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20-Aug, 2020
Overview
Scope
• The method covers the determination of polypropylene ethylene rubber content of
polypropylene block copolymer.
Filtration
PER & Dry N-decane Filtration
Acetone
Vacuum oven
105oC @ 10 mmHg
Balance @ 0.1mg
Oil
bat
h
Chemicals
Chemicals
1. N-Decane (98% grade or higher)
2. Acetone.
3. Dry ice (solid carbon dioxide).
4. Heat resistant stabilizer (BHT)
5. Polyethylene glycol – No. 400 (used for oil bath)
Safety Check
Chemicals
1. Heat resistant gloves (for handling samples in oil bath and dry ice).
2. Chemical gloves.
3. Use mask when handling powder samples.
Procedure
Polymer Dissolution 5 ± 0.1 g
2 phases slurry.
9. During waiting time, assemble the filtering apparatus as in Fig. 2.
Polymer Filtration
10. Transfer the slurry to the filter funnel and filter the slurry using 325 mesh filter.
11. Rub off the polymer sticking to the inner wall of the flask with the silicon-
coated glass rod.
12. Wash the inner wall of the flask with n-decane to remove all the remaining
polymer.
13. Press slightly the cake-like polymer remaining on the wire mesh with glass rod.
Procedure
PER Separation and Filtration
Calculation
PER Content = b/a x 100 (wt%).
Report
Report to first decimal place. (e.g. 1.0 %, 10.0 %)