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160mm Thick 316L SS EBW Welding
160mm Thick 316L SS EBW Welding
A R T I C L E I N F O A B S T R A C T
Keywords: The maximum thickness of flanging position on the vacuum vessel (VV) window collar of China Fusion Engi
Electron beam welding neering Test Reactor (CFETR) is 160 mm. Electron beam welding can achieve one-time penetration of the thick
Microstructure plate without groove and the deformation after welding is quite small. The cross section of weld was sampled for
Mechanical properties
microscopic observation and mechanical properties tests to explore the difference in microstructure and per
Solidification mode
Composition overcooling
formances of 160 mm thick 316 L stainless steel electron-beam-welded joints. The results showed that the weld
depth-width ratio reached up to 16:1, and the microstructure of weld was composed of ferrite and austenite with
different morphologies which was mainly coarse cellular crystal in heat affected zone (HAZ). The equiaxed grain
orientation in the root region (denoted as “R region”) was mostly [001] and the columnar grain orientation along
the temperature gradient was mostly [101]. The microstructure along the depth direction was quite different,
which was mainly related to the solidification mode and composition overcooling. The high strength
(YS=715.22 MPa) of R region was due to the smaller temperature gradient and the larger cooling rate, the
position of fracture suggested that the strength of weld was higher than that of the base metal. The micro
hardness measurement results showed that the hardness increased gradually along the depth direction of weld
(Top:156.5 HV, Root: 238.7 HV) and fluctuated along the width direction. The tensile properties along the
thickness direction exhibited a trend of decreasing first and then increasing, which was mainly related to the
characteristics of electron beam deep penetration welding and the difference of grain structure along the
thickness direction.
1. Introduction replacing internal components and installing auxiliary heating and. etc.
As a connecting part between windows and the main body of VV, the
As a core safe component of China Fusion Engineering Test Reactor window collar has the characteristics of complex contour and large
(CFETR), the vacuum vessel (VV) provides a stable vacuum environment thickness as shown in Fig. 1(a). The flanging is a key position where
for plasma fusion reaction[1–3]. The VV serves in a complex connects the main body of VV, thus the control of welding deformation
mechanical-temperature-electromagnetic coupling environment, is more stringent. The maximum size of the window collar of the CFETR
requiring all welds to achieve full penetration. Besides, the arc welding VV is about 4.2 m × 2.7 m.
defect level realizes the ISO5817: 2014-B quality standard and the The vacuum EBW can realize the micro-deformation welding of large
electron beam welding (EBW) defect level realizes the ISO13919–1: thickness structure with the advantages of small post-welding defor
2019-B quality standard. The VV has a complex hyperboloid structure mation, narrow heat affected zone (HAZ) and large aspect ratio. How
with the cross section of double-layer D-shaped, and contains an upper ever, the vacuum chamber and welding motion system of electron beam
window, a middle window and a lower window for diagnostic systems, welding machine is unable to weld the large window collar parts
* Corresponding author.
E-mail address: zhliu@ipp.ac.cn (Z. Liu).
https://doi.org/10.1016/j.fusengdes.2023.113973
Received 10 July 2023; Received in revised form 23 August 2023; Accepted 23 August 2023
Available online 30 August 2023
0920-3796/© 2023 Elsevier B.V. All rights reserved.
J. Ma et al. Fusion Engineering and Design 195 (2023) 113973
2. Experimental procedure
Table 1
Electron beam welding process parameters.
Voltage Ua/ Beam current Ib/ Focus current If/ Velocity v/(mm•s −
Working distance L/ Scanning Amplitude A/ Oscillation frequency fp/
1
kV mA mA ) mm shape mm Hz
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J. Ma et al. Fusion Engineering and Design 195 (2023) 113973
Table 3
Solidification mode of austenitic stainless steel.
Solidification mode Solidification structure Creq / Nieq
A L→L+γ→γ <1.25
AF L→L+γ→L+γ+δ→γ+δ 1.25~1.48
FA L→L+δ→L+γ+δ→δ+γ 1.48~1.95
F L→L+δ→δ→δ+γ >1.95
Table 2
Composition of 316L(wt.%).
C Si Mn P S Ni Cr Mo Cu N
0.022 0.50 1.36 0.032 0.004 10.12 16.31 2.04 0.3 0.037
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J. Ma et al. Fusion Engineering and Design 195 (2023) 113973
Fig. 6. Microstructure of weld center in different depth: (a) T region; (b) U region; (c) M region; (d) L region; (e) R region; (f) Pore in L region.
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J. Ma et al. Fusion Engineering and Design 195 (2023) 113973
Fig. 8. IPF of different sampling regions: (a)T-region; (b)U-region; (c)M-region; (d)L-region; (e)R-region.
[100] orientation of equiaxed crystal in the center, [001] orientation of with a coarse grain size of up to 200 μm displayed cellular and columnar
columnar crystal on both sides, and the dendritic ferrite dispersed in the morphology as shown in Fig. 8(b) and (c). It was clarified that the grain
austenite matrix. The weld microstructure demonstrated substantial size of T and U regions was significantly larger than that of L and R
inhomogeneity from T region to R region. The top microstructure of region, which suggested that coarse grain size mainly arose due to the
weld displayed a composition of axial coarse grain and columnar grain, high energy density, low cooling rate of electron beam welding and long
while the root grain structure transformed into columnar and equiaxed residence time at high temperature. The coarsening of microstructure
fine crystal. It was believed that the faster cooling rate contributed to resulted in a sharp compromise of performances.
form the fine equiaxed crystal structure. The HAZ near the fusion line The size of grains mainly depends on the ratio of nucleation rate N to
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J. Ma et al. Fusion Engineering and Design 195 (2023) 113973
growth rate G. It was observed that the grain size decreased with the
ratio of N/G increased as shown in Fig. 9, both N and G were closely
related to the overcooling degree under unbalanced solidification con
ditions [16]. However, N and G decreased when the overcooling degree
increased to a certain value, increasing the degree of overcooling
moderately can refine the grain. Scanning deflection is often added to
produce stirring effect in industry, so as to increase the degree of over
cooling, improve the weld morphology and enhance the mechanical
properties of electron-beam-welded joints.
Affected by the welding thermal cycle and thermal exchange, the
energy received by the HAZ from the near base metal side to the near
weld side enhanced gradually, and the microstructure showed the
characteristics of continuous transition. The HAZ showed a high auste
nitizing temperature and large grain sizes near the weld, while the HAZ
near the base metal underwent grain refinement after recrystallization.
Therefore, there were significant differences in grain orientation and
morphology between both sides near the fusion line where represented
the ideal location for forming a continuous liquid film with low melting
point impurities and brittle phases which usually caused mechanical
property degradation. In addition, HAZ also supply a favorable site for Fig. 10. Hardness distribution along thickness direction.
residual stress concentration and crack propagation. Hence, the HAZ is
deemed as the weakest area of weld [17]. microstructure. From T region to M region of the weld, grains changed
from coarse dendrites to fine dendrites, the grain size became smaller
and the hardness increased. From M region to R region, the change of
3.2. Mechanical properties of weld along the thickness direction solidification mode led to the decrease of ferrite quantity, and the
refinement of grains led to the increase of grain boundary quantity,
3.2.1. Microhardness analysis which resulted in the increase of hardness.
Microhardness is a critical parameter for evaluating the quality of Fig. 11 depicted the microhardness variations taken from R region
welded joints, which depends on not only the material but also the along the width direction of the weld. Hardness levels displayed a
microstructure and welding defects. The DHV-1000 Vickers hardness decreasing trend from the weld center to base metal. The microhardness
tester was subjected to measure the cross-sectional hardness of the of the weld center was 15–20 HV higher than that of the base metal. The
welded joint along the thickness and width directions. Fig. 10 presented equiaxed dendrite distribution range of the weld center was believed to
the outcomes of the weld center in T, U, M, L, and R regions. The be the highest hardness area of the welded joint. The main reason why
hardness exhibited an increasing trend from the top to the root, which the hardness near the fusion line not much different from that of the base
ranged between 150 and 160HV in T region, 200–220HV in U and M metal was that the grains near the fusion line were slender columnar
regions, and 220–230HV in L region. The largest hardness of R region crystals, which were coarser than the weld center, which reduced the
increased to 242.5HV, which exhibited 56% higher than that of T region hardness.
(156.5HV). Grains in the top of weld were coarse because of the most
significant welding heat input. The coarse network ferrite precipitated 3.2.2. Tensile properties analysis
during the solidification process, leading to a notable hardness reduction Tensile strength is another essential parameter to evaluate the me
in T region when compared to base metal (~217HV). From T region to M chanical properties of electron-beam-weld joints. The test results of the
region, the decreasing temperature gradient (G) resulted in the trans tensile specimens in different regions showed that the tensile strength
formation of coarse reticular crystals to fine dendrites and equiaxed from T region to R region along the thickness direction of the weld was
crystals. The solidification mode changed from FA to AF along the highly inhomogeneous as shown in Fig. 12. The tensile properties along
thickness direction with the decreasing ferrite content. The composition
overcooling inflicted changes from dendritic crystal to equiaxed crystal,
resulting in further grain refinement and increased hardness. In sum
mary, the variation of hardness was closely related to the
Fig. 9. Relationships between N, G and △T. Fig. 11. Hardness distribution along width direction (R region).
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J. Ma et al. Fusion Engineering and Design 195 (2023) 113973
with fracture location were listed in Table 4. It was observed that the
fracture position of all specimens was located at base metal as shown in
Fig. 13, which indicated that the weld strength was higher than that of
the base metal.
The ultimate tensile strength (UTS) from the T region to the R region
specimens along the thickness direction of the weld exhibited a high
inhomogeneity. The T region and R region specimens showed high
strength with an average UTS exceeded 700 MPa and the U region and L
region was about 688 MPa, while the M region exhibited the lowest. This
distribution law was mainly related to the microstructure and weld
surface characteristics. The weld grains in the T region were mostly
equiaxed fine dendrites, which were greatly affected by fine grain
strengthening and thus kept high strength. The grains in T region were
coarse columnar crystals which resulted in a low hardness. However,
due to the characteristics of electron beam deep penetration welding,
the top of weld was subjected to a high heat input which caused the large
weld width, and the protective effect of weld on the joint was the
strongest [18]. The tensile properties reflected the average mechanical
properties of a larger area, while the microhardness represented the
performance changes in the small local area. Hence, the T region
exhibited the high strength-low hardness feature, and the high strength
of the U region also came from the protection of the weld. Compared
with the L region, the difference in performance between the M region
and L region mainly came from the transformation of the microstruc
ture. It can be observed from the previous content that the trans
formation of the microstructure was mainly related to the composition
overcooling determined by the cooling rate (R) and the temperature
Table 4
Tensile properties along thickness direction.
Region UTS / MPa Fracture location
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