Technip FMC TC No.: EC0442
Date: 24.08.2022
Die No. : 1433 Heat Code : MMO
PO No : 4500639058 Line Item No : 00010
Offer Qty. : 125 Nos.
Part No/ Rev : 3245916 Rev R Drg No / Rev : DU500001419 Rev G
Part Name : DETACHABLE NUT FORGING Serial No. : -
UNION 4 FIG 1502

I. Material
A. Material Type : AISI 4140
B. Material Spec/ Rev. : As per Spec no : M25070 Rev No. F (16.07.2021)
C. Material Test Report No : Mill Heat No : C67346

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 8 Nos

III. Secondary Process : Heat Treatment

A. Process Name : Normalised
Heat Lot No. : AE-527 Process Spec : Q00025 Rev S

B. Process Name : QT
Heat Lot No. : AE-530 Process Spec : Q00025 Rev S

IV. NDE
A. Process Name : MPI
Q00207 Rev D ,
Certificate No : EC0442 Process Spec :
ASTM E709-2021 Ed.

A. Process Name : UT
Certificate No : NA Process Spec : NA

This is certified that subjected material is manufactured from material mentioned above &
verified by us as per written sample size & found conforming to requirements.
For Heat Treatment batch traceability point, "A" stamped near to Heat code. Letter 'A' denotes the heat
treatment batch number AE-530
Above material meets the requirements of ASTM A788-22

Sign with Stamp

Ajay Joshi (HEAD-MQC, HT & NDT)

 Mechanical Test Annexure
Die No.: 1433 Material Grade: AISI 4140

Heat No.: C67346 HT Lot No. : AE-530

Heat Code: MMO TC No.: EC0442

TENSILE TEST
UTS YS Elg RA
QTC Test QTC Hardness after
Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW
KSI KSI % %

L 311, 311 Ambient D-22-914-P 1 152.16 136.91 17.97 57.84

0.5" Below
HT Surface
277-331 Spec. Min. 120.00 100.00 16.00 35.00

IMPACT TEST
QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
52 64 46 54.00
Single - 32 J Min
L LE - 0.50 mm Min 0.62 0.75 0.57 0.65

%Shear - Report 45 55 40 46.67

-29°C
Avg. - 28 J Min
54 58 54 55.33
Single - 18.7 J Min
T LE - Report 0.64 0.70 0.65 0.66

0.5" Below %Shear - Report 45 50 45 46.67

Avg. - 27 J Min
D-22-914-P 1
HT Surface 40 44 44 42.67
Single - 20 J Min
L LE - Report 0.56 0.60 0.61 0.59

%Shear - Report 30 35 35 33.33

-40°C
Avg. - 20 J Min
54 42 48 48.00
Single - 13.5 J Min
T LE - Report 0.66 0.54 0.60 0.60

%Shear - Report 45 35 40 40.00

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory
 Mechanical Test Annexure
Die No.: 1433 Material Grade: AISI 4140

Heat No.: C67346 HT Lot No. : AE-530

Heat Code: MMO TC No.: EC0442

TENSILE TEST
UTS YS Elg RA
QTC Test QTC Hardness after
Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW
KSI KSI % %

L 311, 311 Ambient D-22-914-P 2 153.09 136.90 20.03 61.42

0.5" Below
HT Surface
277-331 Spec. Min. 120.00 100.00 16.00 35.00

IMPACT TEST
QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
66 74 70 70.00
Single - 32 J Min
L LE - 0.50 mm Min 0.80 0.91 0.86 0.86

%Shear - Report 55 60 60 58.33

-29°C
Avg. - 28 J Min
58 52 58 56.00
Single - 18.7 J Min
T LE - Report 0.76 0.70 0.75 0.74

0.5" Below %Shear - Report 50 45 50 48.33

Avg. - 27 J Min
D-22-914-P 2
HT Surface 46 32 46 41.33
Single - 20 J Min
L LE - Report 0.60 0.46 0.60 0.55

%Shear - Report 40 25 40 35.00

-40°C
Avg. - 20 J Min
46 28 46 40.00
Single - 13.5 J Min
T LE - Report 0.60 0.41 0.61 0.54

%Shear - Report 40 20 40 33.33

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory