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Materials
Ao
• Stress and strain: What are they and why are they used instead of load
and deformation?
Elastic behavior: When loads are small, how much deformation
occurs? What materials deform least?
Plastic behavior: At what point do dislocations cause permanent
deformation? What materials are most resistant to permanent
deformation?
Toughness and ductility: What are they and how do we measure
them?
2
Chapter Outline
From a fatigue plot for given material, compute the fatigue lifetime (at
a specified stress level), fatigue strength (at a specified number of
cycles).
Discuss the factors that affect fatigue life and suggest suitable remedies
to overcome.
Discuss the significance of creep rate while choosing a material for high
temperature application.
Given a creep plot for some material, compute steady state creep rate
and rupture life and comment on the suitability of the material for
given application.
Introduction
Consistency is needed when performing the tests and interpreting their results.
6
Engineering stress
Area, A Area, A Fs
Fs
Ft Fs
Ft Ft
Ao F
Ao
original area
before loading Stress has units:
N/m2 or lb/in2
7
Stress states
• Simple compression:
Ao
F Note: compressive
Balanced Rock, Arches structure member
National Park
(photo courtesy P.M. Anderson)
Ao
9
Other stress states
z > 0 s h< 0
10
Modes of loading and states of stress
11
12
Deformations occurring in structural
components subjected to axial loading.
13
The definitions of stress, strain and elastic moduli.
14
Engineering strain
Strain is always
= tan dimensionless.
/2 -
/2 /2
15
True Stress
True
F
T Corrected
Ai
F Engineering
E
Ao
Because of the geometry of the neck a triaxial stress state occurs and
the corrected axial stress is really less than the true stress.
16
True Strain
li lo li
E T ln
lo lo
Before necking occurs engineering and true stress and strain are related as follows.
T E (1 E ) T ln(1 E )
A approximation of the relationship between true stress and
true strain in the region between yield and necking is
T K Tn
where K and n are material constants.
17
True stress: load divided by actual area in the necked-down region, continues to rise to the
point of fracture, in contrast to the engineering stress.
18
Elastic deformation
bonds
stretch
return to
initial
F
F Linear-
elastic
an imposed stress. For most metals that are stressed in tension and at relatively
low levels, stress and strain are proportional to each other through the relationship
E
This is known as Hooke’s law, and the constant of proportionality E (Gpa) is
22
Elastic Deformation
For most typical metals the magnitude of this modulus ranges between 45
The moduli of elasticity are slightly higher for ceramic materials, which range
Polymers have modulus values that are smaller than both metals and
23
Room-Temperature Elastic and Shear Moduli, and Poisson’s Ratio for Various
Materials
24
Young’s moduli: Comparison
Graphite
Metals Composites
Ceramics Polymers
Alloys /fibers
1200 Semicond
10 00 Diamond
800
600
400 Tungsten
Molybdenum
Si carbide
Al oxide
Si nitride
Carbon fibers only E ceramics
Steel, Ni CFRE(|| fibers)*
E(GPa) 200 Tantalum
Platinum
Cu alloys
<111>
Si crystal
<100> Aramid fibers only > E metals
10 0 Zinc, Ti
80
>> E polymers
Silver, Gold AFRE(|| fibers)*
Aluminum Glass -soda Glass fibers only
60
Magnesium, G FRE(|| fibers)*
40 Tin
Concrete
10 9 Pa 20 GFRE*
CFRE * Based on data in Table B2,
G raphite G FRE( fibers)* Callister 6e.
10
8 CFRE( fibers) * Composite data based on
6 AFRE( fibers) *
Polyester reinforced epoxy with 60 vol%
4 PET
PS
of aligned carbon (CFRE),
2 PC Epoxy only aramid (AFRE), or
PP
glass (GFRE) fibers.
1 HDP E
0.8
0.6 Wood( grain)
PTF E
0.4
0.2 LDPE
25
26
Elastic Deformation (Cont.)
proportional.
The greater E is, the stiffer the material (or the smaller the elastic strain
27
Elastic Deformation (Cont.)
Types:
Linear elastic deformation:
Slope = Young’s modulus.
Non-linear elastic behavior:
Tangent or secant modulus.
28
Linear & Non-linear elastic behavior
29
Elastic Deformation (Cont.)
30
As temperature increases, E decreases
31
Elastic Properties of Materials
32
Poisson’s Ratio
F F
y
z y
z x x x
Elastic
initially
permanent (plastic)
after load is removed
p engineering strain,
p lastic strain
34
Plastic Deformation
Elastic deformation persists only to strains of about 0.005. Beyond this point,
move relative to one another. Upon removal of the stress, atoms do not return
35
Permanent Deformation
Most structures are designed to ensure that only elastic deformation results
36
Tensile properties :
(1) Yielding and yield strength
Most structures are designed to ensure that only elastic deformation will
result when a stress is applied. THUS, need to determine Yield.
Proportional limit (Yielding point): Initial departure from linearity of the
stress-strain curve.
Yield strength determination:
For materials with linear elastic regions: Use strain offset region ( =
0.002).
For materials with nonlinear elastic region: Use stress required to produce
some amount of strain (e.g. = 0.005).
37
Elastic & plastic deformation
38
(1) Yielding and yield strength (Cont.)
in stress.
Lower yield point: Continued deformation fluctuates slightly about some
39
Yield strength: Comparison
Graphite/
Metals/ Composites/
Ceramics/ Polymers
Alloys fibers
Semicond
20 00
Steel (4140) qt
y(ceramics)
10 00 >>y(metals)
y (MPa)
Ti (5Al-2.5Sn) a
700
600
W (pure)
Cu (71500) cw
>> y(polymers)
500 Mo (pure)
Room T values
Hard to measure,
200 Steel (1020) hr
Hard to measure
¨
Ti (pure) a
Ta (pure)
Cu (71500) hr
Yield strength,
LDPE
Tin (pure)
10
40
(2) Tensile strength
results.
41
Typical engineering stress-strain Behavior to fracture.
42
43
• Localized deformation of a ductile material during a tensile test produces a
necked region;
• The image shows necked region in a fractured sample.
45
The stress-strain curve for an aluminum alloy.
(c)2003 Brooks/Cole, a division of Thomson Learning, Inc. Thomson Learning™ is a trademark used herein
under license.
Strain Testing
• Tensile specimen • Tensile test machine
load cell
Often 12.8 mm x 60 mm
specimen
extensometer
• Other types:
-compression: brittle materials (e.g., concrete)
-torsion: cylindrical tubes, shafts.
47
(2) Tensile strength (Cont.)
Polymers: occurs when polymer backbones are aligned and about to break.
Yield strength (not tensile stress) is used to cite strength of material since at
became useless.
48
Tensile strength: Comparison
Graphite/
Metals/ Composites/
Ceramics/ Polymers
Alloys fibers
Semicond
5000 C fibers
Aramid fib
TS (ceram)
3000 E-glass fib
~TS (met)
(MPa)
20 00 Steel (4140) qt
AFRE (|| fiber)
10 00 W (pure)
Ti (5Al-2.5Sn) a
Diamond GFRE (|| fiber) ~ TS (comp)
Steel (4140) a CFRE (|| fiber)
Cu (71500) cw Si nitride
Cu (71500) hr
Steel (1020) Al oxide >> TS (poly)
300 Al (6061) ag
Ti (pure) a Room T values
Tensile strength, TS
200 Ta (pure)
Al (6061) a Based on data in Table B4,
100 Si crystal wood(|| fiber)
<100> Nylon 6,6 Callister 6e.
Glass-soda PC PET
40 Concrete
PVC GFRE ( fiber) a = annealed
PP CFRE ( fiber)
30 hr = hot rolled
AFRE( fiber)
HDPE ag = aged
20 Graphite
LDPE cd = cold drawn
cw = cold worked
10 qt = quenched & tempered
AFRE, GFRE, & CFRE =
aramid, glass, & carbon
wood ( fiber) fiber-reinforced epoxy
composites, with 60 vol%
fibers.
1
49
Yield strength and tensile strength vary with thermal and mechanical treatment,
impurity levels, etc. ; Variability related to behavior of dislocations (Elastic moduli are
relatively insensitive).
Yield and tensile strengths and modulus of elasticity: Decrease with increasing
temperature.
51
(3) Ductility
Importance:
before fracture.
It specifies degree of allowable deformation during fabrication
operations.
Brittle material:
Experiences very little or no plastic deformation upon fracture.
Having a fracture strain of less than 5%.
Most metals possess at least a moderate degree of ductility at room
temperature. Some become brittle as temperature is lowered.
52
smaller %EL
Engineering (brittle if %EL<5%)
tensile
stress, larg er %EL
(ductile if
%EL>5%)
53
(3) Ductility (Cont.)
l f l0
% EL 100
l0 Ao
Lo Af Lf
A0 A f
% RA 100
A0
%AR and %EL are often comparable:
--Reason: crystal slip does not change material volume.
--%AR > %EL possible if internal voids form in neck.
54
Ductile Vs Brittle Materials
Only Ductile materials will exhibit necking.
Ductile if EL%>8% (approximately)
Brittle if EL% < 5% (approximately)
AX X
C
Engineering Stress
B
X
D X
Brittle Ductile
A&B C&D
Engineering Strain
55
Tensile strength Yield strength
56
(4) Resilience
Area under the elastic part of the stress strain curve represents energy
absorption per unit volume.
Ur = 0.5 (y)2 / E
Resilient materials (used in springs) are those having high yield strengths
and low moduli of elasticity.
57
Resilience, Ur
Sy Su
Engineering Stress, S=P/Ao
ey X
Ur S de
o
Sy e y
E 2
Sy 2
2E
ey
Engineering Strain, e = DL/Lo)
Mat. Sc. & Metallurgy by IGS 58
Determination of modulus of resilience
59
(5) Toughness
Static (low strain rate) loads: Toughness is the area under the stress-strain
curve till fracture.
60
Toughness, Ut
Su
Engineering Stress, S=P/Ao
Sy
X
ef
Ut S de
o
(S y Su ) EL%
2 100
A “tough” material
has strength and
ductility.
Approximated by
the area under the
stress-strain curve.
62
• Energy to break a unit volume of material
• Approximate by the area under the stress-strain curve.
smaller toughness-
unreinforced
polymers
21
Toughness & Resilience
energy/unit volume
64
65
(6) Hardness
66
Hardness: Various Definitions
indentation hardness.
67
apply known force measure size
e.g., (1 to 1000g) of indent after
10mm sphere removing load
Smaller indents
D d mean larger
hardness.
increasing hardness
68
Chart of different materials ranked by hardness (Knoop Hardness)
Vickers
Knoop
Rockwell
Brinell
Mat. Sc. & Metallurgy by IGS 70
Johan August Brinell
71
Hugh Rockwell Stanley Rockwell
74
Conversion of
Hardness Scales
76
Correlation between
Hardness and Tensile
Strength
78
Factors affecting stress-Strain behavior
Prior deformation
Presence of impurities
Temperature:
80
Effect of temp. on stress-strain behavior of iron.
81
Fatigue, Creep & Fracture
Fatigue
83
Fatigue
fluctuating stresses;
Failure occurs at stress levels lower than yield or tensile stresses for
static loads;
have maximum values less than (and often much less than) the static yield strength
of the material.
The process of fatigue failure can be divided into different stages, which, from
the standpoint of metallurgical processes, can be divided into five stages:
5. Final failure.
This division is defined by the characterization of the underlying fatigue damage
of a material. It also clearly defines the requirement of plastic deformation for the
onset of crack initiation;
In general, three simultaneous conditions are required for the occurrence of
fatigue damage: cyclic stress, tensile stress, and plastic strain;
If any one of these three conditions is not present, a fatigue crack will not initiate
and propagate;
The plastic strain resulting from cyclic stress initiates the crack; and the tensile
stress (which may be localized tensile stress caused by compressive loads) promotes
crack propagation.
Fatigue is an important form of behavior in all materials including metals,
Ex: aircraft wings are subjected to repeated loads, oil and gas pipes are often
subjected to static loads but the dynamic effect of temperature variation will
cause fatigue;
Irregular or random stress cycle; for ex. an aircraft wing subjected to wind
loads.
The most important fatigue data for engineering designs are the S-N curves,
which is the Stress-Number of Cycles curves.
For some iron and titanium alloys, the S-N curve becomes horizontal at higher
number of cycles N;
Essentially it has reached a fatigue limit, and below this stress level the material
will not fatigue;
The fatigue limit represents the largest value of fluctuating stress that will not
cause failure for an infinite number of cycles.
The point at which the curve flatters out is termed as fatigue limit and is well
below the normal yield stress;
The significance of the fatigue limit is that if the material is loaded below this
stress, then it will not fail, regardless of the number of times it is loaded;
Materials such as aluminium, copper and magnesium do not show a fatigue
limit; therefore they will fail at any stress and number of cycles;
The fatigue life can be defined as the number of cycles required for a
material to fail at a certain stress.
Fatigue life: indicates how long (no. of cycles) a
component survives a particular stress.
The total number of cycles to failure is the sum of cycles at the first and the second stages:
N f = Ni + N p
Nf : Number of cycles to failure
Ni : Number of cycles for crack initiation
Np : Number of cycles for crack propagation
High cycle fatigue (low loads): Ni is relatively high. With increasing stress level, Ni decreases and
Np dominates.
Fatigue Failure
Fatigue fracture results from the presence of fatigue cracks, usually initiated by
The initial stress concentration associated with these cracks are too low to
cause brittle fracture they may be sufficient to cause slow growth of the cracks
into the interior.
Eventually the cracks may become sufficiently deep so that the stress
The extent of the crack propagation process depends upon the brittleness of
In brittle materials the crack grows to a critical size from which it propagates
right through the structures in a fast manner, whereas with ductile materials
the crack keeps growing until the remaining area cannot support the load
and an almost ductile fracture suddenly occurs.
Fatigue Failure
For a typical fracture ,Two distinct zones can be distinguished – a smooth zone
near the fatigue crack itself which, has been smoothened by the continual
rubbing together of the cracked surfaces, and a rough crystalline-looking zone
which is the final fracture.
Occasionally fatigue cracks show rough concentric rings which correspond to
As the crack grows in size, it reaches the critical length a c where it is unstable
Fast
fracture
Fatigue
striations
Crack
origin
Common Origins of Fatigue Cracks
Figure -- Mechanism of Fatigue Crack Growth
109
Fatigue Life Prediction
Usually there is an intended life or “design life” for the component , which is
The localized stress at the point of failure can be determined by finite element
analysis. Knowing localized stress, one can compare the actual cycles to failure
with that predicted from the S-N curve taken from a simple specimen in the lab
test.
Figure 3. Usually the mean is plotted on the S-N curve, so failures can occur
earlier than predicted.
Figure 2 : Rotating Bending Fatigue Test
(a)
(c)
(b)
Figure 3 : Scatter in Fatigue Life Data
Fatigue Mechanism
da typ. 1 to 6
K
m
dN
~ a
increase in crack length per loading cycle
• Failed rotating shaft crack origin
-- crack grew even though
Kmax < Kc
-- crack grows faster as
• Ds increases Adapted from
• crack gets longer Fig. 9.28, Callister &
Rethwisch 3e. (Fig. 9.28
• loading freq. increases. is from D.J. Wulpi,
Understanding How
Components Fail,
American Society for
Metals, Materials Park,
OH, 1985.)
Factors affecting fatigue properties
Surface finish:
Scratches dents identification marks can act as stress raisers and so reduce
the fatigue properties.
Electro-plating produces tensile residual stresses and have a detrimental
effect on the fatigue properties.
Temperature:
As a consequence of oxidation or corrosion of the metal surface increasing,
Heat treatment:
Hardening and heat treatments reduce the surface compressive stresses; as a result
the fatigue properties of the materials are getting affected.
Stress concentrations:
These are caused by sudden changes in cross section holes or sharp corners can
more easily lead to fatigue failure. Even a small hole lowers fatigue-limit by 30%.
Design for Fatigue
Modification of the design to avoid stress concentration eliminating sharp recesses and
Precise control of the surface finish by avoiding damage to surface by rough machining,
Control of corrosion and erosion or chemical attack in service and to prevent surface
surface stress
(to suppress surface near zero or compressive m
cracks from growing) moderate tensile m
larger tensile m
N = Cycles to failure
120
Time dependent and permanent deformation of materials when
subjected to a constant load or stress;
temperature.
Metals/alloys do not exhibit time dependent deformation
under normal service condition.
Metals subjected to a constant load at elevated temperatures
327°C, W 3407°C.
Material will creep when the temperature will be < 0.5Tm (Tm
.
creep = f ( T, , t )
Thermally activation deformation
at constant stress
over time.
Steam pipes ?
What is high temperature ?
Applications:
Light bulbs
replace every ~500-1,000 hrs.
Jet engines
check every ~1,000 hrs.
Car engines
2hrs/day x 5 days/wk x 50 wks/yr x 5yrs = 2,500 hrs.
Steam pipes
???
High Temperature Applications
/t
130 tr
Stages of creep
10 -2 10 -1 1
Steady state creep rate
Tertiary creep :
This stage is period of increasing strain rate;
Tertiary creep occurs when there is an effective reduction in
cross-sectional area due to necking or internal void formation;
If the stress is kept constant of the load or if true strain is taken
into consideration then the resulting fracture due to creep
would be at ‘B’.
Creep Demonstration
Lo
L
t=0
TIME
Types of Creep
Creep are classified based on temperature
Logarithmic Creep
Recovery Creep
Diffusion Creep
At low temperature the creep rate decreases with time and the logarithmic
creep curve is obtained.
At high temperature, the influence of work hardening is weakened and there
is a possibility of mechanical recovery. As a result, the creep rate does not
decrease and the recovery creep curve is obtained.
At very high temperature, the creep is primarily influenced by diffusion and
load applied has little effect. This creep is termed as diffusion creep or plastic
creep.
Alloys for High-Temperatures
(turbines in jet engines, hypersonic airplanes, nuclear reactors, etc.)
Stainless steels
Refractory metals (containing elements of high melting point, like Nb,
Mo, W, Ta)
“Superalloys” (Co, Ni based: solid solution hardening and secondary
phases)
Creep is characterized by:
For long life applications by: Steady state creep (slope of the secondary
portion of creep curve).
For relatively short life situations by: Time to rupture.
Proposed mechanisms (each leads to different stress exponent; n):
Stress-induced vacancy diffusion.
Grain boundary diffusion.
Dislocation motion.
Grain boundary sliding.
Creep
Dependence of creep strain rate on stress; stress v/s rupture lifetime for a low
carbon-nickel alloy at 3 temperatures.
Creep: stress and temperature effects
s K 2 n exp
Qc
RT
Qc = activation energy for creep
K2 and n are material constants
Mechanisms of Creep
Different mechanisms act in different materials and under different loading and
temperature conditions:
Stress-assisted vacancy diffusion
Grain boundary diffusion
Grain boundary sliding
Dislocation motion Different mechanisms different n, Qc.
The creep rate is established by the ease with which the dislocation
move across obstacles such as precipitates, GB etc.
Grain Boundary
Dislocation
Vacancy
Mutual movement of dislocations & vacancies.
This occurs at high temperature
(T>0.4Tm) &
When dislocation cause across obstacles,
they use vacancies/or interstitial atoms to climb and go around them for
slip &
hence plastic deformation continues.
Diffusion creep
It occurs when temp. is high & at relatively low stresses.
diffusion of vacancies controls the creep rate.
But edge dislocation is not involved in them.
vacancies move from the surface of the specimen towards the stress
axis
Stress axis
i.e when load is applied & kept constant ,the vertical boundaries are
At low temp the Grain boundaries will not flow viscously & provide
obstacles to dislocation motion.
At elevated temp , the grains in polycrystalline materials are able to
move relative to each other, this is called grain boundary sliding and is
an shear process which occurs in the direction of grain boundary [GB] .
a large no. of grains sliding with each other results in plastic deformation
due to creep .
GB sliding is promoted by increases the temp. T & or decreasing the
strain rate.
In fine grained materials because of large no. of grains this type of creep is
more ,so to avoid it large-coarse grained materials are to be used.
Ex : Ni-based super alloy with single crystals in jet engine blades, eliminates
the possibility of creep at high temp aided by grain boundary sliding
Creep testing
Furnace
Creep properties
OR
It is the stress to cause a creep strain of 1% in fixed time say 10 5 hours.
2) Creep rupture strength:- it is defined as the highest stress that a material
can withstand without rupture for a specified length of time.
Ex : For the same turbine blade . the rupture strength is that stress which
produces a fracture in 1000HR OR 10000HR OR 100 000 hrs at 800oC.
Thus creep rupture strength is also defined as the limiting stress below
which creep is so slow that will not result in fracture within any finite
length of time.
It is also called as” stress ruptures strength”.
3) Creep life:
0
C
Factors affecting Creep:
Load :
Temperature:
Composition:
Grain size
Heat treatment
Factors affecting Creep
Heat Treatment:
Creep resistance of steel is affected by heat treatment.
At temperatures of 300°C or higher maximum creep resistance is usually
produced. But the quacking and drawing decreases the creep resistance.
Grain size:
The major factor in creep is grain size; Normally large grained materials
exhibit better creep resistance than fine grained one based on the
temperature.
At temperatures below the lowest temperature of recrystallization, a fine
grained structure possesses the greater resistance whereas at temperature
above this point a large grained structure possesses the greater resistance and
we must select it for high temperature applications.
161
Factors affecting Creep
Strain Hardening:
Strain hardening of steel increases its creep resistance.
Particularly below the equi-cohesive temperature at which the fracture changes
from intra crystalline to inner-crystalline strain hardening increases the creep
resistance and hence there is no measurable creep. So the second stage of creep
curve is almost horizontal.
At temperature above the equi-cohesive temperature yield rate exceeds the strain
hardening rate and creep will proceed even under low stresses.
Alloying additions:
At temperatures, below the lowest temperatures of recrystallization the creep
resistance of steel may be improved by the finite forming elements like nickel, cobalt
and manganese or by the carbide forming elements like chromium molybdenum,
tungsten and vanadium.
Factors affecting Creep- Summary
165
Fundamentals of fracture
Simple fracture:
Ductile.
Brittle.
166
Ductile
Fracture
Brittle
Temperature
State of stress
167
Fracture of a material by cracking can occur in many ways, principally
the following:
1.Slow application of external loads.
2.Rapid application of external loads (impact).
3.Cyclic or repeated loading (fatigue).
4.Time-dependent deformation (creep).
5.Internal stresses, such as thermal stresses caused by anisotropy of
the thermal expansion coefficient or temperature differences in a
body.
6.Environmental effects (stress corrosion cracking, hydrogen
embrittlement, liquid metal embrittlement, etc.)
168
The process of fracture can, in most cases, be subdivided into
the following categories:
1. Damage accumulation.
2. Nucleation of one or more cracks or voids.
3. Growth of cracks or voids. (This may involve a coalescence of
the cracks or voids.)
169
Fundamentals of fracture
170
Behavior described Terms Used
171
Tension
Torsion
Fatigue
Conditions of fracture
Creep
Temper embrittlement
Hydrogen embrittlement
172
Ductile fracture
173
Ductile fracture (Moderately)
• Evolution to failure:
void void growth shearing
necking fracture
nucleation and linkage at surface
• Resulting 50m
50 m
fracture
surfaces
(steel)
100 m
particles
serve as void
nucleation
sites.
174
Ductile fracture
176
Ductile fracture
177
Brittle fracture
178
Brittle fracture
179
• Ductile-to-brittle transition temperature (DBTT)
polymers
Brittle More Ductile
Temperature
Ductile-to-brittle
transition temperature
180
Fracture modes
182
Ductile vs. brittle fracture
Ductile Brittle
deformation extensive little
crack propagation slow, needs stress fast
necking yes no
183
Summary