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Applications in Engineering Science 6 (2021) 100043

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Applications in Engineering Science


journal homepage: www.elsevier.com/locate/apples

Inverse characterization of UHPC material based on Hopkinson bar test


Mohammad Reza Khosravani
Chair of Solid Mechanics, University of Siegen, Paul-Bonatz-Str. 9-11, Siegen 57068, Germany

a r t i c l e i n f o a b s t r a c t

Keywords: Coupling scientific researches with engineering applications leads to significant increase in development of in-
Inverse method novative materials. Since time-consuming and expensive experimental tests are required for characterization of
Hopkinson bar materials under dynamic loading regime, utilizing inverse characterizations of material has been increased. In
Ultra-high performance concrete
this paper, an effective inverse methodology is proposed and it is utilized to determine dynamic behavior of
Dynamic material properties
cement-based composite material. This inverse procedure is based on the experimental test via split Hopkinson
Material characterization
pressure bar which is one of the most widely used devices in investigation of material response to high rate
loading. In the current study, Holmquist–Johnson–Cook constitutive model is used to present dynamic behavior
of ultra-high performance concrete that is a new generation of concrete and has higher strength compared to
traditional concrete. The reflected and transmitted waves obtained from the experiments are utilized as input in
the inverse procedure. Moreover, genetic algorithm with intergeneration projection is adopted as an inverse oper-
ator to determine inversed parameters. Based on the obtained results, the recommended characterization method
indicates effectiveness in the material characterization. The proposed methodology can accurately estimate the
desired parameters of material under the high strain rates.

1. Introduction a method was presented for characterization of material subjected to


dynamic loading. To this aim, inverse modeling was performed which
There is no doubt that material development play a crucial role in hu- includes finite element analysis of the tension test. It was reported es-
man lives. Indeed, materials science is recognized as one pillar of devel- timated parameters were used to obtain true stress-strain curves. These
opment of modern society and material characterization is an important curves were validated by comparison with experimental results. Later,
aspect of materials science. Currently there are various experimental sci- in (Sedighi et al., 2011) electromagnetic ring expansion test results were
entific techniques for the material characterizations. Thermal investiga- used to identify parameters of the material constitutive model. More in
tions (Kakar et al., 2019), fractographic analysis (Azevedo et al., 2014), deep, the experimental data were processed using a finite element opti-
soft computing (Pichler et al., 2003) and mechanical testing (Khosravani mization procedure. By minimizing the standard deviation of differences
and Weinberg, 2017b) are examples of experimental methods in mate- between calculated stress-strain curves and experimental results, an op-
rial characterization. Due to some difficulties in the experimental tests, timal set of material constants was obtained. Recently, in (Lattanzi et al.,
utilizing non-experimental methods in material characterization has sig- 2020) inverse identification strategies were used to identify constitu-
nificantly increased (Altenbach and Eremeyev, 2014; Chi et al., 2017; tive parameters of material. To this aim, researchers used heterogeneous
Jin et al., 2002; Pucci et al., 2019). Different methods based on nu- full-field strain data and virtual fields method as an inverse technique.
merical simulations and artificial intelligence techniques have been de- Moreover, they used numerical data for validation. Considering com-
veloped in mechanical engineering over the years (Anghelescu et al., parison of identification results and the standard calibration process, it
2019; Bigoni et al., 2008; Chisari et al., 2015; Fraternali, 2007; Jordan is documented that proposed method is appropriate for identification
and Christov, 2005; Lefik and b. A. Schrefler, 2003; Nasiri et al., 2017; the material properties. In several studies high speed imaging was used
Poltronieri et al., 2014). However, because of complexity in materials for material calibration under high rate of loading (Avachat and Zhouo,
and their behavior, some characterization methods need a large compu- 2015; Chiappini et al., 2017; Parab et al., 2019; Rossi et al., 2008; Sasso
tation time. et al., 2015; Xing et al., 2018). For example, in (Sasso et al., 2015) a
Literature investigation indicated that inverse characterization of fast and effective method was proposed to calibrate constitutive model
different materials under dynamic loading have been performed over in characterization of an aluminum alloy. To this aim, the profile of the
the years (Kajberg and Lindkvist, 2004; Kajberg and Wikman, 2007; test coupon was post-processed and deformation history was derived.
Sedighi et al., 2010). For instance, in (Kajberg and Lindkvist, 2004) In experimental practice, a series of compression and tension tests was
conducted under high rate of loading. The obtained coefficients form
the proposed method, were compared to simulation results and a good
E-mail address: mohammadreza.khosravani@uni-siegen.de agreement was documented.

https://doi.org/10.1016/j.apples.2021.100043
Received 15 October 2020; Received in revised form 22 February 2021; Accepted 2 April 2021
Available online 15 April 2021
2666-4968/© 2021 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license
(http://creativecommons.org/licenses/by-nc-nd/4.0/)
M.R. Khosravani Applications in Engineering Science 6 (2021) 100043

In work (Messineo et al., 2016), an inverse estimation methodol- In the proposed method, reflected and transmitted waves obtained from
ogy was employed to characterize a layered material. In this context, the SHPB test are used as input, and the optimum set of material pa-
the researchers utilized inverse problem theory to identify mechanical rameters is determined by optimization procedure. The rest of this pa-
properties of a three layers material. Indeed, it was planned to use the per is structured as follows: next section describes material properties
proposed method in order to estimate acoustic impedance and transit identification. In Section 3 forward problem and sensitivity analysis are
time which are related to the mechanical properties such as density and outlined. The obtained results are mentioned in Section 4. Finally, the
elastic modulus. In detail, error between experimental results and the main conclusions are presented in Section 5.
waveform was determined from an equivalent model. Based on the re-
sults, it was claimed that the proposed method estimated desired pa-
rameters accurately, with error within an acceptable range. Later, in
(Nightingale and Labrosse, 2018) an inverse finite element method is 2. Material properties identification
utilized for characterization of a biomaterial. To this aim, the researches
developed an inverse methodology in MATLAB and used previous stress- 2.1. Inverse material characterization
strain data in conjunction with finite element results, and optimize the
parameters. Based on the obtained results, efficiency of the proposed When material parameters are unknown, and experimental tests can
method is documented. However, the inverse methodology can be used be performed to determine behavior of material, solving the equations
for characterization of a wide range of materials. can describe the material parameters. Due to this, the mathematical
Concrete is the most widely used building material in the world procedure is called inverse solution of material characterization. In the
(Randle et al., 2014), and its composition has been significantly mod- inverse material characterization, it is needed to utilize experimental
ified throughout history. However, several engineering demands have results such as force, displacement, and strain. Moreover, integrated ap-
led to technical development of different concretes. Ultra-high perfor- proaches must be used and experimental results should be combined
mance concrete (UHPC) is a relatively new generation of concrete which with numerical methods in order to recover the parameters. With this
exhibits preferable mechanical properties and unique responses un- procedure the parameters can be recovered by minimizing an objective
der various loading regimes compared to traditional concrete. Cement- function. As the finite element analysis usually is used for the numerical
based materials like UHPC, asphalt concrete, and reinforced concrete models, attempts should be done to reduce computational cost (Schmidt
are complex in their response characterization (Krishnan and Rajagopal, et al., 2015). In (Grediac et al., 2002) and (Pierron et al., 2007), al-
2003; Silva et al., 2019). Although numerous studies investigated me- ternative approaches have been developed to improve computational
chanical properties of UHPC with different recipes, UHPC material char- efficiency of material characterization, but as utilizing finite element
acterization is a current research topic in today’s research world (Tong simulation is avoided, some disadvantages are observed.
et al., 2020; Xie et al., 2019; Zhang et al., 2020). Indeed, several prop- In this work, a model has been considered which is widely used
erties such as flexural behavior, blast resistance, and fatigue behavior in analysis of problem under dynamic loading regime. The Holmquist–
of UHPC have been studied in the past years. Since structural elements Johnson–Cook (HJC) constitutive model (Holmquist et al., 1993) is one
made of UHPC experience dynamic loading during their lifetime, char- of the most popular material models which can be used for materials un-
acterization of this engineering cementitious material under this type der dynamic loading and it has been used in various researches (Brown
of loading have been performed in previous studies (Astarlioglu and et al., 2017; Hou et al., 2018). Previous successful researches (Fing and
Krauthammer, 2014; Hassan and Wille, 2018; Khosravani et al., 2019; Zhang, 2013; Kristoffersen et al., 2019; Mirone et al., 2019a; Qu et al.,
Wu et al., 2017). Here, the term ”dynamic loading” refers to ”high strain 2016) which used HJC model to study different concrete materials un-
rate”. Since behavior of brittle composites and concrete-like materials der high strain rates, confirmed that the HJC model is a suitable method
are complicated by a combination of brittleness and micro fracture, in the numerical study of UHPC material under test via SHPB. In detail,
accurate experimental test is required to obtain response of material the HJC model is connected by three different parts: power hardening
under dynamic loading (Bahei-El-Din and Zikry, 2003; Pearson et al., law is shown by the first multiplicative term. This part is utilized to
2007). For this loading scenario, split Hopkinson pressure bar (SHPB) describe metallic hardening functions in quasi-static modeling contexts.
has been widely used for various materials including: cement-based ma- The second term indicates the natural logarithmic dependence on the
terials (Khosravani et al., 2018; Li et al., 2020), biomedical materials dimensionless equivalent plastic strain rate. The last term referred to
(Khosravani, 2019; Trexler et al., 2011), metals (Galvez et al., 2009; the power dependence on the homologous temperature. In this term,
Mirone et al., 2019b), composites (Kumar and Naik, 2018; Periasamy the current temperature is considered as the reference temperature
and Tippur, 2012), adhesively bonded joints (He and Ge, 2017; Sassi In the present study, HJC constitutive model is utilized, and the ma-
et al., 2018), and ceramics (Li et al., 2015; Luan et al., 2018). The test terial characterization is performed in four steps as follows: (a) A series
via SHPB is the popular method to investigate the mechanical properties of experimental tests via SHPB are conducted on the UHPC specimens.
of materials at medium and high strain rates (Khosravani and Weinberg, (b) The reflected and transmitted waves obtained from experimental
2017a). Although Hopkinson bars have been employed in numerous re- practices are saved and used as input in the inverse procedure. (c) A
searches, this experimental practice is a challenging task regarding to finite element model of the dynamic load on UHPC is implemented in
the impedance properties and the difficulty to achieve a dynamic equi- ABAQUS software, and a set of trial material parameters is utilized. The
librium. Literature investigations indicated that due to some uncertain- simulation results are obtained with respect to the assumed parame-
ties in measured stress in the experimental tests, material parameters are ters. (d) The problem of UHPC parameter identification is transformed
totally different in various experimental data. However, owing to inex- for an optimization, where the deviations of responses of experimental
pensive computing resources, applications of inverse characterization of finding and numerical observation are reduced. In order to solve the
materials by different methods have been increased. optimization problem, the genetic algorithm (GA) with intergeneration
The inverse technique in estimation of material parameters make projection is applied, and parameter sensitivity analysis is performed.
a relationship between experimental findings and material parameters. In Fig. 1 this material characterization is schematically illustrated.
The present paper aims to clarify the importance of the inverse method- In engineering analysis, numerical modeling as an alternative to ex-
ology in regards to characterization of UHPC material. It is a step to- perimental investigation have been widely used, but usually there are
wards for better prediction of UHPC behavior under dynamic loading differences between the experimental finding and numerical results. In
by finding a linkage between simulation and experimental practice for this regard, optimization process can be employed to minimize the de-
inverse characterization of material. In this study, inverse method is em- viations of results achieved by experiments and finite element simula-
ployed to determine parameters of UHPC under high strain rate loading. tions. The objective function of optimization problem can be expressed

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M.R. Khosravani Applications in Engineering Science 6 (2021) 100043

Input Fig. 1. Schematic description of computa-


tional procedure for UHPC characterization
based on SHPB test.

I R T

Experimental findings Output

Trial Genetic Optimum


parameters Algorithm parameters

Simulation results

Fig. 2. A schematic of split Hopkinson pressure bar (Khosravani, 2018).

as follows: Moreover, a data acquisition system is utilized to record the experimen-


𝑛
∑ tal data. The specimen must be placed between the bars, and the impact
exp
𝑓 (𝑥) = ∥ 𝜎𝑖 − 𝜎𝑖sim (𝑥) ∥2 (1) of the striker on the incident bar induces a longitudinal compressive
𝑖=1 wave which travels through the incident bar. Some part of the pulse
exp
where 𝑓 (𝑥) is an estimated function which represents sum of errors, 𝜎𝑖 propagates on the transmission bar and the rest back to the incident bar
and 𝜎𝑖sim refer to obtained response of materials measured in experiment at the interface. A schematic of SHPB is illustrated in Fig. 2.
and simulation, respectively. Moreover, 𝑥 and 𝑛 are an inversed param- It should be noted that, experiment via SHPB is based on several
eter vector and number of data point, respectively. It shows summation assumption. It is assumed that the bars are linear, isotropic and free
over each data point in the time history of the strain signals. of wave dispersion effects during loading. Moreover, the specimen is
assumed to be in dynamic force equilibrium, with equal force imposed
2.2. Experimental test via SHPB at both specimen-bar interfaces. The stress (𝜎), strain (𝜀) and strain rate
(𝜀̇ ) on the specimen as a function of time are respectively calculated by:
The non-linear behavior of UHPC material until the failure is a com-
𝐸𝐴𝑏
plicated theme, especially in high strain rates. In this regard, SHPB is the 𝜎(𝑡) = 𝜀 (𝑡) (2)
most widely used method to run experiments under high rate of loading 𝐴𝑠 𝑇
(e.g., tensile, compressive and torsional dynamic loads). In (Khosravani 𝑡
2𝑐0
and Weinberg, 2018) a comprehensive review on usage of SHPB in char- 𝜖(𝑡) = 𝜀 (𝑡)𝑑𝑡 (3)
𝑙𝑠 ∫0 𝑅
acterization of cementitious materials under dynamic loading regime
is presented. A traditional SHPB consists of a gas gun, a striker, inci- 2𝑐0
𝜀̇ (𝑡) = 𝜀 (𝑡) (4)
dent bar, transmission bar, and a damper at the end of transmission bar. 𝑙𝑠 𝑅

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M.R. Khosravani Applications in Engineering Science 6 (2021) 100043

Fig. 3. A circular UHPC specimen under dynamic


loading conditions via SHPB.

Fig. 4. A typical strain history of a test via SHPB.

where 𝐴𝑏 and 𝐴𝑠 are the cross-sectional area of the bar and the specimen, with a resistance of 120.0±0.1Ω and a sensitivity coefficient of 2.14±1%.
respectively. Also, 𝐸, 𝑙𝑠 and 𝑐0 show elastic modulus, specimen length Here, experiments were conducted under different velocities of striker
and the wave speed in the bar, respectively. The subscripts 𝑇 and 𝑅 which led to strain rates of 30 s−1 and 95 s−1 . In a well-defined strain
represent transmitted and reflected waves. rate, the incident pulse reaches to its maximum with a long rise time. In
In the current study, dynamic Brazilian tests on UHPC circular spec- several studies, researchers suggested utilizing pulse shaper in st espe-
imens are performed. In detail, two aluminum bars with diameter of cially for brittle materials Hopkinson bar test (Frew et al., 2002; Pang
20 mm and length of 1800 mm are used as incident and transmission et al., 2019; Weinberg et al., 2018). It is noteworthy that, we have used
bar. The impact of an aluminum striker with length of 100 mm gener- paper and aluminum paper as pulse shaper. The pulse shaper with a
ates a pulse that propagates through the bars. The examined specimens thickness of 0.8 mm was attached to the aluminum incident bar. The
with a thickness of 15 mm and diameter of 50 mm are constructed by pulse shaper increased the incident stress wave rising time, which has
filling the material into the designed mold. In Fig. 3 a circular UHPC led to an increase in the loading time. In Fig. 4 the full strain history of
specimen located between the bars before impact test on SHPB is illus- test under strain rate of 95 s−1 without using pulse shaper is depicted.
trated. Dynamic tensile strength and dynamic elastic modulus of material can
In the experimental practice, the strain is measured by means of be obtained by dynamic Brazilian test via SHPB. Mechanical properties
strain gauges placed in the middle of the incident and transmission bars such as impact strength and tensile resistance under dynamic loading

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M.R. Khosravani Applications in Engineering Science 6 (2021) 100043

Fig. 5. Typical pictures of a Brazilian specimen during its failure process.

Fig. 6. Fractured UHPC circular specimens.

Fig. 7. Stress-strain curve (left), and stress-time of examined UHPC specimen under strain rate of 30 s−1 (right).

are hard to obtain under reproducible conditions. In the current study, tained from the tests, as the cracks were observed at the same position
comparison of the response curves at each strain rate, confirmed that in every test.
the conducted tests indicated reproducible results.
The experimental observations showed that the crack is initiated in 2.3. Numerical simulations
the center of the specimen and growth along the loading diameter direc-
tion until the specimen was split into two halves. Brazilian test is valid For numerical simulations, the commercial finite element software
only when crack initiated at the center of the specimen (Rastiello et al., ABAQUS was used and explicit numerical method was utilized for as it
2018). In the current study, this issue is confirmed by analysis of the can effectively handle nonlinear behavior. In this study, the 3D finite
movies recorded by a high speed camera. Fig. 5 shows crack propaga- element model includes the incident bar, circular specimen and trans-
tion in a Brazilian specimen at different instants of time. mission bar was established. As in experimental test, the striker is only
After crack initiation in center of the specimen, it propagates along utilized to generate stress wave, it is not necessary to model this part
the loading diameter and towards the two ends till final fracture. In in the numerical simulation. In this regard, a stress wave is imposed
Fig. 6 fractured specimens are illustrated. Later, crack initiation and its on finite element modeling of the incident bar. It should be noted that
propagation are illustrated in simulation results (see Fig. 9). the stress wave at the middle of the incident bar is considered as the
In Fig. 7 stress-strain curve and stress versus time history are illus- reference incident waveform in the finite element simulation.
trated. Both curves are obtained from the experiment under strain rate The geometries of the bars and specimen are the same as experimen-
of 30 s−1 . It is worthwhile to note that reproducible results were ob- tal tests. In order to reduce computation cost, elements with different

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M.R. Khosravani Applications in Engineering Science 6 (2021) 100043

Fig. 8. Finite element model of the specimen placed


between the bars.

sizes were used for bars and specimen. For the incident and transmitted Table 1
bars density of 2700 kg/m3 and elastic modulus of 68.9 GPa are con- Experimental and numerical results of studied the circular UHPC specimens.
sidered. It should be mentioned that material properties and boundary Specimen No. 𝐹max [kN] 𝜎exp [MPa] 𝜎sim [MPa]
conditions were kept same as experimental tests. In this simulation, the
1 23.1 19.61 21.18
FE model has a total of 82600 hexahedral elements (C3D8R ABAQUS
2 23.8 20.21 18.07
type). Fig. 8 shows FE model of the incident and transmitted bars and 3 23.2 19.71 20.12
circular specimen. 4 22.7 19.27 21.76
In the test via SHPB, the dynamic equilibrium in the specimen should 5 23.1 19.61 20.31
6 22.8 19.63 18.92
be achieved. Since the dynamic equilibrium is an important issue, we
7 22.6 19.19 19.81
have checked this equilibrium in numerical simulation as well. In order 8 23.2 19.71 21.45
to check equilibrium in the UHPC specimen throughout the numerical 9 23.8 20.21 20.72
simulation, we recorded the histories of the resultant forces at both ends 10 22.6 19.19 19.86
of the specimen. In the experimental practice, the forces on either side Avg. 23.09±0.4 19.63 ±0.43 20.22 ±0.52
of the specimen is calculated by:
Table 2
𝐹1 = 𝐸 𝐴𝑏 (𝜀𝐼 + 𝜀𝑅 ) and 𝐹2 = 𝐸 𝐴𝑏 𝜀𝑇 (5)
Dimensions and units of the HJC parameters.
where the indices 1 and 2 refer the specimen-incident bar interface 𝐴: stress [MPa] 𝑁: non-dimensional 𝜀̇ : strain rate [s−1 ]
andthe specimen-transmission bar interface, respectively. There are dif- 𝐵: stress [MPa] 𝐶: non-dimensional 𝑃 : pressure [GPa]
ferent evaluation methods to check equilibrium. For instance, if 𝐹1 = 𝐹2
the specimens is in equilibrium. Moreover, a stress ratio of 𝜎𝑇 ∕𝜎𝐼 + 𝜎𝑅
indicates equilibrium when it approaches one. In the current study, the
high strain rate:
recorded forces at the front and rear specimen-bar interface proved that
[ ][ ]
dynamic equilibrium has been achieved in performed numerical simu- 𝜎 ∗ = 𝐴(1 − 𝐷) + 𝐵𝑃 ∗𝑁 1 + 𝐶 𝑙𝑛 (𝜀̇∗ ) (6)
lations. Fig. 9 shows crack propagation in 2D model at three instances.
where 𝜎 ∗ = 𝜎∕𝑓𝑐 and 𝑃 ∗ = 𝑃 ∕𝑓𝑐 are the normalized equivalent stress
As can be seen, there are similar number of elements at the both ends of
and the normalized pressure, respectively. Also, 𝑓𝑐 and 𝜎 are compres-
crack. Moreover, the contour shows similar force at the front and rear
sive strength and actual equivalent stress, respectively. As shown in
specimen-bar interface.
Eq. (6), the HJC model has several constants, 𝐴, 𝐵, and 𝐶 are cohe-
As already mentioned, Brazilian experiment is a valid test only when
sive strength coefficient, pressure coefficient, and strain rate coefficient,
start-split location is at the center of the specimen. As can be seen in
respectively. These material constants and 𝑁 are determined by fitting
Fig. 9, crack is initiated at the center of the specimens and it propagates
the model to experimental data. Moreover, 𝐷 denotes a scalar damage
along the loading directio until failure.
variable. In the current study, we attempt to find HJC parameters: 𝐴,
In Table 1 experimental and numerical results are summarized. In
𝐵, 𝑁 and 𝐶. In Table 2, dimensions and units of the parameters are
the numerical simulation of the incident and transmitted bars, a linear
reported. In HJC model, an elastic-viscoplastic constitutive model con-
elastic material constitutive model was utilized.
tains (a) strength criterion, (b) damage evolution and (c) equation of
state (Holmquist et al., 1993). In this regard, there are parameters that
3. Forward problem and sensitivity analysis some of them can be determined by the experiments and the rest must
be obtained in indirect way.
The HJC model, was developed to describe behavior of cement-based • HJC background
material under high strain rates, large strains, and high pressures. Since
effect of strain rate and compression damage are synthetically consid- In computational constitutive models for materials, Johnson, Cook,
ered in this model, it can describe the dynamic behavior of cement- and Holmquist contributed to research on several materials over the
based materials under the conditions of high strain rates very well. The years. Dynamic constitutive models contain complicated parameters of
following equation illustrates a mathematical interpretation of the HJC physical properties and some sensitive coefficients. Here, aforemen-
model which can be used for concrete subjected to high pressure and tioned criteria are briefly presented.

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M.R. Khosravani Applications in Engineering Science 6 (2021) 100043

Fig. 9. Simulated fracture process in UHPC


specimen under Brazilian test.

Fig. 10. The material model of the HJC concrete, equivalent strength model (left), damage failure model (right).

- Strength criterion
The strength equation is expressed in Eq. (6), where 𝜎 ∗ ≤ 𝑆max is
dimensionless equivalent stress, and 𝑆max is the maximum dimensionless
strength of concrete material.
- Damage evolution
In HJC model, damage evolution is expressed as:
∑ Δ𝜀𝑝 + Δ𝜇𝑝
𝐷= (7)
𝜀𝑓𝑝 + 𝜇𝑃𝑓

where Δ𝜀𝑝 and Δ𝜇𝑝 are increments of equivalent plastic strain and plas-
tic volumetric strain, respectively. 𝐷 is the damage degree (0≤D≤1).
Moreover, 𝜀𝑓𝑝 and 𝜇𝑃𝑓 are equivalent plastic strain and plastic volumet-
ric strain under normal pressure. Their summation is the total plastic
strain under a constant pressure until fracture.

𝜀𝑓𝑝 + 𝜇𝑃𝑓 = 𝐷1 (𝑃 ∗ + 𝑇 ∗ )𝐷2 ≥ 𝐸𝐹 𝑀 𝐼 𝑁 (8)

where 𝐷1 and 𝐷2 are the constants of damage related to the examined


material, and 𝐸𝐹 𝑀 𝐼 𝑁 is a material constant which is utilized to sup- Fig. 11. Hydrostatic pressure vs. volumetric strain.
ports fracture from weak tensile waves. Moreover, 𝑇 ∗ is the normalized
tensile strength, 𝑇 ∗ = 𝑇 ∕𝑓𝑐 and 𝑇 is the maximum tensile strength of
material. As it shown in Eq. (7) damage is described by the accumula- where 𝜇 is the modified volumetric strain: 𝜇 = (𝜇 − 𝜇1 )∕(1 + 𝜇1 ), and 𝜇1
tion of equivalent plastic strain and plastic volumetric strain. In Fig. 10 is volume strain. Also, 𝐾1 , 𝐾2 and 𝐾3 are material constants.
an original HJC material model strength and also damage model for
• HJC for characterization of UHPC
cement-based material are illustrated.
- Equation of state In the current study, UHPC specimens were tested under strain rate
In HJC model, the relationship between volume strain and hydro- of 30 s−1 and 95 s−1 , and the hydrostatic pressure volume of material
static pressure of material is described by the three regions. Fig. 11 cannot reach the third region. However, the HJC model is totally empir-
shows hydrostatic pressure and volumetric strain curve. The first region ical, a series of different tests are needed to determine HJC parameters.
(OA) is linear elastic. The second area (AB) is transitional region and As some parameters have negligible effect on the numerical simulation
the air voids of in material should be gradually compressed. The last of SHPB, recommended values in the literature references for the most
region (BC) is compact region and the material should transfer to com- similar UHPC mixture can be used.
pact material without air voids, damaged and then begins to produce In the inverse method of parameter identification, sensitivity of the
destructive cracks (Luo, 2019). 𝜇𝑐𝑟𝑢𝑠ℎ and 𝜇𝑙𝑜𝑐𝑘 are volumetric strain at input vector to the output vector can reduce ill-posedness. It is crucial to
the elastic limit 𝑃𝑐𝑟𝑢𝑠ℎ and at the compacting pressure 𝑃𝑙𝑜𝑐𝑘 , respectively. consider the influence of the inversed parameters on the responses. This
can be conducted via parameter sensitivity analysis based on numerical
𝑃 = 𝐾1 𝜇 + 𝐾2 𝜇 2 + 𝐾3 𝜇 3 (9) simulation. In (Morris, 1991) an approach is proposed to compute the

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M.R. Khosravani Applications in Engineering Science 6 (2021) 100043

Fig. 12. Sensitivity analysis for unknown parameters based on SHPB simulation.

sensitivity. It is an effective method which can be used to determine Table 3


sensitivity of the result with respect to the parameters. In the current Dimensions and possible units of the HJC parameters.
study, the sensitivity analysis is performed in numerical computation at Inversed parameters Initial range Inversed results
a strain rate of 95 s−1 . In this regard, the initial values of the inversed pa-
A [0.1, 1.8] 0.821
rameters are set and for sensitivity analysis another two values are given
B [0.4, 2.0] 1.583
for each parameter. Afterward, the unknown parameters 𝐴, 𝐵, 𝑁 and 𝐶 N [0.1, 1.5] 0.725
are varied independently in the numerical simulations. In this regard, C [0.001, 0.009] 0.007
we used a small MATLAB code and investigated which input variable
is contributing significantly to the output. Based on this investigation,
exp
we documented that value of stress (𝜎𝑖 ) has the most important influ- analysis. The reflected and transmitted waves of experimental practice
ence on the value of output parameters. In Fig. 12 results of sensitivity are used as input of the inverse method. Moreover, in the reflected and
analysis for two parameters 𝐴 and 𝐵 are illustrated. transmitted waves a series of samples points are considered where the
As can be seen the reflected and transmitted wave responses are response is strongly sensitive to the inversed parameters. These points
different and depend on the parameter significantly. It means, the re- are utilized to make the objective function. The inversed procedure
sponses are significantly sensitive to the mentioned three parameters (Fig. 13) is used to determine parameters. The estimated values of ex-
which are here considered as inversed parameters. amined UHPC parameters are presented in Table 3. The obtained results
In the current study, genetic algorithm with intergeneration projec- indicated that the proposed inverse method for parameter identification
tion is employed to minimize the objective function and reduce the re- of UHPC material recommended values within initial range.
quired number of forward analyses. Genetic algorithm with intergenera- In Fig. 14 experimental results and numerical findings which are cali-
tion projection is a robust algorithm which can find the global optimum brated by the described procedure are shown. These curves are achieved
instead of the local optimum for a provided initial range (Liu et al., under strain rate of 95 s−1 . It is noteworthy that experimental input
2002; Yang and Liu, 2010). The details of parameter identification and pulses are used as input strain pulse in the finite element analysis which
inverse procedure are illustrated in Fig. 13. has led to a good agreement between experimental results and com-
It should be pointed out that, for the first guess of the parameters, putational findings. It confirmed reliability of this inverse method in
results of our experimental tests and also researches on similar UHPC parameter estimation. It is assumed that the experimental results repre-
mixture were used and fitting process was performed. As an example, for sent the real behavior of the material under test with specific measuring
strain rate coefficient, slops of the linear fits through the data sets were errors. Therefore, usually there is a difference between experimental
used. Indeed, parameters were estimated from the slope and intercept results and numerical findings. Dynamic Increase Factor (DIF) in the
of the fitted curves. obtained result for a specific strain rate can be compared to the tests
under different strain rates (for similar UHPC mixtures). DIF is ratio of
4. Results the dynamic value to the quasi-static value, which is widely used for
behavior analysis of cement-based material under high rate of loading.
The initial range of the inversed parameters (𝐴, 𝐵, 𝑁 and 𝐶) can For further evaluation of accuracy and precision of the proposed
be set via combining experimental results and the parameter sensitivity method, here R-square coefficient (𝑅2 ) is calculated. 𝑅2 is the absolute

Table 4
HJC constitutive model parameters of studied UHPC.

Parameters Parameters

Density 𝜌 [kg/m ]
3
2382.7 Crushing pressure [MPa] 45.8
Shear modulus 𝐺 [GPa] 17.28 Crushing volumetric strain 2.3 × 10−3
Normalized cohesive strength 𝐴 0.821 Locking pressure [MPa] 7.8 × 102
Normalized pressure hardening 𝐵 1.583 Locking volumetric strain 0.1
Strain rate coefficient 𝐶 0.007 Damage constant 𝐷1 0.04
Pressure hardening exponent 𝑁 0.725 Damage constant 𝐷2 1
Compressive strength 𝑓𝑐 [MPa] 159.6 Pressure constant 𝐾1 [MPa] 8.7 × 104
Tensile hydrostatic pressure 𝑇 [MPa] 8.4 Pressure constant 𝐾2 [GPa] −1.5 × 105
Normalized maximum strength 𝑆max 7 Pressure constant 𝐾3 [GPa] 2.1 × 105

8
M.R. Khosravani Applications in Engineering Science 6 (2021) 100043

Fig. 13. Flowchart of the technique used in this study.

Fig. 14. Experimental results and numerical simula-


tion data (𝜀̇ =95 s−1 ).

fraction of variance of a parameter. Indeed, it denoted reliability of the noted that 𝜎predict and 𝜎experiment are assumed to be equal to 𝜎𝑖sim and
achieved outcomes that replicated by the experiment. The value of 𝑅2 exp
𝜎𝑖 , respectively. According to the obtained values form experimental
is in the range of 0 to 1. The estimated value by the proposed method tests and proposed method under strain rate of 95 s−1 we have obtained
is nearer to the experimental result when 𝑅2 is closer to 1. It can be 𝑅2 =0.8962 which further indicates capability of the inverse method in
determined by: material characterization.
∑𝑁 Here, we present the parameter values of the HJC constitutive model
𝑖=1 (𝜎predict − 𝜎experiment )
2
for examined UHPC material. These values of the inversed parameters 𝐴,
𝑅2 = 1 − ∑𝑁 (10)
𝐵, 𝑁 and 𝐶 are achieved in the current study, and other parameters have
𝑖=1 (𝜎predict )
2
been documented from literature references (Kimberley and Lamberson,
where 𝑁 is the number of test. Moreover, 𝜎predict and 𝜎experiment are 2018). The corresponding model parameters for UHPC specimen are
the predicted value and experimental result, respectively. It should be presented in Table 4.

9
M.R. Khosravani Applications in Engineering Science 6 (2021) 100043

It should be noted that different experimental practices (e.g., uniaxial Bigoni, D., Gei, M., Movchan, A.B., 2008. Dynamics of a prestressed stiff layer on an elastic
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needed to obtain the values presented in Table 4. For instance, static Brown, L.B., Hazell, P.J., Grouch, I.G., Esobedo, J.P., Brwon, A.D., 2017. Computational
uniaxial compressive test is needed to obtain compressive strength (𝑓𝑐 ). and split Hopkinson pressure bar studies on the effect of the jacket during penetration
of an AK47 bullet into ceramic armour. Mater. Des. 119, 47–53.
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for concrete subjected to large strains, high strain rates, and high pressures. In: Pro-
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tween experimental and numerical results was observed. This proves finite-time blow-up of acoustic acceleration waves. J. Sound Vib. 281, 1207–1216.
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dynamic loading via Hopkinson bar. The recorded results proved that by inverse modelling based on in-plane displacement fields. Int. J. Solids Struct. 41,
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ters. This is related to the strain rate dependency of UHPC material, as iments and inverse modelling - speckle measurements and high-speed photography.
this material shows higher compressive strength and tensile strength at Int. J. Solids Struct. 44, 145–164.
Kakar, M.R., Refaa, Z., Worlitschek, J., Stamatiou, A., Partl, M.N., Bueno, M., 2019. Ther-
high strain rate loading. It is worth mentioning that in evaluation of the mal and rheological characterization of bitumen modified withmicroencapsulated
results, not only the experimental and numerical curves are compared, phase change materials. Constr. Build. Mater. 215, 171–179.
but also 𝑅-square coefficient is calculated which indicates accuracy of Khosravani, M.R., 2018. Experimental investigations on the dynamic behavior and frac-
ture of composite materials. University of Siegen, Germany Ph.D. thesis.
the inverse method in material characterization. In the situation where Khosravani, M.R., 2019. Mechanical behavior of restorative dental composites under var-
complicated dynamic experimental results are lacking for the constitu- ious loading conditions. J. Mech. Behav. Biomed. Mater. 93, 151–157.
tive model, the proposed inverse method can be considered as a feasible Khosravani, M.R., Silani, M., Weinberg, K., 2018. Fracture studies of ultra-high perfor-
mance concrete using dynamic Brazilian tests. Theor. Appl. Fract. Mech. 93, 302–310.
choice for determining the parameters. The reported results showed a
Khosravani, M.R., Wagner, P., Froehlich, D., Weinberg, K., 2019. Dynamic fracture in-
great significance application of the inverse methodology in material vestigations of ultra-high performance concrete by spalling tests. Eng. Struct. 201,
characterization. Based on DIF, results of different strain rates for simi- 109844.
Khosravani, M.R., Weinberg, K., 2017. Experimental fracture studies of ultra-high perfor-
lar UHPC mixture can be compared.
mance concrete using Brazilian test by split Hopkinson pressure bar. In: Proceedings
of the 14th International Conference on Fracture, Rhodes, Greece, pp. 59–60.
Declaration of Competing Interest Khosravani, M.R., Weinberg, K., 2017. Experimental investigations of the environmental
effects on stability and integrity of composite sandwich T-joints. Materialwiss. Werk-
stofftech. 48, 753–759.
None. Khosravani, M.R., Weinberg, K., 2018. A review on split Hopkinson bar experiments on
the dynamic characterisation of concrete. Constr. Build. Mater. 190, 1264–1283.
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