Dr.

Babasaheb Ambedkar Technological University

Lonere - 402 103
(Diploma Wing)

Proposed Curriculum
For
II Year Diploma (Chemical branched)
(W. E. F. 2024-25)

1
 INDEX

Sr. Course Page

Course Title
No. Code No.
Semester – III
1 DCH 2101 Plant Utilities
2 DAM 2101 Applied Mechanics
3 DCH 2102 Mechanical Operation
4 DCH 2103 Technology of Inorganic Chemicals
5 DCH 2104 Industrial Stoichiometry
6 DCH 2105 Plant Utilities Lab
7 DAM 2102 Applied Mechanics Lab
8 DCH 2106 Mechanical Operation Lab
9 DCH 2107 Technology of Inorganic Chemicals Lab
Semester – IV
10 DCH 2201 Fluid Flow Operation
11 DCH 2202 Chemical Engineering Thermodynamics
12 DCH 2203 Technology of Organic Chemical
13 DCH 2204 Chemical Process Instrumentation and Control
14 DCH 2205 Chemical Industrial Safety and Maintenance
15 DCH 2206 Fluid Flow Operation Lab
16 DCH 2207 Technology of Organic Chemical Lab
17 DCH 2208 Chemical Process Instrumentation and Control Lab
18 DCH 2209 Chemical Industrial Safety and Maintenance Lab

2
 Dr. Babasaheb Ambedkar Technological University, Lonere
Proposed Learning and Assessment Scheme for Diploma Programs (W. E.F. 2024-25)
Diploma in chemical engineering
Semester – III
Sr. Course Title Course Course Total Learning Scheme Credits Assessment Scheme
No. Code Type IKS Actual Contact SL NL
Hrs Hrs./Week Hrs/ Hrs/
for CL TL LL Week Week SL FA- SA- FA- PR/ Total
Sem MSE ESE TW OR
1 Plant Utilities DCH 2101 DSC 3 3 - - 1 4 4 20 20 60 -- -- 100
2 Applied Mechanics DAM 2101 AEC 3 3 - - 1 4 4 20 20 60 -- -- 100
3 Mechanical Operation DCH 2102 DSC 3 3 - - 1 4 4 20 20 60 -- -- 100
4 Technology of Inorganic DCH 2103 DSC 3 3 - 1 4 4 20 20 60 -- --
Chemicals 100
-
5 Industrial Stoichiometry DCH 2104 AEC 3 3 - - 1 4 4 20 20 60 -- -- 100
6 Plant Utilities Lab DCH 2105 DSC - - - 2 2 2 60 40 100
-- -- --
7 Applied Mechanics Lab DAM 2102 AEC - 2 2 60 40

- - 2 -- -- -- 100

8 Mechanical Operation Lab DCH 2106 DSC 60 40

- - - 2 2 2 -- -- -- 100
9 Technology of Inorganic DCH 2107 DSC 60 40
Chemicals Lab - - - 2 2 2 -- -- -- 100
Total 15 15 00 08 05 28 28 100 100 300 240 160 900

3
Abbreviations: CL-Classroom Learning, TL-Tutorial Learning, LL-Laboratory Learning, FA-Formative Assessment, SA-
Summative Assessment, PR/OR – Practical/Oral, MSE-Mid Sem Examination, TW-Term Work, IKS- Indian Knowledge
System, NL-National Learning

*SL-Subject wise Self learning includes online course, assignments/models, case study, industry exposure/internship,
etc. (Self-Learning hours shall not be reflected in Time Table)

Course Category: DSC – Discipline Specific Course; AEC – Ability Enhancement Course; SEC – Skill Enhancement
Course; VEC – Value Education Courses, @ Internal Assessment, #-No Theory Examination

4
 Dr. Babasaheb Ambedkar Technological University, Lonere
Proposed Learning and Assessment Scheme for Diploma Programs (W. E.F. 2024-25)
Diploma in chemical engineering
Semester – IV
Sr. Course Title Course Course Total Learning Scheme Credits Assessment Scheme
No. Code Type IKS Actual Contact SL NL
Hrs for Hrs/Week Hrs/ Hrs/
Sem CL TL LL Week Week SL FA-MSE SA-ESE FA-TW PR/OR Total
1 Fluid Flow Operation DCH 2201 DSC 4 3 1 - 1 5 5 20 20 60 -- -- 100
2 Chemical Engineering DCH 2202 DSC 4 3 1 - 1 5 5 20 20 60 -- -- 100
Thermodynamics
3 Technology of Organic DCH 2203 DSC 3 3 - - 1 4 4 20 20 60 -- -- 100
Chemical
4 Chemical Process DCH 2204 DSC 3 3 1 4 4 20 20 60 -- -- 100
Instrumentation and
Control
5 Chemical Industrial Safety DCH 2205 AEC 2 2 - - - 2 2 20 20 60 -- -- 100
and Maintenance
6 Fluid Flow Operation Lab DCH 2206 AEC - - - 2 - 2 2 60 40 100
-- -- --
7 Technology of Organic DCH 2207 60 40 100
AEC - - - 2 - 2 2 -- -- --
Chemical Lab
8 Chemical Process DCH 2208 60 40 100
AEC - - - 2 - 2 2 -- -- --
Instrumentation and
Control Lab
9 Chemical Industrial Safety DCH 2209 60 40 100
AEC - - - 2 - 2 2 -- -- --
and Maintenance Lab
Total 16 14 2 08 04 28 28 100 100 300 240 160 900

5
Abbreviations: CL-Classroom Learning, TL-Tutorial Learning, LL-Laboratory Learning, FA-Formative Assessment, SA-
Summative Assessment, PR/OR – Practical/Oral, MSE-Mid Sem Examination, TW-Term Work, IKS- Indian Knowledge
System, NL-National Learning
*SL-Subject wise Self learning includes online course, assignments/models, case study, industry exposure/internship,
etc. (Self-Learning hours shall not be reflected in Time Table)

Course Category: DSC – Discipline Specific Course; AEC – Ability Enhancement Course; SEC – Skill Enhancement
Course; VEC – Value Education Course.

6
 PROPOSED
SYLLABUS OF
SEMESTER III

7
 SEMESTER III
Course Title PLANT UTILITY Course Code DCH 2101
Learning Scheme Assessment Scheme: Credits-3
Classroom Learning (CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) -- Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives: The aim of this course is to help the student to attain the following industry competency
through various teaching learning experiences.
Course Outcomes:
Course Outcomes (CO):
1. Explain the importance of water and various methods for water softening and purification
2. Classify the different types of fuels and boilers used in process industries for the generation of steam
3. Identify the different types of compressors and blowers for handling air and inert gases
4. Summarize the different types of equipment used for humidification, and dehumidification
5. Select a suitable refrigeration system for a typical application in process industries
6. Interpret the application of correct type of insulation system for control of heat losses and learn about proper
utilization of inert gases on the process plants.

Unit Contents Hrs Marks

SL FA SA
Unit-1 Water and Steam. 7 4 8 5
Requisites of Industrial Water and its uses; Water treatment methods -
ion exchange, demineralization,
membranes technology, reverse osmosis. Water resources management.
Properties of steam, Boiler
types and mountings, boiler accessories, Indian Boiler Act, 1923.Steam
distribution and utilization, steam economy, waste heat utilization

Unit-2 Industrial fuels 5 3 6 8

Solid, liquid and gaseous fuels used in chemical process industries for
power generation, Typical combustion calculations

Unit-3 Compressed Air 6 3 6 7

Types of fans, axial, reciprocating and centrifugal compressors, rotary
blowers and vacuum pumps and their performance characteristics.
Methods of vacuum development, ejectors and their limitations, materials
handling under vacuum, piping systems.

8
Unit-4 Refrigeration & Ventilation 6 2 -- 6
Principle of refrigeration, Refrigeration system like compression
refrigeration, absorption refrigeration, and chilled water system; Types of
refrigerants; Concept of cryogenics and cryogenics characteristics. Air
blending, exhaust ventilation and flaring

Unit-5 Industrial insulation and Inert Gases. 6 4 -- 16

Importance of insulation, insulation material and their effect on various
materials of equipment piping, fitting and valves, insulation for high,
intermediate, low and subzero temperatures including cryogenic insulation
Introduction, properties of inert gases & their use, sources and methods of
generation, general arrangement for inserting system; operational,
maintenance and safety aspects

Unit-6 Effluent treatment 6 4 - 18

Disposal of solid, liquid and gas wastes; pollution control measures –
compliance to statutory norms; Effluent Treatment – Case studies like
treatment of effluents from paper mills, Dye and Textile industries,
petrochemical industries, plastic and rubber industries.

Total 36 20 20 60

Sr. No Reference Books

1 A Textbook of Plant utilities, Mujawar B. A Nirali prakashan Publication,
3rd ed. India 2007.
The properties of gases and Poling B.E, Prausnitz J.M, O McGraw Hill, USA, 2008.
2
liquid, 5th ed. “Connell J.,
Chemical Engineers Perry, R.H., Green, D. W., McGraw Hill, USA, 2007.
3
Handbook, 8th ed. Perry “s
Process utility system, 3rd ed. Broughton j. Institution of chemical
4
engineers, U.K. 2004

9
 SEMESTER III
Course Title MECHANICAL Course Code DCH2102
OPERATIONS

Learning Scheme Assessment Scheme: Credits- 4

Classroom Learning CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) 0 Hrs/Week Formative Assessment (FA) 20Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60Marks
Course Objectives:
1.Introduce the basic information and the systematic diagrams of Unit operations involved in chemical industries
2. Learn the concepts of design, operation details and schematic of industrial equipment
3. Choose the right separation technology for easy separation of chemical components

Unit Contents Hrs. Marks

SL FA SA
Unit-1 Introduction to Particulate Solids and Particle Separation 5 3 6 6
Particle Shape, Size, Mixed Particle Sizes and Size Analysis – Cumulative
and Differential Analysis –Various Mean Diameters – Screen Analysis
Standard Screens – Various Industrial Screens
Introduction to Particle Separation – Electrostatic Precipitation and
Magnetic Separation - Storage of Solids

Unit-2 Size Reduction 4 4 7 7

Reduction – Principles of Comminution - Energy and Power Requirements
in Comminution - Mechanical Efficiency-Laws of Crushing-Size
Reduction Equipment – Crushers- Grinders Cutting Machines – Open and
Closed-Circuit Operation

Unit-3 Particulate Solids Flow 5 3 7 7

Motion of a Particle through a Fluid – Terminal Velocity–Free and
Hindered Settling. Classification: Separations Ratio – Classification
Equipment – Gravity Settling Tank –Elutriator – Cone Classifiers – Bowl
Classifier – Centrifugal Classifier – Cyclone Separator-Wet Scrubber

Unit-4 Hydro-Mechanical Separations 7 3 - 13

Sedimentation: Gravity Sedimentation – Mechanism – Continuous
Sedimentation – Thickener – Design of thickener – Classifier and Clarifier
– Settling Area – Centrifugal Sedimentation Centrifuges - Hydro clones.
Floatation: Equipment – Modifiers – Collectors - Frothing Agents

10
Unit-5 Filtration 7 3 - 12
Filtration– Filter Media – Filter Aids – Principles of Cake Filtration –
Constant Pressure Filtration – Constant Rate Filtration - Pressure Drop
Through Filter Cake –Compressible and Incompressible Filter Cakes -
Specific Cake Resistance - Filter Medium Resistance. Filtration Equipment
– Filter Presses – Leaf Filter - Rotary Continuous Filters. Principles of
Centrifugal Filtration-Washing of Filter Cakes

Unit-6 Agitation and Mixing 8 4 - 15

Agitation and Mixing of Liquids – Principles of Agitation – Agitation
Equipment –Impellers – Flow Pattern in Agitated Vessel - Power
Consumption in Agitated vessel. Flow number – Power Correlation -
Calculation of power consumption. Blending and mixing - Jet mixers –
Motionless Mixers. Mixing of Solids: Mixtures for Cohesive solids – Power
requirements Criteria for mixer effectiveness. Mixers for free-flowing
granular solids - Rate of mixing

Total 36 20 20 60

Reference Books

1. McCabe W., Smith J., Harriott P., Unit Operations of Chemical Engineering, 7th ed., McGraw Hill
Education; USA, 2014.

2. Coulson J.M., Richardson J.F., Chemical Engineering, Volume 2 (Particle Technology &Separation Processes),
5th ed., Butterworth – Heinemann Publishing Ltd., USA, 2001.

3. Narayanan C.M., Bhattacharya B.C., Mechanical Operations for Chemical Engineers, 3rd ed.,
Khanna Publishers, India, 2011.

4. Patil K.D., Mechanical Operations (Fundamental Principles and Applications), 3rd ed, Nirali Prakasam, India,
2012.

11
 SEMESTER-III
Course Title Technology of Course Code DCH2103
Inorganic Chemicals
Learning Scheme Assessment Scheme: Credits- 4
Classroom Learning CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) -Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
The students should be able to know basic principles of chemical industry; different manufacturing processes
an engineering consideration of chemical processes. In addition, they will get elementary knowledge of chemical
reaction & chemical equilibrium. Students will understand how chemical & engineering principles used in each
process & industry. Apply basic concepts of inorganic chemistry in chemical engineering applications.
Course Outcomes
After completion of this course the students are expected to be able to demonstrate following knowledge, skills
and attitudes:
1. Manufacture the inorganic acids in chemical process industries.
2. Prepare Ammonia-based fertilizers in chemical process industries.
3. Select the raw material for phosphate-based fertilizer manufacturing.
4. Prepare caustic soda in chemical process industries.
5. Manufacture industrially important gases.
6. Synthesize the cement of known composition.
Unit Contents Hrs Marks
SL FA SA
Unit-1 Manufacturing of Sulfuric Acid 5 3 3 7
1.1 Unit operation and unit process concepts, introduce symbol
regarding chemical process, chemical processing and role of
chemical engineers.
1.2 Advantages of Contact process, Physico-chemical principles,
contact process (DCDA), Raw materials, Reaction, Major
engineering problems, Process flow diagram, uses.
Unit-2 Manufacturing of Nitrogenous chemicals 7 4 4 9
2.1 State Le Chatlier Principle, Importance of mixed fertilizer
2.2 Raw material, Reaction, Process flow diagram, Process description
& uses- Ammonia, Nitric Acid, Urea, Ammonium Sulphate,
Ammonium Nitrate, Ammonium Phosphate
Unit-3 Manufacturing Process of Phosphorous Chemicals 7 4 4 9
3.1 Distinguish between yellow and Red phosphorus, Compare between
single and Triple super phosphate, State leaching
3.2 Manufacturing of Phosphorus-Raw material, Reaction, Process flow
diagram, Electro thermal, Electric arc process, Uses
3.3 Manufacturing of Phosphoric Acid-Raw material, Reaction, Process
12
 flow diagram, Uses
3.4 Manufacturing of Single Super Phosphate-Raw material, Reaction,
Process flow diagram, Uses
3.5 Manufacturing of Triple Super Phosphate-Raw material, Reaction,
Process flow diagram, Uses
3.6 Manufacturing of Di-Ammonium phosphate- Raw material, Reaction,
Process flow diagram, Uses
Unit-4 Chlor-alkali Industries 6 3 3 12
4.1 Definition of Electrolysis, Define calcinations, Principle of absorption
4.2 Manufacturing of Chlorine and Caustic soda- Raw material,
Diaphragm cell, Mercury cell, Cell reaction, Process flow diagram,
Uses
4.3 Manufacturing of Hydrochloric Acid- Raw material, Reaction,
Synthesis Process, Salt and Sulfuric Acid Process, Process flow
diagram, Use
4.4 Manufacturing of Soda Ash- Raw material, Reaction, Process flow
diagram, Function of Ammonization and Carbonating tower, Uses
Unit-5 Manufacturing of Industrial Gases 6 3 3 12
5.1 Raw material, Reaction, Process flow diagram, Uses of: Oxygen and
Nitrogen,
5.2 Principle of Linde and Claude’s Process,
5.3 Hydrogen by natural gas, Water gas,
5.4 Producer Gas, Carbon dioxide, Acetylene.
Unit-6 Manufacturing of Cement & other products 5 3 3 11
5.5 Define calcinations, define hardening and settling of cement, types of
cement
5.6 Manufacturing of Gypsum- Raw material, Reaction, Block diagram,
Uses
5.7 Plaster of Paris-Raw material, Block diagram, Uses
5.8 Manufacturing of Cement- Types, contents, theory of hardening and
settling, raw material, wet and dry process, process flow diagram
Total 36 20 20 60

13
Sr. Suggested tasks for Self-Learning
No
1 Prepare a power point presentation on a topic list of inorganic chemicals manufacturing industries
in India.
2 Conduct/participate in MCQ/Quiz.
3 Collection of different fertilizer sample from market.
4 Collect information by library survey regarding Unit Operations used in chemical industry.
Sr. Reference Books
No
Title Author Publication
1
Dryden’s Outlines of Chemical Rao M. G. & Sittig M East- West Press Pvt. Ltd;
Technology Third 1997 Affiliated london
2
Shreve’s Chemical Process Austin G.T., McGraw Hill Inc., 1998
Industries - International Student
Edition, 5th Edition
3 Groggins P. H
Unit process of Organic synthesis McGraw Hill Inc., New York,
1958
Sr. Suggested Learning Websites/Portals/App
No

1 http://www.classcentral.com
2 http://onlinecourses.nptel.ac.in
3 http://ocw.mit.edu

14
 SEMESTER-III
Course Title Industrial Course Code DCH 2104
Stoichiometry
Learning Scheme Assessment Scheme: Credits- 6
Classroom Learning CL) 4 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) 1 Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
Formulate material balances to solve for compositions and flow rates of process streams 2. Incorporate single and
multiple reactions into unit operations within chemical processes 3. Perform material and energy balance
calculations in various systems
Course Outcomes:
After successful completion of course, the students will be able to:
1. Apply mole concept and ideal gas equation to express the composition of mixtures
2.Understand the concept of humidity and usage of psychrometric chart
3.Understand the method of solving steady state material balances without chemical reactions
4.Estimate the extent of reaction in material balances for systems involving chemical reactions
5.Analyze the processes involving recycling and bypass involving chemical reactions
6.Apply simultaneous material & energy balances to industrial processes.

Unit Contents Hrs Marks

SL FA SA
Unit-1 Units and Dimensions, Basic Chemical Calculations: 06 3 3 10
1.1 Units and dimensions, Conversion factors, Mole concept – Concept of
normality, molarity, and molality, Density and specific gravity, Methods
of expressing composition of mixtures and solutions, Weight fraction,
Mole fraction, Volumetric composition (Concepts and problems).
1.2 Gases, Gaseous mixture, Ideal gas law, Dalton’s law, Amagat’s law,
Relationship between partial pressure and mole fraction, Average
molecular weight of gas mixture, Density of gas mixture, Raoul’s law,
Henry’s law- (statement and problems).
Unit-2 Material Balances without Chemical Reaction: 05 4 3 9
2.1 Law of conservation of mass, Process flow sheet, Material balance.
2.2 Calculations involving drying, dissolution, distillation, crystallization,
evaporation, absorption and extraction, blending.

Unit-3 Material Balance with Chemical Reaction: 05 3 4 10

3.1 Define Concepts: Stoichiometric equation – stoichiometric ratio –
limiting reactant – excess reactant, percent excess, conversion, yield.
3. 2 Material balance problems with chemical reactions for calculating %
conversion, % excess, % yield. Recycle, Purge, Bypass calculation.

15
 Unit-4 Energy balance: 08 3 4 11
4.1 Standard heat of formation, Standard heat of combustion, Standard
Heat of reaction – Hess’s law.
4.2 Determination of heat of reaction at temperatures other than standard
temperature using specific heat relationships, Calculation of theoretical
flame temperature.

Unit-5 Fuel and Combustion calculations: 06 4 3 10

5.1 Fuel: Types of fuels :(Solid, liquid and gaseous fuel) Calorific value
of fuels, Flue gas analysis, Orsat analysis,
5.2 Theoretical and excess air requirement for solid, liquid and gaseous
fuels.

Unit-6 Vapor pressure and Humidity calculations: 06 3 3 10

6.1 Vapor pressure and Temperatures, Antoine equation, Vapor pressure
of immiscible liquids and ideal solutions, Raoult’s law, Humidity and
Saturation, Relative and percentage saturation, Wet bulb and dry bulb
temperature, Dew point.
6.2 Use of humidity chart for engineering calculations.

36 20 20 60
Total

Sr. No REFERENCE BOOKS: Author Publication

01 Elementary Principles of Chemical Processes Felder R, Rousseau R 3 rd. ed., John Wiley
& Sons, 2000.

02 Stoichiometry and Process calculations Narayanan K.V, Prentice Hall India

Lakshmikutty B, Limited, New Delhi,
2006.
03 Basic Principles and Calculations in Chemical Himmelblau D.M 8 th ed., Prentice
Engineering Hall, India, 2012.

04 Stoichiometry Bhatt B.I., Thakore S. Hill Book Company,

B. New Delhi, 2011.

16
Course Title PLANT UTILITY (lab) Course Code DCH 2105
Learning Scheme Assessment Scheme: Credits-02
Laboratory Learning (LL) 2Hrs./Week Formative Assessment (FA) 60 Marks
Summative Assessment (SA) 40 Marks
Course Objectives:
The course should be taught and implemented with the aim to develop required skills in students
Course Outcomes:
1) Select Various Methods for Water Softening and Purification.
2) Explain Different Types of Steam Generators and Compressors along with their components.
3) Select Refrigeration for Various Applications.
4) Apply concepts of energy efficiency and green chemistry for conservation of utilities.

Sr. No List of Experiments

1 To determine the suspended & dissolved impurities in water.
2 To determine alkalinity of water.

3 To determine total hardness of water by soap solution method.

4 To determine total hardness of water by E.D.T.A. method.

5 To determine permanent hardness of water

6 To determine chloride content in water
7 To study ion exchange unit.

8 To study natural draft, forced draft & induced draft cooling tower,

9 To study different boiler such as Lancashire, Cochran boiler, Babcock& Wilcox boiler.

10 To study mechanism & working of different types of steam traps.

11 To determine humidity of air,

12 To study different types of refrigeration systems.

13 To study refrigerants with industrial applications.

14 To determine flash point, fire point & viscosity of oil.

15 To determine calorific value of a given fuel.

16 To do analysis of flue gas

17
 Course Title Mechanical Operation (LAB) Course Code DCH2106

Learning Scheme Assessment Scheme: Credits-02

Laboratory Learning (LL) 2 Hrs./Week Formative Assessment (FA) 60 Marks
Summative Assessment (SA) 40 Marks
Course Outcomes:
By the end of this course, the student should be able to:
• To understand the importance of various mechanical operations used in process industry.
• To apply principles of basic sciences and chemical engineering for designing various size reduction, separation
and conveying equipment’s
• Understand and apply the basic methods of characterization of particles and bulk solids, e.g. Average particle
size, settling velocity.
• Describe the operation of filter processes and types of filters used to perform solid-liquid separations, and
calculate their power requirements.
Sr. No List of Experiments
1 To determine the average particle size of a mixture of particles by sieve analysis
2 To Study and operation of Jaw crusher and thereby verification of Rittinger’s constant and to
determine the reduction ratio, maximum feed size and theoretical capacity of crushing rolls
3 To find out the enrichment of the coal sample by forth floatation cell
4 To find out the effectiveness of a vibrating screen.
5 To study the operation of a Hammer mill and a pulveriser and finding their reduction ratio
6 To study the operation of a cyclone separator and finding their efficiency
7 To determine the angle of repose of sand particles using sieve analysis
8 To study the operation of magnetic separator and finding their efficiency.
9 To Study and operation of Roll crusher (Ball mill) and thereby verification of Rittinger’s
constant and to determine the reduction ratio, maximum feed size and theoretical capacity of
crushing rolls
10 To study the batch sedimentation process.
11 To determine the characteristic of plate and frame filter press at a constant pressure and to calculate
the filter cake resistance ‘a’ and the filter cake resistance ‘Rm’
12 To determine the specific cake resistance and the filter medium resistance for the filtration of the
calcium carbonate slurry using the vacuum leaf/vacuum filter.
13 To study the operation fluid energy mill and finding their efficiency
14 To study the operation of Gravity settling tank and finding their efficiency
15 To study the operation of batch type top driven centrifuge and finding their efficiency
16 To study the operation of the screw-conveyor.
17 To study the operation of various types of impellers.
18 To determine the mixing index (Ribbon blender) of given sample.

18
 SEMESTER-III
Course Title Technology of Inorganic Chemicals Course Code DCH2107
(Lab)
Learning Scheme Assessment Scheme: Credits- 02
Laboratory Learning (LL) 02 Hrs./Week Formative Assessment (FA) 60Marks
Summative Assessment (SA) 40Marks
Course Objectives:
Apply basic concepts of inorganic chemistry in chemical engineering applications. To understand basic
chemical reactions and proper use of different analytical instruments. To expose the students on how raw
materials are converted into useful products.
Course Outcomes:
After successful completion of the course, the student will be able to:
1. Manufacture the inorganic acids in chemical process industries.
2. Prepare Ammonia-based fertilizers in chemical process industries.
3. Select the raw material for phosphate-based fertilizer manufacturing.
4. Prepare caustic soda in chemical process industries.
5. Manufacture industrially important gases.
6. Synthesize the cement of known composition.
Sr. No List of Experiments
1 To determine % purity of Sulphuric Acid
2 To determine % purity of HCl Acid
3 To find percentage purity of commercial Nitric Acid
Determine the strength of given Nitric acid by pH meter.
4 Estimate the actual content of soda ash
5 Analysis of Potassium Permanganate
6 Analysis of Hydrogen peroxide.
7 Analysis of potassium dichromate
8 To determine purity of given ferrous sulphate crystals
9 To determine % yield of product NaCl in the given reaction
10 Solubility

11 Determine ammonia content in given sample of fertilizer of ammonium sulphate

12 Determine ammonia content in given sample of fertilizer of ammonium chloride

13 determine the percentage purity of given sample of caustic soda

14 Determine nitrogen content in given sample of ammonium fertilizer.
15 Determine the calcium content in cement.
16 Determine the insoluble ingredients in cement
19
 PROPOSED
SYLLABUS OF
SEMESTER IV

20
 SEMESTER-IV
Course Title Fluid Flow Operation Course Code DCH 2201
Learning Scheme Assessment Scheme: Credits- 6
Classroom Learning CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) - Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
To understand the fundamental aspects of fluid motion, fluid properties, flow regimes, pressure variation, fluid
kinematics and methods of flow description and analysis.
To study the conservation laws in their integral and differential forms, and their use in analyzing and solving the
fluid flow problems.
Course Outcomes:
After successful completion of course, the students will be able to:
1. Determine the fluid pressure and use various devices for measuring fluid pressure.
2. Calculate hydrostatic force and use of law of conservation mass to fluid flow.
3. Apply Bernoulli’s equation to fluid flow problems and boundary layer theory to determine lift and drag
forces on a submerged body.
4. Apply appropriate equations and principles to analyses pipe flow problems.
5. Use of different fluid flow measuring devices.

Unit Contents Hrs Marks

SL FA SA
Unit-1 Fundamentals of Fluid Flow Operations 05 3 3 10
1.1 Fluids and properties of fluids, Newton’s law of viscosity pressure
and temperature dependence, introduction to rheology of fluids, types
of flow, lines to describe the flow.
1.2 The basic equation of fluid statics, pressure-depth relationship,
pressure forces on surfaces, pressure measurements. Engineering
applications of fluid flow operations, pressure measuring devices,
rheological classification of fluids

Unit-2 Momentum and Energy Balance Equations: 04 4 3 9

2.1 Mass and energy balance equations, Bernoulli’s equation;
variable head and variable area meters.
2.2 Flow measuring devices.
Unit-3 Dimensional Analysis and Boundary Layer Theory 05 3 4 10
3.1 Fundamental dimension of quantities, dimensional homogeneity,
Rayleigh’s method and Buckingham’s π method.
3.2 Concept of hydrodynamic boundary layer, growth over a flat plate,
change in nature of boundary layer, and different thicknesses of boundary
layer, drag on flat plate, coefficient of drag and its variation.
hydrodynamic, thermal and concentration boundary layers.

21
 Unit-4 Flow through Conduits 05 3 4 11
4.1 Shell balance-based solution for laminar flow through circular tube
(Hagen Poiseuille equation), on inclined plane, through annular space.
4.2 Concept of Reynolds number; transition and turbulent flow in pipes,
Darcy-Weisbach equation, friction factor chart.

Unit-5 Pipe Fittings & valves: 04 4 3 10

5.1 Various types of fittings, equivalent length of pipe fittings,
5.2 Classification of valves-construction, working, advantages of Gate,
Globe, Ball, Needle, Diaphragm, Control valve, Safety valve, Non-Return
Valve.
Unit-6 Transport of Fluids: 04 3 3 10
6.1 Minor losses and major losses in pipes, concept of equivalent pipe,
series and parallel pipe systems, cavitation and water hammer.
6.2 Transportation of fluids, centrifugal pump.
6.3 Compressors, fans and blowers.
Total 36 20 20 60

Sr. No REFERENCE BOOKS: Author Publication

01 Unit Operations in Chemical Engineering. McCabe W.L. and McGraw Hill, 5th
Smith J.C edition, 2007.

02 Valves, Piping, and Pipelines Handbook Valves, Piping, and Valves, Piping, and
Pipelines Handbook Pipelines Handbook
03 Process Fluid Mechanics Den M.M. Prentice Hall, 1998.

04 Fluid Mechanics-Fundamentals and John M. Cimbala. Tata McGraw Hill,

Applications 2006.

22
 SEMESTER-IV
Course Title Chemical Engineering Course Code DCH2202
Thermodynamics
Learning Scheme Assessment Scheme: Credits- 5
Classroom Learning CL) 3Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) 2 Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
To introduce the principles of Chemical Engineering Thermodynamics and illustrate their application to design
of chemical process plants. To make students competent to apply the principles of chemical engineering
thermodynamics in Chemical Process Industry.
Course Outcomes:
After successful completion of course, the students will be able to:
1. Ability to understand the basic concepts of thermodynamic such as temperature, pressure, system,
properties, process, state, cycles and equilibrium
2. Apply first law of thermodynamics in chemical process industry.
3. Explain the given vapor-liquid Equilibrium
4. Apply concept of entropy for the given system
5. Use the application of thermodynamics to flow processes.
6. Describe chemical equilibrium for the given system
Unit Contents Hrs Marks
SL FA SA
Unit-1 Thermodynamic System & Equilibrium 6 4 3 8
1.1 Dimensions and units, Measures of Amount or size, Force,
Temperature, Pressure, Work, Energy, Heat.
1.2 System, Surrounding, Boundary, Homogeneous & Heterogeneous
systems, Types of thermodynamic systems- Isolated system, open
system, Closed system, Intensive & extensive properties
1.3 Thermodynamic states, Equilibrium state, Non-equilibrium state.
Thermodynamic processes- Isothermal process, Adiabatic process,
Isobaric process, Isochoric process, Cyclic process
1.4 Reversible & Irreversible process, Difference between Reversible &
irreversible process

23
 Unit-2 The First Law of Thermodynamics 7 3 4 9
2.3 The First Law of Thermodynamics: Law of Conservation of Energy,
Mathematical Statement. Internal Energy, Internal Energy as a state
function
2.4 Work and Heat as path Function, Enthalpy, Heat Capacity, Specific
Heat, Heat capacity at Constant Volume, Heat Capacity at constant
Pressure
2.5 Temperature dependence of heat capacity, Relation between Cp &
Cv, Processes involving ideal gases: constant volume process,
Constant pressure process, constant temperature process, Adiabatic
Process
2.6 Joule's Experiments, Numerical
Unit-3 Vapour/Liquid Equilibrium Introduction 6 3 3 7
3.7 The Phase Rule, Phase diagram for: Water system, Carbon
dioxide system and Sulphur System
3.8 Duhem’s Theorem, VLE: Qualitative behavior, Simple models for
vapor/liquid equilibrium
3.9 VLE by modified Raoult’s Law, VLE from K- value correlations

Unit-4 The Second law of Thermodynamics 6 3 3 12

4.5 Statement of the Second law, Concept of entropy, Relation
between first and second law of thermodynamics
4.6 The Heat Engine; Thermodynamic Temperature Scales
4.7 Entropy changes of an ideal gas; Mathematical statement of the Second
Law; Entropy balance for open systems
4.8 Clausius inequality: Statement & mathematical expression,
Numerical
4.9 Third Law of thermodynamics: statement
Unit-5 Applications of thermodynamics to flow processes 6 4 3 12
5.9 Duct flow of compressible fluids; Turbines (expanders); Compression
processes
5.10 Refrigeration and liquefaction: The Carnot Refrigerator; the vapor-
compression cycle; The Choice of refrigerant
5.11 Absorption Refrigeration; The heat pump; Liquefaction Processes

24
Unit-6 Chemical Equilibria 5 3 4 12
6.1 Concept of chemical equilibrium, Relation between Kp, Kc & Ky,
Numerical
6.2 Application of equilibrium criteria to chemical reactions
6.3 the standard Gibbs energy change and equilibrium constant, Effect
of temperature on the equilibrium constants

Total 36 20 20 60

25
Sr.no Suggested tasks for Self-Learning
1 Prepare the presentation based on chemical thermodynamic process.
2 Conduct/participate in MCQ/Quiz.
3 Search the different thermodynamic simulation tools.
Sr. Tutorials
No
1 Problem based on basic conversions of pressure, temperature, heat energy
2 Problem based on phase rule
3 Calculation of heat capacity at constant pressure and temperature
4 Mass and Energy balance on close system/ open system
5 Work and energy problems on reversible closed system
6 Explain the different thermodynamic diagram
7 Enthalpy and entropy problems on reversible closed system
8 Molar volume calculations
9 Problems on heat of reaction
10 Problems on heat of formation
11 Problem on heat of combustion
12 Calculation of compressibility factor
13 Problems on Raoult’s law
14 Problems on heat engine and refrigeration
15 Problems on Gibbs energy change
16 Problems on Kp, Kc, Ky
Sr. Reference Books
No
Title Author Publication
1
Chemical Process Principles (Part - Hougen O.A, Watson. K.M and Asia Publishing House
II), 2nd edition Ragatz R.A.
2
Introduction to Chemical Smith J.M, Van Ness H.C and 7th Edition, McGraw Hill
Engineering Thermodynamics Abbott M.M. International (2001)
3 Butterworth Publishers, London.
Phase Equilibria in Chemical Stanley M. Walas
Engineering
Sr. Suggested Learning Websites/Portals/App
No
1 www.nptel.ac.in
2 www.msubbu,in
3 http://ocw.mit.edu
3 http://www.classcentral.com

26
 SEMESTER-IV
Course Title Technology of Organic Course Code DCH2203
Chemicals
Learning Scheme Assessment Scheme: Credits- 3
Classroom Learning CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) 1 Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
This subject will provide information towards raw materials, process & industrial application for manufacturing
of organic chemicals like alcohol, oil, soap, polymer, phenols, pulp & paper these technologies will provide
necessary skill to perform the job role.

Course Outcomes
After completion of this course the students are expected to be able to demonstrate following knowledge, skills
and attitudes:
7. Use fermentation process for manufacturing of alcohol & its product.
8. Use hiding power principle for manufacturing of paint, varnishes & lacquers.
9. Prepare the soap & detergent using relevant oils.
10. Prepare pulp & paper using sulphate & sulphite process.
11. Use polymerization process for preparation of various polymers.
12. Apply relevant process to upgrade refinery product.
Unit Contents Hrs Marks
SL FA SA
Unit-1 Alcohol 7 3 4 8
1.1 Raw Materials, Reactions, Flow sheet/Block diagram,
manufacturing process of products & their uses- Ethyl alcohol by
Corn &Molasses
1.2 Acetic Acid by Oxidation of Acetaldehyde
1.3 Ethyl acetate & Butanol
Phenol
1.4 Raw Materials, Reactions, Flow sheet/Block diagram,
manufacturing process of phenol &their uses- Cumene Peroxidation
Process,
1.5 Toluene Oxidation Process,
1.6 Rasching Process
Unit-2 Paint 6 4 3 8
2.7 Paint: Raw materials, manufacturing process, process block
diagram, industrial applications.
2.8 Lacquers: Raw materials, manufacturing process, process block
27
 diagram, industrial applications
2.9 Varnishes: Raw materials, manufacturing process, process block
diagram, industrial applications
Unit-3 Oil, Soap & Detergent 6 4 3 10
3.10 Oil: Definitions - Acid value, Iodine value, Saponification value of
oil, Extraction of Oil by solvent process, Hydrogenation of Oil
3.11 Soap: Classification of Cleansing Compounds, Manufacturing of
Soap by- Batch Saponification Process, Continuous Hydrolysis &
Saponification, Cleansing action of Soap.
3.12 Detergents: Manufacturing of detergents by - Sulfated Fatty
Alcohols, Alkyl-Aryl Sulfonates
Unit-4 Pulp & Papers 6 3 4 12
4.10 Raw Materials, Reactions, Flow sheet/Block diagram,
manufacturing process of product & their uses- Pulp by Sulfate
(Kraft) process & Sulphite process recovery of Chemicals
4.11 Paper from pulp Rayon (viscous rayon) form cellulose
Unit-5 Polymer 6 3 3 12
5.12 Polyvinyl chloride: Raw materials, chemical reaction, process flow
diagram, manufacturing process, uses.
5.13 Polyester: Raw materials, chemical reaction, process flow diagram,
manufacturing process, uses.
5.14 Polyethylene: Raw materials, chemical reaction, process flow
diagram, manufacturing process, uses.
5.15 Polycarbonate: Raw materials, chemical reaction, process flow
diagram, manufacturing process, uses.
Unit-6 Petroleum refining and basic petrochemicals 5 3 3 10
6.1 Main constituents of petroleum, major refining processes & its
different products,
6.2 boiling ranges & applications, thermal cracking, catalytic cracking,
reforming, concepts of octane number

Total 36 20 20 60

28
Sr. Suggested tasks for Self-Learning
No
1 Prepare a power point presentation on a topic list of Organic chemicals manufacturing industries in
India.
2 Conduct/participate in MCQ/Quiz.
3 Collection of different polymer sample from market.
4 Collect two samples from four companies. Classify the samples on the basis of content. Identify the
location of industry, prepare a report based on content & cost.
Sr. Reference Books
No
Title Author Publication
1
Dryden’s Outlines of Chemical Rao M. G. & Sittig M East- West Press Pvt. Ltd;
Technology Third 1997 Affiliated london
2
Shreve’s Chemical Process Austin G.T., McGraw Hill Inc., 1998
Industries - International
Student Edition, 5th Edition
3 J.A. Brydson,
Plastic Materials, 7th edition Oxford Auckland boston
Johannesburg Melbourne new
delhi
4 Groggins P. H
Unit process of Organic synthesis McGraw Hill Inc., New York,
1958
Sr. Suggested Learning Websites/Portals/App
No

1 www.classcentral.com/course/swayam-organic-chemical-technology-184172
2 https://www.acs.org/chemicalsafety
3 www.chemistry.harvard.edu

29
 SEMESTER-IV
Course Title CHEMICAL PROCESS Course Code DCH2204
INSTRUMENTATION AND
CONTROL

Learning Scheme Assessment Scheme: Credits- 3

Classroom Learning CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) - Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
1. Understand the basic concepts of measuring instruments used in process industries
2. Explain the importance of process control mechanism and their applications in chemical process industries
3. Describe principles of modes of controllers and their general characteristics and study the stability analysis of digital
control system

Unit Contents Hrs. Marks

SL FA SA
Unit-1 Process Control 5
Principles and classification of process control - Types of Controllers,
Hardware elements of control system- chemical process, sensors,
transducers, transmission, controller. Digital computers in process control-
direct digital control, supervisory computer control, scheduling computer
control.

Unit-2 Introduction to Process Control 8

Laplace transformation - transform of simple functions - derivatives and
integrals - Open loop system - Transfer functions - Forcing functions -
step, Ramp, impulse and sinusoidal - Higher order system dynamics - First
order systems- linearization and its characteristics in process control -
Transportation lag.

Unit-3 Feedback Control Block Diagram 6

Closed loop system- Block diagram - Development of block diagram -
Servo and Regulator problem - Negative Feedback Versus Positive
Feedback - Measuring Element- Controller and Final Control Element

30
 Unit-4 Controllers and Control Action 6
Transfer function of controllers and control valve - Characteristics of ON-
OFF, Proportional, Integral and Derivative control modes - P - PI - PD -
PID control modes - Principles of Pneumatic and Electronic Controllers -
I/P converter - Control valve - Construction - Sizing - Characteristics.

Unit-5 Time and Frequency Domain Analysis` 6

Stability criteria- Routh's stability criteria - Root locus diagram -
Frequency response analysis - Gain margin - Phase margin and cross over
frequency - Bode plot - Polar plot and Nyquist plot.
Controller Tuning
Process reaction curve - Cohen-Coon method - IMC tuning - Ziegler Nichols
method
Unit-6 Advanced Process Control 5
Introductions to multivariable control - Computer applications in process
control - Advanced control strategies - Cascade control - Ratio control -
Feed-Forward control - Inferential control - Adaptive control - Control of
Reactor - Distillation towers - Heat Exchangers

TOTAL 36

Reference Books

1. Coughanowr C. R., Koppel L. M., Process System Analysis and Control, 3rd ed., McGraw Hill, New Delhi,
2013.

2. Seaborg D. E., Edgar, T. F., Mellichamp D. A., Process Dynamics and Control, 3rd ed., Wiley India, New Delhi,
2013.

3. Stephanopoulos G., Chemical Process Control, 1 st ed., Pearson Education India, New Delhi, 2015.

31
 SEMESTER-IV
Course Title CHEMICAL INDUSTRIAL Course Code DCH2205
SAFETY AND MAINTENANCE

Learning Scheme Assessment Scheme: Credits-3

Classroom Learning (CL) Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
The students should be able to learn the safety procedure/rules while working in a plant,
to understand the loss prevention concept for the chemical plants, to understand all types
of hazards associated in a chemical industry & learn to analysis for prevention of accidents,
also, able to prepare safety audit report & safety report. Student should understand
procedure for preventive maintenance, on-line maintenance, shut down maintenance.

Unit Contents Hrs Marks

SL FA SA
Unit-1 Plant Hazards: 5
Industrial hazards due to process & its precautions, Plant Safety
provisions, Electrical hazards - Common Sources, precautions,
Mechanical hazards, Explosion hazards -Classification of explosives,
precautions while handling explosives, Radiation hazards –Health hazards
of infrared radiation & X rays, Noise hazard - Sources, protection,
Chemical hazard - hazards due to NH3, Cl2, H2SO4

Unit-2 Personal Protective equipment’s: 6

Working of different respiratory equipment’s, selection of proper
respiratory device, Respiratory protective equipment - Air purifier type,
supplied air type, Self-contained breathing apparatus, selection of proper
devices, Non-respiratory personal protective equipment - Eye& face, ear,
head, torso & body, hand, foot & leg protection.

Unit-3 Fire Prevention: 6

Types of fire, fire triangle, Principle of extinguish of fire, Classification of
fire and suitable type of extinguisher, Principle, Construction & working
of following fire extinguisher -Soda Acid type, Foam type, Dry Chemical
powder, Fire buckets and Fire hydrant.

Unit-4 Storage & Transportation of Chemicals: 7

Methods of Storage- Bulk storage, bin storage, underground storage,
liquid storage, gas storage; Storage of flammable & combustible liquid
chemicals shock sensitive chemicals, Packing of solids - bags, boxes,
drum, container, Vibrating hopper, Screw feeder. Functions & Principles
of material handling- Construction & working of screw conveyor, belt
conveyor, bucket elevator (Spaced bucket positive discharge), Pneumatic
conveyor - (Positive, negative), Wooden pallets for unit load,
32
 Transportation of hazardous Chemicals –Flammable liquids, corrosives or
oxidizing materials, water reactive chemicals, igniting substances, toxic
chemicals

Unit-5 Plant Maintenance: 6

Objectives of plant maintenance functions & responsibilities of plant
maintenance department, Types of maintenance, Corrective or breakdown
maintenance, Scheduled maintenance, Preventive maintenance, Predictive
maintenance, Online maintenance (e.g. Rota meter/ Steam trap), Shut
down maintenance, Procedure for shutdown & startup of plant.

Unit-6 Hazard & operability studies: 6

Chemical hazards, its identification Acts: -ESI act (1948) – scheme &
compensation for loss of ability to work, factory act (1948) -
safety, the workmen compensation act (1923) – accident reporting &
prevention, employee’s liability for compensation, notice & claim for
accident Safety Audit: Objectives of safety audit, procedure for safety
auditing.

TOTAL 36

Reference Books

1. Coulson J.M. & Richardson R.F. Chemical Engineering (Volume VI) First 1983
Pergamon Press Ltd; Oxford, England

2. A. K. Rohatgi, Safe Handling of Hazardous Chemicals, J. K. Enterprises

3. S. S. Apte, Plant Maintenance, Delhi Productivity Council

4. Fawceett H.H. & Wood W.S. Safety & Accident Prevention in Chemical Operation
Second 1982 John Wiley & Sons Inc, New

5. King R.W. & Magid J. Industrial Hazards & Safety Handbook First 1982 Butterworth
Heinemann publication, Boston

33
Course Title Fluid Flow Operation (Lab) Course Code DCH 2206
Learning Scheme Assessment Scheme: Credits- 02
Laboratory Learning (LL) 02 Hrs./Week Formative Assessment (FA) 60Marks
Summative Assessment (SA) 40Marks
Course Objectives:
It is an introductory course where flow behavior, fluid forces and analysis tools are introduced. The goals of the
experiments include determination of forces generated when fluid flow takes place over a solid object,
applications of the control volume approach, demonstration of the momentum and energy equations, viscosity
measurement and engineering correlations.
Course Outcomes:
After successful completion of the course, the student will be able to:
1. Identify, name, and characterize flow patterns and regimes.
2. Understand basic units of measurement, convert units, and appreciate their magnitudes.
3. Utilize basic measurement techniques of fluid mechanics.
4. Discuss the differences among measurement techniques, Department!
5. Measure fluid pressure and relate it to flow velocity.
6. Demonstrate practical understanding of the various equations of Bernoulli.
7. Demonstrate practical understanding of friction losses in internal flows.
8. Demonstrate practical understanding of boundary layers, separation, drag, and lift.
Sr. No List of Experiments
1 To measure static pressure of fluid by different manometers.
2 To determine Reynolds experiment.
3 To determine Verification Bernoulli equation.
4 To determine coefficient discharge of orifice meter.
5 To determine coefficient discharge of venturi meter.
6 To study Calibration of rotameter
7 To Determination of mean velocity by Pitot-Tube.
8 To Determination of frictional losses in pipes
9 To Determination of operating characteristics of centrifugal pump.
10 Determination of pressure drop per unit length as a function of superficial velocity of fluidization
medium
11 Determine fanning friction factor at different flow rate and plot friction factor vs
Reynolds number for a given pipe.
12 Measure the viscosity of starch solution of different concentration.
13 To study Viscosity, Velocity & Pressure measuring device.
14 To determine Free and Forced Vortex.
15 To determine the coefficient of discharge of Notch (V, Rectangular and Trapezoidal types).

34
 SEMESTER-IV
Course Title Technology of Organic Chemicals Course Code DCH2207
(Lab)
Learning Scheme Assessment Scheme: Credits- 02
Laboratory Learning (LL) 02 Hrs./Week Formative Assessment (FA) 60Marks
Summative Assessment (SA) 40Marks
Course Objectives:
Apply basic concepts of inorganic chemistry in chemical engineering applications. To understand basic
chemical reactions and proper use of different analytical instruments.
Course Outcomes:
After successful completion of the course, the student will be able to:
1. Prepare ethyl acetate from ethanol & acetic acid.
2. Determine the percentage of thinner in given sample of oil paint.
3. Prepare soap by batch saponification process.
4. Perform decolorization of paper by bleaching
5. Determine acid value of given sample of polymer.
6. Determine density & boiling point of sample.
Sr. No List of Experiments
1 To estimate the strength of glacial acetic acid
2 To determine aniline point of given petroleum sample
3 To determine acid value of given oil sample
4 To determine iodine value of given oil sample
5 To determine saponification value of given oil sample
6 To manufacture soap on laboratory scale
7 To determine TFM of a given soap sample
8 To determine moisture content, acidity & alkalinity of a given soap sample
9 To determine hiding power of paint sample

10 To do analysis of paint with respect to pigment content & thinner

11 To determine acid value of given polymer sample
12 To do different testing of polymers

13 To study polymerization process of polyester/polystyrene/ PVC.

14 Prepare ethyl acetate from ethyl alcohol and acetic acid by esterification and determine its density
and boiling point
15 Determine viscosity of groundnut oil using redwood viscometer
16 Determine viscosity of soybean oil using redwood viscometer

35
Course Title PROCESS Course Code DCH2208
INSTRUMENTATION AND
CONTROL(LAB)

Learning Scheme Assessment Scheme: Credits-02

Laboratory Learning (LL) 2 Hrs./Week Formative Assessment (FA) 60 Marks
Summative Assessment (SA) 40 Marks
Course Objectives:
The students should be able to understand basic ideas of measurement techniques for various process variables,
qualitative understanding of process control, & application of control systems
Course Outcomes:
a. Select the Instrument for various chemical Processes.
b. Use temperature measuring instruments in chemical industry.
c. Use Pressure measuring instruments in chemical industry.
d. Measure the flow level using various measuring instruments in chemical industry.
e. Select control system for various actions in chemical industry
Sr. No List of Experiments
1 Measurement of temperature using RTD
2 To test pressure with dead weight pressure tester.
3 Measurement of temperature using thermocouple
4 Measurement of pressure by using LVDT
5 To measure the level by air purge method.
6 Dynamics of non-interacting tanks.
7 Dynamics of interacting tanks.
8 Measurement and control of temperature using ON/OFF controller.
9 Measurement of level using capacitive transducer
10 To demonstrate gas liquid chromatography.
11 Measurement and control of temperature using PI controller.
12 Measurement and control of temperature using PID controller.
13 Determination of valve coefficient of control valves
14 To study flapper nozzle system.
15 Time constant thermometer.
16 Bourdon tube.

36
Course Title CHEMICAL INDUSTRIAL Course Code DCH2209
SAFETY AND MAINTENANCE
(LAB)

Learning Scheme Assessment Scheme: Credits-02

Laboratory Learning (LL) 2Hrs./Week Formative Assessment (FA) 60 Marks
Summative Assessment (SA) 40 Marks
Course Objectives:
• To achieve an understanding of principles of safety management.
• To enable the students to learn about various functions and activities of safety department.
• To enable students to conduct safety audit and write audit reports effectively in auditing situations.
• To have knowledge about sources of information for safety promotion and training.
• To familiarize students with evaluation of safety performance.

Sr. No List of Experiments

1 To study different types of fire extinguisher and about their safety procedures
2 To study Different Types of conveyor
3 To study Maintenance of reactor.
4 To study pump and prepare the checklist of given pump.
5 To study the safety garments for body protection.
6 To study preventive maintenance of control valve.
7 To study maintenance of gate valve.
8 To study maintenance schedule.
9 To Study Different types of pipe fitting.
10 To study respiratory protection equipment’s
11 To study Ear Protection Equipment.
12 To study, foot and leg protection.
13 To demonstrate protective safety, garment (hand protection)
14 Head protection safety garments.
15 To determine the noise pollution of a given unit.
16 To study and identify various types of traffic symbols.
17 To study Light meter.
18 To perform an emission test on a given unit and determine the pollutant concentration.
19 To study the MSDS manual of given sample.
20 To study Standard operating procedure of given assembly/unit.
21 To prepare a checklist for the given assembly/unit for maintenance.

37
38