Data File C:\CHEM32\...APS 240411\04 ABRIL 2024 HAPS 2024-04-11 16-20-03\240322-03 170ML.

D
Sample Name: 240322-03 170ML

=====================================================================
Acq. Operator : ALEJANDRO Seq. Line : 10
Acq. Instrument : Instrument 1 Location : Vial 32
Injection Date : 4/11/2024 10:36:52 PM Inj : 1
Inj Volume : 2 µl
Acq. Method : C:\CHEM32\1\DATA\240319\04 ABRIL 2024 HAPS 2024-04-11 16-20-03\231009 HAPS.
M
Last changed : 4/4/2024 5:41:17 PM by ALEJANDRO
Analysis Method : C:\CHEM32\1\METHODS\ALEJANDRO AGUAS\HAP\231010 CUANTIFICACION HAPS.M
Last changed : 3/20/2024 9:07:01 AM by ALEJANDRO
FID1 A, Front Signal (1-LABORATO...\HAPS 240411\04 ABRIL 2024 HAPS 2024-04-11 16-20-03\240322-03 170ML.D)
pA
9.209

400

350
11.909

300
12.099 - Acenaftileno

250

200
15.120 - Pentacloronitrobenceno

23.932 - Benzo (k) fluoranteno

150
9.116

12.450 - Acenafteno
9.378 - Naftaleno

18.760 - Pireno

100
11.764
8.680
9.024

9.631
9.612
8.715
8.938

14.186
10.392

13.325
8.986

11.674
10.881
10.936

11.626
8.065

12.004
10.283

11.564

12.969
10.329

11.160
8.792

13.950
11.311

14.602
11.360
10.216

14.087
10.096
9.408

10.771

12.677
13.204
9.542

12.336
10.055
10.517
10.544

13.384
10.592

16.232

22.200
15.343

16.636

22.545

25.893
50 21.953

22.835

24.128
18.502
9.295
8.022

9.778
9.946
9.991
8.322

9.702
8.240
8.274
8.454
8.517
8.556

8 10 12 14 16 18 20 22 24 26 min

=====================================================================
External Standard Report
=====================================================================

Sorted By : Retention Time

Calib. Data Modified : Wednesday, March 20, 2024 9:06:24 AM
Multiplier : 1.0000
Dilution : 1.1800
Use Multiplier & Dilution Factor with ISTDs

Signal 1: FID1 A, Front Signal

RetTime Sig Type Area Amt/Area Amount Grp Name

[min] [pA*s] [mg/L]
-------|--|------|----------|----------|----------|--|---------------
9.378 1 VV 18.95511 2.55205e-4 5.70818e-3 Naftaleno
12.099 1 VB 173.64595 2.91302e-4 5.96884e-2 Acenaftileno
12.450 1 VV 10.35684 2.80158e-4 3.42384e-3 Acenafteno
13.478 1 - - - Fluoreno
15.120 1 BB +I 1.34066 0.00000 0.00000 Pentacloronitrobenceno
15.541 1 - - - Fenantreno
15.656 1 - - - Antraceno
18.250 1 - - - Fluoranteno

Instrument 1 4/12/2024 9:34:19 AM ALEJANDRO Page 1 of 2

Data File C:\CHEM32\...APS 240411\04 ABRIL 2024 HAPS 2024-04-11 16-20-03\240322-03 170ML.D
Sample Name: 240322-03 170ML

RetTime Sig Type Area Amt/Area Amount Grp Name

[min] [pA*s] [mg/L]
-------|--|------|----------|----------|----------|--|---------------
18.760 1 BB 1.12601 1.17478e-3 1.56092e-3 Pireno
21.588 1 - - - Ben (a) antraceno
21.668 1 - - - Criseno
23.932 1 BB 3.96489 7.57981e-4 3.54627e-3 Benzo (k) fluoranteno
24.018 1 - - - Benzo (a) pireno
24.610 1 - - - Benzo (b) fluoranteno
26.679 1 - - - Indeno (1,2,3-cd) pireno
26.726 1 - - - Dibenz (a,h) antraceno
27.116 1 - - - Benzo (g,h,i) perileno

Totals : 7.39276e-2

2 Warnings or Errors :

Warning : Calibrated compound(s) not found

Warning : Negative results set to zero (cal. curve intercept), (Pentacloronitrobenceno)

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Summed Peaks Report
=====================================================================

=====================================================================
Final Summed Peaks Report
=====================================================================

Name Sig Total Area Amount

[pA*s] [mg/L]
---------------|---|----------|----------|
Naftaleno 1 18.95511 5.708e-3
Acenaftileno 1 173.64595 0.0597
Acenafteno 1 10.35684 3.424e-3
Fluoreno 1 0.00000 0.0000
Pentacloronitro 1 1.34066 0.0000
Fenantreno 1 0.00000 0.0000
Antraceno 1 0.00000 0.0000
Fluoranteno 1 0.00000 0.0000
Pireno 1 1.12601 1.561e-3
Ben (a) antrace 1 0.00000 0.0000
Criseno 1 0.00000 0.0000
Benzo (k) fluor 1 3.96489 3.546e-3
Benzo (a) piren 1 0.00000 0.0000
Benzo (b) fluor 1 0.00000 0.0000
Indeno (1,2,3-c 1 0.00000 0.0000
Dibenz (a,h) an 1 0.00000 0.0000
Benzo (g,h,i) p 1 0.00000 0.0000

Totals : 7.3928e-2

Compound-related custom fields:

*** End of Report ***

Instrument 1 4/12/2024 9:34:19 AM ALEJANDRO Page 2 of 2