Tadi arte, Min main real vate - As o ) yh Cf) A ws _O ~ ng ; Lone oO ee errs Rea Emin) Rn) My. Veps (5) 206) Uo -) oF om ( Masny ee oe GB abd a ols Le (Sen) oO TEs WG _O@ ( Prch Tone) Glalation of Maximum Savert vate (Ss Hax) AC) UK 6) Bre _O fea, ROGPR ahen Fe) Vey (Ban 3 a3 @ Os ce (Sena) io eS Sa c F Haan . x yaar Frans 9 SR c \ tS 2)CH 321: Separation Processes: Lets Problem Sheet 9 re WO LAN A chemical plant provides 10,000 tbm/hr of « mixture that contains 60 weight percent toluene ue 40 weight percent isopropyl alcohol, uslog pure water asa solvent. A mass of water equal to 80 percent of the weight of the feed stream to each at ce Is fed to each stage, How many stages Wil be needed to reduce the alcohol concentention in the raffinate to 8 welght percent? If all of the solvent streams are mixed (ogether, what fs the ale concentration in water? librium data are as follows, Water Layer wt% Toluene Layer wt% Toluene) yy Water oor 0.00 0300) o09 0.28 on 042” 1,32 7 102 3,20 1.25 5.03 1.46 7.90 37.40) 59.64 2.96 opr isa 88.75 433 15.08 52.32 558 1745 48.78 7.09 21.84 46.80 847 ass 46.50 44.00 950” 25.24 ) Calculate the number of theoretical stages required to extract acetone from 5,000 kg/hr of a binary mixture of 35 weight percent acetone and 65 weight percent ‘methyl isobutyl ketone in a ountereurrent liquid-liquid extraction column at 25%, The solvent is water containing 3 weight percent keton, The concentration of acetone inthe rafioate stream leaving the eolume ig be2 weight percent, The ratio of the actual solvent rate to the minimum is 1.7, ‘Alexandria University Faculty of Engineering ‘The Department of Chemical EngineeringFall 2015 ¥ 0321: Separation Processes-1 ” a Q. A liquid-liquid ternary phase diagram for isopropyl alcohol(IPA),Toulene and water at 25°C 's shown Feed flow rate is 100 Ke/hr,and feed composition is 40 w% IPA and 60 wi% toluene.Fresh solvent is pure water at 2 flow rate of 100 ke/hr.Determine the number of cauitibrium stages required to produce a raffinate stream that contains 2.5 wt% IPA. QD > (8) 4.50% solution of solute Ain solvent is extracted with a second solvent $ in a counter Current multiple contact extraction unit. The weight of $ is 25% that of the feed solution, and the equilibrium data are given in figure. Determine the number of ideal stages required and the weight and concentration of the first extract if the final raffinate contains 15 wi% A. {5) Acetone is to be recovered from acetone-methyl isobutyl ketone mixture ina iquid-iquid extractor using pure water as a solvent. Feed is 17,000 Ibm/hr and 40 weight percent acetone. The concentration of acetone in the raffinate Is 5 weight percent. The extractor contains sixtheoretical stages. =~ C a. How much solvent must be used? b. What is the ratio of the actual to minimum solvent flow rate? & What is the percent recovery of acetone? (6) A liquid-liquid extraction column removes ethylene slycol from water using a furfural Pat solvent.The fat solvent stream leaving the column contains 48 wt% glycol and has a ow Fate of 8800 Ke/hr. ‘The raffinate stream leaving the column has a flow rate of 10500 kg/hr and contains 2 14% glycol.The fresh solvent is pure furfural.The feed contains no furfural, a Calculate the feed composition. b- Calculate the flow rates of the feed and the fresh solvent. & Calculate the number of ideal stages in the column. yrler Clawx Problem sheet (9) SS i OF % = leoco We-| hw) -» boil (Cr) -4e + {so Pro ful aleckel Solvect Cwaler) » Sz 02% Feed TB each Saye YeQ a WW =p) > To et ny og aleokel in | Qs St we a op he ee oe | | mixed togeher » oka ig alcohol Cnty in water? (solar) @. draw che Fiyare) D. Sraw FY Yo J. alco Goes yy. eo | y : locoo 7 Eas, \oooe to -B¥ lore fou loo Alf lesbo 5 92 -/}. > Ge ie IZ (Sg ee To a \ ee 3 oe oa J 4 2 N fre —— eS Hz Me aes = s RS \.3 10 Gn dros) 1 i} Cn OEE Si} Ne ete ) 4 i Ce) 202 OFF )sng 9f STS 5 QZ STaVe Bry, GRe 2° G = sy ve, Se Ey a syle Te For Stray = eee = e S,> «24s a BF icood apiece | . Fes ee hy Ve Re ee Ry Se (18) [[peoe = Err 8) ess rR sv 4. 6. @ aaa ee E,< \So000 - Ry Wt Mak [ WeLA o\F +R Loe ; > Re Hose Tet) D> \ ts Bose Tel} 1000 (Cox lw), oy O ™ ee (oe Gus eee ———— Swetal = Gooo + 2 8¥* Bo00 =\ 4 yoo (ton) | — — Cron Oo fy s ee GN ¢\o-B Ss \Fs. = \Vo- Loe \ a ees OFS by weg hrL TL tip T cap 5a 8 eT ester py Be i. JEEE] extract clCeTone Fre, 5000 fes/f cone 9 65% HIEBK _ Sewet water 2+]. Ker se / stay 2 W) leavinsy 2 Ut Psa NF @- tex W) binary wit 356 AC County Corest Vig = Wg Kncetone ( So\ation) : Soen F 2LR F 35+. ACetwe poe ele a Perene @.dren Ne Vife From (fF) Te Ey @. 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Ses Cem Figareca) Srok = \4ooe HENS) C\5olb ee 159357 ) x to yet Wemave oe vial and) Otter Saat _——_ @ a el assume Fal = Value fo ctveen ~ Sal Vie \ineg Solve froen Ss Mares ant ve Yeack Ae Ra TE Rn % 7 gralce ew 25Sanfio Reed. acca oe Ve wal wath ve eT Sack —5@ i @ < Z A Sm Sack eS hen Yeq ein ¢ sc ~ «@® & ‘ = - ect L ReCosory of acetone = feed Pree G — AB) 2-44 Too 0 A Rav 0-05 z\e0 \ & os) = Ey Rn os eRe el > ens Sire uF Cy Roe 4 26, ORnr 7z= > es & FS FR zn 8 aes @)ater Sms a Fur fore, ©. Ug. iq yemoveg EQ From = B Goo (eo ler) Fat solvent 5 494 EG Gl? «ate Ry = \eG00 (Kk lwr) Ri 2 LEG - we Gar Fura Fed Galams ve fac Fural @. carotate Gaad Com Position @. 95 R QW ; — (solution ) ¢ : overall ‘ ) . Ss \ Gat SINR fete hol ey Gongive of G2 494 66 @ weGie GE, w Ov ag ft EG Tekh > to A. chests Ra w Ovo L6G (o5e6ta har) Qo ie ae Vue err Ey 19 sot Ry @Q- draw lice H paar Sw Me Ev Re bee, €. 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