This document outlines the experiments for a Physical Chemistry practical course. Students must complete one experiment worth 30 marks. The experiments include determining heat of solution/neutralization, rate constants of reactions like hydrolysis and saponification, distribution coefficients using partition methods, specific and molar rotation, rate constants using polarimetry, dissociation constants, and solubility products. Students will also be assessed on a viva voce and their notebooks.
This document outlines the experiments for a Physical Chemistry practical course. Students must complete one experiment worth 30 marks. The experiments include determining heat of solution/neutralization, rate constants of reactions like hydrolysis and saponification, distribution coefficients using partition methods, specific and molar rotation, rate constants using polarimetry, dissociation constants, and solubility products. Students will also be assessed on a viva voce and their notebooks.
This document outlines the experiments for a Physical Chemistry practical course. Students must complete one experiment worth 30 marks. The experiments include determining heat of solution/neutralization, rate constants of reactions like hydrolysis and saponification, distribution coefficients using partition methods, specific and molar rotation, rate constants using polarimetry, dissociation constants, and solubility products. Students will also be assessed on a viva voce and their notebooks.
Full Marks_ 50 Credits_S Any one experiment- 30 Marks
1. Water equivalent of calorimeter
and determination of (i) Heat ofsolution ofpotassium nitrate (ii) Heat of neutralization ofstrong acid and strong base. (iii) Basiciry ofpolybasic acids. 2' Determination of rate constant of hydrolysis of methyl acetate in acid medium. 3. The study ofsaponification ofethyt acetate by sodium hydroxide and determination of rate constant. 4. To determine the distribution coefficient of (i) Acetic acid (iD Benzoic acid Between water and benzene by partition method. 5. Determination of specific and molar rotation of sucrose in different concentrations and to determine the concentration ofgiven solution. 6' Determination of rate constant by inversion of cane sugar by polarimetrically 7. Determination of (0 Dissociation constart ofacetic acid. (ii) Acid-basetitration. (iii) Solubiliry product of sparingly soluble salt. Viva- voce- 15 Note books-S
Quantitative Determination of Thiourea & Some of Its Derivatives With Nbsa Reagentquantitative Determination of Thiourea & Some of Its Derivatives With Nbsa Reagent