H-No 8a 8b 8c 8d

Triazole C-H 7.77, s

H-2 & H-6 7.68, d, J=
Benzamide
H-3 & H-5 6.96, d, J=
Benzamide
N-H amide 6.07, t , J =
H-1 galactopyranose 5.47, d, J=
5.21 (s, 2H)
H-3 and H-6b galactopyranose 4.61, m
H-5 galactopyranose 4.42 (dd, J= and
H-2 galactopyranose 4.30, dd, J= 4.8 and 2.5-,
H-4 and H-6a galactopyranose 4.15, m
CO-CH2- amide alkyl chain 3.38 (q, J=
CO-CH2-CH2- amide alkyl chain 1.56, pentate, J=
CH3 x 4 isopropylidine 1.45, 1.33, 1.32, 1.25, each
s
amide alkyl chain CH2 x 10 1.68, 1.22, broad singlet
alkyl chain terminal CH3 0.84 (t, J=
 13
C-NMR (CDCl3, 125 MHz)  ppm:

C-No 8a 8b 8c 8d
(NH-C=O) 166.9
Galactopyranoside
C-1 96.2
C-2 70.3
C-3 70.7
C-4 71.1
C-5 67.2
C-6 61.9
Isopropylidine:
(O-C(CH3)2-O) 109.9 ad 109.0
CH3 x4 25.9, 25.8,
24.8, 24.3
Triazole:
C-4’ 143.2
C-5’ 128.5
P-hydroxybenzoate:
C-1” 160.6
C-3” and C-5” 128.5
C-4” 127.6
C-2” and C-6” 114.6
NH-CH2 50.6
NH-CH2-CH2 40.03
NH-(CH2)2-CH2 31.86
NH-(CH2)3-CH2 29.7
NH-(CH2)4-CH2 29.6
NH-(CH2)5-CH2 29.5
NH-(CH2)6-CH2 29.5
NH-(CH2)7-CH2 29.5
NH-(CH2)8-CH2 29.3
NH-(CH2)9-CH2 26.9
NH-(CH2)10-CH2 22.6
- CH3 14.07