Result Analysis Report

Sample Name:
N_157

SOP Name:

Measured:
27 August 2012 14:40:06

Sample Source & type:

Measured by:
User1

Analysed:
27 August 2012 14:40:07

Sample bulk lot ref:

Result Source:
Averaged

Particle Name:
AKD

Accessory Name:
Hydro 2000SM (A)

Analysis model:
General purpose

Sensitivity:
Normal

Particle RI:
1.530
Dispersant Name:
Water

Absorption:
0.1
Dispersant RI:
1.330

Size range:
0.020
to 2000.000 um
Weighted Residual:
4.511
%

Obscuration:
17.48 %
Result Emulation:
Off

Concentration:
0.0031
%Vol

Span :
1.304

Uniformity:
0.386

Result units:
Volume

Specific Surface Area:

8.54
m/g

Surface Weighted Mean D[3,2]:

0.703
um

Vol. Weighted Mean D[4,3]:

1.001
um

d(0.1):

0.318

um

d(0.5):

0.994

um

d(0.9):

1.614

Volume (%)

Particle Size Distribution

um

110

14

100

12

90
80

10

70
60

50

40

30
20

10

0
0.1

10

Particle Size (m)

Size (m) 27
Volume
In %
Size (m)
Volume In %
N_157,
August
2012
14:40:06
0.010
0.011
0.013
0.015
0.017
0.020
0.023
0.026
0.030
0.035
0.040
0.046
0.052
0.060
0.069
0.079
0.091
0.105

Operator notes:

0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00

0.105
0.120
0.138
0.158
0.182
0.209
0.240
0.275
0.316
0.363
0.417
0.479
0.550
0.631
0.724
0.832
0.955
1.096

0.00
0.00
0.06
0.62
2.02
2.62
2.50
2.10
1.90
1.99
2.34
2.95
4.00
5.57
7.73
10.20
12.27

Size (m) Volume In %

1.096
12.85
1.259
11.36
1.445
8.33
1.660
5.00
1.905
2.41
2.188
0.90
2.512
0.24
2.884
0.03
3.311
0.00
3.802
0.00
4.365
0.00
5.012
0.00
5.754
0.00
6.607
0.00
7.586
0.00
8.710
0.00
10.000
0.00
11.482

Size (m) Volume In %

11.482
0.00
13.183
0.00
15.136
0.00
17.378
0.00
19.953
0.00
22.909
0.00
26.303
0.00
30.200
0.00
34.674
0.00
39.811
0.00
45.709
0.00
52.481
0.00
60.256
0.00
69.183
0.00
79.433
0.00
91.201
0.00
104.713
0.00
120.226

Size (m) Volume In %

120.226
0.00
138.038
0.00
158.489
0.00
181.970
0.00
208.930
0.00
239.883
0.00
275.423
0.00
316.228
0.00
363.078
0.00
416.869
0.00
478.630
0.00
549.541
0.00
630.957
0.00
724.436
0.00
831.764
0.00
954.993
0.00
1096.478
0.00
1258.925

Size (m) Volume In %

1258.925
0.00
1445.440
0.00
1659.587
0.00
1905.461
0.00
2187.762
0.00
2511.886
0.00
2884.032
0.00
3311.311
0.00
3801.894
0.00
4365.158
0.00
5011.872
0.00
5754.399
0.00
6606.934
0.00
7585.776
0.00
8709.636
0.00
10000.000

Average of 2 measurements from N_157_12

Malvern Instruments Ltd.

Malvern, UK
Tel := +[44] (0) 1684-892456 Fax +[44] (0) 1684-892789

Mastersizer 2000 Ver. 5.60

Serial Number : MAL1005534

File name: N_157_12

Record Number: 65
27/08/2012 16:18:53

Result Analysis Report

Sample Name:
N_161

SOP Name:

Measured:
27 August 2012 15:07:52

Sample Source & type:

Measured by:
User1

Analysed:
27 August 2012 15:07:54

Sample bulk lot ref:

Result Source:
Averaged

Particle Name:
AKD

Accessory Name:
Hydro 2000SM (A)

Analysis model:
General purpose

Sensitivity:
Normal

Particle RI:
1.530
Dispersant Name:
Water

Absorption:
0.1
Dispersant RI:
1.330

Size range:
0.020
to 2000.000 um
Weighted Residual:
3.677
%

Obscuration:
13.83 %
Result Emulation:
Off

Concentration:
0.0025
%Vol

Span :
1.334

Uniformity:
0.417

Result units:
Volume

Specific Surface Area:

6.42
m/g

Surface Weighted Mean D[3,2]:

0.934
um

Vol. Weighted Mean D[4,3]:

1.252
um

d(0.1):

0.517

um

d(0.5):

1.161

um

d(0.9):

2.066

Particle Size Distribution

14

110
100

12

90
80

10
Volume (%)

um

70
8

60

50
40

30
20

10

0
0.1

10

Particle Size (m)

Size (m) 27
Volume
In %
Size (m)
Volume In %
N_161,
August
2012
15:07:52
0.010
0.011
0.013
0.015
0.017
0.020
0.023
0.026
0.030
0.035
0.040
0.046
0.052
0.060
0.069
0.079
0.091
0.105

Operator notes:

0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00

0.105
0.120
0.138
0.158
0.182
0.209
0.240
0.275
0.316
0.363
0.417
0.479
0.550
0.631
0.724
0.832
0.955
1.096

0.00
0.00
0.00
0.01
0.10
0.44
0.78
1.13
1.51
1.95
2.46
3.05
3.87
5.00
6.55
8.38
10.18

Size (m) Volume In %

1.096
11.36
1.259
11.40
1.445
10.17
1.660
8.06
1.905
5.72
2.188
3.68
2.512
2.15
2.884
1.14
3.311
0.55
3.802
0.24
4.365
0.09
5.012
0.04
5.754
0.01
6.607
0.00
7.586
0.00
8.710
0.00
10.000
0.00
11.482

Size (m) Volume In %

11.482
0.00
13.183
0.00
15.136
0.00
17.378
0.00
19.953
0.00
22.909
0.00
26.303
0.00
30.200
0.00
34.674
0.00
39.811
0.00
45.709
0.00
52.481
0.00
60.256
0.00
69.183
0.00
79.433
0.00
91.201
0.00
104.713
0.00
120.226

Size (m) Volume In %

120.226
0.00
138.038
0.00
158.489
0.00
181.970
0.00
208.930
0.00
239.883
0.00
275.423
0.00
316.228
0.00
363.078
0.00
416.869
0.00
478.630
0.00
549.541
0.00
630.957
0.00
724.436
0.00
831.764
0.00
954.993
0.00
1096.478
0.00
1258.925

Size (m) Volume In %

1258.925
0.00
1445.440
0.00
1659.587
0.00
1905.461
0.00
2187.762
0.00
2511.886
0.00
2884.032
0.00
3311.311
0.00
3801.894
0.00
4365.158
0.00
5011.872
0.00
5754.399
0.00
6606.934
0.00
7585.776
0.00
8709.636
0.00
10000.000

Average of 2 measurements from N_157-167.mea

Malvern Instruments Ltd.

Malvern, UK
Tel := +[44] (0) 1684-892456 Fax +[44] (0) 1684-892789

Mastersizer 2000 Ver. 5.60

Serial Number : MAL1005534

File name: N_157-167.mea

Record Number: 65
27/08/2012 16:25:12

Result Analysis Report

Sample Name:
N_166

SOP Name:

Measured:
27 August 2012 15:40:05

Sample Source & type:

Measured by:
User1

Analysed:
27 August 2012 15:40:06

Sample bulk lot ref:

Result Source:
Averaged

Particle Name:
AKD

Accessory Name:
Hydro 2000SM (A)

Analysis model:
General purpose

Particle RI:
1.530
Dispersant Name:
Water

Absorption:
0.1
Dispersant RI:
1.330

Size range:
0.020
to 2000.000
Weighted Residual:
3.122
%

Concentration:
0.0038
%Vol

Span :
1.302

Uniformity:
0.404

Specific Surface Area:

5.35
m/g

Surface Weighted Mean D[3,2]:

1.121
um

Vol. Weighted Mean D[4,3]:

1.483
um

d(0.1):

0.626

um

d(0.5):

1.392

um

Sensitivity:
Normal
um

Obscuration:
18.55
%
Result Emulation:
Off
Result units:
Volume

d(0.9):

2.437

Particle Size Distribution

110
100

12

90
80

10
Volume (%)

um

70
8

60

50
40

30
20

10

0
0.1

10

Particle Size (m)

Size (m) 27
Volume
In %
Size (m)
Volume In %
N_166,
August
2012
15:40:05
0.010
0.011
0.013
0.015
0.017
0.020
0.023
0.026
0.030
0.035
0.040
0.046
0.052
0.060
0.069
0.079
0.091
0.105

Operator notes:

0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00

0.105
0.120
0.138
0.158
0.182
0.209
0.240
0.275
0.316
0.363
0.417
0.479
0.550
0.631
0.724
0.832
0.955
1.096

0.00
0.00
0.00
0.00
0.01
0.08
0.31
0.58
0.94
1.35
1.79
2.26
2.85
3.62
4.71
6.14
7.87

Size (m) Volume In %

1.096
9.61
1.259
10.95
1.445
11.41
1.660
10.77
1.905
9.14
2.188
6.87
2.512
4.50
2.884
2.52
3.311
1.16
3.802
0.42
4.365
0.09
5.012
0.02
5.754
0.00
6.607
0.00
7.586
0.00
8.710
0.00
10.000
0.00
11.482

Size (m) Volume In %

11.482
0.00
13.183
0.00
15.136
0.00
17.378
0.00
19.953
0.00
22.909
0.00
26.303
0.00
30.200
0.00
34.674
0.00
39.811
0.00
45.709
0.00
52.481
0.00
60.256
0.00
69.183
0.00
79.433
0.00
91.201
0.00
104.713
0.00
120.226

Size (m) Volume In %

120.226
0.00
138.038
0.00
158.489
0.00
181.970
0.00
208.930
0.00
239.883
0.00
275.423
0.00
316.228
0.00
363.078
0.00
416.869
0.00
478.630
0.00
549.541
0.00
630.957
0.00
724.436
0.00
831.764
0.00
954.993
0.00
1096.478
0.00
1258.925

Size (m) Volume In %

1258.925
0.00
1445.440
0.00
1659.587
0.00
1905.461
0.00
2187.762
0.00
2511.886
0.00
2884.032
0.00
3311.311
0.00
3801.894
0.00
4365.158
0.00
5011.872
0.00
5754.399
0.00
6606.934
0.00
7585.776
0.00
8709.636
0.00
10000.000

Average of 2 measurements from N_157-167.mea

Malvern Instruments Ltd.

Malvern, UK
Tel := +[44] (0) 1684-892456 Fax +[44] (0) 1684-892789

Mastersizer 2000 Ver. 5.60

Serial Number : MAL1005534

File name: N_157-167.mea

Record Number: 66
27/08/2012 16:25:53

Result Analysis Report

Sample Name:
N_167

SOP Name:

Measured:
27 August 2012 15:50:51

Sample Source & type:

Measured by:
User1

Analysed:
27 August 2012 15:50:53

Sample bulk lot ref:

Result Source:
Averaged

Particle Name:
AKD

Accessory Name:
Hydro 2000SM (A)

Analysis model:
General purpose

Particle RI:
1.530
Dispersant Name:
Water

Absorption:
0.1
Dispersant RI:
1.330

Size range:
0.020
to 2000.000
Weighted Residual:
3.217
%

Concentration:
0.0037
%Vol

Span :
1.309

Uniformity:
0.412

Specific Surface Area:

5.85
m/g

Surface Weighted Mean D[3,2]:

1.026
um

Vol. Weighted Mean D[4,3]:

1.344
um

d(0.1):

0.623

um

d(0.5):

1.222

um

Sensitivity:
Normal
um

Obscuration:
19.29
%
Result Emulation:
Off
Result units:
Volume

d(0.9):

2.222

Particle Size Distribution

14

um

110
100

12

90
80

Volume (%)

10

70
8

60
50

40
4

30
20

10

0
0.1

10

Particle Size (m)

Size (m) 27
Volume
In %
Size (m)
Volume In %
N_167,
August
2012
15:50:51
0.010
0.011
0.013
0.015
0.017
0.020
0.023
0.026
0.030
0.035
0.040
0.046
0.052
0.060
0.069
0.079
0.091
0.105

Operator notes:

0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00

0.105
0.120
0.138
0.158
0.182
0.209
0.240
0.275
0.316
0.363
0.417
0.479
0.550
0.631
0.724
0.832
0.955
1.096

0.00
0.00
0.00
0.04
0.16
0.41
0.53
0.63
0.77
1.03
1.46
2.14
3.21
4.73
6.67
8.74
10.52

Size (m) Volume In %

1.096
11.52
1.259
11.45
1.445
10.34
1.660
8.55
1.905
6.51
2.188
4.57
2.512
2.94
2.884
1.70
3.311
0.87
3.802
0.38
4.365
0.11
5.012
0.03
5.754
0.00
6.607
0.00
7.586
0.00
8.710
0.00
10.000
0.00
11.482

Size (m) Volume In %

11.482
0.00
13.183
0.00
15.136
0.00
17.378
0.00
19.953
0.00
22.909
0.00
26.303
0.00
30.200
0.00
34.674
0.00
39.811
0.00
45.709
0.00
52.481
0.00
60.256
0.00
69.183
0.00
79.433
0.00
91.201
0.00
104.713
0.00
120.226

Size (m) Volume In %

120.226
0.00
138.038
0.00
158.489
0.00
181.970
0.00
208.930
0.00
239.883
0.00
275.423
0.00
316.228
0.00
363.078
0.00
416.869
0.00
478.630
0.00
549.541
0.00
630.957
0.00
724.436
0.00
831.764
0.00
954.993
0.00
1096.478
0.00
1258.925

Size (m) Volume In %

1258.925
0.00
1445.440
0.00
1659.587
0.00
1905.461
0.00
2187.762
0.00
2511.886
0.00
2884.032
0.00
3311.311
0.00
3801.894
0.00
4365.158
0.00
5011.872
0.00
5754.399
0.00
6606.934
0.00
7585.776
0.00
8709.636
0.00
10000.000

Average of 2 measurements from N_157-167.mea

Malvern Instruments Ltd.

Malvern, UK
Tel := +[44] (0) 1684-892456 Fax +[44] (0) 1684-892789

Mastersizer 2000 Ver. 5.60

Serial Number : MAL1005534

File name: N_157-167.mea

Record Number: 67
27/08/2012 16:26:58