Calibration

Correlation Calibration
All Produced Water Applications!
1. Set instrument
sensitivity.
2. Store raw fluorescence
of High and Low
Standards.
3. Collect samples while
reading raw
fluorescence.
4. Measure oil content of
samples.
5. Repeat 3 and 4 as
required to span
measurement range.
6. Use Excel workbook to
compute ppm of High
and Low Standards.
7. Enter ppm values using
keypad.
Correlation Scatter Plot
y =0.3373x - 0.7768
R
2
=0.9756
0
5
10
15
20
25
30
0 10 20 30 40 50 60 70 80 90
Raw Fluorescence
O
i
l

C
o
n
c
e
n
t
r
a
t
i
o
n
,

p
p
m
TD-4100XD Correlation Calibration.xls
Sample Date Time Raw Fluorescence Oil Concentration Notes
Setup 12/28/04 13:00 29.52 NA Initial Sensitiviy Setup Min. Conc., ppm 0
High STD 12/28/04 14:09 33.47 10.4 High Standard Max. Conc., ppm 50
Low STD 12/28/04 14:11 20.85 6.1 Low Standard Desired Range, ppm 50
3 12/28/04 14:15 30.79 9.1 set floculant to 1.5 ppm Sample Range, ppm 25.5
4 12/28/04 14:30 37.16 9.7 set floculant to 1.5 ppm Range Coverage, % 51
5 12/29/04 8:30 12.51 2.8 set floculant to 3.0 ppm
6 12/29/04 8:45 8.52 1.9 set floculant to 3.0 ppm
7 12/29/04 9:05 13.58 3 set floculant to 3.0 ppm
8 12/29/04 10:20 15.12 5.2 set floculant to 1.5 ppm #Samples 15
9 12/29/04 11:25 17.6 4.9 set floculant to 1.5 ppm m 0.3372918
10 12/29/04 13:15 37.22 12.1 shut off floculant pump b -0.7767679
11 12/29/04 13:45 85.24 27.4 shut off floculant pump
R
2
0.9755924
12 12/29/04 14:00 55.79 18.8 shut off floculant pump
13 12/29/04 14:30 40.37 12.3 shut off floculant pump
14 12/29/04 16:45 32.39 11.9 Normal ops, floculant: 0.5 ppm
15 12/29/04 17:00 33.02 12.5 Normal ops, floculant: 0.5 ppm
16
17 Raw Fluorescence Hi Std Conc
18 33.47 10.512
19
20
21 Raw Fluorescence Low Std Conc
22 20.85 6.256
23
24
25
26
27
28
29
30
31
32
33
34
35
36
TD-4100XD Calibration Values
Calculated High STD Concentration
Calculated Low STD Concentration
(559) 253-1414
For assistance, contact:
Service@oilinwatermonitors.com
Version 1.0 November 3, 2004
TD-4100XD Correlation Calibration
ppm =m(Raw Fluorescence) +b
Monitoring Range
Correlation Results
Calibration Bottles & Valves
May be necessary for introducing samples from another location.
Calibration Reset
12 PPM
CAL 28 DAYS AGO
ENT
HOME
1. Calibration
2. Cal data
1
<1> High <2> Low
<3> Reset Cal
3
Reset CAL deflts
Press <*> 5 times
* * * * *
ESC
CALIBRATION
reset to default
Calibration Low Standard
12 PPM
CAL 28 DAYS AGO
ENT
HOME
1. Calibration
2. Cal data
1
<1> High <2> Low
<3> Reset Cal
2
Low Standard
Lower conc!
ENT
Low Standard:
XXX.X
Low Standard:
XXX.X WAIT
FINISHED!
Press <ENT>
*
ENT
Calibration High Standard
12 PPM
CAL 28 DAYS AGO
ENT
HOME
1. Calibration
2. Cal data
1
<1> High <2> Low
<3> Reset Cal
1
High Standard
Highest conc!
ENT
High Standard:
XXX.X
High Standard:
XXX.X WAIT
FINISHED!
Press <ENT>
*
ENT
Calibration Standard Values
12 PPM
CAL 28 DAYS AGO
0
HOME
<1> Hi Std Conc
<2> Low Std Conc
1
Hi Std Conc:
15.000 PPM
Type new value
15.000
New:
ENT
15.000
New: 30.000
0
ENT
30.000
New:
(Same procedure for <2>)
Concentration Units
1
12 PPM
CAL 28 DAYS AGO
1
HOME
Conc Units
Display Option
ENT
Unit Display:
PPM
ENT
Unit Display:
PPB
ENT
Unit Display:
NO UNIT
Calibration Timing Hint
Press when water
level is near bottom of
label.
ENT
High Standard:
XXX.X
Open PVC valve.
Wait for readings to stabilize.
Readings must be <142
High Standard:
XXX.X WAIT
FINISHED!
Press <ENT>
*
*
Calibration Abort
ESC
<1> - Abort Cal
<ESC> - Continue
1
<1> High <2> Low
<3> Reset Cal
High Standard
Highest conc!
OR FROM
Low Standard
Lower conc!
OR Beyond
2023 North Gateway, Suite 101
Fresno, CA 93727 USA
Phone: +1 559 253-1414
FAX: +1 559 253-1090
Service@oilinwatermonitors.com
www.oilinwatermonitors.com
Mark A. Fletcher, PhD
Dale F. Brost, PhD
Nic Pittman