MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : TechnipFMC TC No. : EC2169 Date : 18.12.2023

Invoice No.:WIF/EX/23-24/ Date :
P.O. No.: 4500796359 Line Item: 00010 PO Date : 13.12.2023 Spec. Ref.: M25124 Rev. : A
Ver. No : 3
Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. PSL Level Ratio Sr.No. Mill
TOP ENTRY BODY FORGING, Forged AISI 4340
1485 P565885 Rev E 11.61 : 1 226 Nos. EAF-LRF-VD-ING
CHECK VALVE, MAX TOP Normalized
ENTRY, 3 15000 CWP AISI 4340 Quenched &
ALLOY STEEL SPEC M25124 Double - SAARLOHA
Tempered,
Heat Code: OTB DU500049322 Rev D Shot Blasted

CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Ni Mo Sn As Sb

HN170537 0.42 0.73 0.24 0.002 0.008 0.83 1.75 0.25 0.0070 0.0026 0.0014
Specn. Min. 0.38 0.65 0.15 - - 0.70 1.65 0.20 - - -
Max. 0.43 0.85 0.35 0.015 0.015 0.90 2.00 0.30 - - -
Grain Size (6 OR Finer) : 7 ASTM
HEAT TREATMENT
Procedure :- Q00025 Rev S

Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)

HT Load No. of N :- CZ-28 HT Load No. of QT :- CZ-52 HT Load No. of DT :- CZ-53-B Qty :- 226 Nos.
Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. I Temper Time II Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs. Temp. Hrs.
7 Hrs 7 Hrs
QTC 11.61 : 1 900⁰C 4 Hrs 40 Min 870⁰C 4 Hrs 40 Min OIL 27°C 58°C 590°C 570°C (Air Cool)
(Air Cool)
7 Hrs 7 Hrs
Forging 11.61 : 1 900⁰C 4 Hrs 40 Min 870⁰C 4 Hrs 40 Min OIL 27°C 58°C 590°C 570°C (Air Cool)
(Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 580⁰C --
Max. 925⁰C 900⁰C -- 80⁰C 680⁰C --
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch

Test Piece Size :- 12.50 mm Dia, 50 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) Mechanical Test Annexure 4) Dimensional Report

Note :- We hereby guarantee that no weld repairs have been performed.

. We hereby certify that the above figures are accurate and are contained in the records of the company.
Method of Forging - Closed Die Forging
Inclusion Rating -
Type A - Thin A - Thick B - Thin B - Thick C - Thin C - Thick D - Thin D - Thick
Actual 1.00 0.50 0.5 - - - 1.0 0.5
Spec. Min - - - - - - - -
Spec. Max 2.00 1.50 2.00 1.00 1.00 1.00 1.50 1.00

Ajay Joshi (GM, MQC & HT)

Authorised Signatory
F-MQC-10 / Rev. 00 / 01-Apr-2016

Works & Registered Office Tel : +91-02137-679819

Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) customerservice@westernindiaforgings.com
www.westernindiaforgings.com CIN : U28910PN1981PTC024155
 HARDNESS TEST REPORT

Customer:- TechnipFMC TC No: EC2169

P.O. No.:- 4500796359 Line Item: 00010 PO Date : 13.12.2023 Date : 18.12.2023
TOP ENTRY BODY FORGING, CHECK
Item : VALVE, MAX TOP ENTRY, 3 15000 CWP Material : AISI 4340
AISI 4340 ALLOY STEEL SPEC M25124
Part No.: P565885 Rev E Heat No. : HN170537
Drawing No.: DU500049322 Rev D Ambient Temp : 26°C
Die No.: 1485 Hardness Range:- 285-341 HBW
Qty.: 226 Nos. Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Deep Throat Hardness Tester
HT Load No.: N CZ-28 QT CZ-52 Sr No. 2015/01
Reference Standard: ASTM E10 DT CZ-53-B Machine Make: FSA
Load Applied: 3000 Kgs Calibration Agency: SME Cal. Center
Type of Penetrator: Dia 10 mm Carbide Ball Certificate No.: SME/23/200

Std Block Details: SH-0098/23 (Hardness value - 304.8 HBW) Calibrated On: 13.01.2023

Entity Performing Test: WIF Sanaswadi Calibration Due On: 12.01.2024

Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 01 & 02.12.2023
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.

Sr. No. Hardness in HBW

226 Nos. 285-321 HBW

Test Performed By Reviewed By Approved By :

Atul Jedhe Satish Gadgil (Sr.Manager HT) Ajay Joshi (GM, MQC & HT)
F-HT-10 / Rev. 00 / 01-Apr-2016
 CERTIFICATE OF COMPLIANCE
Customer : TechnipFMC TC No.: EC2169
Date: 18.12.2023
Die No. : 1485 Heat Code : OTB
PO No : 4500796359 Line Item No : 00010
Offer Qty. : 226 Nos.
Part No/ Rev : P565885 Rev E Drg No / Rev : DU500049322 Rev D
Part Name : TOP ENTRY BODY FORGING, Serial No. : -
CHECK VALVE, MAX TOP ENTRY, 3
15000 CWP AISI 4340 ALLOY STEEL
SPEC M25124
I. Material
A. Material Type : AISI 4340
B. Material Spec/ Rev. : As per Spec no : M25124 Rev No. A
C. Material Test Report No : Mill Heat No : HN170537

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 08 Nos
III. Secondary Process : Heat Treatment
A. Process Name : Normalised
Heat Lot No. : CZ-28 Process Spec : Q00025 Rev S
B. Process Name : QT DT
Heat Lot No. : CZ-52 CZ-53-B Process Spec : Q00025 Rev S

IV. NDE
A. Process Name : MPI
Certificate No : NA Process Spec : NA

A. Process Name : UT
Certificate No : NA Process Spec : NA

This certifies that the subjected material is manufactured from the material mentioned above. It has
been verified by us according to the specified sample size and found to conform to the requirements.
Method of Forging - Closed Die Forging

Sign with Stamp

Ajay Joshi (GM, MQC & HT)

 Mechanical Test Annexure
Die No.: 1485 Material Grade: AISI 4340

Heat No.: HN170537 HT Lot No. : CZ-52

Heat Code: OTB TC No. : EC2169

TENSILE TEST
UTS YS Elg RA
QTC Test QTC Hardness after
Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW
PSI PSI % %

L I-23-433-P 154412 139087 19.64 56.61

0.5" Below HT
331, 321 Ambient 1
Surface
T I-23-434-P 152032 136199 18.80 52.86

285-341 Spec. Min. 130000.00 110000.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
92 94 96 94.00
Single - 32 J Min
L LE - 0.38 mm Min I-23-435-P 1.08 1.10 1.13 1.10

%Shear - Report 65 65 65 65.00

0.5" Below HT
-40°C 1
Surface Avg. - 28 J Min
86 84 84 84.67
Single - 18.7 J Min
T LE - Report I-23-436-P 1.03 1.00 1.01 1.01

%Shear - Report 65 65 65 65.00

Ajay Joshi (GM, MQC & HT)

Authorised Signatory