HCMC UNIVERSITY OF TECHNOLOGY

AND EDUCATION PRACTICE OF

FACULTY OF CHEMICAL AND FOOD ORGANIC CHEMISTRY
TECHNOLOGY

LAB REPORT

#2 EXTRACTION TECHNIQUE

Date: 10/03/2023 Grade

Class: Group: 7

Name: Đào Ngọc Bảo Trân Student ID:22128078

Name: Trần Thanh Trúc Student ID:22116023 Signature

Name: Dịp Ngạn Chương Student ID:22116005

A. PREPERATION

(Students must finish before class)

1. Purpose of experiment:
• Describe the principles of extraction and dissolution techniques

by an acid-base reaction.

• Apply extraction techniques to separate compounds with different acid - base

properties from the mixture.

• Apply the melting temperature measurement technique to determine the purity

of the extracted compound.
 2. Chemical properties and safety
mp bp
Compound Structure MW density safety
(oC) (oC)

Aspirin 180.16 140 135 1.40 Toxic

121-
β-Naphthol 144.17 285 1.217 Toxic
123

Toxic,
Naphthalene 128.17 80.2 218 1.14
Flammable

- Toxic,
Diethyl ether 74.123 34.6 0.7134
116.3 Flammable

Clear
colorless
Hydrochloric
HCl 36.46 - 74 53 1.09 liquid;
acid 6M
pungent
odor

NaOH 10%
NaOH 0 118 1.353 Danger
Solution

NaHCO3
NaHCO3 -- 100 1.01 Void
5% Solution

Na2SO4
Na2SO4 142.06 888 1100 2.671
(anhydrous)

Litmus paper
3. Experimental procedure

Filling the separatory funnel

Mixing and venting

Overcoming and emulsion

Idenntifying the layers

Seperating the layers

Drying the organic

Concentrating layer
in vacuo