MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : TechnipFMC TC No. : EC0251 Date : 11.06.2022

Invoice No.: WIF/EX/22-23/ Date :
P.O. No.: 4500608712 Line Item: 0010 PO Date : 08.04.2022 Spec. Ref.: M25124 Rev. : A

Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. PSL Level Ratio Sr.No. Mill
TOP ENTRY BODY FORGING, F/ AISI 4340
1485 P565885 Rev C 5.02 : 1 100 Nos. BF-EOF-LRF-VD-CCM
CHECK VALVE, MAX TOP ENTRY, NQDT / SB
3 15000 CWP AISI 4340 ALLOY
STEEL SPEC M25124 - JSW STEEL LTD

Heat Code: MGL DU500049322 Rev B

CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Ni Mo Sn As Sb

F05376 0.40 0.73 0.25 0.006 0.010 0.86 1.77 0.26 0.004 0.002 0.001
Specn. Min. 0.38 0.65 0.15 - - 0.70 1.65 0.20 - - -
Max. 0.43 0.85 0.35 0.025 0.025 0.90 2.00 0.30 - - -
Grain Size (6 OR Finer) : 7 ASTM
HEAT TREATMENT
Procedure :- Q00025 Rev S

Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)

HT Load No. of N :- AE-287 HT Load No. of QT :- AE-288 HT Load No. of DT :- AE-289-B Qty :- 100 Nos.
Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. I Temper Time II Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs. Temp. Hrs.
QTC 5.02 : 1 900⁰C 5.00 870⁰C 5.00 OIL 31°C 64°C 585°C 7½ (Air Cool) 555°C 7½ (Air Cool)
Forging 5.02 : 1 900⁰C 5.00 870⁰C 5.00 OIL 31°C 64°C 585°C 7½ (Air Cool) 555°C 7½ (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 580⁰C --
Max. 925⁰C 900⁰C -- 80⁰C 680⁰C --
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch

Test Piece Size :- 12.50 mm Dia, 50 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) Mechanical Test Annexure 4) Dimensional Report

Note :- We hereby guarantee no weld repairs performed.

. We hereby certify that the above figures are correct as contained in the records of the company
Macrostructure - C2R2S2
Inclusion Rating -
Type A - Thin A - Thick B - Thin B - Thick C - Thin C - Thick D - Thin D - Thick
Actual 1.00 0.50 - - - - 1.0 0.5
Spec. Min - - - - - - - -
Spec. Max 2.00 1.50 2.00 1.00 1.00 1.00 1.50 1.00

Ajay Joshi (GM, MQC & HT)

Authorised Signatory
F-MQC-10 / Rev. 00 / 01-Apr-2016

Works & Registered Office Tel : +91-02137-679819

Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) customerservice@westernindiaforgings.com
www.westernindiaforgings.com CIN : U28910PN1981PTC024155
 HARDNESS TEST REPORT

Customer:- TechnipFMC TC No: EC0251

P.O. No.:- 4500608712 Line Item: 0010 PO Date : 08.04.2022 Date : 11.06.2022
TOP ENTRY BODY FORGING, CHECK
Item : VALVE, MAX TOP ENTRY, 3 15000 CWP Material : AISI 4340 EC0191
AISI 4340 ALLOY STEEL SPEC M25124
Part No.: P565885 Rev C Heat No. : F05376
Drawing No.: DU500049322 Rev B Ambient Temp : 30°C
Die No.: 1485 Hardness Range:- 285-341 HBW
Qty.: 100 Nos. Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Deep Throat Hardness Tester
HT Load No.: N AE-287 QT AE-288 Sr No. 2015/01
Reference Standard: ASTM E10 Machine Make: FSA
Load Applied: 3000 Kgs Calibration Agency: SME Cal. Center
Type of Penetrator: Dia 10 mm Carbide Ball Certificate No.: SME/22/183
Std Block Details: SH-0001/22 (Hardness value - 300.4 HBW) Calibrated On: 14.01.2022
Entity Performing Test: WIF Sanaswadi Calibration Due On: 13.01.2023
Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 23 & 24.05.2022
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.

Sr. No. Hardness in HBW

100 Nos. 285-321 HBW

Test Performed By Reviewed By Approved By :

Atul Jedhe Satish Gadgil (Sr.Manager HT) Ajay Joshi (GM, MQC & HT)
F-HT-10 / Rev. 00 / 01-Apr-2016
 Certificate of Compliance

Customer : TechnipFMC TC No.: EC0251

Date: 11.06.2022
Die No. : 1485 Heat Code : MGL
PO No : 4500608712 Line Item No : 0010
Offer Qty. : 100 Nos.
Part No/ Rev : P565885 Rev C Drg No / Rev : DU500049322 Rev B
Part Name : TOP ENTRY BODY FORGING, Serial No. : -
CHECK VALVE, MAX TOP ENTRY, 3
15000 CWP AISI 4340 ALLOY STEEL
SPEC M25124

I. Material
A. Material Type : AISI 4340
B. Material Spec/ Rev. : As per Spec no : M25124 Rev No. A
C. Material Test Report No : Mill Heat No : F05376

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 8 Nos

III. Secondary Process : Heat Treatment

A. Process Name : Normalised
Heat Lot No. : AE-287 Process Spec : Q00025 Rev S

B. Process Name : QT DT
Heat Lot No. : AE-288 AE-289-B Process Spec : Q00025 Rev S

IV. NDE
A. Process Name : MPI

Certificate No : NA Process Spec : NA

A. Process Name : UT

Certificate No : NA Process Spec : NA

This is certified that subjected material is manufactured from material mentioned above &
verified by us as per written sample size & found conforming to requirements.

Sign with Stamp

Ajay Joshi (GM, MQC & HT)

 Mechanical Test Annexure
Die No.: 1485 Material Grade: AISI 4340

Heat No.: F05376 HT Lot No. : AE-288

Heat Code: MGL

TENSILE TEST
UTS YS Elg RA
QTC Test QTC Hardness after
Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW
PSI PSI % %

L C-22-55-P 138664 118189 21.10 63.85

0.5" Below HT
321 , 321 Ambient 2
Surface
T C-22-56-P 138556 119960 22.44 64.27

285-341 Spec. Min. 130000.00 110000.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
76 84 100 86.67
Single - 32 J Min
L LE - 0.38 mm Min C-22-55-P 1.05 1.18 1.35 1.19

%Shear - Report 60 65 65 63.33

0.5" Below HT
-40°C 2
Surface Avg. - 28 J Min
72 74 90 78.67
Single - 18.7 J Min
T LE - Report C-22-56-P 1.06 1.08 1.30 1.15

%Shear - Report 60 60 65 61.67

Ajay Joshi (GM, MQC & HT)

Authorised Signatory
 Mechanical Test Annexure
Die No.: 1485 Material Grade: AISI 4340

Heat No.: F05376 HT Lot No. : AE-288

Heat Code: MGL

TENSILE TEST
UTS YS Elg RA
QTC Test QTC Hardness after
Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW
PSI PSI % %

L C-22-57-P 137822 116608 21.00 60.85

0.5" Below HT
321 , 321 Ambient 3
Surface
T C-22-58-P 139880 120735 20.40 64.69

285-341 Spec. Min. 130000.00 110000.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
90 80 78 82.67
Single - 32 J Min
L LE - 0.38 mm Min C-22-57-P 1.25 1.12 1.09 1.15

%Shear - Report 65 60 60 61.67

0.5" Below HT
-40°C 3
Surface Avg. - 28 J Min
72 90 90 84.00
Single - 18.7 J Min
T LE - Report C-22-58-P 1.05 1.25 1.27 1.19

%Shear - Report 60 65 65 63.33

Ajay Joshi (GM, MQC & HT)

Authorised Signatory
 Mechanical Test Annexure
Die No.: 1485 Material Grade: AISI 4340

Heat No.: F05376 HT Lot No. : AE-288

Heat Code: MGL

TENSILE TEST
UTS YS Elg RA
QTC Test QTC Hardness after
Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW
PSI PSI % %

L C-22-59-P 133552 112305 20.42 60.42

0.5" Below HT
321 , 321 Ambient 4
Surface
T C-22-60-P 135732 115874 20.60 62.61

285-341 Spec. Min. 130000.00 110000.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
68 68 80 72.00
Single - 32 J Min
L LE - 0.38 mm Min C-22-59-P 0.85 0.86 1.00 0.90

%Shear - Report 60 60 65 61.67

0.5" Below HT
-40°C 4
Surface Avg. - 28 J Min
76 76 72 74.67
Single - 18.7 J Min
T LE - Report C-22-60-P 0.97 0.98 0.90 0.95

%Shear - Report 60 60 60 60.00

Ajay Joshi (GM, MQC & HT)

Authorised Signatory