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Processing of Hydrocarbons

Schematic of a typical production facility

Sweetening Dehydration Hydrocarbon Recovery Sales


Gas

Ex wells

Separation

water oil

Receiving Treating Sales


Tank Tank Tank

Treatment Disposal

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Conventional Separators

Conventional Separator Internal Design

Modern separators, regardless of their shape or size, should include:

1. a primary or initial separation section

2. a secondary or gravity settling section

3. a mist extraction or coalescing section and

4. a sump or liquid collecting section.

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Conventional Separators

Primary or Initial Separation Section

The primary section is used to collect the majority of the liquid in the
inlet stream.

It contains the inlet nozzle, which is usually tangential or a diverter


baffle to take advantage of as much of the available vessel volume
as possible.

Centrifugal force or an abrupt change of direction is used to throw


the major portion of entrained liquid outwards from the gas stream.

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Conventional Separators

Secondary or Gravity Settling Section

This section is normally designed to utilize the force of gravity.

It consists of a portion of the vessel through which the gas moves


at a relatively low velocity with little turbulence.

In some designs, straightening vanes are employed to reduce


turbulence.

The vanes also act as droplet collectors and their use reduces the
distance a droplet must fall to be removed from the gas stream.

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Conventional Separators

Mist Extraction or Coalescing Section

A mist extractor is used in this section and can be one of several


designs:

a series of vanes,
woven wire-mesh pad
or cyclonic passage.

Many of the more recent designs use the woven wire-mesh pad.

The mist extractor removes the very small droplets of liquid in one final
separation before the gas leaves the vessel.

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Conventional Separators

Sump or Liquid Collecting Section

The sump section acts as a receiver for all liquid removed from the gas
in the first three sections.

Room is provided for the installation of a liquid level control device.

Depending on shape and requirements, the liquid section would have a


certain amount of surge volume over the normal level of collected liquid.

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Separator Design Characteristics

A properly designed separator essentially cleanly separates free gases


from the free hydrocarbon liquids.

If these functions are to be accomplished, the basic separator must have


the following characteristics:

1. Be constructed with adequate strength to withstand the


required working pressure.

2. Control the well stream flow as it enters the vessel.

3. Provide adequate space for the accumulation of liquids.

4. Internals arranged so as to provide minimum pressure


drop.
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Separator Design Characteristics

5. Minimize turbulence in the gas section of


the separator and reduce velocity.

6. Eliminate re-entrainment of the separated


gas and liquid.

7. Provide an outlet for gases, with suitable


controls to maintain preset operating
pressure.

8. Provide outlets for liquids, with suitable


liquid-level controls.

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Separator Design Characteristics

9. If necessary, provide clean-out ports at points where


solids may accumulate.

10. Control the accumulation of froths and foams in the


vessel.

11. Provide relief from excessive pressures in case of


closed or plugged gas or liquid outlets.

12. Provide a ready means of disposing of excess liquids


to avoid flooding.

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Conventional Separators

THE VERTICAL SEPARATOR

The vertical separator is the most common type of separator and is


normally used for the separation of gas from relatively large volumes of
liquid.

These vessels are normally installed near oil wells and range from 1 to 4
meters in diameter.

A typical oil and gas separator is shown below.

Other types of separators may use different types of mist extraction


equipment, but the basic operation is the same.

                                                                                                                     
                                                                     

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Conventional Separators

THE VERTICAL SEPARATOR

In operation, the mixture of liquids


and gases enters the inlet (A),
where it is given a swirling motion
by a spiral inlet baffle in the
separator space or chamber (B).

At this point there are two forces


tending to separate the liquids
from the gas.

The first is the effect of gravity;


the second is due to the whirling
action, which causes the heavy
liquid particles to collect on the
walls of the separator.
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Conventional Separators

THE VERTICAL SEPARATOR

The gas, which still contains some oil in


the form of small drops and spray, rises
through the chamber (B).

As the gas enters the swirl cylinder (C), it


moves faster and is again caused to whirl
so that the oil is forced against the side of
the deflector cone (E).

This liquid drains down through tubes (F)


to the bottom of the separator.

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Conventional Separators

THE VERTICAL SEPARATOR

After passing through the swirl cylinder, the


only condensate remaining in the gas is in
very small drops.

These drops are taken out of the gas by the


scrubber dome or mist extractor (G).

The dry gas then passes through another


chamber (H) and then leaves the separator
through the gas outlet (I).

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Conventional Separators

THE VERTICAL SEPARATOR

Condensate leaves the separator at


the oil outlet (J).

The liquid level is regulated by a float


(L) and control valve, so that liquid
covers the drain tubes (F) and the oil
outlet (J).

The separator can be cleaned through


the drain connection (K) in order to
remove any sand, mud or other
material.

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Conventional Separators

THE VERTICAL SEPARATOR

The pressure in the vessel and indirectly the rate of flow of


gas

from the vessel, is controlled by a back pressure valve which


is installed

on the gas outlet line.

The rate of liquid flow from the vessel is regulated by a liquid

level-controlled dump valve.

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Conventional Separators

THE VERTICAL SEPARATOR

Advantages of vertical separators:

They are easy to clean

The liquid level control in the vessels is not as critical since they will
handle large quantities of foreign material such as sand without
plugging up or otherwise affecting the operation of the vessel.

Disadvantages:

They are expensive for their size and volume

Will not adapt readily to a skid-mounted unit

Have a lower capacity than any other type of separator when


compared on the basis of effective diameter.
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Conventional Separators

The Horizontal Separator

The horizontal separator is most commonly used for the


separation of large volumes of gas from small volumes of liquid

This type of unit is used on gas wells, gas-condensate wells and


as inlet separating devices at gas processing plants.

Advantages of a horizontal unit

It is cheaper than a vertical unit because it has approximately


one-and-a-half times the capacity for gas flow as that of a vertical
separator of the same diameter

It is readily adaptable to skid mounting;

It is easier to hook up, due to the fact that the connections are
more accessible.
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Conventional Separators

The Horizontal Separator

Disadvantages of a horizontal separator

The liquid-level control is extremely critical compared to


that of the vertical unit;

It is difficult to clean out once sand or other foreign


material has accumulated in the vessel.

Feature of horizontal separator

The horizontal separator has a much greater gas-liquid interface


area consisting of a large, long, baffled gas-separation section
which permits much higher gas velocities.

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The Horizontal Separator

Sectional View of Horizontal Separator

Figure above shows a cutaway section of a single-tube horizontal


separator.

The liquid and gas mixture enters at (A) and strikes an angle baffle (B)
where the direction of flow is changed.

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The Horizontal Separator

Sectional View of Horizontal Separator

The heavier liquids fall to the bottom of the tank while the gas and
spray rise.

This wet gas passes into a chamber (C) where small drops gather into
larger drops and fall into the liquid at the bottom of the tank.

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The Horizontal Separator

Sectional View of Horizontal Separator

The partly-dried gas goes through a final element where the last liquid
particles of smallest size are removed from the gas by a mist extractor
(R), generally similar to the scrubber dome described in a vertical
separator.

The dried gas then goes through the top portion of the tank and into
the gas outlet (S).
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The Horizontal Separator

Sectional View of Horizontal Separator

The liquid from which the gas has been removed moves along the
bottom of the tank past the plates (F & G) to the oil outlet (W).

The plates act as baffles to keep waves from forming in the liquids.

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SIZING AND SELECTING SEPARATORS

In general, when considering size and type of separation, the


following are of assistance:

• Liquid flow rate (oil and water), barrels per day at minimum
and peak instances.

• Gas flow rate, cubic feet per day.

• Specific gravities of oil, water and gas.

• Required retention time of fluids within the separator;


retention time is a function of physical properties of the fluids.

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SIZING AND SELECTING SEPARATORS

• Temperatures and pressures at which the separator


will operate and design pressure of the vessel.

• Whether the separator is to be two-phase, such as


liquid and gas or threephase; that is, oil, water and gas.

• Whether or not there are solid impurities, such as


sand or paraffin.

• Whether or not there are foaming tendencies.

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SEPARATOR EQUIPMENT PROBLEMS AND REMEDIES

Foaming

Foaming is one of the major problems encountered in separator


operations.

The presence of solid particles such as sand, sludge and pipeline


scale may cause severe foaming.

Liquids such as methanol, glycol and filming amines which have been
injected into the well or pipelines to control corrosion or prevent
hydrates are often responsible for foaming in separators.

Wells which produce quantities of heavier hydrocarbons are also more


likely to cause foaming in separators.

This problem is remedied by the design of suitable mist extractors,


cleaning of the unit, careful monitoring of injected fluids and/or
injection of antifoam agents.
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SEPARATOR EQUIPMENT PROBLEMS AND REMEDIES

Liquid Surging

This is the rapid entry of liquid slugs into the separator from the lower
portions of the pipeline.

This problem can be prevented by proper selection and design of the


unit as well as correct operation of the gathering system.

Some separators are also equipped with dump valves designed to


dispose of the excess liquids from the bottom of the vessel.

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SEPARATOR EQUIPMENT PROBLEMS AND REMEDIES

Corrosion

Corrosive substances in the well fluid may cause severe metal loss
on the separator walls and internal parts.

Some of the more frequently found corrosive substances are H2S


(hydrogen sulphide), CO2 (carbon dioxide) and water - either fresh or
saturated with salt (brine).

Selection of metals with high resistance to corrosion is perhaps the


best way to reduce corrosion.

It is also the most costly method.

In practical applications the use of lower cost metals, combined with


the careful application of corrosion inhibitors, is the most cost-
effective method and is the method most widely used in the gas
industry to control corrosion in separators.
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