MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : TechnipFMC TC No. : E8550 Date : 07.11.2021

Invoice No.: WIF/EX/21-22/ Date :
P.O. No.: 4500544691 Line Item: 10 PO Date : 01.07.2021 Spec. Ref.: M25070 Rev. : F (Date:16.07.2021)

Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. 502 PSL Level Ratio Sr.No. Mill
BODY FORGING, ULT F/
1299 PLUG VALVE 1 ULT150 F/3 3257105 Rev K 17.68 800 Nos. AISI 4140 BF-EOF-LRF-VD-CCM
NQT/SB
IN UNION ENDS AISI 4140
- JSW STEEL LIMITED
Heat Code: LHK DU500001271 Rev B
CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Mo Grain Size
F00913 0.40 0.91 0.21 0.009 0.01 1.06 0.22 7.0
Specn. Min. 0.38 0.75 0.15 - - 0.80 0.15 6
Max. 0.43 1.00 0.35 0.025 0.025 1.10 0.25 -
HEAT TREATMENT
Procedure :- Q00025 Rev Q

Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)

HT Load No. of N :- AD-285 HT Batch No. of Q&T:- AD-288 Qty :- 800 Nos.
Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. 1st Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs.
QTC 17.68 900⁰C 3.20 870⁰C 3.20 OIL 36°C 49°C 570°C 5 (Air Cool)
Forging 17.68 900⁰C 3.20 870⁰C 3.20 OIL 36°C 49°C 570°C 5 (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 540⁰C
Max. 925⁰C 900⁰C --- 80⁰C 700⁰C
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Refer annexure for testing details

Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch
Test Piece Size :- 8.75 mm Dia, 35 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) Dimensional Report 4) Testing Annexure

Note :- We hereby guarantee no weld repairs performed.
. We hereby certify that the above figures are correct as contained in the records of the company
For Heat Treatment batch traceability point, "AD-288" stamped near to Heat code.

Mr. Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory
F-MQC-10 / Rev. 00 / 01-Apr-2016
 HARDNESS TEST REPORT

Customer:- TechnipFMC TC No: E8550

P.O. No.:- 4500544691 Line Item: 10 PO Date : 01.07.2021 Date : 07.11.2021
BODY FORGING, ULT PLUG VALVE 1 ULT150 F/3
Item : IN UNION ENDS AISI 4140 Material : AISI 4140

Part No.: 3257105 Rev K Heat No. : F00913

Drawing No.: DU500001271 Rev B Ambient Temp : 28°C
Die No.: 1299 Hardness Range:- 277 - 331 HBW
Qty.: 800 Nos. Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Brinell Hardness Tester
HT Load No.: N: AD-285 QT: AD-288 Sr No.19/05/007
Reference Standard: ASTM E10 Machine Make: SAROJ
Load Applied: 3000 Kgs Calibration Agency: MM Engineers
Type of Penetrator: Dia 10 mm Carbide Ball Certificate No.: MME/CAL/261/21-22
Std Block Details: SH-266 (Hardness value - 295.0 HBW) Calibrated On: 14.08.2021
Entity Performing Test: WIF Sanaswadi Calibrated Due On:13.02.2022
Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 23.10.2021
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.
Qty. Hardness in HBW
800 Nos. 285-321 HBW

Test Performed By Reviewed By Approved By :

Atul Jedhe Satish Gadgil (Sr.Manager HT) Mr. Ajay Joshi (HEAD-MQC, HT & NDT)
F-HT-10 / Rev. 00 / 01-Apr-2016 Page 1
 Mechanical Test Annexure
Die No.: 1299 Material Grade: AISI 4140
Heat No.: F00913 HT Lot No. : AD-288
Heat Code: LHK TC No. : E8550

TENSILE TEST

QTC Test QTC Hardness after UTS YS Elg RA

Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW KSI KSI % %

0.5" below
L 302, 311 Ambient G/21/2485/P 1 148.07 125.97 20.09 62.60
HT Surface

277 - 331 Spec. Min. 120.00 100.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
88 74 78 80.00
Single - 32 J Min
LE - 0.51 mm Min -29°C 1.02 0.86 0.91 0.93
%Shear - Report 65 60 60 61.67
L Avg. - 27 J Min
38 40 42 40.00
Single - 20 J Min
LE - Report -40°C 0.51 0.53 0.55 0.53

%Shear - Report 25 30 30 28.33

0.5" below
Avg. - 28 J Min 1
HT Surface 72 80 48 66.67
Single - 18.7 J Min
-29°C
LE - Report 0.85 0.93 0.60 0.79
%Shear - Report 60 60 35 51.67
T
Avg. - 20 J Min
36 30 38 34.67
Single - 14 J Min
LE - Report -40°C 0.48 0.41 0.51 0.47

%Shear - Report 25 20 25 23.33

Mr. Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory
 Certificate of Compliance

Customer : TechnipFMC TC No.: E8550

Date: 07.11.2021
Die No. : 1299 Heat Code : LHK
PO No : 4500544691 Line Item No : 10
Offer Qty. : 800 Nos.
Part No/ Rev : 3257105 Rev K Drg No / Rev : DU500001271 Rev B
BODY FORGING, ULT PLUG VALVE
Part Name : Serial No. : -
1 ULT150 F/3 IN UNION ENDS AISI
4140

I. Material
A. Material Type : AISI 4140
B. Material Spec/ Rev. : As per Spec no : M25070 Rev No. F (Date:16.07.2021)
C. Material Test Report No : Mill Heat No : F00913

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 8 Nos.

III. Secondary Process : Heat Treatment

A. Process Name : Normalised
Heat Lot No. : AD-285 Process Spec : Q00025 Rev Q

B. Process Name : QT
Heat Lot No. : AD-288 Process Spec : Q00025 Rev Q

IV. NDE
A. Process Name : MPI

Certificate No : NA Process Spec : NA

B. Process Name : UT
Certificate No : NA Process Spec : NA

This is certified that subjected material is manufactured from material mentioned above &
verified by us as per written sample size & found conforming to requirements.
For Heat Treatment batch traceability point, "AD-288" stamped near to Heat code.

Sign with Stamp

Mr. Ajay Joshi (HEAD-MQC, HT & NDT)