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Title of experiment:
:Method
.weight 5 gm of sample-1
dissolve the sample in 50 ml -2
ethanol
titrate the mixture using 0.1M -3
NaOH
solution with ph.ph as
indicator
acid value = 0.561* titre / weight -4
.of sample
:Method
clean S.g bottle by shaking with acetone -1
.then ether
.weight empty S.G bottle -2
fill the S.G bottle with the sample and cover -3
.it
.weight the fill S.G bottle -4
.repat using Dis.water in place of the sample -5
:calculate -6
S.G = weight of the sample in S.G bottle /
.weight of water in S.G bottle
TAG
+
glycerol
3 KOH
3 alkali salt +
:Method
.Weight 2 gm of oil into glass flask
add 25 ml of alcoholic KOH sol. And boil - 2
for 1 hour under a condenser, shaking
the content of the flask at frequent
.intervals
determine the excess of alkali by- 3
titration with HCL using 0.5 ml of the
indicator
set a blank test upon the same quantity - 4
of KOH at the same time and under the
.same conditions
:calculate- 5
Saponification value = 28.05 ( T1-T2 )/W
:Where
T1= vol. in ml of HCL required for testing the
.blank
T2 = vol. in ml of HCL required for testing the
.sample
W = weight of sample
Where W is the weight of the sample in gm
and
is half of the m.w of KOH ( 56.05 ), since 28.05
.0.5N acid was used in both titrations