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Department of Chemistry, School of Science, University of Management and Technology Lahore Pakistan
Abstract :
ZnO nanoparticles and Ni doped ZnO nanoparticles with different concentration of (Zn 1-xNixO) (X = 0, 9, 25, 33,
41 ) wt% were prepared by co-precipitation method and Poly Acrylic Acid microgel and its (composite with good
degradation) by varying percentage of Ni doped ZnO were synthesize by reverse phase polymerization these are
characterized by XRD, FTIR, TEM, SEM, SPS to find out its morphology. Photocatalytic activity of these samples
were testified by photo degradation of Methylene blue as standard dye. The results reveled that synthesize composite
.
Introduction
Microgel are highly swollen milky white suspended particles highly Responsive in nature which are
cross linked three dimensional polymeric network which swells in response of stimuli such as
temperature and pH. Doped zinc oxide nanoparticles that shows us a unique optical, magnetic and
catalytic properties depending upon nature (size, shape) of inorganic nanoparticles. Metal loaded nano
composites use in many fields such as drug delivery, photocatalytic activity chemical separation, oil
recovery, and Nano technology.
Material and chemicals:
Three neck flask, Beakers, N2 gas cylinder, stirrer, pipes, nickel nitrate, zinc acetate,,
, PVA, NaOH, TEMED, APS, MBA, AAc,
Spectrophotometer. Methylene blue , distilled water
2.5
1.5
Study of Photodegradation of different concentration by UV spectrophotometer after 30 min. 1
Study
0.5
of Photodegradation by UV
Study of Photodegradation of different concentration
by UV spectrophotometer after 60 min
spectrophotometer
0
800779758737716695674653632611590569548527506485464443422401380359338317296275254233212
-0.5
REFERENCES
• Robina, B.; Khalida, N.; Zahoor, H, F.; A review of responsive hybrid microgels fabricated with silver nanoparticles: synthesis, classification, characterization and application, 2015.
• Zahoor, H. F.; Hafeez, U. K.; Sayed, M. S.; Mohammad, S.; Stability of poly ( N isopropyl acrylamide –c0-AA) polymer microgel under various conditions of temperature, pH and salt
concentration, Arabian journal of Chemistry, 2017,10 ,329-335.
• Fabbiyola, S.; Sailaja, V.; kennedy, L. J.; Bououdina, M.; Vijay, J. J.; Optical and magnetic properties of Ni-doped ZnO nanoparticles, Journal of Alloys and Compounds, 2017, 694, 522-531
• K. Raja; P. S Ramesh; D Getta; Synthesis, structural and optical properties of ZnO and Ni-doped ZnO, hexagonal nanorods by Co-precipitation method, Molecular and Biomolecular Spectroscopy,
2015, 120 19-24.