Autoclave-Catalog Amar Equipments

High Pressure Systems
Pressure Reactor Specialist

TM
Volume 07
®
Our Profile
Experience
The company was founded in 1974 by Mr. Naresh Shah (Managing Director & Chairman)
after completing B.Tech. Mechanical from IIT Mumbai & Masters of Science from University
of Michigan, United States. He was later joined in 1998 by his son Mr. Vishal Shah who
graduated with a bachelors' degree in Mechanical Engineering from V.J.T.I Mumbai. Ever
since 1974, Amar has built its foundation on a strong technical team with a blend of vast
experience & technological / commercial understanding.
The Journey
The beginning journey was with general fabrication of large pressure reactors, vessels, heat
exchangers etc. Today, we specialize in high pressure autoclaves / reactors / systems,
magnetic drive coupling & flow reactors. Our vision is to provide import substitutes in India
& new technologies globally, while maintaining quality & costs. Through high pressure
systems Amar can offer customized turnkey solution for virtually all applications from high
pressure chemical reactors, corrosion testing, supercritical fluid extraction system etc for
chemical, pharmaceutical, oil & gas, defence, educational & chemical research purposes.
Certifications
We are a ISO 9001 – 2008, CE – PED, ASME U, U2 certified company offering products with
Explosion proof (Ex), ATEX , UL, CSA, CRN certified systems on request.
Facilities
We have complete in-house setup well-equipped to design, manufacture & test all the
products & components with latest gauges, measuring instruments & machines including:
• CNC turning centre • Cutting machines
• Vertical machining centre (VMC) • Calibration instruments
• Conventional lathes • Drilling machines
• Plasma cutting machine • Welding machines
• Overhead EOT cranes • Grinding machines
• Buffing / polishing/ cleaning equipment • PMI machine
• Laser marking • Packaging machines etc.
Team
We are a team of around 125 people with qualified staff, skilled workers including a core
team of 30 highly skilled & experienced professional engineers, required to produce the
desired quality with accuracy & precision as per international quality standards & design
codes.
Vision
• To provide import substitutes in India & new technologies globally, while maintaining
quality & costs
• To become a leading global player in manufacturing & supply of all our products
• To continuously upgrade the quality of our products and always offer the latest & the
best
• To build products that are technically complete, physically reliable, economically
competent & ergonomically superior
Mission
• To develop technically complex, challenging, customised turnkey solutions
• At Amar, we strongly follow Hon. Indian Prime Minister Narendra Modi’s campaign of
MAKE IN INDIA
Global Footprints
Pioneers & largest manufacturer of high pressure reactor, magnetic drive couplings & continuous flow reactor in India year after year for
over 40 yrs with around 75% market share in India and substantial share globally. Over 5000 successful installations world over with more
than 1000 delighted customers. Exports to more than 50 countries worldwide with presence of local distributors & 5 distributors in different
parts of India for local support.
Product Range
• High Pressure Autoclaves • Non Stirred Pressure Vessels • Acid Digestion Bombs • Continuous Flow Micro Reactors
• High Throughput Catalyst Screening • HPHT Corrosion Testing • Shaker Hydrogenator • Photo Chemical Flow Reactors
• Automated Parallel Autoclaves • Supercritical Fluid Extraction • Pilot Plants • Magnetic Couplings / Stirrers
• Gas Induction Reactors • Reaction Calorimeters • CSTR • Heating & Cooling Circulators
• Glass Autoclaves • Gas Hydrate System • Fixed Bed Tubular Reactors • Lab Agitated Nutsche Filters
®
Certifications & Approvals

• An ISO-9001-2008 certified company.
• All our pressure vessel designs are as per ASME codes-section Vlll Div 1 / Div 2.
• Our welders are qualified as per ASME section IX codes for welded pressure vessels.
• PED, U/U2 Stamp, CRN for Canada, ASA 1210 for Australia & DOSH for Malaysia certified systems.
• CE, UL / CSA certified systems offered on request.
• Explosion proof / flame proof systems with Class 1 Div. 2, ATEX Zone I Ex electrical & mechanical certified system for hazardous area.
• DQ, IQ, PQ, OQ documentation can be given on special request.
®
Index
Sr. No. Title Page no. Sr. No. Title Page no.
1 Autoclave types, features, applications . . . . . . . . . . . . 1 22 Optional accessories . . . . . . . . . . . . . . . . . . . . . . . . . . 44
2 High pressure stirred autoclaves Gas pressure regulator . . . . . . . . . . . . . . . . . . . . . . . . 44
A 1000 series: 50 ml - 250 ml . . . . . . . . . . . . . . . . . . . . . 2 Gas booster . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
A 2000 series: 500 ml - 5 ltr . . . . . . . . . . . . . . . . . . . . . . 4 Thermal Gas mass flow meter / controller . . . . . . . . . 44
A 3000 series: 10 ltr - 100 ltr . . . . . . . . . . . . . . . . . . . . . 8 Coriolis gas-liquid mass flow meter / controller . . . . . 44
3 Multiple autoclaves (M4/M6): 50 ml - 2 ltr . . . . . . . . 12 Digital pressure indicator / controller . . . . . . . . . . . . . 44
4 High throughput catalyst screening: 50 ml - 750 ml . . 15 Liquid / slurry / gas charging pressure charging pot . . 45
5 Eco catalyst screening: 10 ml - 25 ml . . . . . . . . . . . . . 15 Ethylene / propylene oxide charging pot . . . . . . . . . . 45
6 Bottom stirred autoclaves: 25 ml - 750 ml . . . . . . . . . 16 Liquid metering pump system . . . . . . . . . . . . . . . . . . . 45
7 Glass autoclaves: 100 ml - 2 ltr . . . . . . . . . . . . . . . . . . 18 Auto cooling system . . . . . . . . . . . . . . . . . . . . . . . . . . 45
8 Material of constructions guide . . . . . . . . . . . . . . . . . . 20 Magnetic drive & pressure sensor cooling system . . . 46
9 Autoclave specification guide Cooling & heating circulators . . . . . . . . . . . . . . . . . . . 46
Head mounting style . . . . . . . . . . . . . . . . . . . . . . . . . . 22 Flow control valves . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Heating types . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22 Reflux condenser. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Nozzle, valves & fittings . . . . . . . . . . . . . . . . . . . . . . . . 23 Condenser . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Body & head sealing. . . . . . . . . . . . . . . . . . . . . . . . . . . 23 Receiver pot . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Motor & drive . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23 Back pressure regulator. . . . . . . . . . . . . . . . . . . . . . . . 47
Magnetic drives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24 Pressure safety valve . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Stirrer types . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 Chain pulley / Hydraulic head lifting system . . . . . . . . 47
Control panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 SCADA software. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Autoclave mounting options . . . . . . . . . . . . . . . . . . . . 26 Liners . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
10 Gas induction / high pressure reactors: 100 - 2000 ltr 27 Catalyst basket . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
11 Non stirred pressure vessels: 25 ml - 2000 ltr. . . . . . . 28 Catalyst filters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
12 Acid digestion bombs: 25 ml - 750 ml . . . . . . . . . . . . . 32 Catalyst addition device . . . . . . . . . . . . . . . . . . . . . . . 48
13 Shaker hydrogenator: 100 ml - 2 ltr . . . . . . . . . . . . . . 33 Catalyst filtration & recycling system . . . . . . . . . . . . . 48
14 Supercritical fluid extraction (SCFE): 100 ml - 1000 ltr 34 Catalyst slurry charging system . . . . . . . . . . . . . . . . . . 48
15 Autoclaves for corrosion testing . . . . . . . . . . . . . . . . . 36 Catch pot . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
16 Autoclaves for gas hydrate formation . . . . . . . . . . . . . 37 Vacuum pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
17 Autoclaves for reaction calorimetry: 100 ml - 2 ltr . . . 38 View window / light & sight glass . . . . . . . . . . . . . . . . 49
18 Continuous stirred tank reactors (CSTR) . . . . . . . . . . . 39 In situ FTIR spectroscopy. . . . . . . . . . . . . . . . . . . . . . . 49
19 Vapour phase Malshe's reactors . . . . . . . . . . . . . . . . . 39 Level, pH, turbidity, DO, redox sensors, torque sensor,
20 Pilot plants / customized systems . . . . . . . . . . . . . . . . 40 ultrasonic transducer, purge panels . . . . . . . . . . . . . . 49
21 Low pressure reactor systems . . . . . . . . . . . . . . . . . . . 43 23 Valued customer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
Product Coding Guide

Autoclaves Net filling volume Pressure (bar) Temperature (°C)
Type Code Series Rating Code Rating Code Rating Code
Stirred A 25 ml 11 6 6 150 0
Multiple stirred M 1000 50 ml 12 10 7 200 2
Bottom Stirred B 100 ml 13 20 8 250 1
Glass G 250 ml 14 50 0 300 3
Non-stirred P 500 ml 21 100 1 350 7
Acid digestion bombs D 750 ml 22 200 2 450 4
Shaker hydrogenator S 2000 1 ltr 23 350 3 500 5
SCFE E 2 ltr 24 500 4 550 8
Reaction calorimeter C 5 ltr 25 700 5 600 6
10 ltr 31 650 9
20 ltr 32
3000 25 ltr 33
50 ltr 34
100 ltr 35
A 1 0 0 0 For example a stirred autoclave of 2 ltr volume 100 bar & 300°C rating shall read as
Temperature A2413 (refer respective stirred autoclave type page for the same)
Pressure Not all volumes will have options of all ratings for all types.
Volume
Type
Trademarks used in the catalogue Abbreviations used in the catalogue
• Viton, Kalrez & teflon are registered trademarks of Dupont • QRC: Quick release coupling • NRV: Non-return valve
• Grafoil is registered trademark of UCAR Carbon Co. • MOC: Material of construction • Temp.: Temperature
• Monel & Inconel are registered trademark of Special Metals Corp. • FLP: Flame proof/Explosion proof • Pr.: Pressure
• Hastelloy is registered trademark of Haynes International • Ø: Phase • NA: Not applicable/ available
• Ltr.: Liter
As development is a continuous process the specifications in the catalogue can change without prior notice
®
High Pressure Autoclaves / Reactors / Pressure Vessels

Types
• High pressure autoclaves
• Multiple parallel reactors
• High throughput catalyst screening
• Bottom stirred autoclaves
• Low pressure glass & interchangeable glass-metal autoclaves
• Gas induction reactors
• Non stirred pressure vessels
• Acid digestion bombs / hydrothermal pressure vessels
• Shaker hydrogenator
• Supercritrical fluid extraction system (SCFE)
• Autoclaves for corrosion testing
• Autoclaves for study of gas hydrate formation
• Autoclaves for calorimetry
• Continuous flow stirred tank reactor (CSTR)
• Pilot plants & customized systems
• Low pressure reactors with heating cooling circulators
Salient Features
• Stirred & non-stirred reactors / pressure vessels
• 25 ml to 2000 ltr volume
• Material: SS-316/316L, Hastelloy B/C, Monel, Inconel, Nickel, Titanium, Tantalum lined, Zirconium etc.
• Max. design pressures upto 700 bar & temperatures upto 650 ºC
• All designs as per ASME codes with CE-PED or U/U2 stamp marking optional
• High torque maintenance free zero leakage magnetic drive coupling
• Complete pilot plant with automatic temperature, pressure, RPM, motor torque/ current, liquid & gas
flow, pH, conductivity, dissolved oxygen, turbidity, IR, level etc. controls, auto cooling system, chiller,
condensor for distillation or reflux, thermic fluid heating / cooling system etc.
• Fully automated PC controlled high pressure systems / pilot plants, pilot plant to continuously monitor,
control & record various parameters with touch panels & receipe management
• Complete flame / explosion proof / ATEX certified systems suitable for group IIA, IIB, IIC gases (optional)
• CE, UL, CSA certified electricals & controls (optional)
• ATEX certified electricals & controls (optional)
Applications
• It is used for high-pressure high-temperature chemical reactions like alkylation, amination,
bromination, carboxylation, catalytic reduction, chlorination, dehydrogenation, esterification,
ethoxylation, halogenation, hydrogenation, methylation, nitration, oxidation, ozonization,
polymerization, sulphonation etc.
– To invent new molecules / chemicals & study reaction parameters
– To produce chemicals in small quantity in batch or continuous mode
– For synthesis of hydrogenation, acetylation, epoxydation, grignard reaction, nitration,
acylation, photchemical reaction
– For quality control & process improvements
– For high throughput catalyst screening
• For supercritical CO2 solvent extraction / reaction / drying / evaporation system
• For reaction calorimetry to study heat of reaction
• For static, dynamic, loop & electrochemical HPHT corrosion testing
• Gas hydrate formation
• For hydrogen disbonding test
• Soaking of diamonds / precious stones
• For high pressure storage & transfer of gas / liquid / slurries
• For acid digestion
In R&D centers, pilot plants & manufacturing facilities of fine & speciality chemicals, bulk drug (API)
pharmaceuticals, dyes, intermediates, paints, oils, agrochemical, petrochemicals, oil & gas etc.
Industries & in chemical engineering colleges / research institutes / defence organisations where
high pressure reactions / testing is carried out.
01
®
A1000 series (50 ml, 100 ml & 250 ml)

Salient Features
• 50 ml to 250 ml net filling volume
• Pressures upto 350 bar &
temperatures upto 500°C
• Material: SS-316/316L, Hastelloy B/C,
Monel, Inconel, Nickel, Titanium,
Zirconium, Tantalum etc.
250 ml autoclave 250 ml table top 100 ml with manual

Standard models for 50 ml volume autoclave raising & lowering
Model No. A 1213 A 1215 A 1223 A 1225 A 1233 A 1235
Design Pressure 100 bar 200 bar 350 bar
Design Temperature 300°C 500°C 300°C 500°C 300°C 500°C
Vessel I/D (mm) 40
Vessel Internal Height (mm) 63
Min. Stirrable Volume (ml) 20
Standard models for 100 ml volume

Model No. A 1313 A 1315 A 1323 A 1325 A 1333 A 1335
Vessel I/D (mm) 40
Standard models for 250 ml volume

Model No. A 1413 A 1415 A 1423 A 1425 A 1433 A 1435
Vessel I/D (mm) 65
Note: The above ratings are only for SS316, Hastelloy C & Inconel materials, for other materials the ratings will change depending on its stress
values & maximum allowable temperature as per ASME code for which refer page 21 in material of construction.
Technical Specifications for 50 ml, 100 ml & 250ml standard models

Sr. Description Specification
A Material of Construction SS 316 wetted parts
B Head Mounting Style Removable head and vessel design
C Heating Type Electrical ceramic band heater with cladding & insulation & heater temperature control for 500°C
D Motor 1/8 hp AC motor with 100-1450 RPM
E Shaft Sealing Zero leakage magnetic drive coupling M8 with 0.8 Nm torque
F Stirrer 4 bladed turbine stirrer
G Standard Nozzles, Valves External Valves &Fittings:
& Fittings Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common
dip tube, solenoid valve at inlet of cooling coil, vent needle valve (All needle valves 1/8" size)
Internal Fittings:
Serpentine cooling coil, dip tube, thermowell with RTD PT100 temperature sensor
H Gasket PTFE up to 300°C and metallic grafoil gasket up to 500°C
I Closure Type Split clamp with clamp bolts
J Control Panel SS control panel with programmable PID temperature controller with high temperature alarm and
variable frequency drive for motor speed control
K Power Supply 1 Ø, 220 V AC, 50 / 60 Hz
L Mounting & Dimensions SS Table Top with 240mm x 310mm x 800mm for reactor assembly & 275mm x 275mm x 300mm
(W x D x H) for control panel
02
®
Nozzle orientation & internals for A1000 series

Pressure relief Cooling coil
valve (optional) inlet & outlet
Pressure gauge Thermowell
Magnetic drive
Vent valve
Dip tube
Thermowell
Stirrer shaft
Sampling valve
Safety Serpentine cooling coil
rupture disc
Gas inlet
Pressure
transmitter (optional) Impeller
Enquiry guide for 50 ml, 100 ml & 250 ml customized models

Enquiry code structure is Standard Model no-A-B-C-D2-D3-E-F-I-J-L-M where A, B, C, D2, D3, E, F, I, J, L & M options can be selected from
below tables. The below options will be in place of standard supply. For example 100 ml, 100 bar, 300°C, Hastelloy C, fixed head autoclave
with ATEX Zone1 certified, heater, motor & panel will read as A 1313-HC6-K-EZ-AZ-ATP
Options
A Material of Construction E Mag Drive Torque
SS 316 L 316L Inconel 625 IN5 2 Nm M20
Hastelloy C 276 HC6 Nickel 200 NK2
Hastelloy C 22 HC2 Titanium Gr. 2 TI2 F Stirrer Options*
Hastelloy B HB Zirconium 702 ZR7 Hollow shaft with gas induction Impeller SH
Monel 400 MN4 Tantalum TAN Ruston turbine SR
Inconel 600 IN6 Paddle SD
Propeller SP
B Head Mounting Style
Fixed head with manual vessel raising lowering K I Closure Type
Threaded cap with FKM (Viton)'O' ring up to 225°C CV
C Heating Style Threaded cap with FFKM (Kalrez) 'O' ring up to 275°C CK
Electrical ex-proof, IIB + H? certified EA
Electrical ex-proof ATEX Zone1 certified EZ J Control Panel
Electrical ex-proof Class 1 Div 2 EC Ex-proof gas group IIA/IIB zone 1 certified F2B
Welded SS 304 jacket with insulation JS Ex-proof gas group IIC zone 1 certified F2C
Welded SS 304 jacket with electrical ceramic heater JH Ex-proof ATEX zone 1 certified ATP
Peltier cooler for -25 to 150°C PL Ex-proof class 1 div. 2 certified C12
Touch screen TSP
D2 RPM
Up to 3000 rpm RT L Mounting & Overall Dimensions (WxDxH)
Trolley 1010 mm x 410 mm x 1300 mm TL
D3 Motor Type
¼ hp ex-proof gas group IIB (Zone 1) XB M Certifications**
¼ hp ex-proof gas group IIC (Zone 1) XC Design approval as per ASME code by notified body DAC
¼ hp ex-proof CE ATEX certified II 2G Ex de IIC T4 AZ CE-PED 2014/68/EU PED
¼ hp ex-proof CSA certified Class 1 Div 2 group A, CD ASME U/U2 stamp coded ASU
B, C, D ATEX certified reactor 2014/34/EU ASA
1/8 hp compact in-line brushless DC motor BD CE marked panel & electrical parts ECE
UL/CSA marked panel & electrical parts USC
Note: 1) Customer is advised to select best suited options for most optimized price & delivery.
2) For other optional accessories please refer page 44.
3) All above options may not be available / possible with all models.
4) Customization of volume, material, pressure, temperature etc. may be possible on request.
5) Different power supply options may be possible on request.
6) Overall dimensions are indicative, they may change depending on the optional accessories or specific design modifications opted.
*Stirrer options can be in place of standard or additional multiple interchangeable.
**Country specific certification like CRN for Canada, AS1210 for Australia & DOSH for Malaysia can be offered on request.
03
®
A2000 series (500 ml, 750 ml, 1 ltr, 2 ltr, 5 ltr)

Salient Features
• 500 ml to 5 ltr net filling volume
• Pressures upto 350 bar & temperatures upto 500°C
• Material: SS-316/316L, Hastelloy B/C, Monel, Inconel,
Nickel, Titanium, Zirconium, Tantalum lined etc.
2 ltr trolley model
1 ltr table top model 500 ml table top

with in-line motor
5 ltr trolley model

5 ltr floor stand model 2 ltr U stamp autoclave with
pneumatic raising & lowering
04
®
500 ml 750 ml 1 ltr 2 ltr 5 ltr

autoclave autoclave autoclave autoclave autoclave
Standard models for 500 ml autoclave
Model No. A 2113 A 2115 A 2123 A 2125 A 2133 A 2135
Vessel I/D (mm) 75 65
Vessel Internal Height (mm) 118 158
Min. Stirrable Volume (ml) 60 50
Standard models for 750 ml autoclave

Model No. A 2213 A 2215 A 2223 A 2225 A 2233 A 2235
Vessel I/D (mm) 75
Standard models for 1 ltr autoclave

Model No. A 2313 A 2315 A 2323 A 2325 A 2333 A 2335
Vessel I/D (mm) 101.6 75

Model No. A 2413 A 2415 A 2423 A 2425 A 2433 A 2435
Vessel I/D (mm) 101.6

Model No. A 2513 A 2515 A 2523 A 2525 A 2533 A 2535
Vessel I/D (mm) 152
05
®
Nozzle orientation & internals A2000 series
Cooling coil
Pressure relief Thermowell inlet & outlet
valve (optional)
Magnetic drive
Pressure gaauge Funnel
Stirrer shaft
Dip tube
Powder inlet
ball valve
Thermowell
Helical cooling coil
Vent valve
Impeller
Sampling valve
Pressure
transmitter (optional)
Safety Gas inlet
rupture disc
Technical Specifications for 500 ml, 750 ml, 1 ltr, 2 ltr, 5 ltr standard models
D Motor ¼ hp AC motor with 100-1450 RPM
E Shaft Sealing Zero leakage magnetic drive coupling M20 with 2 Nm torque
F Stirrer 2 stage 6 bladed turbine stirrer
& Fittings Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube,
vent needle valve (all needle valves are ¼" size)
Internal Fittings:
Helical cooling coil, dip tube, thermowell with RTD PT 100 sensor
J Control Panel SS control panel with programmable PID temperature controller with high temperature alarm and
variable frequency drive for motor speed control
L Mounting & Dimensions SS Trolley
(WxDxH) mm Reactor Volume Dimensions with control panel
500 ml & 750 ml 1010 x 410 x 1340
1 ltr & 2 ltr 1040 x 410 x 1350
5 ltr 1100 x 410 x 1350
Interchangeable autoclave: 50 ml & 100 ml or 500 ml & 750 ml

or 1 ltr & 2 ltr interchangeable vessels, heater & internal fittings
with common head, external fittings, panel, motor, mounting
etc. can be offered. However diameter being same the higher
volume model can do the minimum stirrable volume of lower
volume vessel hence there is no advantage.
50ml & 100ml interchangeable
reactors with fixed head design
06
®
Enquiry guide for 500 ml, 750 ml, 1 ltr, 2 ltr, 5 ltr customized models
Enquiry code structure is Standard Model no. A-B-C-D1-D2-D3-E-F-G-I-J-L-M where A, B, C, D1,D2, D3, E, F, G, I, J, L & M options can be
selected from below tables. The below options will be in place of standard supply. For example 500 ml, 100 bar, 300°C, Hastelloy C, fixed
head autoclave with ATEX Zone1 certified, heater, motor & panel will read as A 2113-HC6-K-EZ-AZ-ATP
Options
A Material of Construction F Stirrer Options*
SS 316 L 316L Inconel 625 IN5 Hollow shaft with gas induction impeller SH
Hastelloy C 276 HC6 Nickel 200 NK2 Anchor (Serpentine cooling coil, max 100 rpm) SA
Hastelloy C 22 HC2 Titanium Gr. 2 TI2 Spiral (No cooling coil, max 100 rpm) SS
Hastelloy B HAB Zirconium 702 ZR7 Ruston turbine SR
Monel 400 MN4 Tantalum TAN Paddle SD
Inconel 600 IN6 Tantalum lined TNL Propeller SP
B Head Mounting Style G Valves & Fittings**

Fixed head with manual vessel raising lowering K Serpentine cooling coil SCC
(500 ml & 750 ml) Ball valve powder inlet (¼") with funnel BVP
Fixed head with pneumatic vessel raising lowering P Flush bottom valve (10 mm) FBV
Fixed head with manual vessel raising lowering & KT Baffle (with serpentine cooling coil) BFL
tilting (500 ml & 750 ml)
Fixed head with pneumatic vessel raising lowering PT I Closure Type (upto 100 bar)
& tilting
Split clamp with 'O' ring-FKM (Viton) up to 225°C CV
C Heating Style Split clamp with 'O' ring FFKM (Kalrez) up to 275°C CK
Electrical ex-proof, IIB + H2 certified EA J Control Panel

Electrical ex-proof ATEX Zone1 certified EZ
Ex-proof group IIA/IIB zone 1 certified F2B
Electrical ex-proof Class 1 Div 2 certified EC
Ex-proof group IIC zone 1 certified F2C
Welded SS 304 jacket with insulation JS
Ex-proof ATEX zone 1 certified ATP
Welded SS 304 jacket with electrical ceramic heater JH
Ex-proof class 1 div. 2 certified C12
D1 Motor HP Touch screen TSP
½ hp H05 L Mounting & Overall Dimensions (WxDxH)

1 hp H10
Mounting Volume Reactor size mm Panel size mm Code
500 ml 280 x 350 x 900
D2 Motor RPM
Table Top 750 ml 280 x 350 x 900 TT
Up to 3000 rpm RT 1 ltr 355 x 400 x 925
Gear box up to 440 rpm R4 500 ml 280 x 350 x 1240 275 x 275 x 300
750 ml 280 x 350 x 1240
D3 Motor Type Floor Stand 1 ltr 355 x 400 x 1250 FS
¼ hp ex-proof gas group IIB (Zone 1) XB 2 ltr 355 x 400 x 1250
¼ hp ex-proof gas group IIC (Zone 1) XC 5 ltr 420 x 420 x 1250
¼ hp ex-proof CE ATEX certified II 2G Ex de IIC T4 AZ
¼ hp ex-proof CSA certified Class 1 Div 2 group A, CD M Certifications***
B, C, D
Design approval as per ASME code by notified body DAC
1/8 hp compact in-line brushless DC motor BD
CE-PED 2014/68/EU PED
ASME U/U2 stamp coded ASU
E Mag Drive Torque
ATEX certified reactor 2014/34/EU ASA
4 Nm M40 CE marked panel & electrical parts ECE
8 Nm M80 UL/CSA marked panel & electrical parts USC
12 Nm (only for 1 to 5 ltr) M120
20 Nm (only for 5 ltr) M200
*Stirred options can be in place of standard or additional multiple interchangeable.
**All option specified in G are addons & multiple/ all of them can be availed at the same time.
***Country specific certification like CRN for Canada, AS1210 for Australia & DOSH for Malaysia can be offered on request.
07
®
A3000 series (10 ltr, 20 ltr, 25 ltr, 50 ltr & 100 ltr)
Salient Features
• 10 ltr to 100 ltr net filling volume
• Material: SS-316/316L, Hastelloy B/C, Monel, Inconel,
Nickel, Titanium, Tantalum lined, Zirconium etc.
25 ltr autoclave
(floor stand model)
10 ltr autoclave
(jacketed model)
50 ltr autoclave
20 ltr autoclave 100 ltr autoclave with hydraulic head

raising lowering arrangement
08
®
50 ltr autoclave
with electrical heater 50 ltr autoclave internals
100 ltr autoclave
Standard models for 10 ltr volume

Model No. A 3113 A 3115 A 3123 A 3125 A 3133 A 3135
Vessel I/D (mm) 183
Min. Stirrable Volume (ltr) 1

Model No. A 3213 A 3215 A 3223 A 3225
Design Pressure 100 bar 200 bar
Design Temperature 300°C 500°C 300°C 500°C
Vessel I/D (mm) 248
Min. Stirrable Volume (ltr) 2.6

Model No. A 3313 A 3315 A 3323 A 3325
Vessel I/D (mm) 248
Min. Stirrable Volume (ltr) 2.6

Model No. A 3403 A 3405 A 3413 A 3415

Model No. A 3503 A 3505 A 3513 A 3515
09
®
Nozzle orientation & internals A3000 series
Cooling coil
Pressure relief Thermowell inlet & outlet
valve (optional)
Magnetic drive
Pressure gaauge Funnel
Powder inlet
ball valve Stirrer shaft
Dip tube
Vent valve
Thermowell
Sampling valve Helical cooling coil
Pressure Impeller
transmitter (optional)
Safety Gas inlet
rupture disc
Technical specifications for 10 ltr, 20 ltr, 25 ltr, 50 ltr & 100 ltr standard models
D Motor ½ hp AC motor for 10 ltr, 20 ltr & 25 ltr locked to 750 rpm
1 hp AC motor for 50 ltr & 100 ltr locked to 500 rpm
E Shaft Sealing Zero leakage magnetic drive coupling M80 with 8 Nm torque for 10 ltr to 25 ltr & M120 with 12 Nm torque
for 50 ltr & 100 ltr reactor
F Stirrer 2 stage 6 bladed turbine stirrer
& Fittings Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube,
vent needle valve, ball valve for powder/ liquid inlet with funnel, flush bottom valve
Size Needle valve Ball Valve FBV
10 - 25 ltr ¼" ¾" 15 mm
50 - 100 ltr ½" 1" 25 mm
Internal Fittings:
Helical cooling coil, dip tube, thermowell with RTD PT100 temperature sensor, baffles
J Control Panel SS control panel with programmable PID temperature controller with high temperature alarm and variable
frequency drive for motor speed control
K Power Supply 1 Ø, 220 V AC 20 amp, 50 / 60 Hz for 10 ltr
3 Ø, 440 V AC, 25 amp, 50 / 60 Hz for 20 ltr - 100 ltr
L Mounting & Dimensions SS Trolley
(W x D x H) mm Reactor Volume Dimensions with control panel
10 ltr 1310 x 585 x 1550
20 ltr 1310 x 585 x 1700
25 ltr 1310 x 585 x 1800
50 ltr 1500 x 675 x 2350
100 ltr 1500 x 780 x 2350
10
®
Enquiry guide for 10 ltr, 20 ltr, 25 ltr, 50 ltr, 100 ltr customized models
Enquiry code structure is Standard Model no. A-B-C-D1-D2-D3-E-F-G-J-L-M where A, B, C, D1,D2, D3, E, F, G, J, L & M options can be selected
from below tables. The below options will be in place of standard supply. For example 10 ltr, 100 bar, 300°C, Hastelloy C, fixed head autoclave
with ATEX Zone1 certified, heater, motor & panel will read as A 3113-HC6-K-EZ-AZ-ATP
Options

SS 316 L 316L Inconel 625 IN5 12 Nm (for 10-25 ltr) M120
Hastelloy C 276 HC6 Nickel 200 NK2 20 Nm (up to 750 rpm, for 10-25 ltr) M200
Hastelloy C 22 HC2 Titanium Gr. 2 TI2 40 Nm (up to 750 rpm) M400
Hastelloy B HB Zirconium 702 ZR7
Monel 400 MN4 Tantalum lined TNL F Stirrer Options*
Inconel 600 IN6
Hollow shaft with gas induction Impeller SH
Anchor (Serpentine cooling coil, max 100 rpm) SA
Spiral (No cooling coil, max 100 rpm) SS
Fixed head with pneumatic vessel raising lowering K Ruston turbine SR
(10 ltr to 25 ltr)
Paddle SD
Fixed head with hydraulic vessel raising lowering H
(50 ltr & 100 ltr) Propeller SP
Fixed head with pneumatic vessel raising lowering & KT
tilting (10 ltr to 25 ltr) G Valves & Fittings
Fixed head with hydraulic vessel raising lowering & HT
tilting (50 ltr & 100 ltr) Serpentine cooling coil SCC
C Heating Style J Control Panel

Electrical ex-proof, IIB + H2 certified EA
Ex-proof group IIC zone 1 certified F2C
Electrical ex-proof ATEX Zone1 EZ
Ex-proof ATEX zone 2 certified ATP
Touch screen TSP
Welded SS 304 jacket with electrical ceramic heater JH
Limpet Coil SS 304 with insulation (20 ltr & 100 ltr) LC
L Mounting & Overall Dimensions (WxDxH)
Mounting Volume Reactor size mm Panel size mm Code
D1 Motor HP
10 ltr 585 x 560 x 1550 275 x 275 x 300
1 hp (for 10-25 ltr) H10 20 ltr 585 x 560 x 1700
2 hp H20 Floor Stand 25 ltr 585 x 560 x 1800 FS
3 hp H30 400 x 380 x 340
50 ltr 675 x 675 x 2350
100 ltr 780 x 780 x 2350
D2 RPM
Gear box up to 440 rpm R4 M Certifications**
D3 Motor Type CE-PED 2014/68/EU PED
Ex-proof gas group IIB (Zone 1) XB
Ex-proof gas group IIC (Zone 1) XC
CE marked panel & electrical parts ECE
Ex-proof CE ATEX certified II 2G Ex de IIC T4 AZ
Ex-proof CSA certified Class 1 Div 2 group A, B, C, D CD
¼ hp compact in line brushless DC motor (10-25 ltr) QD
5) Different power supply options may be possible on request
*All option specified in F are in place of standard or addons & multiple/ options can be selected at the same time.
**Country specific certification like CRN for Canada, AS1210 for Australia & DOSH for Malaysia can be offered on request.
11
®
Multiple Autoclaves / Parallel Synthesizer
M6 model with fixed head design

& inline BLDC motors
Salient Features
• 4 or 6 nos. of 50 ml to 2 ltr parallel overhead stirred autoclaves
• Common mounting & control panel with remote monitoring & control
• Simultaneous reactions can be carried out in each reactor with different parameters &
comparative studies can be done from the data received. It saves lot of space & helps in
advanced & faster research i.e. high throughput testing
• The optional accessories can be common or separate for all autoclaves
Standard models for multiple autoclave 50 ml

Description M4 or M6
Model No. 1213 1215 1223 1225 1233 1235
Vessel I/D (mm) 40

Model No. 1313 1315 1323 1325 1333 1335
Vessel I/D (mm) 40

Model No. 1413 1415 1423 1425 1433 1435
Vessel I/D (mm) 65
12
®

Model No. 2113 2115 2123 2125 2133 2135

Model No. 2213 2215 2223 2225 2233 2235
Vessel I/D (mm) 75
Standard models for multiple autoclave 1 ltr

Model No. 2313 2315 2323 2325 2333 2335
Standard models for multiple autoclave 2 ltr

Model No. 2413 2415 2423 2425 2433 2435
Note: The above ratings are only for SS316, Hastelloy C & Inconel materials, for other materials the ratings will change depending on its stress value
& maximum allowable temperature as per ASME code for which refer page 21 in material of construction.
Technical specification for multiple autoclaves standard models

D Motor 1/8 hp AC motor with 100-1450 RPM (50 ml to 250 ml)
¼ hp AC motor with 100-1450 RPM (500 ml to 2 ltr)
E Shaft Sealing Zero leakage magnetic drive coupling M8 with 0.8 Nm torque for 50 ml - 2 ltr & M20 with 2 Nm torque
for 450 ml - 2 ltr
F Stirrer 4 bladed turbine stirrer (50 ml to 250 ml)
2 stage 6 bladed turbine stirrer (500 ml to 2 ltr)
G Standard Nozzles, External Valves &Fittings:
Valves & Fittings Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube, vent
needle valve, solenoid valve at inlet of cooling coil (50 ml to 250 ml)
Internal Fittings:
Serpentine cooling coil (50 ml to 250 ml), Helical cooling coil (500 ml to 2 ltr), dip tube, thermowell with
RTD PT 100 sensor
J Control Panel SS control panel with programmable PID temperature controller, high temperature alarm and variable
frequency drive for motor speed control
L Mounting Table top (50 ml to 1 ltr)
SS Trolley (2 ltr)
13
®
Enquiry guide for multiple autoclaves customized models

Enquiry code structure is Standard Model no. A-B-C-D1-D2-D3-E-F-G-I-J-L-M where A, B, C, D1,D2, D3, E, F, G, I, J, L & M options can be
selected from below tables. The below options will be in place of standard supply. For example 4 nos. of 500 ml, 100 bar, 300°C, Hastelloy C,
fixed head autoclave with ATEX Zone1 certified, heater & motor will read as M4 2113-HC6-K-EZ-AZ
Options
SS 316 L 316L Inconel 625 IN5 2 Nm (for 50 ml - 250 ml) M20
Hastelloy C 276 HC6 Nickel 200 NK2 4 Nm (for 500 ml - 2 ltr) M40
Hastelloy C 22 HC2 Titanium Gr. 2 TI2 8 Nm (for 500 ml - 2 ltr) M80
Hastelloy B HAB Zirconium 702 ZR7 12 Nm (for 1 ltr - 2 ltr) M120
Monel 400 MN4 Tantalum TAN
Inconel 600 IN6 Tantalum lined TNL F Stirrer Options*
Hollow shaft with gas induction Impeller SH
Anchor (with serpentine cooling coil, max 100 rpm) SA
Fixed head with manual vessel raising lowering K Spiral (No cooling coil, max 100 rpm) SS
(50 ml to 750 ml)
Ruston turbine SR
Fixed head with pneumatic vessel raising lowering P
(500 ml to 2 ltr) Paddle SD
Fixed head with manual vessel raising lowering & KT Propeller SP
tilting (50 ml to 750 ml)
Fixed head with pneumatic vessel raising lowering & PT G Valves & Fittings** (for 500 ml - 2 ltr)
tilting (500 ml to 2 ltr)
Serpentine cooling coil SCC
C Heating Style Ball valve powder inlet (¼") BVP
Flush bottom valve (10 mm) FBV
Electrical ex-proof, IIB + H2 certified EA
Baffles (with serpentine cooling coil) BFL
Electrical ex-proof ATEX Zone1 certified EZ
Welded SS 304 jacket with insulation JS I Closure Type
Welded SS 304 jacket with electrical band heater JH Threaded cap with 'O' ring-FKM (Viton) upto 225°C CV
Peltier cooler for -25 to 150°C (for 50 ml - 250 ml) PL Threaded cap with ‘O’ ring FFKM (Kalrez) upto 275°C CK
Split clamp with 'O' ring-FKM (Viton) upto 225°C CV
D1 Motor HP (upto 100 bar, 500 ml - 2 ltr)
¼ hp (50 ml - 250 ml) H02 Split clamp with ‘O’ ring FFKM (Kalrez) upto 275°C CK
(upto 100 bar, 500 ml - 2 ltr)
½ hp (500 ml - 2 ltr) H05
D2 Motor RPM J Control Panel

Up to 3000 rpm RT Touch screen -HMI panel TSP
Gear box up to 440 rpm R4
L Mounting
D3 Motor Type SS Trolley (50 ml to 1 ltr) TL
Ex-proof gas group IIC (Zone 1) XC M Certifications***
1/8 hp compact in line brushless DC motor BD
¼ hp compact in line brushless DC motor QD
*Stirred options can be in place of standard or additional multiple interchangeable.
**All option specified in G are addons & multiple/ all of them can be availed at the same time.
***Country specific certification like CRN for Canada, AS1210 for Australia & DOSH for Malaysia can be offered on request.
14
®
Fully Automated High Through-put Catalyst Screening

• Faster screening of catalysts by running all autoclaves in similar conditions
• Volumes: 50 ml - 750 ml, 4 or 6 nos. parallel autoclaves
• Pressures upto 350 bar & temperatures upto 500 °C
• Material: SS 316, Hastelloy B/C, Monel, Inconel, Titanium, Tantalum etc.
• Fully automated process without human intervention with manual mode
for emergency/ malfunction/ bypass
• SCADA software with suitable laptop for remote set points, control &
recording of temperature, pressure, speed control, H2 gas flow rates, total
H2 consumed with batch reports & online / history graphs
• Highly advanced programming & recipe management for leak test, N2 / H2
flushing, temperature profiling, speed control, H2 purging, pressure
control with H2 gas uptake, heating, cooling, vent etc.
• Safety alarm & suitable interlocks for high & low temperature / pressure
along with suitable safety rupture discs
• Highly advanced & compact for fitting in fume hood
• Complete SS construction
• For multiple autoclave specifications & enquiry refer page 12 - 14
Eco Catalyst Screening

Salient Features:
• Eco-cat 6 - 25: 6 parallel reactors of 25ml volume each with common
bottom stirring, heating & lid
• Eco-cat 7 - 25: 7 parallel reactors of 25 ml volume each with common
bottom stirring, heating & independent lid
• Eco-cat 24 - 10: 24 parallel reactors of 10 ml volume each with common
bottom stirring, heating & lid
• Design pressure of 100 bar at 200°C
• Maximum stirring speed 1000 RPM
• Material: SS 316, Hastelloy C, Inconel, Monel, Titanium & Tantalum etc.
• Very compact & economical system
• Ideal for high through-put catalyst screening
• Optional glass/ PTFE liner
Eco-cat 6 - 25 Eco-cat 7 - 25
15
®
Bottom Stirred Autoclaves
Salient features
• Single or multiple bottom stirred autoclaves
• Very compact & economical
• Fully covered SS enclosure for vessel stability
• Uniform circumferential heating & accurate temperature control
Standard models for bottom stirred autoclaves

Volume 25 ml 50 ml 100 ml
Model No. B 1112 B 1122 B 1212 B 1222 B 1312 B 1322
Design Pressure 100 bar 200 bar 100 bar 200 bar 100 bar 200 bar
Design Temperature 200°C
Vessel Internal Height (mm) 40 63 83
Volume 250 ml 500 ml 750 ml

Model No. B 1412 B 1422 B 2112 B 2122 B 2212 B 2222
Design Pressure 100 bar 200 bar 100 bar 200 bar 100 bar 200 bar
Design Temperature 200°C
Vessel Internal Height (mm) 80 118 193
Note: The above ratings are only for SS316, Hastelloy C & Inconel materials, for other materials the ratings will change depending on its stress value
& maximum allowable temperature as per ASME code for which refer page 21 in material of construction.
Multiple bottom stirred autoclaves

• Add the number of autoclaves (4 or 6) as suffix after B in all models above for multiple bottom stirred autoclaves
• Example for 6 autoclaves of 100 ml, 100 bar model number will be B6 1312
16
®
Nozzle orientation & internals for bottom stirred autoclaves

Pressure relief Thermowell Cooling coil
Pressure gauge Funnel
Powder inlet
ball valve
Vent valve
Dip tube
Sample valve
Thermowell
Pressure
transmitter (optional) Helical
Gas inlet
Safety
cooling coil
rapture disc
Technical specifications for bottom stirred autoclaves standard models

A Material of Construction SS 316
C Heating Type Electrical ceramic band heater with cladding & insulation
D Stirrer Bottom magnetic stirrer & teflon bar
E Standard Nozzles, External Valves &Fittings:
Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube, vent
needle valve, solenoid valve at inlet of cooling coil
Internal Fittings:
Serpentine cooling coil (50 ml to 250 ml), Helical cooling coil (500 ml & 750 ml), dip tube, thermowell with
RTD PT 100 sensor
F Gasket PTFE
G Closure Type Split clamp with clamp bolts
H Control Panel Built in control panel with microprocessor based programmable PID temperature controller with high
temperature alarm & motor speed indicator mounted on it
I Power Supply 1 Ø, 220 V AC, 50 / 60 Hz
J Mounting & Dimensions Mounting Reactor Volume in ml Dimensions in mm
(W x D x H) SS Table Top 25, 50, 100 & 250 280 x 320 x 480
500 280 x 320 x 570
750 280 x 320 x 570
4 x 25 / 50 / 100 / 250 1200 x 320 x 480
4 x 500 1200 x 320 x 570
4 x 750 1500 x 320 x 570
6 x 25 / 50 / 100 / 250 1750 x 320 x 480
6 x 500 1750 x 320 x 570
6 x 750 1750 x 320 x 570
Enquiry guide for bottom stirred autoclave customized models

Enquiry code structure is B/B4/B6 Standard Model No A-G where A, G options can be selected from below tables. The below options will be
in place of standard supply. For example 250 ml, 200 bar, 200°C, Inconel 600, threaded cap with 'O' ring-FKM (Viton) up to 225°C autoclave code
will read as B 1422-IN6-CV
Options
A Material of Construction G Closure Type
SS 316 L 316L Inconel 625 IN5 Threaded cap with 'O' ring-FKM (Viton) upto 225°C CV
Hastelloy C 276 HC6 Titanium Gr. 2 TI2 (50 ml - 250 ml)
Threaded with ‘O’ ring FFKM (Kalrez) upto 275°C CK
Hastelloy C 22 HC2 Zirconium 702 ZR7 (50 ml - 250 ml)
Hastelloy B HAB Tantalum TAN Split clamp with 'O' ring-FKM (Viton) upto 225°C CV
Monel 400 MN4 Tantalum lined TNL (upto 100 bar, 500 / 750 ml)
Inconel 600 IN6 Split clamp with ‘O’ ring FFKM (Kalrez) upto 275°C CK
(upto 100 bar, 500 / 750 ml)
17
®
Glass Autoclaves
Bottom heated Glass-PEEK Interchangeable glass & metal autoclaves

glass autoclave jacketted autoclave
Salient features
• 100 ml to 2 ltr net filling volume • Bottom heated, jacketed & triple walled options
• Pressures upto 10 bar & temperatures upto 200°C • Interchangeable glass & high pressure metal autoclaves
• Glass with metal/PEEK • With suitable safety guard
Standard models for glass autoclaves
Volume 100 ml 500 ml 1 ltr 2 ltr
Model No. G 1360 G 1370 G 2160 G 2170 G 2360 G 2370 G 2460 G 2470
Design Pressure 6 bar 10 bar 6 bar 10 bar 6 bar 10 bar 6 bar 10 bar
Design Temperature 150°C (option up to 200°C in Jacketed glass vessel)
Vessel I/D (mm) 40 75 101.6
Vessel Internal Height (mm) 83 118 163 303
Min. Stirrable Volume (ml) 20 60 130
Note: The above ratings are only for glass material, for other materials the rating will change depending on its stress value & maximum allowable
temperature as per ASME code for which refer page 21 in material of construction.
Technical specification for glass autoclaves standard models

A Material of Construction Borosilicate glass cylinder with other wetted parts of SS 316
C Heating Type Electrical plate heater from bottom (jacket optional)
D Motor 1/8 hp AC motor with 100-1450 RPM (100 ml)
¼ hp AC motor with 100-1450 RPM (500 ml to 2 ltr)
E Shaft Sealing Zero leakage magnetic drive coupling M8 with 0.8 Nm torque for 100 ml,
Zero leakage magnetic drive coupling M20 with 2 Nm torque for 500 ml to 2 ltr
F Stirrer 4 bladed turbine stirrer (100 ml)
2 stage 6 bladed turbine stirrer (500 ml to 2 ltr)
G Standard Nozzles, External Valves & Fittings:
Valves & Fittings Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle
valve with common dip tube, vent needle valve, solenoid valve at inlet of
cooling coil (100 ml)
Internal Fittings:
Serpentine cooling coil (100 ml), Helical cooling coil (500 ml to 2 ltr), dip
tube, thermowell with RTD PT 100 sensor
H Gasket PTFE
I Control Panel SS control panel with programmable PID temperature controller & high
temperature alarm and variable frequency drive for motor speed control
J Power Supply 1 Ø, 220 V AC, 50 / 60 Hz
K Mounting & Dimensions Mounting Reactor Volume Dimensions in (mm)
(W x D x H) without control panel*
SS Table Top 100ml 300 x 300 x 700
500 ml 320 x 300 x 700
1 ltr 380 x 310 x 910
2 ltr 380 x 310 x 1050
L Guard Polycarbonate guard will be provided around glass body
*For table top models control panel is 275 mm x 275 mm x 300 mm (W x D x H) 2 ltr jacketed glass
18
®
Enquiry guide for glass autoclave customized models

Enquiry code structure is Standard Model no-A-B-C-D1-D2-D3-F-G-I-K-L-M where A, B, C, D1, D2, D3, F, G, I, J, K, L & M options can be
selected from below tables. The below options will be in place of standard supply. For example 1 ltr, 6 bar, 200°C, Hastelloy C, fixed head with
pneumatic vessel rasing lowering autoclave, jacketed glass vessel, ¼ hp, ex-proof CE ATEX certified motor, ruston turbine autoclave code
will read as G 2360-HC6-P-EJ-H02-AZ-SR
Options
A Material of Construction (other wetted parts) F Stirrer Options**

PEEK PEK Nickel 200 NK2 Hollow shaft with gas induction Impeller SH
Hastelloy C 276 HC6 Titanium Gr. 2 TI2 Anchor (with serpentine cooling coil, max 100 rpm)) SA
Hastelloy B HAB Zirconium 702 ZR7 Spiral (no cooling coil, max 100 rpm) SS
Monel 400 MN4 Tantalum TAN Ruston turbine SR
Inconel 600 IN6 Tantalum lined TNL Paddle SD
Propeller SP
Fixed head with manual vessel raising lowering K G Valves & Fittings (for 500 ml - 2 ltr)***
(100 ml & 500 ml)
Fixed head with manual vessel raising lowering & KT Serpentine cooling coil SCC
tilting (500 ml) Ball valve powder inlet ¼" with funnel BVP
Fixed head with pneumatic vessel raising lowering P Flush bottom valve (10 mm) FBV
(500 ml to 2 ltr) Baffles (with serpentine cooling coil) BFL
Fixed head with pneumatic vessel raising lowering & PT
I Control Panel
C Heating Style* Touch screen TSP
Jacketed glass vessel (up to 200°C) EJ
Triple walled double jacket glass vessel for heating & ET K Mounting & Overall Dimensions (approx)
vacuum insulation (up to 200°C)
Mounting Autoclave Autoclave with control panel Code
Volume approx. dia (WxDxH) in mm
D1 Motor HP 100 ml 1010 x 410 x 1450
¼ hp (for 100 ml) H02 Trolley 500 ml 1010 x 410 x 1450 TL
½ hp (for 500 ml to 2 ltr) H05 1 ltr 1040 x 410 x 1660
2 ltr 1040 x 410 x 1800
D2 Motor RPM
L Interchangeable Metal Autoclave
Up to 3000 rpm RT
Gear box up to 440 rpm R4 Interchangeable metal vessel of same volume up to IM
100 bar & 250°C
D3 Motor Type
M Mag Drive Torque
2 Nm (100 ml) M20
Ex-proof gas group IIC (Zone 1) XC
4 Nm (500 ml to 2 ltr) M40
8 Nm (500 ml to 2 ltr) M80
12 Nm (1 & 2 ltr) M120
1/8 hp compact in line brushless DC motor BD
¼ hp compact in line brushless DC motor QD
*Internal cooling coil & PID temperature controller will be removed for jacketed options.
**Stirrers can be in place of standard or can be offered additionally as interchangeable stirrers.
***All option in G are addons & can be inquired in single enquiry.
19
®
Material of Construction (MOC)

All wetted parts are made from SS-316 as standard. Material Selection Guide
Optional: AMAR gives recommendation for material selection for
SS-316L, Hastelloy B/C, Titanium, Monel, Nickel, Inconel, particular media, however it does not guarantee 100% corrosion
Zirconium, Tantalum, Carbon Steel etc. for different liquids resistance of a particular material to a particular corrosive
corrosive to SS-316. Other special alloys like A286, Alloy 20, media, as the same depends on various parameters like
duplex steel etc. can also be offered. temperature, pressure, concentration etc. of the reactions.
Reactor vessels of material SS316, upto 5 ltr are machined from
Note: Amar offers all the internal & optionally external wetted
rolled / forged bar stock & reactors above 5 ltr are normally
parts in the same material of construction as that of body &
fabricated from plates. SS316 autoclaves upto 100 ltr have lids
head to give fully corrosion resistant autoclaves.
made from rolled / forged bar stock. The material listed below
may not be available in all possible sizes.
General corrosion properties of some metals & alloys* :

RATINGS
0. Unsuitable: Not available in the form required or not suitable for fabrication requirements or not suitable for corrosion conditions.
1. Poor to fair
2. Fair: For mild conditions or when periodic replacement is possible. Restricted use only.
3. Fair to good
4. Good: Suitable when superior alternatives are uneconomical
5. Good to excellent
6. Normally excellent
Small variations in service condition may appreciably affect corrosion. Therefore whenever possible, material choice is guided by a
combination of experience and laboratory site tests.
Materials Non-oxidizing or reducing media Liquids Gases

Acid Neutral Alkaline solutions e.g. Oxidizing Media Halogen and derivatives
solutions, solutions, Caustic Ammonium Acid Neutral Pitting Halogen Halide Hydrogen
excluding e.g. and mild hydroxide solutions, or media, Moist, Dry, e.g. acids, halides,
hydrochlo- many alkalies, and e.g. alkaline acid ferric e.g., fluorine moist, e.g. dry, e.g.,
ric, Phos- Non- excluding amines nitirc solutions chloride chlorine above hydrochloric dry,
phoric, oxidizing ammonium e.g. per solutions below dew point hydrolysis Hydrogen
sulfuric, salt hydroxide sulfates, dew products chloride
(most solutions, peroxides, point of organic
condition chlorides, chromates halides
many sulfates
organics)
Stainless Steel, 4 5 5 6 5 6 1 0 3 2 4<220°C
(SS 316) 3<400°C
Hastelloy C 5 6 5 6 4 6 5 5 4 4 4<400°C
276 3<480°C
Hastelloy B 6 5 4 4 0 3 0 1 3 5 4<400°C
3<480°C
Inconel 600 3 6 6 6 3 6 1 2 5 3 5<220°C
4<480°C
Monel 400 5 6 6 1 0 5 1 2 6 3 6<220°C
3<400°C
2<480°C
Nickel 200- 4 5 6 1 0 5 0 2 6 2 6<220°C
commercial 5<400°C
4<480°C
Titanium 3 6 2 6 6 6 6 6 0 1 0
Zirconium 702 3 6 2 6 6 6 2 6 1 6 0
• The above table is just for reference. Customers are advised to carry out their own tests with sample coupons under desired working conditions.
• From perry, chemical engineer's handbook
20
®
Stainless Steel 316/316L Inconel 600 / 625

SS316 & 316L have almost identical corrosion resistance It is a nickel alloy & offers excellent resistance to
properties, only difference being 316L is a low carbon stainless • Caustic acids & chlorides at high temperature & pressure
steel. when sulfur compounds are present
It has excellent corrosion resistance to • Reducing - oxidizing environment
• Most organic acid systems like acetic, formic etc. • Sulfur free gases
• Ammonia & most ammonia compounds • Very high temperature
• Many salts except chlorides
• Most commercial gases at moderate temperature & pressures.
• Hydrogen chloride, fluoride & chloride in scrupulously Nickel 200
anhydrous systems It offers excellent corrosion resistance to
It has poor resistance to • Handling concentrated alkalis
• Organic halides • Hot caustic environment
• Dilute sulfuric, phosphoric & nitric acids at high temperatures & • Chlorinated solvents & Phenol
pressures.
• Halogen acids at low temperature & in dilute forms
• Caustics, halogen salts, chlorides etc. Titanium Gr 2 / Gr 4
It is lighter material & has excellent corrosion resistance to
Hastelloy C 276 / C22/ C2000 • Oxidizing agents such as aqua regia & other mixed acids
• Nitric acid at all concentrations except red fuming nitric acid
Next most popular after SS316, it is a nickel, chromium, • Chloride ions, ferric chloride, cupric chloride & other hot
molybdenum alloy that has the widest corrosion resistance & is the chloride solutions.
most widely used alloy for corrosive media.
• Mild reducing media such as sulfuric & hydrochloric acid
It has excellent corrosion resistance to
• Titanium burns vigorously in presence of oxygen at high
• Variety of chloride compounds & chlorine contaminated temperatures & pressures.
material
The material becomes softer above 200°C & hence not
• Strong oxidizing chloride solutions such as wet chlorine & advisable above 200°C.
hydrochloride & sodium hypochlorite solutions
• Concentrated hydrochloric, sulfuric & phosphoric acids
Depending on the application C276, C22 or C2000 can be selected Zirconium
but C276 is the most common & easily available grade.
It offers excellent corrosion resistance to
• Reducing environments
Hastelloy B
• All chlorides except ferric & cupric
It is a nickel molybdenum alloy & offers excellent corrosion • Hydrochloride & sulfuric acids below 70% concentration
resistance to solutions of hydrochloric, sulfuric & phosphoric acid • Phosphoric, nitric acids & alkaline solutions
in all concentrations & at all temperatures in the absence of
oxidizing agents. It has poor resistance to oxidizing agents.
Monel 400 Tantalum

It has better resistance than nickel in reducing environments. It has Tantalum is practically inert to many oxidizing & reducing acids.
excellent corrosion resistance to It offers the best & most outstanding resistance to wide variety
of corrosive media including hydrochloric, nitric, sulfuric &
• Caustic solutions phosphoric acids. It is attacked by hot alkalis & hydrofluoric acid.
• Chlorinated salts The costs are prohibitive, however tantalum liner or tantalum
• Fluorine & hydrogen fluoride lined wetted parts can be offered. Small sizes such as
It has poor resistance to nitric acid & ammonia systems. 50 ml - 250 ml can be manufactured completely in Tantalum.
The maximum temperatures are restricted to 250°C only.
Chemical composition of different material of construction (major elements in %)

Sr. No. Material Fe Ni Cr Mo C Other Max. design temp. in °C
1. Stainless Steel SS316 60-67 9-12 18-21 2-3 0.08 2.0 Si, 1.5 Mn 600
2. Hastelloy-C276 4-7 55-63 14.5-16.5 15-17 0.01 Co 2.5, 3-4.5W 600
3. Hastelloy-B2 2 67-71 1 26-30 0.01 Co 1 427
4. Monel - 400 2 65 — — 0.3 2.3 - 3.1 Al, 482
0.35-0.85 Ti, 30 Cu
5. Inconel - 600 6-10 73-80 14-17 — 0.15 — 600
6. Inconel - 625 5 58 min 22-23 8-10 0.1 — 650
7. Nickel - 200 0.4 99.4 — — 0.15 — 316
8. Titanium Gr. 2/Gr. 4 99% Pure Titanium — — 316
9. Zirconium 702 95.5 — Zr, 4.5 HF — — 371
21
®
Autoclave Specifications
Head Mounting Style
Removable head design
This is the most commonly used option & available for all sizes of autoclaves. Here the body
rests on the stand / trolley & the head is lifted for charging, discharging & cleaning. The vessel
can be removed for charging / discharging / cleaning. This option is more common as the head
& vessel can be taken out easily for pressure testing, fitting accessories, servicing etc. The head
can be lifted & lowered by chain pulley or hydraulic arrangement on special request for
autoclaves above 5 ltr volume.
Optional:
a) Fixed head design with raising & lowering
In this system the head of the autoclave is fixed with motor stand & the vessel & heater are
raised & lowered manually by sliding or manually by scissor lift for 50 ml - 250 ml or by rotating
screw for 500 ml - 1 ltr or pneumatically / hydraulically. The vessel or heater can be slided
manually up & down for assembly or disassembly for 50 ml to 250 ml autoclaves, manually
screwed up & down for 500 ml to 1 ltr autoclaves & pneumatic lift is provided for 500 ml to 25 ltr
& hydraulic lift for 50 to 100 ltr autoclaves. This system is useful when head of the autoclave has
lot of fittings & accessories, making it difficult to lift the head & detach all the fittings after every
batch. Further, removing the heater for faster cooling & ease of lifting or lowering the vessel is
advantageous.
b) Fixed head design with raising, lowering & tilting
In this system head of the autoclave is fixed while a manual, pneumatic or hydraulic lift allows
the vessel (with heater) to be raised & lowered. When lowered the vessel can be tilted. This
system is very useful where a vessel needs cleaning after every batch & for highly viscous 50 ml & 100 ml interchangeable
material to discharge them easily just by tilting. reactors with fixed head design
750 ml fixed head design with 2 ltr fixed head with 2 ltr fixed head with pneumatic
manual screwed vessels raising lowering pneumatic vessel lift raising, lowering & tilting
Heating Types
Electrical ceramic band heater with ceramic wool insulation & cladding.
Optional:
a) Flameproof / explosion proof IIB + H2 certified, aluminium cast Heater for H2 gas with totally
enclosed heating element inside metal tube. Optionally the heater also has inbuilt cooling
coils & is useful when internal cooling coils are not possible / required. These are suitable (a)
when the maximum temperature inside the autoclave is less than 300°C. Heating rates are
lower in FLP heaters in comparison to ceramic band heaters
b) Sealed heater in SS enclosure with ex-proof group IIC / ATEX zone 1 / class 1 div. 2 certified
junction box
c) SS-304 jacket for oil / steam heating with insulation & cladding .
d) If direct electric heating is not permitted (due to spot heating), heater can be provided on
jacket with oil inside. The heater can heat the oil which can in turn heat autoclave uniformly.
e) External heater temperature thermocouple is provided with the cascade temperature (b) (c)
control to ensure safety of heater, vessel & accurate temperature control. It is a standard
feature in aluminum cast heaters.
f) All ceramic band heaters are CE marked.
22
®
Autoclave Specifications
Nozzles, Valves & Fittings
Pressure gauge, vent needle valve, safety rupture disc (rated to rupture at MAWP), internal
cooling coil, thermowell (with RTD-PT-100 temperature sensor) gas inlet & liquid sampling
needle valves with a common dip tube (sparger) upto the bottom. (a)
Optional:
a) Ball valve with funnel for powder / slurry / liquid inlet. These valves are 1/4”- 2” size &
depending on autoclave volume they can be used to charge solids or liquid slurry at (b)
atmospheric pressure or higher, provided a high pressure liquid charging pot is also ordered.
b) Flush bottom valve with almost zero dead volume (some times additional ball valve at the
outlet of flush bottom valve can be provided on special request).
c) Serpentine cooling coil instead of helical for easy cleaning (500 ml to 100 ltr)
d) Removable internal baffles for better stirring
e) Diaphragm pressure gauge: Teflon coated SS diaphragm, Hastelloy C / Tantalum etc.
diaphragm pressure gauge or Monel pressure gauge for corrosive media in non SS
autoclaves. (d)
Options (a), (b) & (d) are standard for autoclaves above 5 ltr volume.
Body & Head Sealing

i) Split clamp bolt design: (c) (e)
Split clamp type quick opening system with clamp bolts & tongue & groove sealing with PTFE
head gasket for temperatures upto 300°C & metallic grafoil head gasket for temperatures
upto 500°C.
ii) Self sealing design:
The head & body can alternatively be sealed by a self sealing design in which there are no
clamp bolts. Only the split clamps & FKM (Viton) / FFKM (Kalrez) 'O' ring can be used to give
sealing under pressure. The head with 'O' ring is fixed to the body by just sliding the split
clamps with latch. This is very easy & convenient for closing & opening the autoclave.
However with viton 'O' ring maximum temp. is 225°C & with Kalrez maximum temperature is
275°C. The more expensive Kalrez has better chemical resistance than viton. This sealing can
be offered for pressures of 100 bar only. While selecting a viton 'O' ring customers have to
check its compatibility with solvents, ammonia etc. as viton gets easily attacked by many of
them. This design is available upto 2 ltr only.
iii) Threaded sealing:
For 50 ml - 250 ml vessels there is alternative 'O' ring seal design with threaded clamp &
threaded vessel for ease of opening & tightening by hand. This design can be offered for
pressures upto 700 bar & temperature upto 225°C for Viton & 275°C for Kalrez 'O' ring.
Motor & Drive

a) Top mounted AC motor
Non flameproof CE marked or Flameproof (FLP)/ Explosion proof AC motor (for Group IIA/ IIB
gases) suitable in hazardous area for all flammable liquids / gases except hydrogen & acetylene Non FLP IIA, IIB IIC FLP motor /
with variable frequency drive & stirrer RPM indication. The motor is coupled to the magnetic AC motor FLP motor ATEX motor
drive directly by specially designed coupling ensuring quick engagement & disengagement of
motor from autoclave head. The direct coupling eliminates pulleys, belts & minimizes
transmission loses, noise, vibrations & maintenance. The frequency drive can indicate motor
current / Torque % (on selection). This is useful to monitor the change in viscosity of the liquid
under stirring. The frequency drive is mounted on a common control panel. It has the facility to Motor with
trip the motor on any overload, over voltage or over current. Variable speed drive gear box
RPM Range: 100 - 1450
Motor Options:
• Flameproof AC motor group IIC, Ideal for H2 gas
• Ex-proof CE ATEX zone 1 certified
• Ex-proof class 1 div. 2 certified
• Motors with gear box can be offered for stirring highly viscous material at low rpm (50 - 440 rpm)
• Motors with 2900 rpm for stirring at high speeds
b) Compact motor drive:
Compact inline brushless DC motor & magnetic drive & speed controller with indicator for 300-1200 rpm
for 50 ml - 25 ltr autoclaves. Very compact, economical & light weight. No external rotating part.
Compact motor drive

23
®
Zero Leakage Magnetic Drive Coupling

Application
These couplings are extremely useful for high pressure or high vacuum
applications where leakages are not permitted for continuous running.
They have replaced gland & mechanical sealing.
Construction & working

It is a zero leakage maintenance free coupling directly driven by the
motor. It consists of external magnet rotor, which is driven by the motor. A Outer rotor
stationary shell is threaded / bolted to reactor head & completely isolates Outer magnet
the external rotor from the inner rotor. As the external rotor rotates, the Inner magnet
internal rotor also rotates in synchronism. The reactor’s shaft is threaded
/ bolted / keyed to the inner rotor. High energy permanent rare earth Inner rotor
magnets are fixed inside the inner & outer rotors. A water cooling jacket
protects the magnets & other components from excessive temperature
arising from the reactor. Cooling jacket
Salient features
• Suitable upto 700 bar & 500°C
• High torque drives from 0.8 to 600 Nm
• Materials: SS316, Hastelloy C, Inconel, Titanium, Tantalum, PEEK etc.
• The gland/mechanical sealing needs replacement after every 200- Housing threaded
1000 hrs of working depending on application & is limited by maximum to reactor lid
pressure where as magnetic drive can run virtually life long without
leakage with minimum maintenance • Very useful for long or
round the clock reactions as in gland/mechanical sealing the whole
batch may be wasted in case of leakage
• Zero leakage implies zero breakdown & zero maintenance, hence large
savings in maintenance costs for years
• Safe while using toxic & hazardous chemicals as its leakage is totally
prevented
• No wastage of expensive liquids through leakage
• Almost no losses since these are friction free in synchronous
operations
• Minimum vibration transmission & hence smooth running
Cross-sectional view of magnetic
• The coupling is flexible & hence any over load results in coupling drive coupling for high pressure
slippage, thus preventing any damage to coupling, shaft or motor application (M series)
Magnetically Coupled Compact Stirrer - MM Series

• Top mounted compact integral Inline motor & magnetic drive
• Zero leakage during rotation under vacuum & under pressure
• No external rotation, rotation inside housing
• Noiseless, vibration free with infinite variable speed regulator &
indicator
• No stand required for mounting of the motor, hence no alignment,
vibration & noise problems
• Light weight, economical & very compact & hence occupies very less
table space
• Brushless DC motor with BL DC drive & rpm indicator.
• Available for autoclaves from 50 ml - 25 ltr capacity
• 300 - 1200 rpm
24
®
Magnetic Drive Coupling Specifications

Models - Magnetic Drive
• M-Series : Magnetic drives for metal autoclaves
• MM-Series : Inline motor & magnetic drive for metal autoclaves
Note: The number after the series indicates the torque capacity in Kg. cm for SS316 &
standard pressure rating. For other materials the actual torque may vary.
Various Models as per Torque Capacity M-Series M-Series MM-Series
Sr. Static torque capacity For reactor volume

No. Model No. Kg-cm. N-m. Standard Optional
(a) M08/MM08 8 0.78 50 ml - 250 ml –
(b) M20/MM20 20 1.96 500 ml - 5 ltr 50 ml - 250 ml
(c) M40/MM40 40 3.92 – 500 ml - 5 ltr
(d) M80/MM80 80 7.85 10 - 25 ltr 500 ml - 5 ltr
(e) M120/MM120 120 11.7 50 - 100 ltr 5 - 25 ltr
(f) M200 200 19.6 – 5 - 25 ltr
(g) M400 400 39.2
(h) M600 600 58.8
(i) M1200 1200 117.6
100 - 10,000 ltr
(j) M2400 2400 235.2
upto 20 hp motor & 300 rpm
(k) M3600 3600 352.8
(l) M4800 4800 470.4
(m) M6000 6000 588
Note: Magnetic drives of higher torque capacity (for reactors of any make0 can be designed on request. Drives with torque higher / lower than
recommended can be used for particular reactor size depending on motor hp / viscosities / stirrer design etc.
Technical Specifications
Description Standard Optional
Material wetted parts SS-316 Hastelloy C, Monel, Inconel, Zirconium, Titanium, PEEK*
Design pressure / max. Full Vacuum to 200 bar for (a) - (d) Upto 690 bar for (a) - (d)
allowable working 100bar for (e) - (g), Upto 350 bar for (e) - (g)
pressure 50 bar for (h) - (m) 100 bar for (h) - (m)
Max. working temperature 500°C with water cooling jacket --
at rated pressure & 200 °C PEEK MOC
Maximum RPM 1450 for (a) - (e) Upto 3000rpm for (a) - (d)
750 for (f) & (g)
500 for (h) - (m)
Note: As the pressure increases torque will decrease for same models.
* For PEEK material, design pressure 10 bar @ 200°C available in model no. (a), (b), (C) & (d) only with 50% torque.
Stirrer Types
a) Single or two stage, 4/6 bladed pitch blade turbine type impeller
(a) (b) (c) (d)
Optional:
b) Propeller. c) Ruston turbine. d) Paddle.
e) Hollow shaft for high mass transfer for any gas-liquid reaction.
f) Anchor / anchor with paddle / anchor with PTFE blades for viscous liquids at low rpm
(max. 100 rpm single or double helix optional).
g) Spiral for highly viscous polymers / mixtures with downward thrust at low rpm
(max. 100 rpm).
h) Helixane (helix cum anchor) for highly viscous material for inside and outside mixing.
Note: 1) Gear box has to be provided & cooling coil has to be removed & plugged or serpentine coil has
(e) (f) (g) (h)
to be opted for (f), (g) & (h).
2) High torque magnetic drive would be recommended for (f) to (h)
25
®
Autoclaves - Specifications
Control Panel
Compact SS-304 (for corrosion resistance & longer life) control panel with microprocessor based
accurate programmable PID temperature controller cum indicator with temperature alarm
system (settable), safety alarm & heater trip system for malfunctioning of controller/ sensor/ 3Ø panel
temperature rise beyond set limit. The motor speed drive is mounted on the same panel for
stirred autoclaves. 3 phase panels are provided with phase current indicator. This helps in
identifying if any of the 3 heaters or phases have failed. Motor, heater, cooling/ solenoid valve/
pump/ sensors etc. utilities are connected to panel by simple plug & socket arrangement. The
panel is very easy to open & all internal components are plug socket type, making replacement
easy. Digital pressure indicator/ controller, flow indicator, flow totaliser, motor torque / current
indicator, heater temperature cascade controller, level, pH, turbidity etc. indicators are provided
additionally on same common control panel depending on the optional accessories selected.
1Ø panels
Optional:
a) Digital temperature indicator in flameproof enclosure mounted on trolley & non FLP SS panel
mounted remotely in safe area.
b) Complete ex-proof - flame proof (FLP) Group IIA/IIB or IIC, ATEX zone 1, class 1 div. 2 certified
control panels mounted on trolley
Note: FLP panels should be opted only if the heater & motors are FLP and area is totally ex-
proof as FLP panels are too bulky & inconvenient for operation & maintenance. (a)
c) Touch screen panel with SCADA software for single or multiple autoclaves.
(b)
d) PLC based control panel with touch panel HMI or remote SCADA software & PC control.
e) Panels with RS 485 port for remote PC communication through SCADA software with local
display.
f) CE, UL / CSA marked control panels can be supplied on request.
3Ø panels (c)
(d)
Power Supply
50 / 60 Hz, 1Ø 230V 16 amp for autoclaves upto 5 ltr. & 20 amp for 10 ltr autoclave (or any size
autoclave with heating through jacket) & 50 / 60 Hz, 3Ø, 415V for 20 ltr & bigger autoclaves with
electrical heating.
Autoclave Mounting Options

Trolley, table / bench top, floor stand, lugs
Complete autoclave with motor drive assembly is mounted on easily movable SS-304 /
aluminum trolley (for corrosion resistance & longer life) with 4 lockable wheels & the trolley top
is big enough to mount the optional accessories & the control panel. Table / bench top model is
for keeping the autoclave on platform & inside fumehood. Table top mounting is offered for
sizes from 25 ml to 2 ltr only. In table top model the panel & accessories have to be mounted
separately. In floor stand mounting the autoclave mounting plate is supported by 4, SS-304 legs
without wheels. This is useful when there is space constraint or panel is mounted remotely. SS
lugs mounting can be provided for 20 - 100 ltr autoclaves.
25 ltr autoclave
500 ml Bench Top Reactor 20 ltr trolley autoclave (floor stand model)
26
®
Gas Induction / High Pressure Reactors
1000 ltr reactor 250 ltr 100 bar reactor 500 ltr reactor
with automated valves
Salient Features
• 100 to 2000 ltr (working) volumes
• Materials SS-316, 316L, Hastelloy B/C, Monel, Inconel, Nickel, Titanium, Zirconium etc.
• Design pressures upto 100bar ( 1450 psi)
• Maximum working temperatures upto 350 °C
• Zero leakage magnetic drive coupling from 20-600 Nm torque capacity
• High mass transfer hollow shaft with gas induction impeller (ideal for hydrogenation,
oxidation, ammination, chlorination, bromination & other gas-liquid reactions) pitch blade
turbine, anchor, propeller, paddle etc. for other applications
• Skid mounted complete pilot plant with accessories & automation
• All designs as per ASME codes
• 'U' stamp coded, PED certified reactors can be offered on request
• CE-ATEX / UL / CSA certified systems offered
• Jacketed or single / double limpet coil with insulation & cladding
• Upto 440 rpm infinite variable speed with suitable gear box
• Body flanges with bolts & teflon / spiral wound metallic gaskets for shell & dish sealing
• Monoblock design without body flange, offered depending on pressures & application
• Internal cooling coil, vent, liquid / powder charging, dip tube, thermowell, safety rupture disc,
pressure safety valve, flush bottom outlet, baffles, light & sight glass, handhole / manhole etc.
nozzles, manual / automated valves, fittings, ex-proof control panel & accessories offered
based on requirement
• Suitable catalyst filtration & recycling system offered for hydrogenation (refer page 48)
• Suitable catch pot & flame arrester to collect the vent (refer page 48)
• Lugs or floor stand skid mounted structure
250 ltr reactor
For other optional accessories refer page 44.
27
®
Non-Stirred Pressure Vessels
Salient features
• 25 ml to 100 ltr net filling volume standard models & 150 ltr to 2000 ltr customized solutions
• Available in different Materials of Construction (MOC) like SS-316, SS-316L, Hastelloy B/C,
Monel, Nickel, Inconel, Titanium, Tantalum, Tantalum lined, Zirconium etc.
• Ex-proof / ATEX / CE / PED / ASME U / U2 / CRN certified systems on request
• Fully automated PC controlled high pressure system / pilot plant to continuously monitor,
control & record various parameters
Applications
• For gas / liquid storage / charging under pressure
• For gas / liquid separation & collection
• For static, loop, electrochemical, corrosion studies
• For study of gas hydrate formation
• For supercritical fluid extraction
• For hydrogen induced disbonding tests
• For soaking of diamonds / precious stones
Standard models for 1000 series

Volume 25 ml
Model No. P 1113 P 1115 P 1123 P 1125 P 1133 P 1135
Vessel I/D (mm) 30
Volume 50 ml
Model No. P 1213 P 1215 P 1223 P 1225 P 1233 P 1235
Vessel I/D (mm) 40
Volume 100 ml
Model No. P 1313 P 1315 P 1323 P 1325 P 1333 P 1335
Vessel I/D (mm) 40
Volume 250 ml
Model No. P 1413 P 1415 P 1423 P 1425 P 1433 P 1435
Vessel I/D (mm) 65
28
®

Volume 500 ml
Model No. P 2113 P 2115 P 2123 P 2125 P 2133 P 2135
Volume 750 ml
Model No. P 2213 P 2215 P 2223 P 2225 P 2233 P 2235
Vessel I/D (mm) 75
Volume 1 ltr
Model No. P 2313 P 2315 P 2323 P 2325 P 2333 P 2335
Volume 2 ltr
Model No. P 2413 P 2415 P 2423 P 2425 P 2433 P 2435
Volume 5 ltr
Model No. P 2513 P 2515 P 2523 P 2525 P 2533 P 2535
Vessel I/D (mm) 152

Volume 10 ltr
Model No. P 3113 P 3115 P 3123 P 3125 P 3133 P 3135
Vessel I/D (mm) 183
Volume 20 ltr 25 ltr

Model No. P 3213 P 3215 P 3223 P 3225 P 3313 P 3315 P 3323 P 3325
Design Pressure 100 bar 200 bar 100 bar 200 bar
Design Temperature 300°C 500°C 300°C 500°C 300°C 500°C 300°C 500°C
Vessel I/D (mm) 248
Volume 50 ltr 100 ltr

Model No. P 3403 P 3405 P 3413 P 3515 P 3503 P 3505 P 3513 P 3515
Design Pressure 50 bar 100 bar 50 bar 100 bar
Vessel I/D (mm) 355 343 456 440
Vessel Internal Height (mm) 558 600 699 739
29
®
Nozzle orientation & internals
Pressure relief Thermowell Cooling coil

Pressure gauge Funnel
Powder inlet
ball valve
Vent valve Dip tube
Sample valve Thermowell
Pressure Helical
transmitter (optional) cooling coil
Gas inlet
Safety
rapture disc
Valve details
Vessel volume Needle Valve Ball Valve Flush Bottom Valve
50 ml - 250 ml 1/8" — —
500 ml - 5 ltr ¼" ¼" 10 mm
10 ltr - 25 ltr ½" ¾" 15 mm
50 ltr - 100 ltr ½" 1" 25 mm
Technical specifications for non-stirred pressure vessel standard models

B Head mounting style Removable head and vessel design
C Standard Nozzles, External Valves &Fittings:
Valves & Fittings Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube, vent
needle valve, solenoid valve at inlet of cooling coil (50 ml to 250 ml), ball valve for powder / liquid inlet
(10 ltr to 100 ltr), flush bottom valve (10 ltr to 100 ltr)
Internal Fittings:
Serpentine cooling coil (50 ml to 250 ml), Helical cooling coil (500 ml to 100 ltr), dip tube, thermowell with
RTD PT 100 sensor
D Gasket PTFE up to 300°C and metallic grafoil gasket up to 500°C
E Closure Type Split clamp with clamp bolts
F Mounting & Dimensions Mounting Vessel Volume Dimensions
(W x D x H) mm 25 ml, 50 ml, 100ml, 250 ml 275 x 230 x 500
500 ml 320 x 270 x 630
SS Table Top
750 ml 320 x 270 x 630
1 ltr 355 x 310 x 710
2 ltr 355 x 400 x 990
5 ltr 420 x 355 x 990
10 ltr 585 x 560 x 1600
Floor Stand 20 ltr 600 x 560 x 1650
25 ltr 600 x 560 x 1650
50 ltr 675 x 675 x 1700
100 ltr 780 x 780 x 1750
30
®
Enquiry guide for non-stirred pressure vessel customized models

Enquiry code structure is Standard Model no-A-B-C-E-F-H-I-J where A, B, C, E, F, H, I & J options can be selected from below tables. The
below options will be in place of standard supply. For example 500 ml, 100 bar, 300°C, Hastelloy C, fixed head autoclave with ATEX Zone1
certified, heater & panel will read as P 2113-HC6-K-EZ-ATP
Options F Mounting & Overall Dimensions (approx)

Mounting Volume Reactor Reactor dia. with control Code
A Material of Construction
panel (W x D x H) mm
SS 316 L 316L Inconel 625 IN5 SS Trolley 25 ml, 50 ml, TL
Hastelloy C 276 HC6 Nickel 200 NK2 1010 x 410 x 850
100 ml, 250 ml
Hastelloy C 22 HC2 Titanium Gr. 2 TI2 500 ml
Hastelloy B HAB Zirconium 702 ZR7 1010 x 410 x 880
750 ml
Monel 400 MN4 Tantalum TAN 1 ltr 1040 x 410 x 890
Inconel 600 IN6 Tantalum lined TNL 2 ltr 1040 x 410 x 1140
5 ltr 1100 x 410 x 1140
B Head Mounting Style 10 ltr 1310 x 585 x 1750
Fixed head with manual vessel raising lowering K 20 ltr 1310 x 600 x 1800
(50 ml to 750 ml) 25 ltr 1310 x 600 x 1800
Fixed head with manual vessel raising lowering & KT 50 ltr 1500 x 675 x 1850
tilting 500 ml & 750 ml) 100 ltr 1550 x 780 x 1900
Fixed head with pneumatic vessel raising lowering P
(500 ml to 25 ltr)
Fixed head with pneumatic vessel raising lowering & PT H Heating Style
Electric ceramic band heater EC
Fixed head with hydraulic vessel raising lowering H
(50 ltr & 100 ltr) Electrical ex-proof IIB + H2 certified EA
Fixed head with hydraulic vessel raising lowering & HT Electrical ex-proof ATEX Zone1 certified EZ
tilting (50 ltr & 100 ltr) Electrical ex-proof Class 1 Div 2 certified EC
C Valves & Fittings* Welded SS 304 jacket with electrical ceramic heater JH
Limpet Coil SS 304 with insulation (50 L & 100 L) LC
Serpentine cooling coil (500 ml - 100 ltr) SCC
Ball valve powder inlet (500 ml - 5 ltr) BVP
Flush bottom valve (500 ml - 5 ltr) FBV I Control Panel
SS control panel with programmable PID temperature STD
E Closure Type (up to 2 ltr) controller & high temperature alarm
Threaded with 'O' ring-FKM (Viton) up to 225°C CV Ex-proof group IIC zone 1 certified F2C
(25 ml - 250 ml)
Threaded with ‘O’ ring FFKM (Kalrez) up to 275°C CK
(25 ml - 250 ml) Ex-proof ATEX zone 1 certified ATP
Split clamp with 'O' ring-FKM (Viton) up to 225°C & CV Touch screen TSP
100 bar, 500 ml - 2 ltr
Split clamp with ‘O’ ring FFKM (Kalrez) up to 275°C & CK J Certificaions**
100 bar, 500 ml - 2 ltr
ASME U stamp coded ASU
5) Customised power supply can be offered on request.
*All option specified in C are addons & multiple/ all of them can be availed at the same time.
**Country specific certifications like CRN for Canada, AS1210 for Australia & DOSH for Malaysia can be offered on request.
31
®
Acid Digestion Bombs / Hydrothermal Pressure Vessels
Salient features
• Design pressures upto 200 bar and temperatures upto 250°C
• Acid digestion vessels made from SS-316 with PTFE liner & PTFE cap
• Non-metallic microwaveable Acid digestion bombs
Applications
• Used for dissolving or digesting inorganic or organic samples in
strong acids or alkalis
Standard models for acid digestion bombs

Volume 25 ml 50 ml 100 ml 250 ml 500 ml 750 ml
Model No. D 1112 D 1212 D 1312 D 1412 D 2112 D 2212
Design Pressure 100 bar
Design Temperature 200°C (optional 250 °C with carbon filled PTFE)*
Vessel I/D (mm) 22 35 44 45 60 60
Vessel Internal Height (mm) 70 55 70 160 180 270
Standard models for microwaveable acid digestion bombs

Volume 25 ml 50 ml
Model No. D 1102 D 1202
Design Pressure 50 bar
Design Temperature 200°C (optional 250 °C with carbon filled PTFE)*
Technical specifications for acid digestion bombs

A Material of Construction PTFE liner & cap inside SS 304 / high temperature resistant polymer for microwaveable models
B Standard Fittings Safety rupture disc.
C Closure Split clamp with clamp bolts for metal models & threaded for polymer models
D Mounting Vessel fixture & Suitable spanner
Note: Customization of volume, material, pressure, temperature etc. may be possible on request.
*Suffix the standard models with C for 250°C option.
32
®
Shaker Hydrogenator
Salient Features
• 100 ml - 2 ltr volume in glass & metal interchangeable vessels
• Pressures upto 20 bar (300 psi) for metal vessel & 3 bar (45 psi) for glass vessel
• Used for synthesizing or modifying organic compounds by catalytic hydrogenation
• Used to study catalyst activity
• Economical considering the interchangeability of different capacity & different material vessels in one unit
Standard models for shaker hydrogenator

Volume 100 ml 500 ml 1 ltr 2 ltr
Model No. SM 1282 SG 1260 SM 2082 SG 2060 SM 2282 SG 2260 SM 2382 SG 2360
Design Pressure 20 bar 3 bar 20 bar 3 bar 20 bar 3 bar 20 bar 3 bar
Technical specification for shaker hydrogenator standard models

A Material of Construction SS 316 vessel for SM series / Glass vessel for SG series
B Drive ½ hp, ex-proof IIA / IIB AC motor with variable speed drive panel for 20 - 200 oscillations / minute rocking
C Gas Cylinder 4 ltr cap. gas cylinder of SS-304 with inlet, outlet valves, pressure safety valve, pressure gauge & flexible
hose pipe with NRV to feed gas into the vessel while in motion
D Standard Fittings Vent valve, dip tube with sampling valve, 2” opening on top for powder / liquid inlet & cleaning,
(for metal vessel only) thermowell, pressure safety valve
E Power Supply 1Ø, 220 V AC, 50 / 60 Hz
F Mounting & Dimensions Mounting Dimensions
(W x D x H) mm Table Top 850 x 700 x 700
G Safety Shield SS wire grid (for glass vessel only)
Enquiry guide for customized models

Equiry code structure is Standard Model no A-F-H-I-J-K where A, F, H, I, J & K options can be selected from below tables. The below options
will be in place of standard supply. For example 500 ml, 20 bar, 200°C, Hastelloy C with ATEX Zone1 certified heater, motor & panel will read
as SM 2182-HC6-EZ-AZ-ATP. For interchangeable vessels add the vessel code & its material code if Hastelloy C for as many vessels required.
Options
A Material of Construction (wetted parts) K Certifications
Hastelloy C 276 HC6 CE marked panel & electrical parts ECE
F Mounting & Dimension (mm) (approx)
Floor Stand 850 x 700 x 1300 (W x D x H) FS L Interchangeable Metal Vessels*
Interchangeable metal vessels 100 ml M13
H Heating Style Interchangeable metal vessels 500 ml M21
Electric band heater EC Interchangeable metal vessels 1 ltr M23
Electrical ex-proof, IIB + H2 certified (only for SM) EA Interchangeable metal vessels 2 ltr M24
Electrical ex-proof ATEX Zone1 certified (only for SM) EZ
Electrical ex-proof Class 1 Div 2 certified (only for SM) EC M Interchangeable Glass Vessels*
Interchangeable glass vessels 100 ml G13
I Motor Type
Interchangeable glass vessels 500 ml G21
Ex-proof gas group IIC (Zone 1) XC Interchangeable glass vessels 1 ltr G23
Ex-proof CE ATEX certified II 2G Ex de IIC T4 AZ Interchangeable glass vessels 2 ltr G24
Note: 1) Customer is advised to select best suited options for most
optimized price & delivery.
J Control Panel 2) For other optional accessories please refer page 44.
3) All above options may not be available / possible with all
SS control panel PID temperature controller STD models.
4) Customization of volume, material, pressure, temperature etc.
Ex-proof group IIC zone 1 certified F2C may be possible on request.
Ex-proof ATEX zone 1 certified ATP 5) Customised power supply can be offered on request.
6) Overall dimensions are indicative, they may change depending
Ex-proof class 1 div. 2 certified C12 on the optional accessories or specific design modifications
Touch screen TSP opted.
*Multiple options can be selected for one unit.
33
®
Supercritical Fluid Extraction Technology (SCFE)

Salient features
• 100 ml lab scale to 1000 ltr commercial plants offered
• Pressures upto 700 bar for lab scale units & upto 450 bar for commercial plants
• Semi or fully automated PLC based plants with CO2 recycling
• PED, U stamp, CE, CSA, UL certification optional
• Customizable designs as per client requirements
World-class technology for natural products

• There is a tremendous demand for high purity & residual solvent free extracts
of natural products. Also there is increasing requirement of eco-friendly
manufacturing processes for the extraction of natural products.
• Supercritical fluid extraction technology provides an economical solution to
providing a safe & eco-friendly way for extraction of natural products. Its
superiority over the conventional technologies of extraction, especially for
natural products in the food and pharmaceutical industry is well recognized.
• Supercritical CO2 textile dyeing is an emerging innovative waterless technology
for dyeing of textile fabrics that will revive the textile industries.
Commercial Applications:
• Extraction of natural products such as spice oil & oleoresins, flavors, fragrances, colors
• Decaffeination of tea & coffee
1 ltr extraction vessels in series & parallel
• Production of uniform &ultra fine particles for 700 bar pressure with CO2 pump for
• Supercritical CO2 (SCO2) textile dyeing of fabrics extraction of natural products
• Supercritical CO2 (SCO2) cleaning of high precision metal components
• Drying of aerogels
Advantages of SCFE
• Extract with delicacy & freshness close to natural
• High potency of active components
• Longer shelf life extracts
• Eco-friendly & green technology with no residual solvent & effluents
• High flexibility of process conditions
• Simultaneous fractionation of extracts
• High yields compared to solvent extracted products
• Low batch times for extraction
• Recycling of CO2
• Low operating cost Supercritical drying of Aerogels
Advantage of CO2 as a solvent

• Carbon dioxide is generally regarded as safe (GRAS) for food products.
Extractor PCV
• Inexpensive & easily available. Flow meter
CO2 Cylinder
• Non-toxic, non-flammable and inert to most materials. To Vent
Process description for lab-scale plants

The Carbon dioxide gas from the cylinder is first liquefied & then pressurized Separator
above the critical pressure of CO2 (73.8 bar) to the required pressure
necessary for extraction. This high pressure liquid CO2 is then heated above
CO2 Pump
the critical temperature of CO2 (31 °C) to the required temperature. CO2 Preheater Condenser
which is now in supercritical phase (SCCO2) enters the extractor where the
raw material is fed in powder form & the extraction is achieved on the basis
of solubility. The compounds dissolved in SCCO2 finally come to the
separator at atmospheric pressure & get precipitated. CO2 leaving the
separator is then measured by passing it through a CO2 gas flow meter. Brine chiller
Cosolvent pump
MEG + water
SCFE flow diagram for lab scale model
34
®
To vent
CO2 supply
CN E Extractor
S S
S1 Separator 1
E E 1 2 S2 Separator 2
T
2 PC Pre-cooler
PH Pre-heater
CN Condenser
T CO2 tank
PH CO2 pump PC
Co-solvent pump
PFD for commercial scale SCFE plant with CO2 recycling
Process description for commercial scale plant

The raw material in powder form is fed to the extractor. The liquid carbon
dioxide from the CO2 tank is precooled by passing it through the precooler.
This precooled liquid carbon dioxide is then pressurized by means of a
positive displacement plunger pump to a pressure above the critical
pressure of C02 (i.e. 73.8 bar). High pressure liquid CO2 is then heated above
the critical temperature of CO2 (i.e 31 °C) by passing it through preheater. CO2
which is now in the supercritical state enters the extractor in which the raw
material is loaded. The SCCO2 dissolves substances on the basis of solubility,
depending on operating conditions. The SCCO2 with soluble extracts enters
the separators where the pressure & temperature are reduced sequentially
so that solubility decreases & extract precipitates in the separators. Finally
the clean CO2 without any traces is recycled back to the CO2 tank via
condenser.
Specifications
MOC SS316
Volume (ltr) Design pressure (bar) Design temp. (°C)
Standard Optional Standard Optional
0.1 to 2 350 500, 700 100 200
5 to 25 350 500 100 200 SCFE plant for extraction of herbs
& production of fine particles.
50 to 100 350 NA 100 150
200 to 1000 350 NA 100 150
SCFE standard models

Model no. Working volume (ltr) Feed cap.* (kg/day)
E1331 0.1 0.24
SCFE plant for
E1431 0.25 0.6 the dyeing of
E2131 0.5 1.2 textile fabrics
E2331 1 2.4
E2431 2 4.8
E2531 5 12
E3131 10 24
E3331 25 60
E3431 50 120
E3531 100 240
E3631 200 480
E3731 500 1200
E3831 1000 2400
* The feed capacity is assuming bulk density of 0.4 kg/ltr of feed,
6 batches / day & one extractor. 5 ltr & above can be offered with 2
extractors & the feed capacity shall double the above given capacity.
• 5 ltr & above systems are offered with CO2 recycling & PLC controls.
35
®
Autoclaves for Corrosion Testing

Salient features
• Volumes from 500 ml to 25 ltr
• Design pressures upto350 bar and temperatures upto 650°C.
• Available in different materials of construction – SS 316, Hastelloy C, Inconel, Titanium etc.
• Stirred /Non-stirred autoclave systems
• Recirculating loop & electrochemical corrosion testing
• For static, dynamic, loop & electrochemical studies
Methods of testing corrosion using autoclave

• Weight loss method with corrosion coupons
• Electrical resistance probe
• Electrochemical probe
• Electrochemical noise in current or potential
Applications
• Autoclaves for corrosion application are mainly used in aggressive environments like H2S &
supercritical waters in oil refineries & defence industries.
• Electro - chemical corrosion measurements in HPHT media-water and other solutions
• Coating and materials evaluation in high pressure simulated deep sea condition (submarine
paint etc) using impedance measurements
• Autoclave for cement curing under deep sea applications as per API standard.
• Polymer testing /curing/processing under HPHT conditions
• Slow strain rate tests for stress corrosion cracking under HPHT conditions
Static & Stirred Autoclave

• Normally corrosion test coupons are suspended in static (non-stirred) or stirred autoclave
systems & corrosion is measured in terms of weight loss. In stirred autoclave system,
sometimes the coupon holders are attached to the shaft & rotated during testing.
• Autoclaves are then fed with the corrosive media & designed temperature & pressure
are reached & maintained in the autoclaves. Optionally suitable electrodes like pH or ORP
(MOC: SS316 / Hast-C) are provided to measure pH & redox potential under pressure.
• Autoclaves with working, counters / reference & auxillary electrodes can also be offered with
potential measurement system for electrochemical corrosion testing.
• For standard model selection refer page 2-11 for stirred autoclave & page 28-31 for non-
stirred pressure vessels
Re-circulating Loop Autoclaves for Corrosion Testing

In this system, the autoclave is connected with a special high pressure pump which can
recirculate water/liquid continuously at very high velocity through the test spool & the
autoclave connected in line with each other.
Rotating
coupon holder
assembly
36
®
Autoclaves for study of Gas Hydrate Formation

Salient features
• For examination / study of gas hydrate formation
• 100 ml to 100 ltr net filling volume
• Analysis of effectiveness & efficiency of thermo dynamic and kinetic gas hydrate
inhibitors
• MOC: SS316 / Hasteloy C etc.
• Glass window with camera for visual observation of gas hydrate formation
• Long term experiments of upto 30 days can be performed
Autoclaves for observation of gas hydrate formation

Gas hydrates are inclusion compounds of gases in a lattice of water molecules. Huge
amounts of methane are stored around the world under the sea floor in the form of solid
methane hydrates. Methane hydrates, represent a new and completely untapped
reservoir of fossil fuel, because they contain, immense amounts of methane, which is the
main component of natural gas. Methane hydrates belong to a group of substances called
Clathrates - substances in which one molecule type forms a crystal-like cage structure and
encloses another type of molecule. If the cage-forming molecule is water, it is called a
hydrate. If the molecule trapped in the water cage is a gas, it is a gas hydrate, like methane
hydrate. Methane hydrate also poses problems during transportation of natural gas.
Temperature and pressure conditions in pipelines especially in cold areas allow the
formation of hydrates. These hydrates form agglomerates and tend to clog valves, pumps,
pipelines and other parts. It is desirable to avoid the formation of hydrates rather than
removal of existing hydrate due to economical and safety reasons. The production as well
as study of artificial gas hydrates are done in special autoclaves like the gas hydrate
autoclave System, under specific pressure and temperature conditions. At room
temperature and normal atmospheric pressure, methane hydrate is unstable dissociating
into water and gas. Pipeline conditions can be simulated in the gas hydrate autoclaves
to check the effectiveness & optimization of hydrate-inhibitors. Pressure-resistant
borosilicate / quartz / sapphire-glass windows in the gas hydrate autoclaves allows the use
of one or multiple boroscope-cameras for observing or recording the processes of gas
hydrate formation inside the autoclave. The autoclaves can also be provided with magnetic
stirrer to simulate turbulent mixing conditions. Overhead stirrer can be connected to a
torque sensor to perform torque measurements to study viscosity changes. Refer page 42
for 25 ltr gas hydrate system.
High pressure vessel system for hydrogen induced disbonding tests

Amar manufactures & supplies systems for Hydrogen Induced Disbonding (HID) tests as per
ASTM G146. These tests are used to simulate & study the effects of hydrogen environment
under very high pressures from 150 - 250 bar & temperatures from 400 - 500°C on
bimetallic plates that are to be used under similar conditions in refineries. The results
indicate the resistance of bimetallic steels & its alloy to hydrogen induced disbonding. Such
tests can be used to decide the material metallurgy, its heat treatment, manufacturing &
fabrication technology for use in refineries in similar environments. The system can be
manually operated or completely automated.
Initially the test samples are put inside the vessel, pressurized with hydrogen to very high
pressure upto 150 - 200 bar & then heated to desired temperature of around 400 - 500°C
for a period of around 48 hrs. After the test is over, the vessel is cooled at a pre-defined rate
of around 150°C/hr till the temperature reaches 200°C. The vessel pressure is then released
completely & cooled further to remove the test samples.
Pressure vessels for soaking of diamonds & precious stones

• High pressure high temperature pressure vessels are often used to purify & improve the
finish of diamonds & precious stones by subjecting them to high pressure & temperature
conditions.
Pressure vessel for gas / liquid storage

• It can be used as a gas/ liquid storage pressure pot to transfer liquid/ gas in the autoclave/
other pressure vessel at higher pressure.
Note: For standard autoclave models refer page 2 to 11 & for non-stirred pressure vessels models
refer page 28 to 31.
37
®
Autoclaves for Reaction Calorimetry

Salient features
• Isothermal & non isothermal reactions
• Isoperibolic reactions
• Adiabatic reactions
• Constant heat balance, even in the reactor & reflux condenser
• Automatic cp-determination
• Fully automated & Excellent control
• 100 ml to 2 ltr volume
• Interchangeable glass & high pressure metal reactors
Applications
• Process development
• Safety
• Kinetic studies
• Scale-up
• Parallel chemistry
• Process optimization
• End point detection
Technical specifications for reaction calorimeter

A Volume 100 ml, 250 ml, 500 ml, 1 ltr & 2 ltr jacketed double or triple walled reactors with internal baffles &
bottom drain
B Material of construction Glass & PTFE, SS 316,Hastelloy C with interchangeable glass & metal vessels
C Pressure range Atmospheric for glass &100 bar for metal reactors to use as automated lab reactor
D Temperature range -50°C to 150°C (optional up to 250°C)
E Accuracy Typically 1 to 5% (dependent on settling time & external conditions)
F Calorimetric techniques Heat flow calorimetry (HFC) or power compensation calorimetry (PCC)
used
G Maximum reaction power 100W/ltr maximum (50W for power compensation calorimetry)
H Safety features Warnings, alarms & automatic shutdown can be set for the whole experiment & each process step
I Stirring options Pitch blade turbine, anchor, propeller, gas induction etc., interchangeable
J Shaft sealing zero leakage magnetic drive for metal reactors
K Motor Motor with control & monitoring of RPM from 100 to 1500 & optional torque indication
L Circulator options Amar, Julabo, Huber
M Dosing options Manual dosing, Syringe / HPLC pump for automatic volumetric dosing or peristaltic pump & balance for
gravimetric dosing
N Standard fittings & • Fast response reaction temperature sensor
sensor options • Jacket inlet temperature sensor
• PC controlled heater power supply
• Reactor heater,
Optional: pH, in-situ FTIR sensor, turbidity, pressure etc.
O Software & parameters PC SCADA software with all parameter monitoring, control & calculation with suitable alarm,
display programmable multistep ramp soak heating & cooling with recipe management
Calorimetry software for calculating enthalpy ( H), adiabatic temperature rise ( Tad), Maximum
temperature of synthesis reaction (MSTR), gas consumption, runaway or kinetics graphs etc.
Model no. for enquiry

C Materials code Volume code I
Glass-G 100 ml - 13 (If interchangeable
SS316-M 250 ml - 14 glass & metal reactor)
Hastelloy C-MHC 500 ml - 21
1 ltr - 23
2 ltr - 24
For example 500 ml glass calorimeter with interchangeable SS reactor will read as C-G-21-I
38
®
Continuous Stirred Tank Reactors (CSTR)
CSTR for hydrogenation
CSTR for hydro-cracking

Salient Features of heavy hydrocarbon oils
• Product is developed / produced on continuous basis for better productivity
• Stirred tank reactors of 25 ml to 2000 ltr net filling volume
• Available in different materials like SS-316 / 316L, Hastelloy C, Monel, Inconel, Nickel, Titanium, Tantalum, Zirconium etc.
• Single or multiple reactors connected in series
• Multiple inlets & outlets for addition & transfer / removal of gases & liquids
• Ex-proof / CE / PED / ASME / U stamp certified system on request
• Fully automated PC controlled systems to continuously monitor, record & control various parameters like temperature pressure, motor
speed, gas /liquid flow etc.
• Gas mass flow controller, metering pumps, level controller, catalyst filtration system with SCADA software etc. are provided for a typical
hydrogenation application.
• For technical specification refer page 2-11 for standard high pressure autoclaves
Interchangeable Liquid & Vapour

Phase Malshe's Reactor*
• Gas recycling through stationary or rotating catalyst basket
• Reactor volumes 100 ml - 100 ltr
• Multiphase reactor
• Materials: 316, Hastelloy, etc.
• Upto 3000 RPM
• Supplied with condenser & gas liquid separator & optionally liquid metering pump & gas
flow controller
• The same reactor setup can be used for liquid phase & vapour phase reactions with
minimum changes of internal components giving it great flexibility & cost economy.
• For technical specifications & enquiry refer page 2-11. Prefix MR with the autoclave code for
vapour phase Malshe's reactor & IMR for interchangeable liquid & vapour phase reactor.
* Patent pending
39
®
Pilot Plants / Customized Systems

10 ltr fully automated ex-proof
alkoxylation pilot plant
100 ltr ex-proof hydrogenation pilot

plant with catalyst charging, catalyst
filter with recycle, auto cooling system,
vacuum pump & catch pot
100 ltr polymerization

reactor for (2 million cP)
viscous polymer with High pressure fischer tropsch
hydraulic vessel raising reactor with gas booster, mass
lowering & tilting mechanism flow controller etc. accessories
& SCADA software
Phase transfer catalyst continuous reactor

system with simultaneous 3 different
impeller speeds at 3 different levels
40
®

Pilot Plant for
Styrene Butadiene
Emulsion Polymerisation
500 Ltr hydrogenation pilot plant

with catalyst filter & recycle
350 bar, 500°C interchangeable

metal autoclaves with
automatic inlet outlet pressure
control, heat exchanger & receiver
Ex-proof pilot plant for EO-PO reactions
Fully automated & semi continuous pilot plant Autoclave with

for styrene butadiene emulsion polymerisation multiple view windows
with pneumatic vessel rasing, lowering & tilting
41
®
Bottom driven autoclave 25 ltr titanium high vacuum

25 ltr autoclave for study of reactor lid with homogenizer &
gas hydrate formation anchor with PTFE wiper blades
50 ltr high pressure system Batch reactor

50 ltr pitch impregnation equipment for for visbreaking process
processing high temperature carbon-fiber,
composites using pitch monomer / coal demoralization
Other special high pressure applications

• Hydrothermal synthesis of zeolites, synthetic clays
• For bauxite digestion
• For alkaline / sulphuric acid leaching of ores
• For napthenic acid corrosion studies
• For crystalization
• For solubility studies of oxides
• For carrying out pulping & pulp bleaching experiment
• Polymer mini reactor for synthesis
2 ltr interchangeable SS & glass Reactor with reflux return

autoclave for ethoxylation or take off
42
®
Low pressure customized reactors with

Heating Cooling Circulators
Salient features
• Low pressure jacketed reactors upto 10 bar & 250°C
• With zero leakage magnetic drive capacity or gland sealing
• 500 ml to 2000 ltr capacity
• Materials: SS316, Hastelloy C, Inconel, Titanium, Tantalum lined etc.
• Supplied along with heating cooling circulators
• From -80°C to 250°C
• Supplied with valves, fittings, control panel, temperature, pressure,
liquid flow controls with automatation & software
1 ltr. table top model jacketed reactor
with full length view window
ATEX certified system
Multipurpose pressure reactor with

column & distillation assembly
High pressure polytest reactor system

43
®
Optional Accessories
Optional accessories are offered to increase the versatility of the equipment, to add value &
feature to the standard product & to provide complete range of instrument/ equipment
required for a particular application. Most of the optional accessories are common for stirred,
non-stirred, glass, shaker & fabricated reactors unless specified. The standard optional
accessories can be enquired by simply mentioning their code & required specifications.
Complete mounting of all the accessories shall be done on autoclave stand / trolley.
All the indicators / controllers are mounted on a common SS panel.
Gas Pressure Regulator (FPR)

To manually charge different gases at desired pressures upto 140 bar / 2000 psi or higher
into the reactor from gas cylinder. Nitrogen, Oxygen & Hydrogen can be charged through
same regulator (with special adaptor). The regulator is made from SS316 & comes with inlet -
outlet pressure gauges & flexible SS braided Teflon PTFE high pressure hose pipe (4m long) with
non return valve.
Optional: 1) Regulators upto 350 bar, automated regulator
2) Regulator for other gases like NH3, CO2 etc. & MOC of Hastelloy C
3) Pressure reducing station with auto changeover
Gas Booster (GB)

Gas Booster
Gas boosters are useful when the cylinder pressures are much lower than the autoclave rated
pressures. In such case the booster takes gas at lower pressure from cylinder & compresses the
same to deliver at higher pressures. They are generally pneumatically operated. Special gas
booster pumps are available for liquid CO2 used in supercritical fluid extraction system. The
booster systems are supplied with air filter regulator, pressure relief valves, inlet-outlet pressure SS mounting with
gauges, valves & flexible hose pipe. all fittings & valves
Optional: • Boosters upto 700 bar pressure
Thermal Gas Mass Flow Meter (MFM) / Controller (MFC)

MFM can be used to measure accurate mass flow rate of gas (in gm/hr or LPH) & totalized
quantity of mass / volume (in gms/ltr) charged in the autoclave at any point. Mass flow
controller (MFC) is used to charge the set flow rate of gas into the autoclave at high pressures up Flow Indicator
to 100 bar or it can be used in pressure control mode to indicate the gas flow & total gas uptake MFC & Totaliser
to maintain desired set pressure inside the autoclave (ideal for hydrogenation). The same MFM /
MFC can be used for multiple gases by just entering the conversion factor for different gas
densities provided the gases are inert to each other. The MFM/MFC comes with high pressure
flexible hose, inlet filter with digital gas flow indicator cum totalizer & additional pressure PID
controller with pressure sensor if the MFC is used in pressure control mode. User has to specify
the maximum flow rate range, pressure, gas & mode (flow control or pressure control) for Ex-proof MFC
ordering MFM/MFC.
Optional: 1) Ex-proof MFM / MFC can be offered on request.
2) MFM/MFC upto 300 bar pressure
Coriolis Gas - Liquid Mass Flow Meter/Controller (CFM/CFC)

These are used for higher & accurate gas or liquid flow rate indication or control in cases where
thermal mass flow meters are not suitable. A common meter can be used for different gases & Coriolis Mass Coriolis Mass Flow
liquids for a particular range of flow. Flow Meter Controller
Optional: • Ex-proof CFM/CFC can be offered on request
Digital Pressure Indicator / Controller (DPI)

It consists of SS316 pressure sensor (transmitter) & digital pressure indicator/ controller
(mounted on common control panel) with pressure alarm & optionally heater cut off for safety.
Digital pressure indicator has pressure reading in bar & psi, where as controller reads any one of
the units. The controller is normally used with mass flow controllers (MFCs) or solenoid/flow
control valves to maintain constant pressure inside the autoclave. With MFC, gas flow indicator
& totalizer are also provided on the same panel. The pressure sensor has temperature limitation
upto 100°C & hence the same is provided with water cooling jacket.
Optional: 1) Intrinsically safe pressure sensor.
2) Pressure sensors with Hastelloy C / Inconel wetted parts can be offered on request.
Solenoid Valve Pressure Sensor
44
®
Liquid / Slurry / Gas Charging High Pressure Pot (HPP)
It is used to transfer liquids, slurries or gases in to the autoclave under pressure. It consists of
high pressure SS-316 pot designed for working pressure 100 bar or higher with port for nitrogen
gas (N2), liquid / slurry inlet with valve & funnel, outlet valve, pressure gauge, pressure safety
valve, high pressure hose & NRV. The liquid to be charged is fed into the pot from top funnel &
pressurized with N2 gas until its pressure is higher than the autoclave pressure & then under
pressure the liquid is charged into the autoclave. The quantity & rate of flow of liquid charged is
not known precisely in this system. However a level indicator or sight glass or weighing balance
or flow meter can be provided optionally to measure the liquid charged or its flow rate. Pots of
different pressure, M.O.C. & sizes can be offered.
These pots can also be used for storage of gases when gas cylinders are located at a far away
place. With this option approximate quantity or flow of gas consumed can also be determined
by measuring the pressure drop.
Volume: 250 ml, ½ ltr, 1 ltr, 2 ltr, 5 ltr, 10 ltr
Optional: a) Forward pressure regulators can be provided at the outlet of (FPR) pot if they are
used as gas charging.
b) Pots upto 200 bar / 350 bar
c) Pots in MOC Hastelloy C, Inconel, Monel, Titanium
Ethylene EO / Polypylene PO Oxide Pot (EPP)

It consists of SS 316 (EO/PO) horizontal pot with inlet, outlet valves, gas inlet with dip tube,
thermowell, pressure gauge & high pressure hose pipe for 10 bar working pressure.
It is used for ethoxylation / propoxylation.
Volume: 1 ltr, 2 ltr & 5 ltr
Optional: Ex-proof weighing balance to measure the quantity of EO/PO charged.
Liquid Metering Pump System (LMP)

This system is used to charge liquid at a desired rate from as low as 1 ml/hr to 100 ltr/hr, when
the autoclave is under pressurized condition. The system comes with a metering pump, flow
indicator, controller, liquid sump, pressure gauge, strainer & high pressure hose.
Pressure safety valve, flow totalizer can be offered on request. Types of pumps offered are: (b)
a) Diaphragm metering pumps for pressures upto 100 bar & minimum flow range of
60-600 ml/hr to maximum 10-100 lit/hr. The flow rates are varied by varying the motor
speed with variable frequency drive. Materials: SS316, option: Hastelloy C, Titanium, PTFE (a)
b) High pressure more accurate HPLC type low flow metering pumps for high pressures upto
350 bar & flow range from 0.01 upto 100ml/min.
These pumps can be used along with precision weighing scales to measure the total liquid
charged at any point of time. Materials: SS316, option: Hastelloy C, Titanium
(c)
c) High pressure syringe, PTFE diaphragm, gear, peristaltic pumps can be offered for pumping
corrosive chemicals at low / high pressures for specific application & flow rate condition. Weighing Scale
In line flow meters can be connected to measure & control the flow of the liquids.
Auto Cooling System (ACV /ACP)

This system is useful to control temperature overshoots for highly exothermic / out of control / (a) with FLP coil
runaway reactions as well as for faster cooling upon completion of reaction.
The control panel of the autoclave gives 230V, 1Ø output to connect external auto-cooling
system. Options available are:
a) Solenoid valve (ACV) for autoclaves upto 25 ltr or
b) Pneumatically actuated ball valves (ACV) for autoclaves above 25 ltr connected at the inlet
of the internal cooling coil with external source of water supply.
This is standard for 50 ml - 250 ml autoclaves, however for bigger autoclaves if the cold water line
pressure is less than 2 bar then it is better to opt for external pump & tank water cooling system.
Normal tap water cooling is not effective at higher temperatures due to steam back pressure
whereas pump & tank auto cooling system gives positive pressures & faster cooling. (b)
45
®
c) Pump & Water Cooling Tank (ACP): It consists of a SS 304 water tank & pump to circulate
water in the internal cooling coil of reactors. Cooling starts automatically if the rate of
heating rises suddenly. It comes with monoblock pump, tank, pipeline & flexible hose pipes
with quick release coupling & is mounted on the autoclave trolley itself. Ice can be put in the
water or the hot water can be discharged & fresh water replenished on continuous basis for
more effective and faster cooling.
Optional: Ex-proof group IIC pump (c)
Magnetic drive & pressure Sensor Cooling System (MCS)

It is a simple 10 ltr SS 304 tank with submersible pump to circulate water in the magnetic drive &
pressure sensor jacket to prevent temperature rise beyond 80°C. It is useful if tap water
connection is not near the autoclave & when water needs to be condensed.
Open Bath Heating Circulator (HB)

It is used to heat jacketed autoclave from ambient to 150°C by circulating thermic fluid inside the
jacket. It consist of bath, pump, level switch, heater & internal cooling coil for cooling from high
temperature to ambient temperature using chilled water or brine solution.
It is suitable for reactors up to 5 liter volume
Optional: Ex-proof heating bath
Closed Loop Heating Circulator (CLH)

It is used to heat jacketed autoclave from ambient to 350°C by circulating thermic fluid. It
consist of a closed pressure withstanding tank, magnetically coupled pump, heater, level
indicator & internal cooling coil for cooling from high temperature to ambient temperature
using chilled water or brine solution.
Suitable for reactors up to 100 ltr volume
Optional: Ex-proof circulator
Low temperature open bath circulator (CB)

It is used to cool or control reactor temperature to -50°C by circulating thermic fluid cooled to
up to -75°C inside the jacket or internal coil. It consists of a bath, pump, compressor, condenser
& level switch.
Heating Cooling open bath circulator (HCB)

It is used to heat, cool & control reactor temperature by circulating thermic fluid in the
autoclave jacket. It consists of a bath, pump, heater, compressor, condenser & level switch.
Temperature range: -25°C to 175°C.
Closed loop heating cooling circulator (CLS)

It is used to heat, cool & control reactor temperature by circulating thermic fluid in the
autoclave jacket. It consists of a bath, pump, heater, compressor, condenser & level switch.
Temperature range: -35°C to 200°C / -80°C to 180°C.
Suitable for reactors up to 1000 ltr volume.
Flow Control Valves (FOV / FCV)

These valves can be connected at jacket inlet for controlling flow of steam/ hot oil/ water for
temperature control from PID or at the inlet or outlet of the autoclaves for control of pressure.
Two options are available:
• (FOV) On/off pneumatic ball valve actuated by 230V output from panel to solenoid valve
inline of air supply
FOV FCV
• (FCV) Pneumatic proportionate flow control valves with I to P convertor (for accurate
temperature / pressure control).
Reflux Condenser (RC)

It is a jacketed single tube SS-316 heat exchanger with packing material inside used to reflux the
condensate back into the reactor & vent off the uncondensed vapours. It is connected directly
on the autoclave lid & works under full autoclave pressure. A receiver pot can be connected at
the bottom of the reflux condenser with valve for reflux take off. It is available in 0.01, 0.02 or
0.05 m² area.
Optional: Reflux condensers can be offered in different materials & area.
46
®
Condenser (CN)
It is a SS-316 shell & tube reverse flow heat exchanger for distillation/condensing vent vapours
from the autoclave upto 10 bar pressure. It is offered in different surface areas such as 0.1, 0.2,
0.5, 1 & 2 m². The condensate can be collected separately in a receiver or optionally refluxed
back into the reactor.
Optional: a) Higher area & pressures upto 350 bar
b) Different materials
c) Corrugated tubes heat exchangers for better efficiency / compact size.
Receiver Pot (RP)

SS 316 receiver pot can be connected at the outlet of the shell & tube or reflux condensor to
collect the condensate separately. It is also provided with a port to apply vacuum & offered in
250 ml, 500 ml, 1 ltr, 2 ltr & 5 ltr volumes. Higher volumes & other materials can be offered on
special request. It can be optionally provided with level indication.
Back Pressure Regulator (BPR)

It is SS 316 regulator mounted on the vent line of the autoclave & is used for maintaining
constant pressure inside the autoclave upto 350 bar. The pressure is maintained by releasing the
excess pressure into the atmosphere or through a hose to safe area. The pressure can be set
initially on the gauge, by manually varying the knob until the gas comes out. Once the set
pressure is exceeded the excess pressure is released until the autoclave pressure becomes equal
to or below the set pressure. The pressure release is slow & gradual & the set pressure can be
varied at any point. (a)
Optional: a) Electronic actuated digital pneumatic back pressure regulator, where the pressure
is set digitally & can be released at preset rate of pressure release (6 bar air supply
is required).
b) Pneumatically actuated pilot operated back pressure regulator (air / N2 gas supply
for rated pressure is required to activate the same) (b)
c) Electronic control unit & forward pressure regulator with 4 mtr. hose for activating
(b) above.
d) Materials: Hastelloy C, PTFE etc.
Pressure Safety Valve (PSV)

High pressure autoclaves are provided with built in safety rupture disc, however additional
safety can be offered by providing pressure safety valve for which release pressure can be set
manually by increasing or decreasing the spring tension or by simply changing the spring. The
set pressure should normally be around the design pressure. Safety relief valves are standard
supply for glass autoclave & shaker hydrogentor where rupture discs are not available for low
pressures. These valves come with PTFE / Kalrez O-rings.
Optional: Materials: Hastelloy C, inconel
Chain Pulley / Hydraulic Head Lifting System (PL/EL/HL)

For autoclave volumes from 10 ltr to 250 ltr & removable head design, the head & vessel are too
heavy to lift manually. Hence chain pulley block mounted on same trolley with SS Stand can be
offered for lifting the head with minimum efforts.
Optional: a) Electric (EL) chain pulley lift PL EL
b) Hydraullic lid (HL) lifting arrangement can be offered on request for any reactor
volume. Refer page 8 for picture of the same.
SCADA Software for remote operation & recording (SCD)

SCADA is a supervisory control & data acquisition software with all controllers / indicators
having RS 485 modbus communication port or PLC & HMI / touch panel, for online display, set
point changes & data logging of various parameters like pressure, temperature, motor RPM,
motor current / torque, liquid / gas flow rate with totaliser, heater temperature, level, pH, ORP,
turbidity, IR etc. remotely from PC as well as locally from panel. It gives continuous online data
logging at predefined (variable) time interval, online graphical representation as well as
historical data & graphs on PC for single or multiple autoclaves. RS 485-232 convertor & cable
upto 50 m or higher is also supplied.
Optional: Wireless data communication from PC to panel or mobile alerts can be supplied on
request.
47
®
Liners (LN)
Removable PTFE / Metal / Glass liners can be offered for autoclaves from 100 ml - 25 ltr. These
liners can be used for reactions that are corrosive, to prevent the autoclave body from corrosion.
PTFE & glass liners can be used upto 200°C & metal upto 500°C. The heat transfer is poor with
PTFE & glass liners. Glass liners cannot be fabricated accurately. Hence, Amar recommends the
use of completely corrosion resistant metal autoclaves made from special alloys like Hastelloy,
Inconel, Titanium etc. over glass/teflon liners. Liners should be used only if cost is the constraint
or corrosive chemicals are to be used sparingly. Metal liners can be offered in Hastelloy C ,
Inconel , Monel , Titanium etc. Teflon Metal Glass
Catalyst Basket (CBS/CBD)

It is provided to improve the efficiency of the catalysts & for holding the catalyst so that it will
not be destroyed or changed by the stirring action of impeller. The baskets are made from SS316
wire mesh & connected to the stirrer so that they rotate with the stirrer. It is available for 450 ml-
100 ltr autoclaves. The catalyst basket can be static which is stationary (CBS) or dynamic (CBD)
which rotates with the impeller.
Catalyst Filters (CF)

These are small 7 microns SS 316 sintered cup filters which are threaded to bottom of the
sampling dip tube so that the catalyst does not come out while sampling liquid. It is very useful
when the catalyst is expensive or pyrophoric. These filters may reduce the rate/ flow of the
sampling liquid due to the resistance offered by the fine mesh, hence they need regular
cleaning to prevent choking. Filters are available for 500 ml - 100 ltr autoclaves.
Optional: a) Different micron sizes
b) Materials: Hastelloy C
Catalyst Addition Device (CAD)

It is used for one time catalyst charging under pressure during the reaction. It consists of a 3 ml to
150 ml (depending on Autoclave size) small container with airtight cap, which is openable. The
powder is filled in the container which is then threaded to the autoclave head from below to a
separate port with needle valve on the top. Under atmospheric & pressurized conditions the
powder remains inside the container as the cap remains closed.
One has to apply gas pressure greater than autoclave pressure from the needle valve on that
port so that the cap opens & releases the catalyst inside the autoclave under pressure.
Depending on the optional accessories selected, the catalyst addition device may not be
possible due to space constraint on the head. Available for autoclave sizes 100 ml - 100 ltr & upto
250°C.
Catalyst Filtration & Recycling System (CFR)

It consists of vertical SS sintered filter cartridges in a SS housing. After the batch is over the
reactor liquid is transferred to the catalyst filter under reactor/nitrogen pressure. After filtration
is over, catalyst is taken back in to the reactor by back washing, thus recycling the same & making
it available for the next batch. Thus catalyst is never exposed to atmosphere & is reused.
Generally this system is suitable & available for 2 ltr to 2000 ltr reactor volume. These filters are
available with zero hold-up volume.
For small autoclaves
Catalyst Slurry Charging System (CSC)

It is a pressure reactor with magnetic drive stirring, inlet & outlet valves, pressure gauge &
nitrogen/vent. Solvent & catalyst are charged in the vessel & the slurry formed by mixing is
transferred under nitrogen pressure into the reactor. The pressure rating & volume of this
system is designed depending on the quantity of catalyst, pressure & temperature rating of the
autoclave. Specially designed control system developed by Amar can be offered to charge the
catalyst slurry in continuous mode at a pre-defined flow rate under pressure. This is very useful
for CSTR, where no suitable pumps are available for slurry. This system is available for any
reactor volume, pressures upto 350 bar & for a wide range materials.
48
®
Catch Pot (CP)
It is used to collect the vent vapours / gases from the autoclave vent / rupture disc /
safety valve port, when the vapour / gas is highly hazardous & cannot be released
directly into the atmosphere. It is a pressure vessel, designed depending on volume of
autoclave & its design pressure. It is provided with inlet, outlet, vent, dip tubes, pressure
gauge, safety valve & optionally a flame / flash back arrester. It is normally filled with
water. The gases / vapours collected are safely released through the flame / flash back
arrester to avoid any hazard. It is suitable & available for any autoclave volume.
Vacuum Pump (VP)

Suitable rotary vane or diaphragm oil fee vacuum pumps can be supplied for vacuum
from 100 mbar upto 0.001 mbar in the reactor. It is used either before starting the batch
or for high vacuum distillation. Suitable analogue or digital vacuum indicator with
controller can be offered on request. The reactor fittings would change for very high
vacuum & this may limit its pressure rating
View Windows / Light & Sight Glass (SG)

These are quartz / sapphire view glass windows / light & sight glass of small diameter or
along the length of the vessel with special cameras & software for continuous online
viewing / recording in jacketed vessels to see the reaction. Suitable for high pressures
upto 200 bar & any autoclave / reactor volume.
In Situ FTIR Spectroscopy (IR) Multiple view Round view Sight glass along
windows window the vessel length
In situ high temperature, high pressure infrared (IR) probe is offered for real time
chemical reaction monitoring. It provides specific information about reaction initiation,
conversion, intermediates & end point. Suitable for 1 ltr to 100 ltr reactors upto 100 bar
& 200°C.
Other Accessories / Options

a) Level transmitter (LT) / switch (LS) with indicator to measure or maintain level inside the
reactor under high pressure. Used mainly in CSTR.
b) pH/ turbidity (TB) / DO / ORP sensors with indicators & controllers for high pressure &
temperature application. pH can be controlled automatically by variable speed acid & base
metering pumps.
c) Sampling pot with condenser for cooling / condensing & collecting the sample taken at high
pressure & temperature.
d) Torque sensor for accurate measurement of the motor torque, where change in torque
indicates change in viscosity of the reaction.
e) High pressure ultrasound transducer for high frequency mixing.
f) Ex-proof certified gas purge panels for electrical accessories / utilities like heating cooling
circulators etc.
(a) (b) (c) (d) (e) (f)
49
®
Some of our valued customers
aether
elementally innovative
L I M I T E D
CSMCRI, NCL, IICT etc. All DRDO Labs
GNFC
(Formerly UDCT) All IIT's
50
All the logos are property of respective owners.
®
Some of our valued customers
RALLIS INDIA LIMITED
S. H. KELKAR & CO.
51
All the logos are property of respective owners.
WORLDWIDE PRESENCE
Exports to over 50 countries worldwide with distributors for sales & service in following countries
• Australia • Colombia • Germany • Mexico • Portugal • Slovakia • Thailand
• Azerbaijan • Czech Republic • Iran • Netherlands • Russia • South Africa • Turkey
• Brazil • Egypt • Israel • Peru • Romania • South Korea • UK
• Cambodia • Estonia • Italy • Phillippines • Saudi Arabia • Spain • USA
• China • France • Malaysia • Poland • Singapore • Taiwan • Vietnam
Sales & service support available from following places in India
• Ahmedabad • Bangalore • Hyderabad • Kolkatta • Mumbai • New Delhi

04/18 Copyrignt ©2013 Amar Equipments Pvt. Ltd.
® AMAR EQUIPMENTS PVT. LTD. ®
Since 1974. C US
6, Parmar Industrial Estate, Bail Bazaar, Kale Marg, Kurla (W), Mumbai - 400 070. India.
Tel: +91-22- 6225 5000 • Website: www.amarequip.com • E-mail: sales@amarequip.com / export@amarequip.com
• High Pressure Autoclaves • Multiple Reactor Systems • Gas Induction Reactors • Ex-Proof & Automated Pilot Plants • Glass Autoclaves
• Super Critical Fluid Extraction • HPHT Corrosion Testing • Magnetic Drive Couplings & Agitators • Lab ANF
• Metal Micro Rectors • Glass Flow Reactors • Photochemical Reactors • Packed Bed Tubular Reactors
• Continuous Stirred Tank Reactors • Heating Cooling Circulators

Autoclave-Catalog Amar Equipments

Uploaded by

Document Information

Original Title

Copyright

Available Formats

Share this document

Share or Embed Document

Sharing Options

Did you find this document useful?

Is this content inappropriate?

Copyright:

Available Formats

Autoclave-Catalog Amar Equipments

Uploaded by

Copyright:

Available Formats

High Pressure Systems

Pressure Reactor Specialist

Certifications & Approvals

Product Coding Guide

High Pressure Autoclaves / Reactors / Pressure Vessels

A1000 series (50 ml, 100 ml & 250 ml)

250 ml autoclave 250 ml table top 100 ml with manual

Standard models for 100 ml volume

Standard models for 250 ml volume

Technical Specifications for 50 ml, 100 ml & 250ml standard models

Nozzle orientation & internals for A1000 series

Pressure gauge Thermowell

Enquiry guide for 50 ml, 100 ml & 250 ml customized models

A2000 series (500 ml, 750 ml, 1 ltr, 2 ltr, 5 ltr)

2 ltr trolley model

1 ltr table top model 500 ml table top

5 ltr trolley model

500 ml 750 ml 1 ltr 2 ltr 5 ltr

Standard models for 750 ml autoclave

Standard models for 1 ltr autoclave

Standard models for 2 ltr autoclave

Standard models for 5 ltr autoclave

Nozzle orientation & internals A2000 series

Interchangeable autoclave: 50 ml & 100 ml or 500 ml & 750 ml

B Head Mounting Style G Valves & Fittings**

Electrical ex-proof, IIB + H2 certified EA J Control Panel

½ hp H05 L Mounting & Overall Dimensions (WxDxH)

20 ltr autoclave 100 ltr autoclave with hydraulic head

Standard models for 10 ltr volume

Standard models for 20 ltr volume

Standard models for 25 ltr volume

Standard models for 50 ltr volume

Standard models for 100 ltr volume

Nozzle orientation & internals A3000 series

A Material of Construction E Mag Drive Torque

C Heating Style J Control Panel

Multiple Autoclaves / Parallel Synthesizer

M6 model with fixed head design

Standard models for multiple autoclave 50 ml

Standard models for multiple autoclave 100 ml

Standard models for multiple autoclave 250 ml

Standard models for multiple autoclave 500 ml

Standard models for multiple autoclave 750 ml

Standard models for multiple autoclave 1 ltr

Standard models for multiple autoclave 2 ltr

Technical specification for multiple autoclaves standard models

Enquiry guide for multiple autoclaves customized models

D2 Motor RPM J Control Panel

Fully Automated High Through-put Catalyst Screening

Eco Catalyst Screening

Bottom Stirred Autoclaves

Standard models for bottom stirred autoclaves

Volume 250 ml 500 ml 750 ml

Multiple bottom stirred autoclaves

Nozzle orientation & internals for bottom stirred autoclaves

Pressure gauge Funnel

Technical specifications for bottom stirred autoclaves standard models

Enquiry guide for bottom stirred autoclave customized models

Bottom heated Glass-PEEK Interchangeable glass & metal autoclaves

Technical specification for glass autoclaves standard models

Enquiry guide for glass autoclave customized models

A Material of Construction (other wetted parts) F Stirrer Options**

Material of Construction (MOC)