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Journal of Oral Rehabilitation 2002 29; 175±183

Fracture characteristics of carbon ®bre, ceramic


and non-palladium endodontic post systems
at monotonously increasing loads
P. OTTL, L. HAHN, H.-CH. LAUER & M. FAY Department of Prosthodontics, School of Dentistry ZZMK
(Carolinum), Johann Wolfgang Goethe University, Frankfurt, Germany

SUMMARY A carbon ®bre post system, three non- carbon ®bre post system (312á5 ‹ 58á8 N). The frac-
palladium and one palladium metal post systems, ture load of non-palladium metal posts (242á3±
two ceramic post systems, and a metal post system 300á4 N) did not differ signi®cantly from that of
with a ceramic core were studied in vitro. The the Perma-dorTM post (265á9 N), which does contain
control group consisted of root-®lled test teeth palladium. Values of 300á3 ‹ 89á3 N (aluminium
without posts. The test teeth were identical arti®cial oxide ceramics) and 193á5 ‹ 57á0 N (zirconia ceram-
roots of an upper central incisor made from a ics) were found for the ceramic posts. The control
posterior composite whose module of elasticity group exhibited a fracture load of 228á8 ‹ 35á7 N.
was similar to that of natural dentine. All posts The mean distance between the vestibular end of
were cemented in the roots using PanaviaTM 21 TC. the fracture gap and the point of force application
Subsequently, standardized full crowns were was between 10á1 ‹ 2á3 and 14á7 ‹ 1á2 mm.
cemented onto all roots. On a universal testing KEYWORDS : in vitro study, materials science, ther-
machine, the test teeth were loaded palatally at apy, non-vital tooth, post-and-core system, fracture
monotonously increasing loads until root fracture. load, all-ceramic restoration, carbon ®bre post
The highest mean fracture loads were found for the

Introduction Materials and methods


Patients and dentists have been making increasing
Post-and-core systems
demands on the aesthetics of dental restorations and
the biocompatibility of the materials used in recent The objects under study were the post-and-core systems
years. Industry has reacted by introducing several (n ˆ 10 specimens each) listed in Table 1. One of these
innovative post-and-core systems for restoring non- posts was made from a palladium alloy (Perma-dorTM
vital teeth. The objective of the present in-vitro study post*) [A]. Three posts were made of a non-palladium
was to compare the fracture characteristics of seven alloy (Perma-dorTM twin* [B]/ER platinum/iridium
different endodontic post systems under monoton- post² [C]/Endo-CoreTM Pt±Ir system/non-palladium
ously increasing loads to those of Perma-dorTM posts, post³ [D]). The non-metallic post systems examined
whose suitability had been demonstrated in an earlier included ER CerapostTM (yttrium-stabilized zirconia
clinical study (Ottl & Lauer, 1998), and to root-®lled ceramics²) [E], an aluminium oxide post-and-core
test teeth. copy-milled from a pre-fabricated block (Lauer, 1996)

*Degussa, Hanau, Germany.


²
Komet, Lemgo, Germany.
³
Metalor, NeuchaÃtel, Switzerland.

ã 2002 Blackwell Science Ltd 175


176 P . O T T L et al.

Table 1. Post-and-core systems examined

Endodontic post system Manufacturer Core Manufacturer


TM
Metal post with palladium Perma-dor Degussa Phantom alloy Degussa
Metal posts without palladium Perma-dorTM twin Degussa Phantom alloy Degussa
ER platinum/iridium post Komet Phantom alloy Degussa
Endo-CoreTM Pt±Ir system/non-palladium Metalor Phantom alloy Degussa
Ceramic posts ER CerapostTM (zirconia ceramics) Komet Clear®lTM Core Kuraray
Alumina blank/CelayTM procedure Vita/Mikrona Alumina blank/ Vita/Mikrona
(aluminium oxide ceramics) CelayTM procedure
Metal post/ceramic core Perma-dorTM Degussa SMH Ducera
Shoulder ceramics
Carbon ®bre post ComposipostTM ( ˆ C-Post) RTD/Hahnenkratt/ Clear®lTM Core Kuraray
Bisco

(Fig. 1) (CelayTM Alumina Blank AB-28§/CelayTM pro-


cess¶) [F] and the carbon ®bre post ComposipostTM
(RTD**) (identical with the C-PostTM²²) [G]. Cores made
from a ®rable alloy, Deva 4TM* were cast to 10 additional
Perma-dorTM posts and then built up in shoulder ceram-
ics (SMH³³) [H] in the area of the post head. The posts
selected were of comparable size, with the Perma-dorTM
post (medium size) serving as reference. Material data
and the dimensions (diameter, length) of the post
systems used are shown in Tables 2a and b.
The cores (Table 1) for post systems A±D (metal alloy)
were pre-formed in wax to identical size using a
template and cast to the posts in a phantom alloy*.
The same template was used to create plastic cores
made of a self-curing composite, Clear®lTM Core§§, for
posts E and G. The core for the Perma-dorTM post
(medium size), made of Celay-TechTM resin¶, was
modelled in the same manner. Finally, the entire
post-and-core setup was copy-milled from an alumin-
ium oxide block using the Celay system (Fig. 1).

Test teeth

The reference was an upper central incisor whose


dimensions corresponded to the average dimensions as
determined by Kraus et al. (1988). Three templates of
this tooth were made from the transparent PalapressTM
resin¶¶ in order to produce precisely identical roots,
Fig. 1. Aluminium oxide ceramics post-and-core during copy
cores and crowns. milling (CelayTM process) from a pre-fabricated ceramic block
§
Vita Zahnfabrik, Bad SaÈckingen, Germany. (CelayTM Alumina Blank AB-28).

Mikrona, Spreitenbach, Switzerland.
**St EgreÁve, France/Hahnenkratt, KoÈnigsbach-Stein, Germany.
²²
The EstiluxTM posterior VS posterior composite¶¶,
Bisco, Schaumburg, IL, USA.
³³
Ducera Dental, Rosbach, Germany
whose module of elasticity (16 400 ‹ 1000 MPa)
§§
Kuraray, Osaka, Japan. (Heraeus Kulzer, 1994) corresponds to that of dentine
¶¶
Heraeus Kulzer, Wehrheim, Germany. (14 000±18 000 MPa) (van Zeghbroeck, 1995), was

ã 2002 Blackwell Science Ltd, Journal of Oral Rehabilitation 29; 175±183


FRACTURE CHARACTERISTICS OF ENDODONTIC POST SYSTEMS 177

Table 2a. Material data and dimensions for the endodontic post systems examined (manufacturer data)

System Perma-dorTM Perma-dorTM twin ER Pt±Ir Endo-CoreTM Pt±Ir

Order no. medium medium 207L12 (ISO 90) A 13á608


Composition Au 60á0 Au 40á0 Pt 80á0 Pt 85á0
(per cent by mass) Pt 24á9 Pt 60á0 Ir 20á0 Ir 15á0
Pd 15á0
Ir 0á1
Module of elasticity (MPa) 118 000 121 000 200 000 150 000

Shape Cylindrical±conical Cylindrical±conical Cylindrical±conical Cylindrical±conical


Total length (mm) 15á0 15á0 15á0 15á0
Coronal diameter (mm) 1á6 1á6 1á8 1á6
Tip diameter (mm) 1á1 1á1 0á9 0á9

ER Pt±Ir ˆ ER platinum/iridium post; Endo-CoreTM Pt±Ir ˆ Endo-CoreTM Pt±Ir system/non-palladium post.

Table 2b. Material data and dimensions for the endodontic post systems examined (manufacturer data)

System CerapostTM CelayTM Alumina ComposipostTM

Order no. 232L12 (ISO 90) Al2O3 100á0* 70á312


Composition ZrO2 > 94á0 Carbon ®bres 64á0
(per cent by mass) Y2O3 5á2 Epoxy matrix
Module of elasticity (MPa) 200 000 240 000 21 000
Shape Cylindrical±conical Cylindrical±conical Cylindrical±conical (two-level)
Total length (mm) 22á0 9á0² 20á0
Coronal diameter (mm) 1á8 1á6 1á8
Tip diameter (mm) 0á9 1á1 1á2

*Original for copying the root portion corresponds to Perma-dorTM medium.


²
Figures for root portion of the post (measured from the bottom of the access cavity).

used for manufacturing the roots (DentacolorTM XS margin was not at the same level as the core margin but
polymerization light¶¶). Control radiographs were used ended approximately 1 mm further cervically in a
to examine the arti®cial roots for porosities. On account chamfer (ferrule design).
of the high hardness of the composite, identical and All posts were conditioned using the RocatecTM
well-®tting root canals were prepared by inserting the process*** and then cemented in place inside the roots
respective post centrally into the non-polymerized using a self-curing composite (PanaviaTM 21 TC§§). The
composite using a positioning stent. After polymeriza- crowns were then cemented on the roots with the
tion and removal of the isolated post, the ®nal root same material. While inserting the posts or crowns, an
canal preparation for all post systems was extended to a axial load of 5 kg was applied for 10 min. Until the
length of 9 mm relative to the bottom of the access fracture load test, the specimens were stored at 100%
cavity, using the endodontic drill for the respective humidity for 24 h.
system and a parallel milling device (F 1*). The same The control group in this study consisted of root-®lled
instrument was used to prepare a standardized oval tooth specimens (EstiluxTM posterior VS) without end-
access cavity at the root canal aperture with an odontic posts that also received crowns as described
orovestibular length of 3 mm, a mesio-distal width of above. The preparation diameter corresponded to a
2 mm, and a depth of 2 mm. medium-size Perma-dorTM post. The ®lling method
An additional template was used to shape standard-
ized full crowns for all post systems from wax, which
were subsequently cast in phantom alloy. The crown ***Espe, Seefeld, Germany.

ã 2002 Blackwell Science Ltd, Journal of Oral Rehabilitation 29; 175±183


178 P . O T T L et al.

and dimension. A tin foil 0á9 mm in thickness was


af®xed to the palatal surface of the crowns to
avoid concentrations of tension as the force was
applied. Test teeth were loaded at a crosshead speed
of 0á5 mm min±1 at a monotonously increasing force
until root fracture. The progress of the trial was traced
by a hysteresis. At the end of each test, the fracture
load was determined, and the distance between the
point of force application and the upper end of the
fracture gap on the palatal and vestibular root surfaces
was measured with a calliper.

Fig. 2. Diagram of the experimental design.


Statistical methods

used was lateral condensation with gutta-percha (100 Measured values were tested for normal distribution
Supra²²²/100 DeTrey White³³³) and a sealant (AH 26 using the Kolmgoroff±Smirnoff test (P £ 0á05). Mul-
silverfree³³³). tiple comparisons of means according to Student±
Newman±Keuls (P £ 0á05) were performed for the
parameters fracture load and distance between point
Loading test
of force application and upper end of the fracture gap
Loading tests were performed on a Zwicki 1120 (palatal or vestibular).
universal testing machine§§§. Test teeth were inserted
in a stainless-steel base directing the force to the
Results
palatal surface of the crowns at an angle of 135°
relative to the long axis of the tooth (Fig. 2). This
Fracture load
angle re¯ects the positions, contacts and loading
characteristics of upper anterior teeth in Class I The fracture loads (Table 3, Fig. 3), of posts made from
occlusion (Lauer et al., 1994). metal alloys ranged from 242á3 ‹ 60á9 N [D] to
The absorptive properties of the desmodontal tissue 300á4 ‹ 70á2 N [C]. The Student±Newman±Keuls test
under load were simulated by embedding the speci- showed no signi®cant differences between these four
men roots in the stainless-steel base (internal socket endodontic post systems. The two ceramic posts differed
shape) using an elastomer material (Permadyne signi®cantly at 300á3 ‹ 89á3 N (CelayTM aluminium
GarantTM***). The teeth were thus ®xated in a
rubber-like environment and exhibited Periotest Table 3. Fracture load of the tested post-and-core systems
values (PeriotestTM¶¶¶) of between 0 and +1. The examined and the control group (n ˆ 10 test teeth each)
thickness of the elastomer layer was approximately
0á2 mm, the average thickness of the desmodontium X s.d. Min Max
(Schroeder, 1986). In addition, the design of the base Post system (N) (N) (N) (N)
and the specimen embedding method followed the Metal posts Perma-dorTM 265á9 47á0 180á2 324á4
biologic width (Ingber et al., 1977), creating a distance Perma-dorTM twin 288á7 91á2 167á2 408á3
of about 3 mm between the crown margin and the ER Pt±Ir 300á4 70á2 146á8 383á4
Endo-CoreTM Pt±Ir 242á3 60á9 138á3 316á7
edge of the arti®cial socket (Fig. 2).
Ceramic posts CerapostTM 193á5 57á0 103á9 302á6
During the test, the test teeth were loaded palatally
CelayTM Alumina 300á3 89á3 155á9 439á8
at 2 mm from the incisal edge using a chisel-shaped Metal post/ Perma-dorTM/ 208á0 67á8 120á0 307á5
steel pin corresponding to a lower incisor in its shape ceramic core Ceramics
²²²
Carbon ®bre post ComposipostTM 312á5 58á8 229á4 449á4
Rocko, Langenau, Germany.
³³³
Control group Root canal ®lling 228á8 35á7 177á0 279á6
Dentsply DeTrey, Konstanz, Germany.
§§§
Zwick, Ulm, Germany. ER Pt±Ir ˆ ER platinum/iridium post; Endo-CoreTM Pt±Ir ˆ Endo-
¶¶¶
Sirona, Bensheim, Germany. CoreTM Pt±Ir system/non-palladium post.

ã 2002 Blackwell Science Ltd, Journal of Oral Rehabilitation 29; 175±183


FRACTURE CHARACTERISTICS OF ENDODONTIC POST SYSTEMS 179

Fig. 3. Mean fracture load for the


post-and-core systems examined and
the control group (n ˆ 10 test teeth
each; ER Pt±Ir ˆ ER platinum/irid-
ium post; Endo-CoreTM
Pt±Ir ˆ Endo-CoreTM Pt±Ir system/
non-palladium post).

oxide post) [F] versus 193á5 ‹ 57á0 N (ER CerapostTM) Table 4. Distance between point of force application and the
[E]. The value for the ceramic-veneered post [H] was upper end of the fracture gap (vestibular) for the post-and-core
systems examined and the control group (n ˆ 10 test teeth each)
208á0 ‹ 67á8 N; for the carbon ®bre ComposipostTM [G]
it was 312á5 ‹ 58á8 N.
X s.d. Min Max
Among the four posts that were identical in dimension
Post system (mm) (mm) (mm) (mm)
(length, diameter) but produced from different materi-
als or combinations of materials (Perma-dorTM [A], Metal posts Perma-dorTM 12á1 1á6 10á2 14á9
Perma-dorTM twin 14á7 2á2 11á1 16á5
Perma-dorTM twin [B], CelayTM aluminium oxide post
ER Pt±Ir 11á7 8á8 10á7 13á5
[F], ceramic-veneered Perma-dorTM post [H]), signi®- Endo-CoreTM Pt±Ir 12á9 1á7 10á6 15á0
cant differences existed only between F and H. Ceramic posts CerapostTM 13á2 1á9 10á8 15á9
The Student±Newman±Keuls comparison of the CelayTM Alumina 11á6 2á2 10á1 17á2
means for the ER CerapostTM and the ER platinum/ Metal post/ Perma-dorTM/ 14á0 1á9 11á4 17á3
ceramic core Ceramics
iridium post, both of which also had identical dimen-
Carbon ®bre post ComposipostTM 12á4 2á0 9á3 15á4
sions, yielded a signi®cant advantage for the metal alloy. Control group Root canal ®lling 10á1 2á3 6á1 13á7
The fracture load for the control group [I] was
228á8 ‹ 35á7 N. This group was not signi®cantly differ- ER Pt±Ir ˆ ER platinum/iridium post; Endo-CoreTM Pt±Ir ˆ Endo-
CoreTM Pt±Ir system/non-palladium endodontic post.
ent from the eight groups with endodontic posts with
regard to fracture load.

(control group) and 14á7 ‹ 1á2 mm (Perma-dorTM twin)


Distance between point of force application and upper end
(Table 4, Fig. 4). The distance from the palatal end of
of the fracture gap
the fracture gap was between 14á0 ‹ 2á7 mm (CelayTM
Qualitatively, the positions of the fracture lines in aluminium oxide post) and 17á7 ‹ 1á8 mm (Perma-
the test roots were similar for all eight endodontic dorTM twin) (Table 5, Fig. 5).
post systems as well as the control group. The No fracture in the crown area (crown margin, contact
characteristic oblique shear fracture started palatally area of the plastic ®lling respective core buildup
between the lower and middle third of the root and material) was seen in any of the 90 test teeth.
ran in a slightly ascending curve to the opposite root Statistical analysis of the data showed signi®cant
surface. differences between the control group (root-®lled test
At a total tooth length of 23 mm, the distance teeth) and posts B, D, E, H (distance between point of
between the point of force application and the vestibular force application and upper end of the fracture gap,
end of the fracture gap was between 10á1 ‹ 2á3 mm vestibular) and post B (distance between point of

ã 2002 Blackwell Science Ltd, Journal of Oral Rehabilitation 29; 175±183


180 P . O T T L et al.

Fig. 4. Mean distance between the


point of force application and the
upper end of the fracture gap
(vestibular) for the post-and-core
systems examined and the control
group (n ˆ 10 test teeth each; ER
Pt±Ir ˆ ER platinum/iridium post;
Endo-CoreTM Pt±Ir ˆ Endo-CoreTM
Pt±Ir system/non-palladium post).

Table 5. Distance between the point of the force application and why our tests used arti®cial test teeth (Milot & Stein,
the upper end of the fracture gap (palatal) for the post-and-core 1992; Lauer et al., 1994) to reduce the in¯uence of
systems examined and the control group (n ˆ 10 test teeth each)
these interindividual differences on measurements.
With regard to their own and other authors' compar-
X s.d. Min Max
Post system (mm) (mm) (mm) (mm)
able in-vitro studies, Heydecke et al. (1999) arrived at
the conclusion that the use of natural teeth for
Metal posts Perma-dorTM 16á3 1á9 14á2 19á4
determining fracture loads may result in standard
Perma-dorTM twin 17á7 1á8 14á6 19á5
deviations of up to 50%. The present study, by contrast,
ER Pt±Ir 16á0 0á8 14á4 16á8
Endo-CoreTM Pt±Ir 14á7 1á2 13á2 17á6 shows standard deviations for fracture loads between
Ceramic posts CerapostTM 15á3 3á3 6á4 17á8 15á6 and 32á6%.
CelayTM Alumina 14á0 2á7 7á8 18á5 Moreover, the root canals were not prepared manu-
Metal posts/ Perma-dorTM/ 16á4 0á9 15á0 17á4 ally but on a parallel milling device using a positioning
ceramic core Ceramics
stent. This ensured a reproducible root canal prepar-
Carbon ®bre post ComposipostTM 17á0 1á4 14á0 18á2
Control group Root canal ®lling 14á6 3á4 9á6 18á2 ation and a good ®t for the various endodontic posts in
all 90 teeth. Moreover, posts of comparable size were
ER Pt±Ir ˆ ER platinum/iridium post; Endo-CoreTM Pt±Ir ˆ Endo-
selected for the various systems and inserted to the
CoreTM Pt±Ir system/non-palladium endodontic post.
same depth.
The testing protocol allows relative comparison of the
force application ± upper end of the fracture gap, results obtained for the eight endodontic post systems
palatal). with regard to fracture load and fracture position. It
would not be appropriate, however, to simply transfer
these absolute values to clinical situations, as it is not
Discussion
possible to achieve an exact physical simulation of the
Most studies of mechanical loading of post-and-core material compound created by connecting silanized
systems have used extracted human teeth. These teeth, posts adhesively to natural dentine (Mendoza et al.,
even if stringent selection criteria are applied, vary with 1997; O'Keefe et al., 2000). Nor can the arti®cial roots
regard to tooth length, bucco-lingual and mesio-distal used simulate the microstructure of natural dentine, a
dimensions, size and location of pulp chamber and root structure that is important from a biomechanical point
canal, water content, degree of calci®cation, and pre- of view. With natural test teeth one would regularly
existing cracks in the hard tissues (Kantor & Pines, expect higher fracture loads than with arti®cial roots
1977; Trope et al., 1985; McDonald et al., 1990). This is (Strub et al., 2000). In an in-vitro study with a study

ã 2002 Blackwell Science Ltd, Journal of Oral Rehabilitation 29; 175±183


FRACTURE CHARACTERISTICS OF ENDODONTIC POST SYSTEMS 181

Fig. 5. Mean distance between the


point of force application and the
upper end of the fracture gap
(palatal) for the post-and-core
systems examined and the control
group (n ˆ 10 test teeth each; ER
Pt±Ir ˆ ER platinum/iridium post;
Endo-CoreTM Pt±Ir ˆ Endo-CoreTM
Pt±Ir system/non-palladium post).

design similar to ours, Kern et al. (1995) examined surface (from machining with various rotary cutting
crowned natural teeth on cast-to ER Perma-dorTM posts instruments or from polishing) and internally, arising
that, however, had a larger diameter (ISO 110) than the during fabrication. On excessive tension, the ceramic
posts used in our study. They found an average fracture material fails at fault points where the fracture strength
load of 552á5 N. For slip-cast InCeramTM post-and- is locally exceeded. The fracture load differences
cores, an average fracture load of 342á0 N was found by already mentioned may therefore have been caused
those authors. by production related factors and are therefore probably
In our study, the positions of the fracture lines within not because of aluminium oxide ceramics being basic-
the roots were similar, independent of the endodontic ally superior to zirconia ceramics. Generally, industrial
post system examined. The fracture lines were located production of dental ceramics (e.g. CelayTM Alumina
in the central third of the root and sometimes extended Blanks) should be preferred to manual production (e.g.
down to where the apical third of the root begins. The InCeramTM slip cast) in order to minimize the incidence
location of the post tip and the palatal start of the of internal porosities or microcracks.
fracture line were related. The therapy of a root fracture In Perma-dorTM posts modi®ed by a ceramic buildup,
in this area is dif®cult, and the clinical prognosis is the multiple heat treatments when casting a ®rable
unfavourable. metal alloy to the post and when adding the ceramic
Quantitative and statistical comparison of the fracture core may result in embrittlement and consequently to a
loads show that the values for the palladium alloy post reduction in mean fracture loads compared with con-
and the three non-palladium alloy posts are similar. This ventionally processed Perma-dorTM posts. These latter
leads to the conclusion that using metal alloys without require only one heat treatment for casting the metal
palladium has no adverse effects on fracture character- core, and that only at lower temperatures.
istics. The carbon ®bre reinforced posts showed the highest
Comparison of the two ceramic post systems showed fracture loads. Their module of elasticity, which at
signi®cantly higher fracture loads for the copy-milled 21 000 MPa resembles that of natural dentine, seems
aluminium oxide posts. This contradicts the ¯exural to have a positive effect on their biomechanical
strength claims for these materials (yttrium-stabilized characteristics (Isidor et al., 1996). In the present
zirconia ceramics: 820 MPa; pre-fabricated aluminium study, the dentine (module of elasticity: 14 000±
oxide ceramics after glass in®ltration: approximately 18 000 MPa) was simulated by a suitably chosen
500 MPa). The material characteristics of ceramics composite resin (module of elasticity: 16 400 MPa)
under load are determined by the number, size and for the test teeth. When bending stress is applied to
statistical distribution (Weibull) of `faults' at their this compound material system consisting of tooth,

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182 P . O T T L et al.

endodontic post and luting composite, a very rigid post The mentioned maximum jaw closing forces consti-
(with a high module of elasticity) will no longer follow tute extreme loads such as those present in bruxism.
the elastic deformation of the tooth beyond a given They are considerably higher than the bite forces
force. Leverage tends to convert originally full-area present in the oral cavity under physiological condi-
contacts between the post and the canal walls to point tions that affect incorporated dental materials by
contacts, creating localized stress peaks inside the root. exposing them to permanent bending stress. A second
Under adverse circumstances, these stress peaks might study to complement the present study is therefore
eventually lead to system failure, i.e. fracture of the currently under way to examine the in¯uence of
root. With carbon ®bre reinforced posts, large-area changing loads on the mechanical characteristics of
contacts between the post surface and the wall of the endodontic post systems.
root canal continue even when the external load
applied is very high. In addition, the carbon ®bres can
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