Engineering Management Inc.: Support

ENGINEERING MANAGEMENT SUPPORT, INC.
West Lake OU-1
STANDARD LEVEL IV
REPORT OF ANALYSIS
WORK ORDER #13-04106-0R
May 16,2013
EBERLINE ANALYTICAL/OAK RIDGE LABORATORY
OAK RIDGE, TN
TABLE OF CONTENTS
SECTION
DESCRIPTION
PAGE
Chain of Custody & pH Check Sheet
0004
II
Sample Acknowledgement
0013
III
Case Narrative
0016
IV
Analytical Results Summary
0020
Analytical Standards
0026
VI
Quality Control Sample Results Summary
0050
VII
Laboratory Technician's Notes
0061
VIII
Analytical Data (Isotopic Uranium)
0100
IX
Analytical Data (Isotopic Thorium)
0249
Analytical Data (Radium-226)
0363
XI
Analytical Data (Radium-228)
0472
XII
Barium-133 Analytical Tracer Data
0490
Last Page Number
0566
STANDARD OPERATING PROCEDURE
MP-001, Rev. 12
Effective: 10131112
Page 14 of14
Sample Receiving
Eberline Services - Oak Ridge Laboratory

LABORATORY DATA SUPPORT CHECKLIST
MP-001-3
1_3_-_0_4_1_0_:_6_____
Eberline Services Work Order # _ _ _
The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial
Initials
Date
Initials.
Checklist Items
Sample Log-In
K13s 'I 1! .. /t'!> K<:.

5/J~/13 &Jif/L~ f{/3).
Data Compilation
First Technical Data Review
J'~JJ:;;~ ~J.--"1'
-s\1'?
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;1'1A_
Second Technical Data Review
Data Entry/Electronic Deliverable
;. ...
Case Narrative
~V/4,:~, I~ './
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,~
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Electronic Deliverable Proof

Samples ~'J'IIyzed within Holding Time
).).52$
Ye<?
INo?
QNQC R'eview
Client in Possession of Data

' or H;,rrl Conv
Invoiced by Laboratory
Technical/Clerical Corrections, Signatures Needed, Problems, Etc
Date/Initials
~
Date package approved by:
~~\
- . 'I'
Laboratory Manager
I \
5ft~t ~
Date
.I
Copy No. _ _ __
Radiochemistry Services
SECTION I
CHAIN OF CUSTODY
&
pH CHECK SHEET
13-04106
REC'D AE.lr6)013
Chain of Custody Record

Project Name:
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601 Scarboro Road

Oak R;oge, TN 37930
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E B I::RI..-1 N_e:
SERVICES
Oak Ridge Laboratory
Internal
Work Order#
13-04106
Chain of
Custody
Lab Deadline
5/7/2013
UUISO - Level 4
Analysis
Water
Sample Matrix
Sample
Comments
04
---------
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Fraction
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Storage
Location
43
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08
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ii
Printed: 4/16/2013 12:37PM:mmm7
Internal
Eee:~ht~~
Chain of
Custody
Lab Deadline
See Comments
UUISO - Level 4
WA
Sample Matrix
Sample
Fraction
HP210!270
Detector Activity
Storage
Location
04
05
06
07
08
09
10
11
12
13
14
15
16
17
43
43
45
45
40
40
47
47
39
39
45
45
44
44
42
42
P1.0
1~~~~re TOTAL
FxRs 06, 07, 09, 11, 13, 15, 17 & I !I are DI559LVED
)fiJi..(
13-04106
Analysis
Comments
Re-Analysis: 2FnRs 04, 0&, OS, 10,
Work Order#
s;,;,3
Original Lab Deadline: 05/14/13

Rerun Lab Deadline: 05/14/13
18
19
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.
EBE::Rl.-tN.::::
SERVICES
Internal
Work Order#
13-04106
Chain of
Custody
Lab Deadline
5/7/2013
ThiSO - Level 4
Analysis
Water
Sample Matrix
Sample
Comments
I
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
06
07
08
09
10
Fxns 05, 07, 09, 11, 13, 15, 17 & 19 are DISSOLVED
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Printed: 4/16/2013 12:37 PM
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EBI::RLINE
SERVICES
Internal
Work Order#
13-04106
Chain of
Custody
Lab Deadline
5/7/2013
Ra226 - Level 4
Analysis
Water
Sample Matrix
HP 210 I 270
Detector Activity i
Sample
Fraction
Comments
43
43 .......
45
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04
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Printed: 4/16/2013 12:37 PM
lill!l HI
E13ERLINE
SERVICES
Internal
Work Order#
13-04106
Chain of
Custody
Lab Deadline
5/7/2013
Ra228 - Level 4
Analysis
Water
Sample Matrix
Comments
Sample
Fraction
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
04
05
06
07
08
09
10
HP 210 I 270
Detector Activity
1-
45
45
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12
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----- --+----------Printed: 4/16/2013 12:37 PM
mm11
Printed: 4/16/2013 11:33 AM
Page 1 of 1
Internal Work Order
13-04106
Sample Receiving Report

(Volumes, pH, & CPM)
Received By
KCOULSTON
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IFR
# Btls
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Date:
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MP-001, Rev 5
11/22/02
Effective:
:IDS12
SECTION II
SAMPLE ACKNOWLEDGEMENT
Client Name
ContractiPO
___Project Type
Engine~-;~g ~~~~gement ~up port, Inc.[ West-~~~~~~~-~

_Projec~,,N,aem,.,e_________
West Lake OU-1

lnternaiiD
Client ID
~entWO
,'
.I west L-;~~-~~~~-r
Date Received
Required Turnaround Days
Environmental
04/16/2013
28
Sa_mple Disp
Lab Deadline
05/07/2013
Sample Date
l Matrix
Storage
~
0:
:em,.,
13-04106
'Tm
05/13/2013
05/14/2013
i'"' "':J5
!"
01
LCS
04/16/13
I WA
Pl.O
02
BLANK
04/16/13
WA
Pl.O
03
DUP
04/16/13
WA
Pl.O
04
PZ-111-KS TOT
04/09/13 15:35 j WA
Pl.O
05
PZ-111-KS DIS
04/09/13 15:35
WA
Pl.O
06
D-6 TOT
04/09/13 15:45
WA
Pl.O
07
D-6 DIS
04/09/13 15:45
WA
Pl.O
08
D-83 TOT
04/09/13 16:16
WA
Pl.O
09
D-83 DIS
04/09/13 16:16
WA
Pl.O
4"
10
DUP OS TOT
04/09/13
oo:oo I
WA
Pl.O
11
DUP OS DIS
04/09/13
oo:oo l WA
Pl.O
12
PZ -102-SS TOT
04/11/13 09:10
I WA
Pl.O
13
PZ-102-SS DIS
04/11/13 09:10
WA
Pl.O
14
PZ-102R-SS TOT
04/11/13 11:30
l WA
Pl.O
15
PZ-102R-SS DIS
04/11/1311:30
I WA
Pl.O
16
PZ-104-SD TOT
04/11/1311:38
WA
Pl.O
17
PZ-104-SD DIS
04/11/1311:38
I WA
Pl.O
18
PZ-104-SS TOT
04/11/13 12:59
WA
Pl.O
19
PZ-104-SS DIS
04/11/13 12:59
WA
Pl.O
4
0
Totals Per Analysis (non QA samples)
16116
16]16
Invoice
~
Iilli
.. .
Paul V. Rosasco. P.E.
o_j_ o
Report Data
I:: R..._lt--1-=::
SERVICES
Voice: (865) 481-0683

Fax:
(865) 483-4621
o I o
7220WestJefferson Avenue. Surte 406
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235
Lakewood, CO 80235
Voioe
Contact
Lyn Fitzgerald
'"'
Voice
303-601-4255
'~
Englneerir>g Management Support. lr>e
303-640-3426
Voice
Sample Log In Report
Paul V. Rosasco, P.E.
Engiooering Management Support. Inc

601 Scarboro Rd.
Oak Ridge, TN 37830
303-940-3426
'"
~- ~
Printed: 4/16/2013 12:37 PM
STANDARD OPERATING PROCEDURE
MP001, Rev. 12
Effective: 10131112
Page 13 of14
Sample Receiving
Eberline Services -Oak Ridge Laboratory

SAMPLE RECEIPT CHECKLIST
MP-001-2
WORK ORDER#
13 - 0 4 1 0 6
SAMPLE MATRIX/MATRICES:
(CIRCLE ONE OR BOTH)
@uEOu)
NON-AQUEOUS
(CIRCLE EITHER YES, NO, OR NIA)

WERE SAMPLES
Received in good condition?
If aqueous, properly preserved
Presenl on outside of package?
Unbroken on oulside of package?
G)
Present on samples?
Unbroken on samples?
G)
Was chain of custody present upon sample receipt?
_...Y)
NIA
WERE CHAIN OF CUSTODY SEALS
IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS: _______________________________________________________
SIGNATURE:
Copy No. _ _ __
d(nimNGsuOrliN
DATE: Lj
/llo/(3
Radiochemistry Services
SECTION III
CASE NARRATIVE
~EBERLINE
~
EBERLINE ANALYTICAL CORPORATION

601 SCARBORO ROAD
OAK RIDGE, TENNESSEE 37830
PHONE (865) 481-0683
SERVICES
FAX (865) 483-4621
EBS-OR-35568
May 16,2013
Engineering Management Support, Inc.
Lakewood, CO 80235
CASE NARRATIVE
Work Order# 13-04106-0R
SAMPLE RECEIPT
This work order contains eight water samples received 04/16/2013. All samples were analyzed as total
and dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENT ID
LAB ID
CLIENT ID
LABID
PZ-111-KS TOT
PZ-111-KS DIS
D-6 TOT
D-6 DIS
D-83 TOT
D-83 DIS
DUP05TOT
DUP 05 DIS
13-04106-04
13-04106-05
13-04106-06
13-04106-07
13-04106-08
13-041 06-09
13-04106-10
13-04106-11
PZ-1 02-SS TOT

PZ-1 02-SS DIS
PZ-102R-SS TOT
PZ-1 02R-SS DIS
PZ-104-SD TOT
PZ-1 04-SD DIS
PZ-104-SS TOT
PZ-1 04-SS DIS
13-04106-12
13-041 06-13
13-04106-14
13-04106-15
13-04106-16
13-04106-17
13-04106-18
13-04106-19
ANALYTICAL METHODS
Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was
analyzed using Method EPA 903.0. Radium-228 was analyzed using Method EPA 904.0.
Laboratory qualifiers are as follows:
J-
Indicates a situation where the result minus the error is less than the detection limit but greater
than zero.
U-
Indicates a situation where the result minus the error is less than or equal to zero.
ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.
Page I of3
-mmt7
ANALYTICAL RESULTS CONTINUED

ISOTOPIC URANIUM
Samples were filtered to disassociate dissolved and total fractions. All samples were prepared by mixed
acid digestions as appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted,
micro-precipitated and mounted on micro-porous filter media. Sample activities were then determined by
alpha spectroscopy using energy specific regions of interest for Uranium-234, Uranium-235 and
Uranium-238. Chemical recovery was determined by the use of a Uranium-232 tracer. Activity of the
Uranium-232 tracer was determined by alpha spectroscopy using an energy specific region of interest.
I'' Analytical Attempt

Samples demonstrated acceptable results for all Uranium analyses. Chemical recovery was low for
sample fraction -16 (Client ID: PZ-104-SD TOT). Chemical recovery was acceptable for all other
samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable
results. Results for the Uranium-234 and Uranium-238 duplicate demonstrated an acceptable relative
percent difference and normalized difference. Results for the Uranium-235 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Uranium-234 and Uranium-238 laboratory control sample demonstrated an
acceptable percent recovery.
2"d Analytical Attempt
Sample fraction -16 (Client ID: PZ-104-SD TOT) was reanalyzed due to a low chemical recovery.
Sample demonstrated acceptable results for all Uranium analyses. Chemical recovery was acceptable for
all samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable
results. Results for the Uranium-234 and Uranium-235 duplicate demonstrated a high relative percent
difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Uranium-238 duplicate demonstrated an acceptable relative percent difference and
normalized difference.
Results for the Uranium-234 and Uranium-238 laboratory control sample
demonstrated an acceptable percent recovery.
ISOTOPIC THORIUM
acid digestions as appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted,
micro-precipitated and mounted on micro-porous filter media. Sample activities were then determined by
alpha spectroscopy using energy specific regions of interest for Thorium-228, Thorium-230 and Thorium232. Chemical recovery was determined by the use of a Thorium-229 tracer. Activity of the Thorium229 tracer was determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228 and Thorium-232 method blank demonstrated acceptable results. The
Thorium-230 method blank demonstrated results slightly greater than the detection limit. Results for the
Thorium-228 and Thorium-232 duplicate demonstrated a high relative percent difference; however,
normalized difference is within acceptable limits for the analytical technique. Results for the Thorium230 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results
for the Thorium-228, Thorium-230 and Thorium-232 laboratory control sample demonstrated an
acceptable percent recovery.
Page2of3
ANALYTICAL RESULTS CONTINUED

RADIUM-226
acid digestions as appropriate. This was followed by selective sulfate precipitations of the Radium.
Samples were then mounted by semi-micro-precipitations onto micro-porous filters. Samples were
counted by alpha spectroscopy using an energy specific region of interest for Radium-226. Chemical
recovery was calculated by the use of a Barium-133 tracer, which was determined by HPGe gamma
spectroscopy.
Samples demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated acceptable results. Results for the Radium226 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results
for the Radium-226 laboratory control sample demonstrated an acceptable percent recovery.
RADIUM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were
then counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium133 tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Samples demonstrated acceptable results for all Radium-228 analyses. Due to slightly low chemical
recoveries for sample fractions -12 and -14 (Client ID: PZ-102-SS TOT and PZ-102R-SS TOT), samples
demonstrated slightly high detection limits. In each case the radiometric and gravimetric recoveries were
acceptable. Chemical recovery was acceptable for all other samples. The Radium-228 method blank
demonstrated acceptable results. Results for the Radium-228 duplicate demonstrated a high relative
percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Radium-228 laboratory control sample demonstrated an acceptable percent
recovery.
CERTIFICATION OF ACCURACY
I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
designee to be accurate as verified by the following signature.
M.R. McLlGI~I
Laboratory Manager
Date: 5/16/2013
Ebcrline A.nalytical wants and encourages your feedback regarding our performance providing radioanalytica\ services. Please
visit http://www.eber!ineservices.com/client.htm to provide us with feedback on our services.
Page 3 of3
SECTION IV
ANALYTICAL RESULTS SUMMARY
Paul V. Rosasco, P. E.
Lakewood, CO 80235
Client Sample ID
LCS13-04106-01
LCS13-04106-01
LCS13-041 06-01
LCS13-04106-01
LCS13-04106-01
LCS13-04106-01
LCS13-041 06-01
LCS13-04106-01
LCS13-04106-01
LCS13-04106-01
LCS13-04106-01
BLANK13-04106-02
BLANK13-04106-02
BLANK13-04106-02
BLANK13-04106-02
BLANK13-04106-02
BLANK13-04106-02
BLANK13-041 06-02
BLANK13-04106-02
BLANK13-04106-02
BLANK13-04106-02
BLANK13-04106-02
PZ-111-KS TOT DUP
PZ-111-KS TOT DUP
PZ-111-KS TOT DUP
PZ-111-KS TOT DUP
PZ-111-KS TOT DUP
PZ-102R-SS TOT DUP
PZ-104-SD TOT DUP
PZ-102R-SS TOT DUP
PZ-104-SD TOT DUP
PZ-1 02R-SS TOT DUP
PZ-104-SD TOT DUP
It~
r.1ll
Project: West Lake OU-1

SDG: 1304106
Received: 04/16/2013
Matrix: Water
Lab Sample ID
Analysis Date/Time
Analvte
13-04106-01
13-04106-01
13-041 06-01
13-04106-01
13-04106-01
13-04106-01
13-04106-01
13-04106-01
13-04106-01
13-04106-01
13-04106-01
05/03/2013 05:44:14
05/14/2013 09:50:16
05/01/2013 12:48:31
05/01/2013 12:48:31
05/01/2013 12:48:31
04/30/201314:35:21
05/06/2013 09:42:03
04/30/2013 14:35:21
05/06/2013 09:42:03
04/30/2013 14:35:21
05/06/2013 09:42:03
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-234
Uranium-235
Uranium-235
Uranium-238
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04106-02
13-04106-02
13-04106-02
13-04106-02
13-04106-02
13-04106-02
. 13-04106-02
13-04106-02
13-04106-02
13-04106-02
13-04106-02
05/03/2013 05:44:15
05/14/2013 09:50:16
05/01/2013 12:48:32
05/01/2013 12:48:32
05/01/2013 12:48:32
04/30/201314:35:22
05/06/2013 09:42:05
04/30/2013 14:35:22
05/06/2013 09:42:05
04/30/201314:35:22
05/06/2013 09:42:05
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
uranium-234
Uranium-235
Uranium-235
Uranium-238
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04106-03
13-041 06-03
13-04106-03
13-04106-03
13-04106-03
13-04106-03
13-04106-03
13-04106-03
13-04106-03
13-04106-03
13-04106-03
05/03/201305:44:09
05/14/2013' 09:50:17
05/01/2013 12:48:27
05/01/201312:48:27
05/01/201312:48:27
04/30/201314:42:51
05/06/2013 09:42:00
04/30/2013 14:42:51
05/06/2013 09:42:00
04/30/201314:42:51
05/06/2013 09:42:00
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-234
Uranium-235
Uranium-235
Uranium-238
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
2J
~EBER!-:_I~_E;
Final Report of Analysis

Date: 5/16/2013
Page 1 of 5
Method
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
10.44
7.23
5.84
5.38
5.42
6.55
7.21
0.60
0.47
7.05
7.39
1.16
0.86
0.88
0.83
0.83
0.94
0.97
0.21
0.18
1.00
0.99
0.20
1.14
0.12
0.09
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.01
0.70
0.01
0.25
0.05
0.03
0.03
0.02
0.01
0.03
0.04
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.29
0.26
0.16
0.18
0.09
4.66
0.55
0.20
0.25
3.53
0.25
0.00
0.~
000
0.12
0.00
0.04
000
0~
o.ro
000
0.00
0.17
0.47
0.10
0.10
0.07
0.64
0.61
0.10
0.48
0.52
0.39
0.08
O.o?
0.08
0.07
0.11
013
0.71
0.12
0.00
o.w
u
u
u
u
u
u
u
0.00
O.W
ow
O.o?
OM
000
865/481-0683
0.17
0~
0.11
0.00
O.W
O.W
0~
OM
0.~
0.00
0~
FAX 865/483-4621
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
O.o?

601 SCARBORO ROAD OAK RIDGE, TN 37830
Qualifier
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
Lakewood, CO 80235
Client Sample ID
lliil
a~
!',)
,,)

SDG: 1304106
Matrix: Water
Lab Sample ID
Analysis Date/Time
Analyte
PZ-111-KS TOT
PZ-111-KS TOT
PZ-111-KS TOT
PZ-111-KSTOT
PZ-111-KS TOT
PZ-111-KS TOT
PZ-111-KS TOT
PZ-111-KS TOT
13-04106-04
13-04106-04
13-04106-04
13-04106-04
13-04106-04
13-04106-04
13-04106-04
13-04106-04
05/03/2013 05:44:10
05/14/2013 09:50:17
05/01/2013 12:48:28
05/01/201312:48:28
05/01/201312:48:28
04/30/2013 14:42:53
04/30/201314:42:53
04/30/2013 14:42:53
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS
13-04106-05
13-04106-05
13-04106-05
13-04106-05
13-04106-05
13-04106-05
13-04106-05
13-04106-05
05/03/2013 05:44:11
05/14/2013 09:53:22
05/01/2013 12:48:29
05/01/201312:48:29
05/01/2013 12:48:29
04/30/2013 14:42:54
04/30/2013 14:42:54
04/30/2013 14:42:54
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
D-6 TOT
D-6 TOT
D-6 TOT
D-6 TOT
D-6 TOT
D-6 TOT
D-6 TOT
D-6 TOT
13-04106-06
13-04106-06
13-04106-06
13-04106-06
13-04106-06
13-04106-06
13-04106-06
13-04106-06
05/03/2013 05:44:13
05/14/2013 09:53:22
05/01/2013 12:48:30
05/01/201312:48:30
05/01/2013 12:48:30
04/30/2013 14:42:56
04/30/2013.14:42:56
04/30/20n14:42:56
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
D-6 DIS
D-6 DIS
D-6 DIS
D-6 DIS
D-6 DIS
D-6 DIS
D-6 DIS
D-6 DIS
13-04106-07
13-04106-07
13-04106-07
13-04106-07
13-04106-07
13-04106-07
13-04106-07
13-04106-07
05/03/2013 05:44:51
05/14/2013 09:53:23
05/01/2013 12:49:00
05/01/2013 12:49:00
05/01/2013 12:49:00
04/30/2013 14:42:57
04/30/201314:42:57
04/30/201314:42:57
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
2J
~EBERk~~~

Date: 5/16/2013
Page 2 of 5
Method
Result
Error
MDA
0.~
0.17
OA1
o.n
1.M
0.11
O.W
Q13
QM
0.11
0.~
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
7W
0.~
O.W
3.10
0.13
om
0~
0.00
0.17
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.31
0.73
-0.01
0.14
0.01
7.01
0.26
2.79
0.13
0.94
0.14
0.08
0.08
0.05
0.06
0.04
1~1
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2 .
0.10
0~
OM
QOO
OM
o.ro
O.W
Q12
OM
0.00
QOO
QOO
0.~
OM
Q12
Q~
0.21
1.66
0.13
0.07
0.07
0.08
0.13
0.07
1.75
2.70
0.02
0.07
0.02
0.25
0.00
0.25
OA7
0~
0.60
0.05
0.06
0.04
0.12
0.03
0.12
1.01
0.10
5.W
0.14
0.13
OM
O.W
1.00
0.10
QM
0.~
0.00
Q12
865/481-0683
J
J
J
u
J
J
J
u
J
QM
0~
0.00
0.~
0.00

Qualifier
FAX 865/483-4621
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sample ID
!i!!i
M
1:.1

SDG: 1304106
Matrix: Water
Lab Sample ID
Analvsis Date/Time
Analvte
D-83 TOT
D-83 TOT
D-83 TOT
D-83 TOT
D-83 TOT
D-83 TOT
D-83 TOT
D-83 TOT
13-041 06-08
13-041 06-08
13-041 06-08
13-04106-08
13-04106-08
13-04106-08
13-04106-08
13-04106-08
05/03/2013 05:44:52
05/14/2013 09:53:24
05/01/2013 12:49:01
05/01/2013 12:49:01
05/01/2013 12:49:01
04/30/2013 14:42:59
04/30/2013 14:42:59
04/30/2013 14:42:59
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
D-83 DIS
D-83 DIS
D-83 DIS
D-83 DIS
D-83 DIS
D-83 DIS
D-83 DIS
D-83 DIS
13-04106-09
13-041 06-09
13-041 06-09
13-04106-09
13-04106-09
13-04106-09
13-04106-09
13-04106-09
05/03/2013 05:44:54
05/14/2013 09:53:26
05/01/2013 12:49:03
05/01/2013 12:49:03
05/01/2013 12:49:03
04/30/201314:43:01
04/30/2013 14:43:01
04/30/2013 14:43:01
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP 05TOT
DUP 05TOT
DUP 05TOT
DUP 05TOT
DUP05TOT
DUP 05TOT
DUP 05TOT
DUP 05TOT
13-04106-10
13-04106-10
13-04106-10
13-04106-10
13-04106-10
13-04106-10
13-04106-10
13-04106-10
05/03/2013 05:44:55
05/14/2013 09:53:27
05/01/2013 12:49:04
05/01/2013 12:49:04
05/01/2013 12:49:04
04/30/2013 14:43:03
04/30/2013.14:43:03
04/30/2013" 14:43:03
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP 05
DUP05
DUP05
DUP 05
DUP 05
DUP 05
DUP 05
DUP 05
13-04106-11
13-04106-11
13-04106-11
13-04106-11
13-04106-11
13-04106-11
13-04106-11
13-04106-11
05/03/2013 05:44:56
05/14/2013 09:53:27
05/01/2013 12:49:05
05/01/2013 12:49:05
05/01/2013 12:49:05
04/30/2013 14:43:05
04/30/2013 14:43:05
04/30/2013 14:43:05
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
~EBERLINE
SERVICES

Date: 5/16/2013
Page 3 of5
Method
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
3.17
5.53
0.20
0.47
-0.01
0.03
-0.02
-0.05
0.72
0.67
0.13
0.19
0.08
0.07
0.09
0.32
0.89
0.14
0.10
0.10
o:16
0.18
0.27
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.79
3.78
0.03
0.21
-0.02
0.04
0.02
0.05
0.49
0.74
0.07
0.12
0.04
0.08
0.07
0.08
0.16
1.20
0.13
0.08
0.11
0.15
0.19
0.14
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.27
2.45
0.05
0.13
0.03
0.29
0.10
0.21
0.44
0.64
0.06
0.08
0.04
0.16
0.12
0.14
0.24
1.12
0.08
0.07
O.D7
0.09
0.16
0.13
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.85
1.79
0.06
0.09
0.01
0.14
0.06
0.13
0.34
0.71
0.08
0.08
0.03
0.12
0.10
0.11
0.23
1.31
0.13
0.10
0.09
0.14
0.17
0.10
O.Q3

865/481-0683
FAX 865/483-4621
Qualifier
u
u
u
u
u
u
u
u
u
u
J
u
J
u
J
u
J
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCill
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sample ID
t~
""

SDG: 1304106
Matrix: Water
Lab Sample ID
Analvsis Date/Time
Analvte
PZ-1 02-SS TOT

PZ-102-SS TOT
PZ-102-SS TOT
PZ-102-SS TOT
PZ-1 02-SS TOT
PZ-102-SS TOT
PZ-102-SS TOT
PZ-1 02-SS TOT
13-04106-12
13-04106-12
13-04106-12
13-04106-12
13-04106-12
13-04106-12
13-04106-12
13-04106-12
05/03/2013 05:44:57
05/14/2013 09:53:32
05/01/2013 12:49:06
05/01/2013 12:49:06
05/01/2013 12:49:06
04/30/2013 14:43:07
04/30/2013 14:43:07
04/30/2013 14:43:07
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-102-SS
PZ-102-SS
PZ-1 02-SS
PZ-102-SS
PZ-102-SS
PZ-1 02-SS
PZ-102-SS
PZ-102-SS
13-04106-13
13-04106-13
13-04106-13
13-04106-13
13-04106-13
13-04106-13
13-04106-13
13-04106-13
05/03/2013 08:20:23
05/14/2013 09:53:33
05/01/2013 12:49:46
05/01/2013 12:49:46
05/01/2013 12:49:46
04/30/2013 14:43:08
04/30/2013 14:43:08
04/30/2013 14:43:08
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-102R-SS TOT
PZ-102R-SS TOT
PZ-102R-SS TOT
PZ-1 02R-SS TOT
PZ-102R-SS TOT
PZ-1 02R-SS TOT
PZ-1 02R-SS TOT
PZ-102R-SS TOT
13-04106-14
13-04106-14
13-04106-14
13-04106-1413-04106-14
13-04106-14
13-04106-14
13-04106-14
05/03/2013 08:20:24
05/14/2013 10:11:48
05/01/2013 12:49:49
05/01/201312:49:49
05/01/2013 12:49:49
04/30/201316:24:43
04/30/2013.16:24:43
04/30/2013.16:24:43
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-102R-SS DIS
PZ-102R-SS DIS
PZ-102R-SS DIS
PZ-102R-SS DIS
PZ-1 02R-SS DIS
PZ-1 02R-SS DIS
PZ-1 02R-SS DIS
PZ-102R-SS DIS
13-04106-15
13-04106-15
13-04106-15
13-04106-15
13-04106-15
13-04106-15
13-04106-15
13-04106-15
05/03/2013 08:20:19
05/14/2013 10:11:49
05/01/2013 12:49:43
05/01/2013 12:49:43
05/01/2013 12:49:43
04/30/2013 16:24:44
04/30/2013 16:24:44
04/30/2013 16:24:44
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
EBERLINE
SERVICES

Date: 5/16/2013
Page 4 of5
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
8.05
7.98
3.24
3.03
4.35
5.70
0.33
4.73
0.95
1.61
0.71
0.67
0.91
0.81
0.14
0.70
0.18
2.67
0.13
0.09
0.09
0.06
0.07
0.05
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.58
2.35
0.10
0.12
0.03
5.76
0.25
3.35
0.66
0.61
0.07
0.08
0.04
0.84
0.13
0.56
0.13
1.04
0.07
0.06
0.07
0.08
0.10
0.08
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
3.18
0.40
0.25
0.27
0.36
4.85
0.30
3.17
1.11
2.08
0.12
0.13
0.15
0.68
0.13
0.50
0.57
4.41
0.06
0.08
0.07
0.06
0.09
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.88
1.50
0.01
0.06
0.01
5.54
0.44
3.40
0.43
0.95
0.02
0.05
0.02
0.77
0.17
0.54
0.13
1.87
0.06
0.06
0.05
0.07
0.09
0.06
Method

865/481-0683
FAX 865/483-4621
Qualifier
J
J
u
J
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
Lakewood, CO 80235
Client Sample ID
:
1\:1
Ull

SDG: 1304106
Matrix: Water
Lab Sample ID
Analvsis Date/Time
Analyte
PZ-104-SD TOT
PZ-1 04-SD TOT
PZ-104-SD TOT
PZ-104-SD TOT
PZ-104-SD TOT
PZ-104-SD TOT
PZ-1 04-SD TOT
PZ-104-SD TOT
13-04106-16
13-04106-16
13-04106-16
13-04106-16
13-04106-16
13-04106-16
13-04106-16
13-04106-16
05/03/2013 08:20:21
05/14/2013 10:11 :49
05/01/2013 12:49:45
05/01/201312:49:45
05/01/2013 12:49:45
05/06/2013 09:42:02
05/06/2013 09:42:02
05/06/2013 09:42:02
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-1 04-SD
PZ-104-SD
PZ-104-SD
PZ-104-SD
PZ-1 04-SD
PZ-104-SD
PZ-104-SD
PZ-104-SD
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
13-04106-17
13-04106-17
13-04106-17
13-04106-17
13-04106-17
13-04106-17
13-04106-17
13-04106-17
05/03/2013 08:20:30
05/14/201310:11:49
05/01/2013 12:49:54
05/01/201312:49:54
05/01/201312:49:54
04/30/2013 16:24:46
04/30/2013 16:24:46
04/30/2013 16:24:46
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
PZ-1 04-SS TOT

PZ-104-SS TOT
PZ-104-SS TOT
PZ-104-SS TOT
PZ-104-SS TOT
PZ-104-SS TOT
PZ-104-SS TOT
PZ-1 04-SS TOT
13-04106-18
13-04106-18
13-04106-18
13-04106-18
13-04106-18
13-04106-18
13-04106-18
13-04106-18
05/03/2013 08:20:26
05/14/201310:11:40
05/01/2013 12:49:51
05/01/201312:49:51
05/01/2013 12:49:51
04/30/201316:24:47
04/30/2013.16:24:47
04/30/2013.16:24:47
PZ-104-SS DIS
PZ-104-SS DIS
PZ-104-SS DIS
PZ-104-SS DIS
PZ-104-SS DIS
PZ-104-SS DIS
PZ-104-SS DIS
PZ-104-SS DIS
13-04106-19
13-04106-19
13-04106-19
13-04106-19
13-04106-19
13-04106-19
13-04106-19
13-04106-19
05/03/2013 08:20:28
05/14/201310:11:40
05/01/2013 16:16:51
05/01/201316:16:51
05/01/201316:16:51
04/30/201316:24:48
04/30/2013 16:24:48
04/30/2013 16:24:48
EBERk~~~~

Date: 5/16/2013
Page 5 of 5
Method
Result
Error
MDA
Qualifier
0.16
1.88
5n
0.~
2.72
1~
0~
0.00
0.07
Q17
0.11
Q~
0~
0.18
0.~
0~
0.~
o.m
0.~
0.08
0.10
0.65
0.91
0.59
u
u
u
u
E903.0
E904.0
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
3.76
1.90
0.02
0.16
0.00
0.26
0.05
0.23
0~
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
1.19
0.80
0.05
0.16
-0.03
0.22
0.01
0.09
0.32
0.46
0.05
0.09
0.03
0.10
0.03
0.07
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
0.81
1.58
0.03
0.08
-0.02
0.13
0.02
0.17
on
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.04
Q10
0.14
0.85
0.07
0.07
om
0.07
0~
0.28
0.25
0.23
0.~
0.12
Q~
0.~
QOO
0.~
o.ro
0.00
Q04
QOO
865/481-0683
u
J
J
J
0.14
QOO
ore
QOO
0.10
Q~
0.07
Q~
0.14
1.17
0.12
0.09
0.08
0.06
0.07
0.04

FAX 865/483-4621
u
J
u
J
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
SECTIONV
ANALYTICAL STANDARDS
()..-8
QA/QG REVIEWED CERTIFICATE OF CALIBRATION

!? qJ-;nitials J1( ALPHA STANDARD SOLUTION
!late
Radionuclide:
HalfUfe:
(4.468
Catalog No.:
Source No.:
,.
TMA BBERLINE
Customer:
OR2778
P.O.No.:
12:00 PST.
Reference Date:
January 11995
Contained Radioactivity: (Total U) 8.016 14Ci
Contained Radioactivity: (Total U) 297 kBq
U-238NAT
0.005) x 10'9 years
7338
479-50
Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
. .'( ~; :;.
: ..
......
. ,. ..
~.
65.2896 g in a 50 ml flame sealed ampoule

Uranyl Nitrate in H20
None
Approximately 1.3202
d. Density:
Radioimpurities
g/ml @20 9 C,
Refer to attached technical data sheet
Radioactive Daughters
Refer to attached technical data sheet
... , ..
Radionuclide Concentration
...,.;
.... :
(Total U) 0.1228
Method of Calibration
lolCilg.
Activity calculations are based upon known specific activity and mass.
,...-
., .;.'"
,.,,
Uucertainty of Measurement
a. Systematic uncertainty io instroment calibration:
b. Random uncertainty in assay:
c. Random uncertainty io weighing(s):
d. Total uncertainty at the 99% confidence level:
3.0%
0.0%
2.0%
3.6%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standarda and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data were taken from "Table of Radioactive Isotopes*, edited by Vu-ginia S. Shirley, 1936.
2. IPL participates in an NJST measurement assurance program to ~!.tablish and maintain implicit ttaceability for a liumber of nuclides,
based on the blind assay (and later NIST certification) of Standard Rcferenc~ Materials (As in NRC Regulatory Guide 4.15) .
. ..... ,.--,-
'I~\./ "'.
/.
.;
P'7 !?euvfhp{? t~f.
Date Signed
/'(':'
.
ISOTOPE
I'RODVCT.S
l.A B 0 !\A TO !t 1 "ES
ISOTOPE PRODUCTS LA BORATORIES

3017 N. SAN FERNANDO BLVD.
BURBANK, CALIFORNIA
91504
8188437000
8188436168
FAX
.:'
QUALITY CONTROL PROGRAM

MP-009
Rev.S; 11/01/03
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY CJ/LUTION RECERTIFICATION

MP009
Reference DateL.I~~\:1:.:,;11:.:,;11::,.:9:.::95::::.~.0::.:;00::.~1
Radionuclide;,c:
'U.
Certified Activity <<8:016E+OO J.LCi
Certified Concentration li<'"" : :.: J.LCi per gram
Ampoule /Solution Gross " 97.:6400 Weight, Grams

Empty Ampoule I.> ::32:5020 Weight, Grams
Solution Net
" 65.1380 Weight, Grams
Total Activity in Ampoule
8.0160 J.LCi
Chemical Com osition of Standard Solution
.:::;.
Dilution Solvent Used
IDilu1Jion instructions:
Dilute to a volume ofl : 1000:00 .. !milliliters
Certified Total Activity ofl
. 8;0160lJ.LCI
Which Eauals
1.780E+07ldpm at the date listed above

This activity concentration Is based on the original
And after dilution the activity of this solution is 1.77955E+04jdpm/mhlference date listed above; All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date:
I Septembers, 2013 I
Date: --"'9/"'26:;.;/2::..:0;.;.12~0::.;;.00;;;...
Date: -.......!J'I/c..::u.:=.r/1....;.'"_
2-- _
~EBER!;-INI;; I QUALITY CONTROL PROGRAM

MP009
~RVIOI'CS
Rev.6; 11101103
Trtle: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES- OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP.009
Solution Reference #IIPL47~50: ..
Principal Radionucllde
Half Life, Years
~?"''
,,.,._ 238(Jj
....
'<bi6BE:.Cti9l
Reference Date f :
Radionuclide of lnterestfW~:2;>'f"'U -]
Parent Solution Conc.r 1:TZ96E+04 tdpmlml
Chemical Comeosltion of Standard Solution
1u;anw Nttiiltei ir: 1~ HNo3
9/6/2012 0:00 t
Datal
::I
Solution #F . -:.u;,aa-i .
Half Life, Da~s
1.632E+12!
'I
Dilution Instructions:
.:
'-1t1i1eilso:oo 1
11M HN03
., .. ,_ ..
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution:

Total Activity:
Final Volume:
_,,,,,_: .A:oooo
ml
7.1182E+04 dpm
'-1000:00 ml
Final Activity Concentration:!
This activity concentration is based on the original

reference date listed above. All activities are
corrected to the date and time of analysis by the
~hn, tory data processing software.
NOTES:
Isotopic Distribution as:
U-238 Atom % ~ 48.239
U-235 Atom % = 2.25
U~234 Atom%= 49.501
All values+/- 3.6%
7.1182E+01!dpm/ml
U-236 71.162 dpmlml X 0.48249 = 34.345 dpmlml

U-235 = 71.182 dpmlmlX 0.0225 =1.602 dpmlml
U-235 = 71.162 dpmlml X 0.49501 = 35.236 dpmlml
Expiration Date:! September 6, 2013
Isotopic ratios from manufacturer's data sheet
(\.
\-:~. ~
:y
Verified & Approved
QCApproval
l'
~JRAAA\1l !\
Dale:
9/26/2012 0:00
Date:
1~UP,(2...
r
.RECORD COPY
Tracer Solution for Environmental Analysis & Disequilibrium Studies
Product Description & Measurement Certificate
Description
Principal radionuclide:
Daughter Nuclide:
Measurement
Reference date:
Radioactive concentration U-232
which is equivalent to
uranium l32 (U-232)

Th-228
Volume of solution
Total activity ofU-232
which is equivalent to
Accuracy
Radiormc/idic
Purity
Product code: UDPl 0050

Batch Number: 921232/67
0 I March 2000
6.739E+03 becquerels per gram of solution
1.821E-Ol microcuries per gram of solution
5.35 gr"'willS
5.035 millilitres
3.61 E+04 becquerels
9.76E-Ol microcuries
Method ofmeasurement (see reverse of this certificate)

Random uncertainty is: 0. 7%
Systematic uncertainty: 0.5%
Overall uncertainty in the radioactive concentration quoted above: I. 7%
Overall uncertainty is defined on the reverse of this certificate.
Any radioactive impurities measured are listed below, expressed as percentages
of the activity of the principle radionuclide at the reference date .
Th-228 and daughter activity removed 2 Feb 2000
U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00
~ne
Isotopic
Purity
isotopic composition, exprossed as atom per cent at the reference date .
,'lot measured
Chemical
Composition
Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution bas been produced 'carrier free'.
Physical
Data
Recommended half lifo of uranium 232: 6.980E+OI years

Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.0%
Branching ratio for alpha emission: I 00%
Calculated specific activity of uranium 232: 8.167E+OS Bq per microgram U-232.
Remarks
For safety information and notes to ensure correct usage by all persons handling this radio'lctive Tracer
solution please read the instructions accompanying the package.
ABA Technology operates a quality management system which bas been independently audited and
approved to ISO 900 I.
Approved
Signatory
Project Ref. AE2315
Roger Wiltshire
Prepared and characteri~ed in the UK, for world wide distribution by Isotrak, AEA Technology, QSA.
T!kcert.wps I 0/03/00
AEA Techn...,logy is the trading name of AEA Teclmology J::" 3 m

MP-009
Rev.8; 11/01/03
Titte:
Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES -OAK RIDGE LABORATORY

PRIMARY DILUTION RE!CERTIFICA T/ON
MP009
CURRENT DATE I
12/13/2012 0:00)
SOLUTION REFERENCE #lr.IAEA/.=:':'~m""'"ers=h"'"am=.9;:;-;21:::23::::2-;;::/6~7,~
. ,.;1
SOLUTION #)<. >: ' U.C1 0 ;
I
Principal Radionuclide
.,.: "-'u
Half Life, Years
Half Life, Days
I . 1.20Qi:+o1l
>"u;
I . . . 2.630E+04I
Reference Date(
Radionuclidel '
Certified Activity ....9.760E-:01 J1Ci
Certified Concentration ' c :. : . : JlCi per gram
i3f1120Qb O:OOJ
""''""'' .......~ -, .- l"'"hl.Empty Ampoule

Solution Net
. . Weight, Grams
. . . . Weight, Grams
0.9760 J1CI
Chemical Composition of Standard Solution
Dilute to a volume of/ 1000.00
Certified Total Activity of/
.. 0.9760/JlCI
/milliliters
Which Eauals
1 .. 2.167E+06/dpm at the date listed above

This activity concentration Is based on tho original
And after dilution the activity of this solution Is J2,167E+03/dpm/ml reference date listed above. All activities are corrected
to tho date and time of analysis by the laboratory date
Expiration Date: December 7, 2013 J
Date:
Date:
12113/2012 0:00
lf3~
I
Rev.8; 11101/03
Title: Radloaetfve Reference Standards Solutions & Records

Reference Date!
IDIIuticn Instructions:
'--3i1120bo:o:odl
J2MHNO.
. .
.. 3. :

Vol. Parent Solution: ' 10.0000 ml
Total Activity: 2.167bE+04 dpm
Final Volume: ' :
ml
1ooo;oo
. 2.1670E+01Jdpmlml

laboratory data processing software.
NOTES:
Expiration Date:! December 7, 2013
Verified & Approved By_.:_:-:;-,r==l==7--:-TI'I~--

QC Approval
*=,u.
Date: _ _1:.:21:..:1.::31:.::2::.01.:..:2::.;0::.:00=-
RTIF'ICATE OF CALffiRATI~,~
,
.'"'"'. . ~L.PHA. STANDARD SOLUTION" ~"' \ ~:~\\~\\
~~~===.!
... 'd.f\. l't~
Radionuclide
Th-230
Half Life:
(7 .54 0.03) X w-4 yeaiS
Catalog No.:
7230
Sonrce No.:
388-116
b. Chemical fonn:
c. Carrier content:
d. Density:
Cuslomer:
TMA EBERIH~ll"" 'fA\~'f;;,~
P.O.No.:
'IT4944
,,~
Reference Date:
November 1 1991
12;00 PST.
Contained Radioactivity:
1.036
. "Ci.
5.0042
Th(N03)4 in 0.1N HN03
None added
1.0016
grams.
gnm/ml 2oc.
Radioimpurities
See attached technical data sheet
See attached technical data sheet
0.207
Metbod of Calibration
Weighed aliquots of the solution were assayed using a liquid scinlilla1ion counter.
Uncertainty .of Measurement

a. Systematic uncertainty in instlllinent calibration:
c. Random uncertainty in weigbing(s):
2.0%
0.5%
0.2%
2.7%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Notes
1. Nuclear data were taken from "Table of Isotopes , Seventh Edition, edited by Virginia S. Shirley.
2. IPL participates in an NIST measurement assunwce program to establish and maintain implicit
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulato:ry Guide 4.15)
ISOTOPE PRODUCTS LABORATORIES

1800 No. Keystone Street.,
Burbank, California 91504
818 843 - 7000
\~
"'
EE3ER!;;:IN.&;
I<RVIC:&
I QUALITY CONTROL PROGRAM

MP-009
Rev.B; 11/01/03

MP-009
Solution Refereno::e #IIPL 3!l8il16 ,.. <
Principal Radionuclide
Half Life, Years
,: ""'iTfi'::.]
1. vi54oE+oi!l
.:.:
Reference Date !::'
Radionuclide of lnterestF''9.trtiiiiitim'iil
Parent Solution Conc.I''/2~30E+il3::.:Jdpm/ml

:-;~_::::.._,:~;' -;._
l"''f\'!IN\':h>~'{~O'~NH~g;.g,.~.:<c'' '-----
~:
Dale!
3/412013 o:oo I
Solution #F ' <::Th-1b.::. .':.. ..c~
Half Life, DaJ!S
.
2.754E+07l
'"
.. ..
~.
,~
'11i~J19s1oWiol
<I
IP41\1+\N93'\:S:i .
::;-<;::
SYI

Total Activity:
Final Volume:
,._
:.:,:';:1,0~0000 ml
2.2999E+04 dpm
;:<~:
"'-""''1000:00 ml
Final Activity Concentration:!::
2.2999E+01 Jdpmlml

NOTES:
{
Recertified
"'>'-.
Verified & Approved By

QCApproval
\:-.~
~
.,_
" "'
I' ~ --:- ~
z.c::.:J!hJ ~AAAA \ \
..
"
Expiration Date:
Date:
Date:
Date:
March 4, 2014
3/2112013 0:00
j..?.t '~
~t)..\(1~
~!i;;:BI;;:B.h~~c~ I

MP.009
Rev.8; 11/01/03

PRIMARY DILUTION RE:CERTIFICA TION
MP009
. 3/4/2013 0:001
CURRENT DATE I
SOLUTION REFERENCE# IPL386"116- . . ~.~
SOLUTION #F< ..,_. -...T:h~1.ii> ,>~
Princioal Radionuclide
Half Life, Years
Half Life, Da:ts
:- '~"'trh '<J
2~754E+o7j
7:54oit+o41
Radionucllde 1 ~':>rtiiirium:
Certified Activity ' '1C:o36Et00 ~tCi
Certified Concentration '.':0:':.
,.ct per gram
Reference Date!': .-_. -.. \1.'\iWiseto:ool
-c:: . .
Ampoule /Solution Gross ._. :; 9.2660

Empty Ampoule ;-:t6218
Solution Net
< 4.6442
1~0360
Weight, Grams
Weight, Grams
Weight, Grams
~tCi
1 of
,- ,-~i;-., .
7-:~T0-:7_7'.'S!t:,>:2[1
DilUtion Solvent Used
Dilute to a volume of!' : -1ooo:oo
Certified Total Activity of
1.0360I,.c
joJN+tNb
- .. .. .... . : ,3 ...
. . --.:,:,::.
..
:';'\.':.:>:::::<:::_:\
>I
. 'I milliliters
Which Eauals
2;300E+06Idpm at the date listed above

And after dilution the activity of this solution Is I 2.300E+o3ldpmlml reference date Usted above. All activities are corrected
to the d~ and time of analysis by the laboratory data
Expiration Date:
--~
QCApproval
'March 4, 2014 _ I
\::l"-
c.~J ~\lAJ
"
Date:
Date:
\..
3/21/2013 0:00
-~-~ 1i.J. ~
74-8
CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION
Radionuclide:
Th-232
Half Life:
(1.405 0.006) x 1010 years
Catalog No.:
7232
Source No.:
435-104-2
b. Chemical form:
c. Carrier content:
d. Density:
TMAEBERLINE
VH1632
Customer:
P,O.No.:
12:00 PST.
Reference Date:
November 1 1993.
(Th-232) 0.0933
,.Ci.
(Th-232) 3.45
I:Bq.
11.9712 g (iri a 10 mi flame sealed ampoule)

Th(N03)4 iri water
None added
Approx. 1.21
g/ml@20C,
None detected (other than daughters).
Radioimpurities
.
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212,Po-212, Tl-208 .
(Th-232) 0.00779
p.Cilg.
Activity calculations are based upon known specific activity and mass.
Uncertainty of Measurement
a. Systematic uncertsirity iri irislrument calibration:
b. Random uncertainty iri assay:
c. Random uncertainty iri weighing(s):.
3.0%
0.0%
2.0%
3.6%
NIST Traceability
This calibration is implicitly traceable to the National Institote of Standards and Technology.
Leak Test(s)
Notes
1. Nuclear d~ -~~ taken from "Tahte. Of Radioactive Isotopes"~ edited by Virgiitia S. Shirley, '1986.
2. 1PL pattic~tes iti an NIST meBsurement assurance program to establish and tnaintaln implicit traceability for a number of nucli~.
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
QUALITY CONTROL
Date Signed
1800 North Keystone Street
818
3-7000

MP~09
Rev.S; 1/10/03
Tille: Radioactive Reference Standards Solutions & Records

PRIMARY DILUTION RECERTIFICATION
MP009
SOLUTION REFERENCE
I"'""''""
1,gg3
. :o: .... ..'""''
,.,,o.ol
Ref erence Dat e.,,
.. , ..,,......,.:..,."
per gram
IDiilution Instructions:
Dilute to a volume ofi\'WHtOOO:fOO:iiH mllllllters
lr.rt<fi"n Total Activity ofl
;;o:0933h.LCi
Which Eauals
L> .::''2;071E+o5ldpm at the date listed above
And after dilution the ar.:tivity of Uli~> 10olutlon isi2;071E+:o:Udpm/ml
This aetivlty concentration Is based on the original

reference date lisled above. All activities ""' corrected
Expiration Date: I,. Ocfobllr9,'2013"
Date:
101912012 0:00
---=-==:::..:..::;.;:::;=
U37
Rev.B; 1/10103

Radlonuclide of Interest!' O:.'F~ ~ ~Tii : ;I

Parent Solution Cono.r .2:07E+02 'ldpm/ml
Reference Date
l' 11t1i199:l'o:oo I
IDilutilon ln$truetions:
IWoNitrieAdd

Vol. Parent Solution: ' '"600:0000 ml
Total Activity: 1.0355E+05 dpm
'1000;00. ml
Final Volume:
Final Activity ConGentration:!
1.0356E+02ldpm/ml

laboratory data proceo;slng software.
NOTES:
Expiration Date:!. October 9, 2013
Verified &Approved
B~ ~
QCApproval
~~11
J1 H (~""'
-. v \r
v
Date:--+~~~:O!:QQ_:OO
Date:
1\ ,.,_/ J't...
-""'+-~,..<....!=:'---
1!' Isotope Products

.
7h-!8
24937 Avenue Tibbitts

Valencia, California 91355
Laboratories
An Eckert & Ziegler Company
Tel 6613091010
Fax 6612578303
ALPHA STANDARD SOLUTION
Th-229
7340 160 years
7229
867-54
Radionuclide:
Half-life:
Catalog No.:
Source No.:
Physical Description:
A. Mass of solution:
B. Chemical form:
C. Carrier content:
D. DE')nsity:
Customer:
P.O. No.:
Reference Date:
(Tb-229 only)
EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST
1.013
J.tCi
37.48
kBq
5.0147 g in 5 ml flame-s!'laled ampoule

Th(N0 3 ) 4 in 0.1 M HN0 3
10~g Th/mL
1.0016 g/ml @ 20'C.
Radioimpurities:
None detected (daughters in equilibrium)
RadionucUde Concentration:
0.2020
JJCVg,
kBq/g
7.474
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in JJCi/g was determined
using gamma ray spectrometry.

Peak energy used for integration:
193.5 keV
Branching ratio used:
0.0441 gammas per decay
Uncertainty of Measurement:
A. Type A (random) uncertainty:
B. Type B (systematic) uncertainty:
C. Uncertainty in aliquot weighing:
D. Total uncertainty at the 99% confidence level:
0.7%
3.0%
0.0%
3.1%
Notes:
- See reverse side for leak test(s) performed on this source.
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification} of Standard Reference
Materials (As in NRC Regulatory Guide 4.15}.
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.
q- JCA/n -ti2Quality 'Control
Date Signed
IPL Ref. No.:
867-54
- - - - - - - - - - - - - - - - - - IS09001CERTJFIED - - - - - - - - - - - - - - - - - -
Medical Imaging Laboratory

24937 Avenue Tibbitts Valencia, California 91355
Industrial Gauging Laboratory

1800 North Keystone Street
llm3:9
~~;;_e~;;;Rn~~Fii I

MP..OD9
Rev.e: 1/10/03
Title:

PRIMARY DILUTION RECERTIF/CA TION

MP009
SOLUTION REFERENCE #fiPL 867-4 ....
PrinciDal Radionuclide
Half Life, Years
. . ":'"Tti . I
7.34oE:+o3l
11/9/2012 0:001
CURRENT DATE I
SOLUTION #I-.:_._,. Theta:.: 'I
.. ..
"I
Half Life, Daxs

.. 2.681 E+06j
I
Reference Date I .:.:
Radionuclide , .... . -.. . ~2.9fii :.. ,

Certified Activity . <M13E+OO. llCi
Certified Concentration ": .: .-:: . ... > flCi per gram
Ampoule /Solution Gross . .
Empty Ampoule ..: .
Solution Net
Total Activity In Ampoule
Chemical Comnosition of Standard Solution
l~h(N()sl41ri .().~ 1\11 l:lNQ3 : . . . .... ~
'TT7 .-:
8.7752
3.7591
5.0161
1.0130
. .
1i15t2oo2'o:ooj
Weight, Grsms
Weight, Grams
Weight, Grams
flCI
''I
io,1rvrHNP3
.. .
Dilute to a volume ofl', 1000.00 : lmillillters
Certified Total Activity of I
1.(.)130l11Ci
Which Eauals
2:249E+06Idpm at the date listed above

And after dilution the activity of this solution Is 1 2.249E+03ldpm/ml reference date listed above. All activities are corrected
Expiration Date:

QCApproval
~~J1N
~
October 9, 2013
11/9/2012 0:00
Date:
Date:
ultz[tz..
i
I
~EBERL,!_~ I QUALITY CONTROL PROGRAM

MP-009
SE:F<VlCEe
Rev.7; 9129/99
Tttle: Radioactive Reference Standards SolutJons & RecordS

MP-009
Solutio!l Reference #IIPL86,7"54
.
Principal Radlonuclide
Half Life, Years
.._.-~'Th ---:t
7.34oe+osl
11/9/2012 0:001
Date!
Solution #I . Th,18a- :.-I
Half Life, Da:ts
2.as1E+osl
.. I
Radionuclide of lntere~ >~-Parent Solution Cone. 2:25E+03
Reference Date
I ...
-111si2oo2o:ool
ldpmlml

ITH<NOsJ41rr0.1MHiiiOs> . .
<
I
lo.1MHNOa
..
.10.0000 ml
Total ActiVIty: . ...
2.2490E+04 dpm
Final Volume:
1000.00 ml
2.2490E+01 dpmlml

NOTES:
Expiration Date:
QCApproval~
--~
..
~
'-...J
October 9, 2013
Date:
1119/2012 0:00
Date:
!l~fZb'k
;
J}ational
3Jn.~titute
of
~tanbatb%
& m:ecbno lo !l!'
cttrttftcate
.,..,..
This Standard ReferenceM,ate,rial(SRM) consist$ o~ radioactive barlum-13~ <;J;lloride,11on~!adioactive barium

chloride, and hydrochloric acid diSsolved in 5 niL of distilled water. The solution is containyd in a flamesealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization thambers and
solic!-state gamma-ray,spectrometry.wstems.
Radiological Hazard
The SRM ~mpoule contains barium-133 with~ total activity of approximateiy 2.5 MBq. Barlum-133 decays
by electron capture and during.\)le decay process X-rays and ga1111Ya:~ays with energies from 4 ..tP 400 ke V are
emitted. Most of these photons escape from the SRM ampoule and can represent a radiatipn hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding ~nd/or distance shoulc! be used to.~e. pe,rsonnel exposure.,,The.SRM.~houlc! be
.~e\1 ouly by persons qUalified to ha11~e radioactiv~ materiaL

Chemical Hazard
The SRM ampoule. contain~ hydr<?chloric acid (HQ) with a concentration of 1 mole per lite~ .o~.water. 'Ihe
solution is corrosive imd represent$ health hazard if it comes in contactwith.eyes or.skin, If the ampoule
is to be opened to transfer the solution,.the recommended procedure is given on page 2. The ampoule should
be opened only by persons qualified to handle ,both radioactive material and strong '!l'id solution.
Storage and Handling

The SRM should be stored and used at a temperature between 5 and 65 oc. The solution in an unopened
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R Hutchinson, Group Leader. The overall technical direction and physical
measurement$ leading to certification were provided by LL. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standard Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
October 1994
SR!v! 4251C, .P~ge l.of 6 ,
Thomas E. Gills, Chief

Standard Reference Materials Program
*Notes and r":ferences_ are.~~ pages-~ and 6.

QCP.009
Rev.B; 11110103
TIUe: Radfoactive Reference standards Solutions & Records

PRIMARY DILUTION RECERTIFICATION
QCP 0091
SOLUTION
!Dilution Instructions:
Dilute to a volume ofj?,:r!:l.000:00''.'"'4mllllliters
'66.5577htCi
Which Eauals
'"1A78E+oaJdpm at the date listed above
And after dilution the activity of this solution isi1.478E+Q5Idpmlml

reference date listed above. All activities are corrected
Expiration Date: lsepteniller 20. 20131
Date: _ _..::9~12':!.7~11::2'---
<t4f..!-z.~'l+=l.::Z:.__
Date: _ _ _
Rev.B: 11/10/03
Title: Radloac:tfve Reference Standards SoluUona & Records
EBERL.INE SERVICES OAK RIDGE L.ABORATORY

RADIOACTIVE REFERENCE STANDARD SOL.UTIONS
':'13aa:
Radionuclide oflnteres '

::.<
Parent Solution Cone. ' j .46E+05 > dpmlml
Reference
Date~!~~.;,9~i1!!.;/1!.:9~9~3~0~:o:!.lol
!Diluticn Instructions:
I1MHCI

Vol. Parent Solution: ' " . :<2s:oooo ml
Total Activity: . 3.6950E+06. dpm
Final Volume:.,.,. ''1000:00 ml
NOTES:
3.6950E+03ldpmlmi

Expiration Date:j September 20, 2013
Date: _ _...,;9:'.!;/2~7'-!./1~2:...___
Date: _ _'I:J;/Z-:::;.'1!4-11:.!:2.::::..__
Radionuclide:
Half Life:
Catalog No.:
1600
Source No.:
Ra-226
Customer:.
TMA EBERUNE
7 years
P,O.No.:
VH1888
7'126
Reference Date:
February 1 1994
12:00 PST.
Contained Radioactivity: (Ra-226) 1.001 JLCi.
Contained Radioactivity: (Ra-226)
37.0 kBq.
453-26
Description of. Solution

b. Chemical form:
c. Carrier content:
d. Density:
5.1864 g (in a 5 ml Flame Sealed Ampoule)

Ra(N03)2 in I N HN03
None added
1.0318
Radioimpurities
g/ml@20"C.
None detected(other t:bail daughters)
Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.
Radionuclide Concenttation
(Ra-226)
0.1929
.. ,.
p.Cilg.
Weighed aliquots of the solution were assayed using gannna spectrometry:
Energy peak(s) integrated under: 186 keV.
Brancbillg ratio(s) used:
0.0351
gauuna rays per decay.
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
c. Random u.ncertainty in weigbing(s):
3.4%
3.1%
0.2%
. 4.6%.
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standarda and Technology.
Leak Test(s)
Notes
1. Nuclear data were _takeil from "Table of Radioactive Isocopes*, edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement 8:ssurance program to e6tabllsh and maintain implicit traceability for a ~r of n~;~clides,
-cased on-tlfifbliii<niSBay-(fi"iHl"litef NIST-certifiCiltiODfOfStindafa 'R.etereii&fMiiteri8.lS\AinifNRC"Regulafuty-Guide-4; 1"5) ~-- ---
QUALITY CONTROL
fib. 1,
[qq If
Date Signed

1800 North Keystone Stteet
Bwbank, California 91504
818 843 -7000

MP009
Rev.8; 11/01/03
RIDGE
PmMARYD~UTIONRECERTIRCATION
MP009
Radionuclide ?~f\i;!diurir
Certified Activity :.1:001 EioOO J.t,Ci
Certified Concentration . " ". ""- J.LCi per gram
Reference
Date~...l-"'-'--"-=-21c..:1.'-i1:.;:~""94.:..""b"":b"""ol
_ _. -_ _ " Weight, Grams

Ampoule /Solution Gross~-Empty Ampoule . .: .-: : .. Weight, Grams
.
Weight, Grams
Solution Net "
Total Activity In Ampoule
1.0010 J.LCI
IDiilution Instructions:
Dilute to a volume ofl " "1000.00 -
1:0010JJ.LCi
j1MHNOa
Imilliliters
. 2.222E+06Jdpm at the date listed above
Which Eauals
This activity concentration is based on the ortglnal
And after dilution the activity of this solution lsi 2.222E+03Jdpm/ml reference date listed above. All activities are corrected
Expiration Date:
Verified & Approved

QC
By_y__:_~-~-----t---:-~--~~~1,;,-,--
Approval_-\a;"""'"""'~""'.:>t..'W"'O...'----\...)-=;.._-
I November 9, 2013
Rev.8; 11/01/03
Trtle: Radioactive Reference Standards Solutions & Records

Radionucllde of lnb-stl.:':~t
Parent Solution vOJOC.Ii
Chemical Com osition of Standard Solution
IDilutic>n Instructions:
Dilution Solve.nt Used

NOTES:
Final Activity Concentration:(

: .,.:)4.4440E+01Idpm/ml
reference date listed above. AU activities are
Expiration Date: I NovemberS, 20131
Verified & Approved By_~-::;o...--,;-~=lt~-----
Date:
1119/2012 0:00
QC Approvai_~..L!IW~..Ubt-_::,w__ _ __
Date:
,,f,z.!,
z_.
I
I
R~-n
ANALYTICS
1380 seaboard Industrial Blvd.

Atlanta, Georgia 30318 U.S.A.
Phone (404)352-8677
Fax
(404)352-2837
Standard Radionuclide Source
62680-416
Ra-228 5 mL Liquid in Flame Sealed Vial
was
prepared
This
standard
radionuclide
source
gravimetrically from a calibrated master solution.
The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
ACTIVITY (dps) :
HALF-LIFE:
CALIBRATION DATE:
Ra-228
2.585 E3
5.75 years
November 7, 2001 12:00 EST
TOTAL UNCERTAINTY*:
4.0%
SYSTEMATIC:
3.0%
1. 0%
RANDOM:
*99% Confidence Level
Impurities: y-impurities (other than decay products) <0.1%

5.07198 grams 0.1M HCl solution with 50
P 0 NUMBER
~g/g
Ba carrier.
9508, Item 1 (Part #4339A)
SOURCE PREPARED BY:

l;;:o
M. D.
Q A APPROVED:
.~.
urr1e, Rad1ochem1st

MP~09
Rev.8; 1/10/03
TrUe:

RECERTIFICATION
MP009
Certified
Certified CoinCe>ntraticmiJi
per gram
JDiilution Instructions:
Dilute to a volume ofH~')l;,:fQOO;'Q!:lN{{mllllllters
1Cc1rtl1~ed Total Activity ofl\ ' .OiCi6!1!1lJl.Ci
Which Ee~uals I ,.,,..r;:1;SSt'E+Q5ldpm at the date listed above
And after dilution the activity of this $Oiution I$1:'1:'551E.,Q2ldpmlml
This activity concentration is based on Ule origfnal

reference date listed above. All activities are corrected
to the dele and time of analysis by the laboratory data
Expiration Date:!:> >AptiiJ2;':2013 c.;.l
Recertified
B:_~__,J'>'-'----=:::::::3~-{""~-
Verified & Approved By _ _ _
---::::>""...,--~.----=--
Date: _ _...;4~/1~6~/1~2_ _
Date:------Date: _
_.f'--f.}-'-&"'-1/u.'I...,.Z-~
SECTION VI
QUALITY CONTROL SAMPLE RESULTS SUMMARY
Eberline Services
Analysis Control Chart
Printed: 5/1/201311:21 AM
Page 1 of 2
wo
Aiialysis
R"'
Activi!l_l:Jnits
13-04106
UUISO
pCi
Client Ni'!!!J~-
Aliauot Units
Laboratory Control Sample

Analyte
U-234
Normalized
Difference
2.85
LCS
Measured
80.82%
'
csu
Measured
LCS
Expected
Uncert
Expected
16.06%
100.00%
3.60%
I
'
Known
8.10E+OO
Known
Result
csu
Standard
='
2.92E-01
6.55E+OO
1.05E+OO
U-Sa
Standard
ACT(dpm)
ID
1.46
89.28%
15.87%
100.00%
3.60%
7.90E+OO
2.84E-01
7.05E+OO
1.12E+OO
U-Sa
Sample
Result
sample
Sample
Aliquot
Standard
ID
Standard
Added (g)
3.52E+01
3.60E+OO
5.10E-01
i 3.44E+01
i 3.60E+OO
5.10E-01
Standard
ACT(dpm)
Standard
'
U-238
Standard
Error
Matrix Spike
Normalized
Difference
Analyte
MSActual
%Rec
Expected
MS Result
Expected
MS Uncert
Actual
MSResult
Actual
MSCSU
csu
Normalized
Difference
RPD
Original
Result
Original
Replicate
Result
Replicate
LCS Relative
csu
csu
Bias
U-234
0.37
4.17
4.85E+OO
7.66E-01
4.66E+OO
7.24E-01
U-238
0.88
10.68
3.17E+OO
5.48E-01
3.53E+OO
5.81E-01
U-235
1.16
40.90
3.01E-01
1.36E-01
1.99E-01
1.05E-01
t<i
~:W,ll
uu
!!->'~
Version
Standard
Added (g)
RepRPD
RepND
QCSummary
Replicate Sample
Analyte
Error%
MS%R
MSND
LCS%R
LCSND
0.81
OK
OK
NA
OK
0.89
OK
OK
NA
OK
OK
OK
NA
OK
Eberline Services
Printed: 5/1/201311:21 AM
Page 2 of 2
Wo
Alia lysis
Run
Activity Units
13-04106
UUISO
pCi
Aliquot Units
Client Name
Replicate Sample RPD
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
--------------i
25.00
20.00
90,00
15.00
BO.OO
10.00
1o.oo t--------~uc_!;:;-;--------,---------cuc_~;;;---------,
2 34
Lower Error
Uooer Error
%R
LCL
Mean
UCL
61.16
100.48.
80.82
80
----
100
120
2 38
5.00
69.82
108.75
89.28
80
100
120
0.00
--Lower Error
Upper Error
RPD
CL
U-234
4.50
3.85
4.17
35
U-238
11.58
9.78
10.68
35
Normalized Difference
3.50-,-------------------------------
~~~
~
Ui
1"_,
Version
No Matrix Spike
U-235
50.77
31.02
40.90
35
Eberline Services
Printed: 516120131:15 PM
Page 1 of 2
wo
Analysis
Activity Units
13-04106
UUISO
pCi
Client Name
Aliauot Units

Nonnalized
Difference
Analyte
LCS
Measured
csu
Measured
LCS
Expected
Uncert.
Expected
Known
Known
Error
Result
csu
Standard
ID
I
U-234
1.69
U-238
0.98
l
i
Standard
Standard
ACT(dpm)
SS.19%
15.29%
100.00%
3.60%
I 8.17E+OO
2.94E-01
7.21E+OO
1.10E+OO
U-Sa
3.52E+01
92.S3%
15.23%
100.00%
3.60%
I 7.96E+OO
2.87E-01
7.39E+OO
1.13E+OO
U-Sa
3.44E+01
Sample
Result
Sample
Sample
Aliquot
Standard
"'''"
3.60E+OO
Standard
Added (g)
5.15E-01
I 3.60E+OO I 5.15E-01
Matrix Spike
Nonnafized
Difference
Analyte
MSActuaf
%Rec
Expected
MSResun
Expected
MS Uncert
Actual
MS Result
Actual
MSCSU
csu
tll
U1
!,.)
Nonnalized
Difference
RPD
Original
Result
Original
Replicate
Result
Replicate
csu
U-234
1.02
99.84
1.84E-01
3.51E-01
5.51E-01
6.12E-01
U-238
0.18
20.57
2.04E-01
3.48E-01
2.51E-01
3.86E-01
U-235
0.52
57.43
4.57E-01
6.03E-01
2.53E-01
4.83E-01
Version
Standard
ACT(dpm)
Standard
Error%
Standard
Added(g)
RepRPD
RepND
QCSummary
Replicate Sample
Analyte
ID
csu
LCS Relative
MS%R
MSND
LCS%R
LCSND
0.88
OK
OK
NA
OK
0.93
OK
OK
NA
OK
OK
OK
NA
OK
Bias
Eberline Services
Printed: 516120131:15 PM
Page 2 of 2
wo
AnalySis
13-04106
UUISO
"""
Activity Units_
Aliauot Units
pCi
Client Name
LCS % Recovery
130.00
~0.00
120.00
35.00
110.00
L _____ _
30.00
100.00
25.00
20.00
90.00
15.00
BO.OO
10.00
7o.oo t--------cuc_234:;-;---------,----------,uc-2o3c8:--------,
-
Lower Error
Upoer Error
%R
LCL
Mean
UCL
69.30
107.08
88.19
80
100
120
I
I
73.99
111.66
92.83
80
100
120
,_00
o.oo j-----~U~-2~34-;-----,-----~U-~2~38;;-----,-----U~-~2~35;-------,
-
Lower Error
Uooer Error
RPD
CL
165.24
34.43
99.84
35
I
I
37.14
4.00
20.57
35
3.50
~---------------------------
3.00
+--------~-~----~------------
2.50
G'!l!
~~
!.II
$;::11J,
Version
+----------------------------
No Matrix Spike
I
I
101.32
13.53
57.43
35
Eberline Services
Printed: 5/2/2013 9:18AM

Page 1 of2
---wo
13-04106
Analysis
Roo
Ac_t_iy_!!x_ Units
ThiSO
pCi
AliQuot Units
Client Name
~~~
Difference
Analyte
...
'
TH-230
TH-232
LCS
Measured
csu
Measured
LCS
Expected
Uncert.
Expected
I
I'
Known
Known
Standard
csu
Standard
ACT(dpm)
Standard
Error
Standard
Added (g)
='
Result
1.73E-01
5.84E+OO
1.04E+OO
Th-8b
1.04E+02
3.60E+OO
1.03E-01
1.06E+OO
Th-1b
2.35E+01
2.70E+OO
5.14E-01
5.42E+OO i 9.59E-01
Th-8b
1.04E+02
3.60E+OO 11.03E-01
121.36%
17.83%
100.00%
3.60%
4.81E+OO
0.11
98.93%
19.73%
100.00%
2.70%
5.44E+OO
1.47E-01 ' 5.38E+OO
1.22
112.51%
17.70%
100.00%
3.60%
4.81E+OO
1.73E-01
1.92
TH-228
ID
Matrix Spike
Normalized
Difference
Analyte
MSActua/
%Rec
Expected
MS Result
Expected
MSUncert
Actual
MS Resutt
Standard
Added (g)
Actual
MSCSU
QCSummary
Replicate Sample
Analyte
trn
l11!
Normalized
Difference
I
1
RPD
Original
Result
Original
Replicate
Result
Replicate
LCS Relative
csu
csu
Bias
LCS%R
LCSND
MS%R
MSND
RepRPD
RepND
TH-228
0.70
33.94
1.11E-01
7.92E-02
1.57E-01
9.91E-02
1.21
OK
OK
NA
OK
TH-230
0.29
10.65
2.04E-01
1.01E-01
1.83E-01
9.87E-02
0.99
OK
OK
NA
OK
TH-232
0.76
37.36
1.25E-01
7.74E-02
8.59E-02
6.70E-02
1.13
OK
OK
NA
OK
ll'~l
Version
'
Eberline Services
Printed: 5/2/2013 9:18AM

Page 2 of 2
wo
Analysis
Ron
Activity_ Units
13-04106
ThiSO
pCi
AliQUOt Units
LCS % Recovery
130.00
40.00
------..oUCL
120.00
Client Name
35.00
110.00
30.00
100.00
j-------------1
25.00
20.00
9{).00
15.00
-------LCL
80.00
10.00
7o.oo
Lower Error
Upper Error
%R
LCL
Mean
UCL
TH-228
99.93
142.79
121.36
80
100
120
-
--lll".o<UU
TH-232
76.50
121.36
98.93
80
100
120
91.21
133.81
112.51
80
100
120
5.00
0.00
- . ---
rn.<:.<:o
45.25
22.63
33.94
35
-.
rn-230
13.40
7.90
10.65
35
3.50~--------------------------
3.00
+-----------~--------~-------
2.50
+---------------------------
tl~i
~~~
l.il
1::1!)
Version
No Matrix Spike
TH-232
50.13
24.59
37.36
35
Eberline Services
Printed: 51312013 12:01 PM

Page 1 of2
---wo
Analysis
Activi~}"-~_!lit~
Ra226
13-04106
Aliquot Uni~~
pCi
Client Name

Nonnallzed
Difference
Analyte
RA-226
0.17
I
I
Measured
LCS
Expected
102.12%
23.87%
100.00%
r-----l
I
csu
LCS
Measured
----+
-- -r-
Uncert.
Expected
4.60%
Known
standard
10
Standard
ACT(dpm)
1.02E+01_4.70_E-O~ ~4E+01 2.49E+~~:5b
4.41E+01
Known
csu
Result
='
- - - -----t
-----
-~---
Standard
Error
standard
Added(g)
5.15E-01
' 4.60E+OO
Matrix Spike
Analyte
Nom~afized
Difference
1
I
MSActual
%Rec
Expected
MS Result
---l-- --+~-
+------
Expected
MS Uncett
Actual
MS Result
Actual
MSCSU
Sample
Resun
Sample
Sample
Aliquot
csu
Standard
ID
Standard
ACT(dpm)
Standard
Error%
Standard
Added(g)
___
--+--
----
----tI
-----------
----'------
----~---
---.-- ------
I__ _ _ _ _
_j__ _____
QCSummary
Replicate Sample
I
Analyte
RA-226
l<li
U1
"I
Version
Normalized
Difference
RPD
0.40
16.46
LCS Relative t
Replicate
csu
Replicate
Result
csu
Bias
1.87E-01
2.95E-01
1.79E-01
1.02
Original
Result
Original
3.48E-01
I
!
LCS%R
LCSND
OK
OK
+L
MS%R
MSND
RepRPD
RepND
OK
OK
Eberline Services
Printed: 513/2013 12:01 PM

Page 2 of 2
wo
Analysis
13-04106
Ra226
--r
Run
Activity Units
pCi
_Nlqu91_,u~n~its~--+---
Client Name
LCS % Recovery
130 00
4000
120 00
35 00
110.00
30 00
100.00
25 00
2000
90.00
1500
8000
1000
7o.oo
- __ L~~~-~r:T.Q~-
__l,,l~~er Error
~-- ~13
RA-226
73.65
130.59
102.12
1::::___"':::_'=&_!:___ _
--.-lyl-~~--- _,____ __ _
1-
-UCL
-----------=f20-
500 i
o oo
1-
1~~rEfl1)r
Upp_e~_l;~r_
RA-226
21.13
f1'.78
RPD
-CL
No Matrix Spike
t"Y:
~~
!,J1
():)1
Version
Eberline Services
Printed: 5/14/2013 2:11PM

Page 1 of 2
wo
An~ly_~~s.
_f3:un
P.~!~!~>:_~n~t~-
13-04106
Ra228
pCi
t-
AHq~ot l,!Q!_~s-~-
__f_~l")~. t'!ame

Analyte
RA-228
Normalized
Dlfference
LCS
CSU
Measured
Measured
1.81
80.70%
25.57%
LCS
expected
I'
Uncert.
Expected
Known
5.10%
8.96E+OO
__ j
1_oo__.ooo/._,_ '.
~'~----+
1-+--
Known
Result
Em"
4.57E-01
7 .23E+OO
.. -
----- -
1.8~E+OO
-- '
.__ _J __ _
csu
Standard
ID
standard
ACT(dpm)
Standard
Em>
Ra-11
5.10E+OO
Standard
Added (g)
5.11E.01
-------
!--
Matrix Spike
Analyte
Normalized
Difference
MSActual
%Rec
Expected
MSResult
Expected
MSUncert.
Actual
MSResult
Actual
MSCSU
Sample
Result
Sample
Sample
Aliquot
csu
_L
Normalized
Difference
RPD
Original
Result
Original
Replicate
Result
Replicate
csu
2.38
121.84
1.08E+OO
4.79E-01
2.62E-01
4.74E-01
csu
LCS Relative
Bias
0.81
LCS%R
LCSND
OK
OK
-+
~I
!Jl
Ul
Version
Standard
ACT(dpm)
Standard
Error%
Standard
Added (g)
RepRPD
RepND
NA
OK
QCSummary
Replicate Sample
RA-228
ID
r--
-~ . .-1
Anatyte
Standard
MS%R
MSND
Eberline Services
Printed: 5/14/2013 2:11 PM

Page 2 of2
wo
Analysis
Run
13-04106
Ra228
~~---L
_ Activ!ty_!!~_
pCi
..9~~t;l.~~ Name
LCS % Recovery
13000
40,00
12000
35 00
110.00
30.00
10000
25.00
20.00
9000
15.00
BOOO
10 00
70.00
- -~~~~-~rT(Jf
- - J!P~~E.~()_r
~
50_03
1:::___-:-:_~_g~ .
-===-~!1~1!1- -UCL
ooo
1-f1.37
80.70
%_R
"'
RA-228
80
1oo120
!-:~-~r:__!?:_~-+---
Upp~~-~~-
RPO
1- -CL
RA-228
165.06
78:61
121.84"
35
3.50
3.00
2.50
2.00
1.50
1.00
0.50
o_oo
!i<ll
ij;,
01
t,:l
version
No Matrix Spike
SECTION VII
LABORATORY TECHNICIAN'S NOTES
ISOUNOTES
Run 1
-f;J&62
Page 1 of 1
Printed: 4/25/2013 9:14AM
jfJ ~BJ:;:RJ...,LN g:
~
SERVICES
Work Order Analysis Notes
#
1
Date
Dept
04/25/13 09:14
PREP
User
JBARNARD

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
13-04106
UUISO
1
Notes
ALIQUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- PRESERVED
SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
Printed: 4/29/2013 6:10PM
Page 1 of 1
~ t;:_j3_i'::;_Rh~t;'lc~

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
13-04106
UUISO
t---------+-- - - - - - - Internal Work Order
Analysis Code
Run Number
Date
Dept
04/25/13 09:14
PREP
JBARNARD
AUQUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- PRESERVED
04/29/1318:10
CHEM
JDEMELAS
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes. rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI- 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
User
Notes
Printed: 4/30/2013 5:38AM
Page 1 of 1

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Date
Dept
User
Internal Work Order
I
Analysis Code
Run Number
13-04106
UUISO
1
Notes
-:- -~-::::;:;;;;_ - ;::~- ~:::~;;__ --~~--~;;i~~~~~i~~~~~:~;I~!~tf~1~~I~;;~~~;;~~~~;~~2~;;;i~:~~~;;t~~;~;-D

columns with 35 ml SN HCl; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml SN
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
I
3
04/30/1305:37
c""H"'E""M;-t--,;R:;cM;-;A-,;Rc;TZ""""--+-A-::Dc;D;;cE'"D=o.""-'17M;;-L---;N;-;E"'O"'D~Y;;;:M;;;IU"M-;:-,;C-;:Ac;RR"'I"'E"R--:,Oo;--_3;;-;--;M'L-"TTriiT'"'A""N-;;0:;-;U:oS--,C"H""L"O""R"ID"'E~,o-&--:;1--;M-;;L---;H-;;F~T;o;O=c"-T"U"B"'E"'S--c;L"E"'T'"'S~;E"'T
I
f
SIT IN ICE BATH FOR ONE HOUR SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML 01 H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.
Eberline Analytical
Printed: 4/30/2013 5:39AM

Page 1 of 1
Internal Work Order
13-04106
e:: . ~. I:::B, hiR!)ic~
Analysis Code
Reagents Used in an Analysis
UUISO
Reagent
ID
Reagent
Name
Reagent
Concentration
Run
1
Analyst
ID
013624P
Nitric Acid
Reagent Grade
JBARNARD
013666P
Anion Exchange Resin
Reagent Grade
JDEMELAS
4/29/2013
0137945
HCI - HF
6.5N - 0.04N
JDEMELAS
4/29/2013
,doric Acid
0.5N
JDEMELAS
4/29/2013
0137345
, oyd;u""uriL Acid
6.5N
JDEMELAS
4/29/2013
013675P
, oyuu~'"u' ~ Acid
Reagent Grade
JDEMELAS
, 4/ L~/ Lll13
0138005
"I
8N
JDEMELAS
41"~9/2013
013810S
HCI
8N- 0.1M
JDEMELAS
4/?9j7f)13
013246S
Carbon substrate
Solution
RMARTZ
012809P
Ethyl Alcohol
R1
1t Grade
RMARTZ
4/30/2013
013221P
Hydrofluoric Acid
Reagent Grade
RMARTZ
4/30/2013
013191S
Neodymium Carrier
1 mg/ml
RMARTZ
' 4/30/2013
0)'!4'!4P
Titanous Chloride
Reagent Grade
RMARTZ
013bi:>UUl
.,
loric Acid
NH41
4/25/2013
4/30/2013
----
4/30/2013
mB-ES
19
:}~~tf1f
:=:~~{i&I@._:
}~il~;
.-.;::.
'O<:c ;,. OC co'. '-~~~-~- ' ...... ... ~ ,,;:1'ioL... .. . .. .... .. . . .. .. .. .. -~===--=-'"''=
.....""'"''C=--=,=.oC~Coo6""-"''~"~..=""<-"""""<~~.
~~
-r----t------------11------+----+-----t-----1---[i
.--1-~----------_--~t--_-...._-_---=-----..-..~==-----.~--.~~~~~-~~~~;~~-~~~~:~~~~~~~~~~~~~~~:~~--.1
i
-t----1------ ----- ~------+----11------1:----+---f

-
- - - - 1 - - - - - - - - - - - - - - - - - - - - ....- 1 - - - - + - - - - - 1 - - - - - - i i - - - 1
-----1------------- ---------+-----+-----1------ii---tA
---.........,1-------------+ -----+----t----'"----+-----J--t;,
- ----11---------..........---1-------+----+-----+------+--.,-_j
!''
---~------ - - - - ------------1---+-----1-----+---~it
fC ''
q
d~---.-. . -----------.-.--
.
..
. . . . . . ..J
.
~..:
'
ISOUNOTES
Run2
Printed: 5/2/2013 9:53AM
~
#
1
Page 1 of 1
1;;-~-~-R-~JR~-~
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Date
Dept
05/02/13 09:53
PREP
User
JBARNARD
Internal Work Order

Analysis Code
Run Number
13-04106
UUISO
2
Notes
AU QUOTED AND ADDED SPIKES AND TRACERS- PRESERVED SAMPLES WITH HN03 AND DRIED
SAMPLES DOWN
Printed: 5/3/2013 5:48PM
Page 1 of 1
~
~J::IJ:::RL.LN.!;;
~

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
SERVICES
Internal Work. Order

Analysis Code
Run Number
13-04106
UUISO
2
Date
'1
05/02/13 09:53
PREP
JBARNARD
ALIQUOTED AND ADDED SPIKES AND TRACERS~ PRESERVED SAMPLES WITH HN03 AND DRIED
SAMPLES DOWN
05/03/13 17:48
CHEM
JDEMELAS
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C~Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml8N
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of O.SN HCI into clean, labeled 100
Dept
User
Notes
Page 1 of 1
Printed: 5/6/2013 5:33AM
:/J
E:aERLINE
~
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
SERVICES
Date
Dept
User
:1I :::::::::::: fI :::: .1 ~::::::
- 3
i'
Analysis Code 1
Run Number
I
I
13-04106
UUISO
2
-i~:~~~E~i~~;::;,:.;;:~.~b::~:::~:~:~~:;;:,:~;d:~;~;:~::~:~::;,;;~;;
_ __
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 m18N
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of O.SN HCI into clean, labeled 100
ml beakers: Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
-L-::'
osto6t13o5:33-lcHEM-
....
I!
Notes
\
I
1
I
i
Internal Work Order
RMARi'Z ___
ADDED o.1 ML NEoDYMiuM cARRIER, o.3 ML TITANous cHLORIDE, & 1 ML HF To c-TuBEs: LET sET
SIT IN ICE BATH FOR ONE HOUR SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES
FROM C-TUBES REMOVED FILTERS LET DRY IN DESSICATOR
Printed: 517/2013 8:30AM
Page 1 of 1
~ e: E:J I:::Rbt~c~
# [
Date
05/02/13 09:53
2- -
05763713.-17":48- ---cHEM --
Dept
PREP
Internal Work Order
Analysis Code
Run Number
13-04106
UUISO
2
Notes
User
JBARNARD
---yoE~iELAS
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
_________
AU QUOTED AND ADDED SPIKES AND TRACERS- PRESERVED SAMPLES WITH HN03 AND DRIED
SAMPLES DOWN
.--Added concentf~ited-HCito-samplebeake;:s-and-heatidtodiyneSS;"Added26nll aNHcL.to sampleSSild___ _
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI- 0.1 N NH4!, 35m!
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 m! of O.SN HCI into clean, labeled 100
05/06/13 05:33
CHEM
RMARTZ
ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET
SIT IN ICE BATH FOR ONE HOUR. SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.
Printed: 5/6/2013 5:36AM

Page 1 of 1
Eber!ine Analytical
,....
~&
1merna1 Work Order
13 04106
El3E::RL,..INE::
n" ,,. ; Code
SERVICES
UUISO

'-
Reagent
Name
Reagent
lD
Run
Reagent
Concentration
Analyst
lD
Date
Nitric Acid
Reagent Grade
JP.AD"4Rn
5/2/2013
HCI - HF
6.5N - 0.04N
JDEMELAS
5/3/2013
Hydrochloric Acid
6.5N
JDEMELAS
5/3/2013
Hydrochloric Acid
8N
JDEMELAS
5/3/2013
, :yd;uc:uu: ,~Acid
R:
1t Grade
JDEMELAS
5/3/2013
013708P
D:
1t Grade
JDEMELAS
5/3/2013
0138315
HCI- NH41
8N
JDEMELAS
5/3/2013
013675002
Hydrochloric Acid
0.5N
JDEMELAS
:i/~/2013
0132465
Carbon substrate
Solution
RMARTZ
5/6/2013
Ethyl Alcohol
D,
'"Grade
RMARTZ
5/6/2013
Hydrofluoric Acid
Reagent Grade
RMARTZ
5/6/2013
Neodymium Carrier
1 mg/ml
RMARTZ
5/6/2013
Titanous Chloride
Reagent Grade
RMARTZ
5/6/2013
013624P
0138045
.....
0137345
.......
0138135
013809P
:...
'
..
012809P
013221P
'
..
.. 0131915
013434P
...... ,_
! .
..
..
0.1M
fiUi75
63
t12"1_
12-c-:!>.4
JuJ-Et
..tvr --- - .-~-'F~t,T~""--tl~i'-----
1'1.-\ '}--_
""--"-" -I
----f=-'::0"0-1-l. ..Lf'"'~"'"'"-'''~ -"'<..>.:c_,~_o-:.-:;
-U CO. (L
.l..l(,_t:)~
~~
... Vr'>
.....
IJ
.Vf.
1...;+u..t._
u ''-"~} ... L-t...; kcA.....

. L{
+dJ--...
l '--\\\ . . I ....C.---- ---11----'---"--=-----+-"---

t'-\_~ .
r-J-1>-
+=- -----t---1-'--""-----:
U']..:") 1-~'-'--.-+-"".L..2,1>--II~~'
.1
tiF. D. 1--,-.Y""~--".::--11--'""'-"'~"1-=--
ll;'l -ti7'~"""'"::._f-_L.'":~~-=~. .
...w
---------+--1-f.vf,l'-.1-11---+-''-"-:. "7-JfC.-'-t.-~= I
- ..~.
. o.a-.._ . ----"=-="'-'=t--"""''-'="~+-"~~
- ...'}.Lf(lt ~~~ ___ l_ -,'0 't 17\'A..... t ..,..,_..
-J-L.VH,I-1----'""'~ ol-ttDJ,()J
0'1'"\..."J
f)' 't""
. - --
~----t ---~~1-
-!-~----+--~
----
- -- - - -1--~-~+--
ISOTHNOTES
llllll77
Printed: 4/25/2013 9:14AM
Page 1 of 1

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
#
1
Date
04/25/13 09: 14
Dept
User
PREP
JBARNARD
Internal Work Order
Analysis Code
Run Number
13-04106
ThiSO
1
Notes
AU QUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- PRESERVED
Printed: 4/30/2013 5:42PM
Page 1 of 1

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04106
ThiSO
1
Date
Dept
04/25/13 09:14
PREP
JBARNARD
04/30/13 17:42
CHEM
JDEMELAS
Added concentrated HN03 to sample beakers and heated to dryness; Added 20 ml 8N HN03 to samples and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged nnsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; Eluted
Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15ml. Set sam tes aside for tater reci itation and filterin
User
Notes
Printed: 5/1/2013 6:04AM
~
~
Page 1 of 1
E;:__!;::f'!,I...,J N ...:::
SERVICES
#
1
Date
04/25/13 09:14
;'
Dept
PREP
User
JBARNARD
Ill
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
,.
!
Analysis Code
Run Number
13-04106
ThiSO
1
Notes
- --o4t3ot13.17:4z-- "" "EHEM-- --J-6-EMEi::i\S"-"--- --Adaed-concentrate-d-HN03-to-sampie-tieak-ersanc!""heateci-to-ciryness;"t.:<:i"ded20-miaNHN03. ia-s;imp-ies-anci"

transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; Eluted
Thorium with 50 ml of BN HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
ll--:c-1-''"==-;;~=-+---o==c-ll-o.-;;7;=;---~1- volume to -15m!. Set samples aside for later precipitation and filtering.
3
05/01/13 06:04
CHEM
RMARTZ
. .
--,""==ell
ADDED 0.75 ML 0.1MG/ML CERIUM CARRIER & 1 ML HF TO C-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES FROM C-TUBES,
REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.
Eberline Analytical
---
Printed: 5/1/2013 6:05AM

Page 1 of 1
----------------------------~~~~~~-
--. -~-~-~--- --r---.-------
~ ~eh~~fi
013624P
ThiSO
013721P
-----------'"
0138005
Reagent
Name
0138035
Reagent
Concentration
Nitric Acid
--
Reagent Grade
I -Reagent Grade. .
-J
ID
JBARNARD
--
~]
ll
Recorde~
-~nalys~--~
.
i 4/25/2013 ;
~20f2013_!
Hydrochloric Acid
8N
JDEMELAS
.... '
..
........... ~
JDEMELAS
4/30/2013
Hydrochloric Acid
Reagent Grade
JDEMELAS
4/30/2013
8N
JDEMELAS
4/30/2013
4/30/2013
------------~~-------------~-----------r------ ------~---' --~~ ~--
----~---------~- +---~-'-~~--- ----------
013675P
0-~d~~-------~---------.-
-----~I~:~~4166---~"~-~

Reagent
ID
Work
~~-t-~rnal
- -
Nitric Acid
---------
----
. . . -~-----+-~~ ~----~--
---+-
013624P
Nitric Acid
Reagent Grade
JDEMELAS
0132465
Carbon substrate
Solution
RM!\RTZ
5/1/2013
0130175
Cerrium Carrier
0.1mg/ml
RMARTZ
5/1/2013
012809P
Ethyl Alcohol
RP~gent
Grade
RMARTZ
5/1/2013
013221P
Hydrofluoric Acid
, "Grade
RMARTZ
5/1/2013
21
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RA-226 NOTES
Printed: 4/25/2013 9:13AM
~ t=:~R
Page 1 of 1
L
L!"U';;:
SERVICES
#
1
......
Date
Dept
04/25/13 09:13
PREP
User
JBARNARD
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04106
Ra226
1
Notes
ALIQUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- DRIED
FRACTION 12 DOWN AND DIGESTED DUE TO SAMPLES BEING VERY DITRY- PH'D SAMPLESPRECIPITATED WITH BAAND PB CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND
CENTRIFUGED- SUBMMITTED RADIUM PRECIPA TO SEPARATIONS
Printed: 5/2/2013 4:18PM
Page 1 of 1
~E:BERL_.INE

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
SERVICES
Internal Work Order
Analysis Code
Run Number
13-04106
Ra226
1
# I
Date
04/25/13 09:13
04/30/13 13:27
PREP
LWALKER
05/02/13 16:02
PREP
LWALKER
FOLLOWED STEPS 12.1 TO 12.8 IN AP-006 REV 12 FOR RA 226 ANALYSIS (SYRINGE FlLTEREDPRECIP-FIL TEREO-DRlED-OBTAlN FINAL WEIGHT) SUBMIT TO COUNT ROOM.
05102!13 16:17 --rPREP-
LWALKER
WHILE SYRINGE FILTERING FRACTION #14 SOME OF THE ORGANICS IN THE BOTTOM OF C-TUBE
FLOATED TO THE TOP WHILE POURING INTO SYRINGE. HAD TO USE SEVERAL FILTERS IN ORDER
TO FILTER ALL THE SAMPLE COMPLETELY.
i
'
Dept
PREP
Notes
User
AU QUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- DRIED
FRACTION 12 DOWN AND DIGESTED DUE TO SAMPLES BEING VERY DITRY- PH'O SAMPLESPRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND
ADDED EOTA TO PRECIP-VORTEX-LET SIT OVERNIGHT TO DIGEST.
JBARNARD
Printed: 5/2/2013 6:13PM

Page 1 of 1
Eberline Analytical
EBERLINE
SERVICES
Ra226
013376P
Ammonium Hydroxide
Reagent Grade
JBARNARD
4/25/2013
013575D01
Ammonium Sulfate
200 mg/ml
JBARNARD
4/25/2013
012766D14
Barium Carrier
1 mg/ml
JBARNARD
4/25/2013
012729D07
Lead Carrier
166 mg/ml
JBARNARD
4/25/2013
013624P
Nitric Acid
Reagent Grade
JBARNARD
4/25/2013
013416P
Perchloric Acid
Reagent Grade
JBARNARD
4/25/2013
009098P
Sulfuric Acid
Reagent Grade
JBARNARD
4/25/2013
013811S
EDTA
0.25M
LWALKER
4/30/2013
011383P
Acetic Acid
Reagent Grade
LWALKER
5/2/2013
013575D02
Ammonium Sulfate
200 mg/ml
LWALKER
5/2/2013
llU!I89
I
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2-. . .r:v.
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'
RA-228 NOTES
Printed: 4/25/2013 9:13AM
Page 1 of 1
)!J ~_!:;: RL!NI:;::

~
SERVICES
#
1
Date
Dept
04/25/13 09:13
PREP
User
JBARNARD

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04106
Ra228
1
Notes
AU QUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- DRIED
Printed: 5/10/2013 2:14PM
Page 1 of 1
~ E:_e.,;:~J,.,JN_J:;:

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
SERVICES
Date
Dept
04/25/13 09: 13
PREP
JBARNARD
User
05/03/1312:53
PREP
LWALKER
05/10/13 14:14
PREP
LWALKER
Internal Work Order
Analysis Code
Run Number
13-04106
Ra228
1
Notes
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1 TO 12.7 IN AP-007 REV 17 (CHEMICAL CLEANUP FOR RA 228)
Page 1 of 1
Printed: 5/14/2013 9:27AM
'J;:: e_!';:R_~jii~c~
Date
Dept
User

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
!!
Analysis Code
13-04106
Ra228
Run Number
II
Internal Work Order
- - - -
i ---
''""'""'''"
.........
""'""'"'""'"""""'""""""
Notes
04/25/13 09:13
PREP
JBARNARD
05/03/13 12:53
PREP
LWALKER
05/10/1314:14
PREP
LWALKER
FOLLOWED STEPS 12.1 TO 12.7 IN AP-007 REV 17 (CHEMICAL CLEANUP FOR RA 228)
05/14/13 09:27
CHEM
RMARTZ
followed procedure Ap-007 rev. 18 step 12.8-12.15 and submitted to count room.
FRACTION 12 DOWN AND DIGESTED DUE TO SAMPLES BEING VERY DITRY- PH'D SAMPLESPRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
Eberline Analytical
Printed: 5/14/2013 2:10PM

Page 1 of 1
Internal Work Order

--
------
__ )
____j
3::-Q41 06_________~
Analysis Code
Run
~----------------------------------r-------

Reagent
ID
Reagent
Name
~----~-!:_337~1'_______ ~m_<Jn_1um~~~ro~~d:.._
Ra228
Reagent
Concentration
_____
--+~eagent c;rade ~:
____Ol35?5D01 _____ LI\r11_momum Su~f_<~te ___________ j_ _2CJO mg/ml

Barium Carrier
012729D07
0 13416P
009098P
Sulfuric Acid
012766014
+JBARNAR__D___
Date
Recorded
I
I
__j
J~~5/201~l
j __J_B!-RN)\RD___ j4/25/2~1?li
1 mg/ml
! JBARNARD
! 4/25/2013,
- ------- ----------.......--(...------~------------------------------~-----------------+------------!
Lead Carrier
1
166 mg/ml
1
JBARNARD
i 4/25/2013 /
!
!
,
1
_ _ ___
Analyst
ID
I
_L__
I
-----------+-
--------~-~:rc~!~~l\~~~~===-~=------=1~~~~~~~!~r~~~ :~-=~-J~A~~A.Ri:>. . ~=-=-t~/~5/~~j:~
-----------
Reagent Grade
JBARNARD
JBARNARD
[ 4/25/20~.?_]
LWALKER
I 5/10/2013/
r---------------------~-----------------~--------------------------- ---------------------------------,--------------------------
~Reagent Grade
013624P
Nitric Acid
011504D22
Ammonium Sulfide
013801S
Yttrium Carrier
_l
r-tt1!:!F__: __:~~~-;.~
'
2%
\4/25/2013\
-- ---------r------------------------- ---1
~ __: =-K~~:~:=-=::::p;~~ ~-~~

l-6-i}g :~~L:: :=~=~~-~~~~~~~~~~::~-= _=::_=_=t: ~-b~~~~~~-:- =-:===: ~~_;g;;f~-=- J~)~~)~~i-i]
:--------------T----------------------,.---------- I
9 mg/ml
I LWALKER
1 5/10/2013\
-----------------------------t---------;--------ml
013624003
Nitric Acid
1N
RMARTZ
[ 5/14/2013~
013686S
Nitric Acid
6N
RMARTZ
~/14/2_D_1_3j
tlllil97
L()Lt Ito /'Le,Q
85
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SECTION VIII
ANALYTICAL DATA (ISOTOPIC URANIUM)
RUNl
Eberline Services
Analysis Sheet
Printed: 4/30/2013 5:39AM

Page 1 of3
13-04106
UUISO
Run 1
I ,
Work Order
Internal
Fraction
I ,
UUISO
Analysis Code
01
Sample
Desc
Client
LCS
LCS
II
ID
Login
Sample
Date
CPM
04/16/13 00:00
1.0000E+OO
04/16/13 00:00
1.0000E+OO
45
i! 04/11/13 11:30
1.0000E+OO
43
04/09/13 15:35
1.0000E+OO
04/09/13 15:35
1.0000E+OO
04/09/13 15:45
1.0000E+OO
04/09/13 15:45
1.0000E+OO
o4to9t13 16:16
1.0000E+OO
I
I
1---- .
Run
02
MBL
BLANK
--~---
4/16/2013
03
5/7/2013
04
05
TRG
PZ-111-KS DIS
43
West Lake OU-1
06
TRG
D-6 TOT
45
07
TRG
D-6 DIS
45
pCi
08
TRG
D-83 TOT
40
Date Received
--
-~--------
Lab Deadline
-------
I-
Client
Project
DUP
PZ-102R-SS TOT
Sample
Aliquot
------
--------------------
TRG
PZ-111-KS TOT
-----
--- ----
Report Level
------------------
Activity Units
----
09
WA
10
Aliquot Units
-------
D-83 DIS
40
04/09/13 16:16
1.0000E+OO
TRG
DUP 05 TOT
47
04/09/13 00:00
1.0000E+OO
04/09/13 00:00
1.0000E+OO
04/11/13 09:10
1.0000E+OO
-----
Method
NAS NS-3050 Modified
11
TRG
DUP 05 DIS
Alpha Spectroscopy
12
TRG
PZ-102-SS TOT
- ---1
47
!
----~- --------
--
Instrument Type
-----------------
TR~---
------~--
Matrix
I!
39
-----
13
U-232
Radiometric Tracer
Radiometric Sol#
U-10a
-----
Tracer Act (dpm/g)
14
DO
15
TRG
TRG
TRG
17
-
04/11/13 11:30
1.0000E+OO
04/11/13 11:30
1.0000E+OO
--
44
PZ-104-SD TOT
44
PZ-104-SD DIS
PZ-104-SS TOT
-------
TRG
-----
PZ-104-SS DIS
04/11/13 11:38
1.0000E+OO
04/11/13 11:38
1.0000E+OO
04/11/1312:59
1.0000E+OO
-- ..
--
TRG
19
---
-----------
..
-----
45
.. .
---
18
1-
1.0000E+OO
45
..
-----
Carrier Cone (mg/ml)
04/11/13 09:10
. -----------
PZ-102R-SS DIS
-
16
Carrier
39
------
PZ-102R-SS TOT
----
19.093
---------
------ --- .
--~
-----
PZ-102-SS DIS
TRG
I - - - - ------
-----------~-
___ i
i
42
42
..
04/11/13 12:59
I
I
1.0000E+OO
------
I
..
~a
1...~,
i<!ll
1\ll
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 4/30/2013 5:39AM

Page 2 of3
13-04106
UUISO
Run 1
Internal
Fraction
Sample
Desc
Tracer
Aliquot (g)
01
LCS
::
~~~-----~~:::: +----:~::
08
TRG
0.5986
09
TRG
0.5987
11.4
10
TRG
0.5964
11.4
TRG
0.5800
11.1
TRG
0.5651
Tracer Total
ACT(dpm)
0.6068
Radiometric
Tracer (pCi)
I Radiometric I Grav Carrier I
% Rec
Added (ml)
Grav Filter
Tare (g)
Grav Filter
Final (g)
Grav Filter
Net(g)
Grav
%Rec
SAF
Mean
%Rec
SAF
1.
2.
0.001
11.6
---+---
11.4
---+----- ------
-------
- - --------
11
12
:13-- ~-~~G~f~~~~5!2~1
14
I
I
DO
0.6005
10.8
10.9
1____ 11.5
0.6005
--+
15
TRG
1-----16
TRG
__ _______
-
0.5995
17
0.5497
)OI
TRG
18
19
! TRG
'
0.
---- .
0.6018
I
,---
-------1-
0.~
.6026
11.5
0.00
11.4
)o
0. )0
J__
I____
0.00
_o.oo
---
!
1
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--~
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i
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---1=~
---
-- II
... -~i
I.
--
~>-
J,
I
----+------
Ill.!
tl~
t,,l
*"'Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
13-04106
Printed: 4/30/2013 5:39AM

Page 3 of 3
UUISO
Run 1
Internal
Fraction
Sample
Desc
Rough Prep
Date
Rough Prep
Prep
Date
By
LCS
01
---
-----~-
Prep
Sep to
Date/Time
By
04/25/13 09:03
I
I JBARNARD
04/25/13 09:03
JBARNARD
-~
MBL
02
Sep to
Sep t1
Date/Time
By
DUP
04
TRG
~--
JBARNARD
04/25/13 09:03
JBARNARD
- - - ~I
04/25/13 09:03
JBARNARD
04/25/13 09:03
JBARNARD
04/25/13 09:03
JBARNARD
---~----
05
06
TRG
07
08
l_ TRG
I
09
------
I
I
i
'
~--
04/25/13 09:03
TRG
JBARNARD
---1-
TRG
--~~
04/25/13 09:03
JBARNARD
---
TRG
04/25/13 09:03
--
JBARNARD
.. ______ '"
------
TRG
- - - - - - - ----
12
...
04/25/13 09:03
JBARNARD
04/25/13 09:03
JBARNARD
'
--~
TRG
--
13
TRG
14
DO
04/25/13 09:03
1--- - ----
15
04/25/13 09:03
04/25/13 09:03 I JBARNARD
TRG
17
18
___
__
__
--1
- - - - - - - - -------~---~---- ~~-~- ----------- ------------
-----
04/25/13 09:03
JBARNARD
04/25/13 09:03
- - --------------
19
I
i
- - - - - 1-
TRG
JBARNARD
--------~-
04/25/13 09:03
TRG
I
'
I
I
JBARNARD
-------
'
'
------------
JBARNARD~
04/25/13 09:03
TRG
------------------------
t--~------ -~----~~-:--
-----~~----~~~-~--~-
----..----.. -------1-------~~-
~-------
i JBA~NAI=m
I
I
TRG
--
16
JBARNARD
I
I'
-------------
---~-
11
~-~
-----
. ------------
10
----
----
II
'
---------
---
-~~
TRG
By
'
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04/25/13 09:03
- - - 1---
Sep t1
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03
------------
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0
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U-234
U-234
06
---
07
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0
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Q.
~
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------
i r~G
__ D-83
TC)~
+-
-j
H
___
Error Estimate!
MOA
LCS
LCS
LCS
RPO
Known
%R
Flag
Flag
~ f--6.55E+OO 1- 9.4~~:~11_ - ~~SE-021- ~~OE+0~:~2-
TpCi/1
::::
:::
2.66E-02,
3.98E-02i
+-
6.47E-02j
----~--
+-I
OK
OK
+---+------,-
=:-:::~:1 ~:~:Q~t=~-:- --:--+-
MOA
Flag
NA
::::::~~ ::::~~ -::::;.~~---~--
OK
Blank
Flag
~-
--
OK
OK
--+---
OK
OK
-
OK
-
OK
OK
P:~~- ~ _3.1s~o2(__7.89E:o2~- _1.64E-01I --~ __-_-__-_-+t---_-----+-+-~==+----t---1
j_
U-234
TRG
PZ-102-SS TOT
13
U-234
TRG
PZ-1 02-SS DIS
14
U-234
15
U-234
_T ____
DUP 05 DIS
~-----
__
--f
1.22~~~1L_2:9E-Ol___ ---!------+---+---+
s.70E+oo~E-o11 s.49E..021
1.39E-011
OK
-
:-I :~;::1 :~:4~-=t=t ~=PH=

pCI/1
---1---
PZ-102R-SS TOT
DO
OK
pCI/1
8.42E-011
OK
7 .98E-02
4.85E+OOI
6.83E-011
OK
S.SOE-02
PZ-102R-SS DIS
TRG
5.76E+OOI
pCI/1
5.54E+OOI
pCi/1
7.75E-011
OK
7.26E-02
---
..."'
:;;
c
17
U-234
"'c
18
U-234
19
U-234
PZ-104-SD TOT
TRG
pCi/1
2.26E-011
----TRG
TRG
t--
PZ-104-SS TOT
---TRG
PZ-104-SS DIS
-----------
_7.01 E-011
1.64E+OO
;.-~;;~~~- ;~~SE-01 - -2.78E-01

----
pCi/1
PZ-104-SD DIS
--+
__j
pCi/l _
pCi/l
---+------+------
INV
-
OK
----
--------
pCi/1
U-234
TRG
16
U-234
--
c
c
--i
11
!----12
a,
U11
MBL
Results
Units
LC~-----
l___t-:s_ --
1
+-----
Activity
~:::: ~~-j----- :.: :~:
-~
~1
Client
Identification
OK
09--f--U-234---~ TRG 1-- ____ D-83 -"'=------~-P:"'_~-~32E-O~- 8.24~04~01+-----+-----j----t----+---t-----1
U-234
TRG
OUP 05 TOT
pCI/1
2.92E-011 1.60E-011 8.81 E-02
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U-234
08-___-_-+j----_-u-=-3~--_____
Printed: 5/1/201311:21 AM
Page 1 of 3
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03
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Fraction
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2.16E-011
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7.72E-021
6.50E-02
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04/09/1315:35
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04/09/1315:35~00E+OO
135.371
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04/09113 15:.,;___ ..
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04/09/13 16:16
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04/09/1316:.16
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118.78r
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129.751
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04111/13 11:30
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143.021
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04/11/13 11:38
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4.53
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132.381
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16
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04130/13 14:35
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Time
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jAip~a:-o{
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170 4.66 E+02
13.00 E-03
170.02 2.32 E+OO
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04/3011314:42
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17011.78 E+01
18.7
I
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1.00 E-03
18.5
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18.3
U-234 --- - i-;.RG
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U-234
04/30/13 16:24
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jAipha_018
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18.2
---
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4.33 E+02
0.00 E+OO
16.8
17014.21 E+02
14.00 E-03
17.8
-
17014.57 E+02
15.00 E-03
15.3
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170 5.32 E+OO
4.00 E-03
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04/30/13 16:24
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17.8
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04/30/13 16:24
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U-238
MBL
03
u-238
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04
U-238
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U-238
TRG
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3.21E-02
4.60E-02j__7~~-
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5.23E-01
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2.495-011
1.205-011
5.845-02
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8.775-021
2.665-01
09 I
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D-83 DIS
pCI/1
4.795-02
8.165-02
. 1.385-011
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pCi/1
2.105-01
1.405-01
1.265-01
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pCi/1
1.35E-01
1.13E-01
9.65E-02
pCi/1
4.73E+OO
6.995-01
5.145-02
~-~~--+- -U~-2~38--1----'1------U-238
TRG
PZ-102-SS TOT
PZ-102-SS DIS
---1------ ----
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---
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I-j
--~---
-------------+-----7.945-02
pCifl
3.35E+OOI
S.SSE-01
pCifl
3.17E+OO
4.99~-+- 9.17E-02
-2.32E-011
7.17E-01
1.93E+OO
2.34E-01
----- -- --- --r-:-:::t----~+--~

pc111
3.40E+ool -~.35E-o.11 s.33E-o2
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14
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DO
PZ-102R-SS TOT
15
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16
U-238
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pCI/1
17
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pCi/1
2.28E-01
2.21E-011
I 18
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pCi/1
8.66E-02
6.67E-021
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pCI/1
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Printed: 5/1/2013 11:21 AM

Page 1 of 3
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04/09/13 16:16
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49.571
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04/09/13 00:00
1.00E+OO
66.121
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04/09/13 00:00
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53.891
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U-238
13
U-238
14 I
U-238
04111/13 09:10
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04/11/13 09:10
00
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04/11/1311:30
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129.75
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04/11/1311:38
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04/09/13 15:45
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---
Printed: 5/1/201311:21 AM
Page 2 of 3
Nuclide
Fraction
01
1.00E+OO
132.38
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04/30/13 14:43
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170 5.83 E+OO
1.00 E-03
17.9
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04/30/13 14:43
A_Spec
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17013.84 E+02
1.00 E-03
18.2
04/30/13 14:43
A_Spec
1Aipha_048
04/30/13 16:24
A_Spec
Aipha_018
TRG
04/30113 16:24
A_Spec
Alpha_022~--- 170~~-81 E+~~3.00~-03 ~---f------1
I TRG
04/30/1316:24
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17012.53 E+o2-t.oo E+oo 1

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17012.77 E+02
1701-6.80 E-01
1.30 E-02
14.00 E-03
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04/30113 16:24
19 I
U-238
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04130/13 16:24
17.1
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17014.66 E+OO
12.00 E-03
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17017.32 E+OO
14.00 E-03
17.3
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17011.68 E+01
11.00 E-03
19.5
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17.8
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18
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E+OO
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~::::-~~1:~:-- :;,: : : : : : I --~ :~:::: 1:::;:~::~~ -:-:~,;~:-t~:-1:::::: :~-;-=-=--=
-----
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I
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0~-30113 14:43
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04/30/13 14:4-;--1 - - - - -- ---r-:;=Spec
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Printed: 5/1/2013 11:21 AM

Page 3 of 3
Nuclide
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U-235
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10
U-235
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11
U-235
-------
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iil
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14
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1.75E-02
7.32E...02
1.88E..01
pCi/1
1.04E-011
1.15E-01j
1.56E-011
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Printed: 5/1/201311:21 AM
Page 1 of 3
Work Order: 13-041 06-UUIS0-1
~~t:~
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E-02
9.76E-02
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1.72E-01
1
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-
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2.46E-011 1.32E-011 9.84E-02
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3.30E-D11
1.45E-01I
7.29E..02
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8.56E-01.1
2.02E+OO
5.04E-021
1.21E-01,
2.53E-01
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1.o1e-o2
1.90E-021
3.61E-02I
6.67E-02
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Printed: 5/1/2013 11:21 AM

Page 2 of 3
Sample
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% Rec
Grav
%Rec
Mean
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04/16/13 00:00
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101.22:
1.~~~-~~~----. 125.36:
04/16/13 00:00
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04/1111311:30
---
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10
11
1.00E+OO
U-235
U~235
12
U-235
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U~235
1.00E+OO
118.78
0.00
0.00
-~-+--~--1- --~-~--
U-235
1.00E+OO
129.75
0.00
0.00
15
U-235
1.00E+OOI
143.02
0.00
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04/11/1311:38
U-235
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04/11/1312:59
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04/1111312:59
04/11/1311:38
---
"-----
11.00E+OOi
... --- -----1~~------------ - -- ---- -- ....

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31.07
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129.301
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(days)
DUP
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04/3011314:42
~:: T~ -: -=~::::=f
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Printed: 5/1/201311:21 AM
Page 3 of 3
Count
amer
Time
t~:~-L~- ~:::;__ _;~ __::::::~;;~:::=it-~----=--j-)~;~: -~~~::~~;:1.

08
U-235
TRG
04/3011314:42
U-235
TRG
04/3011314:42
Bkg
ounts
1701:.;[:.::
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170J1.48 E+01
11.00 E-03
18.2
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Alpha_041
170,--~.10-~-~~~~:~~-~~~;+-19.8-~----
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-~;~-:;0 E_;;;=F;-~-~;- ____:;;.---+--~
U-235
TRG
04/30/13 14:43
10
U-235
TRG
04/30/13 14:43
A_Spec
Alpha_044
17014.00 E+OO
0.00 E+OO
19
11
U-235
TRG
04130/13 14:43
A_Spec
Alpha_046
17012.00 E+OO
0.00 E+OO
17.9
12
U-235
TRG
04/30113 14:43
A_Spec
Alpha_047
17012.17 E+01
2.00
18.2
1Aipha_04f
17+-50E+01
O.OOE+OO
A_ Spec
Alpha_018
17012.11 E+01
5.00 E-03
17.8
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17012.91 E+01
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04/30/13 16:24
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Count Room Report

Client: Engineering Management Su
Printed: 4130/2013 5:39AM

Page 1 of1
13-04106-UUISOc1 (pCi/1) in WA
Tracer ID: U-1 Oa
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;,.
Internal
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Sample
Desc
Client
ID
01
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LCS
02
MBL
BLANK
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Date
Sample
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05
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04/09/13 15:45
~RG_l_
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04/09/13 15:45
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04/09/13 16:16
09
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10
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04/11/13 09:10
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Run
.EU .. WP.i .. i
U-234
f---U-238
Activity
dpm!g
Sol#
s Code
UUISO
LCS & Matrix Spikes

Isotope
LCS
Solution
Date
Approx
Addition
Volume
Used(g)
U-Ba
35.2401
4/25/2013
o.5oOI
0.5103
i-
U-Ba
34.3501
4/25/20131
0.5001
0.51031
01
MS
LCSD
Volume
Used(g)
Isotope
I
Activity
dpm/g
Initials
h
LCSD
MSD
Volume
Used(g)
Known
pCi
MSD
Error
Estimate
Sol#
Date
U-232_1 _U-10a
03
U-232
U-10a
19.093! 4/25/2013[
0.6009
04
U-232
U-10a
19.0931 4/25/20131
0.5979
U-10a
05
U-232
06
U-232
Approx
Addition
0.000
0.00
0.000
0.00
0.000
0.00
0.000
0.6300
0.6030
0.6300
-0.6300
-0.6300
-1 3.093[_~!~-~~013
r-- u-1o:;-t-1
0.6300
--
l.093 4/25/2013
0.6300
0.6300
07____l U-232
U-10a
19.093 4/25/2013
1
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U-10a
1
19 093! 4t2512o-;3
U-232
---
19.093 4/25/2013
1
10
U-232
U-10a
19.093 4/25/2013
1
11
U-232
U-10a
1
19.093 4/25/2013
12
U-232
U-10a
119.093 4/25/2013
II
U-232
U-10a
19.093 4/25/2013
0.5723
0.6300
14
U-232
U-10a
19.093 4/25/2013
D.6005
0.6300
15
U-232
U-10a
19.093 4/25/2013
0.6005
0.6300
16
U-232
U-10a
19.093 4/25/2013
0.5995
17
U-232
U-10a
18
U-232
19
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0.6300
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Version 2.0 08/99
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0.6300
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0.6300
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0. 5103 '3
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0.5497
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19.093 4/25/2013
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tfi
02
13
i".l<J
JBARNARD
4/25/2013 9:01
Tracers
fraction
.,.,ti,
Date
Volume
Used(g)
I
-
Page 1 of 1
Printed: 4/25/2013 9:03AM
Spike and Tracer Worksheet
--0" 580r~t 3
-0.5651 '3
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6026 9
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Matrix Spike
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Printed: 412512013 9:03AM

Page 1 of 1
Aliquot Worksheet
JBARNARD
No of Dils
Dil Factor
Comments
e1-~t.
tj)
~
..
Techn1c1an:
Date:~~
Ratio
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
SPIKE
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000567
1304106A-UU
01
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_Ol3
13
System Bkgd 55738
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
1. OOOE+OOO +I- O.OOOE+OOO liter

4/30/2013
7:18:03 AM
4/30/2013
2:35:21 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232_UU-10A
0.607 mL
0.1892 +/- 0.0108
0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM
1.0122 +/- 0.0606
Control Certificate Name: NatU U-SA

Chern. Recov. of Control:
U-238
Peak Match Tolerance:
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.278
4.735
4.395
4.153
Net
Pk Area
370.47
466.49
34.83
504.49
0.870338 +/-
AREA
0.068123
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
10.21
9.08
33.31
8.73
1.53
0.51
0.17
0.51
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
25.8
22.6
6.4
20.0
Tracer Peak used for Effective Efficiency
NUCLIDE ANALYSIS RESULTS

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.996
0.995
0.999
0.993
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.20E+OOO
6.55E+000
6.03E-001
7.05E+000
+I+I+I+I-
5.80E-001
9.42E-001
2.12E-001
9.99E-001
MDA
(pCi/liter
9.98E-002
7.36E-002
7.23E-002
7.33E-002
+I+I+I+I-
1.11E-002
8.22E-003
8.06E-003
8.18E-003
/1(.,
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0000056751.CNF
Live Time :10200.000 sec
Real Time :10200.000 sec
Start:
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Acq. Start :Tue Apr 30 14:35:21 2013
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Channel Data Report
5/1/2013
Page
5:01:32 AM
*******************************************************
*****
S P E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
10200
Channell------l-------1-------l-------l-------l-------l-------l------1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
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161:
169:
177:
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0
1
3
2
1
3
1
2
4
5
7
13
22
2
0
0
0
0
1
2
0
1
1
0
0
0
0
1
0
0
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0
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0
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0
1
0
0
0
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0
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0
2
5
8
10
17
21
3
0
0
0
0
0
0
0
2
2
0
1
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
1
1
1
6
2
2
8
17
14
17
1
0
1
0
0
0
0
0
1
1
0
1
1
1
0
1
1
0
0
0
0
0
0
0
0
0
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1
0
0
1
0
1
1
0
0
2
0
1
2
4
5
5
15
14
15
2
0
0
0
1
0
1
1
3
1
0
0
0
2
0
0
3
fJ 119
Channel Data Report

369:
5/1/2013
1
Sample Title:
Page
5:01:32 AM
1
01
Channell------l-------l-------l-------l-------l-------l-------l-------1
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:
0
0
2
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8
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9
15
6
0
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2
5
5
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18
12
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0
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6
6
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0
0
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0
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0
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0
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0
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3
3
11
10
11
19
1
0
0
0
0
0
0
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0
0
0
0
0
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0
0
3
1
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5
13
10
12
2
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0
0
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0
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0
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0
0
0
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0
0
0
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0
0
0
0
0
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1
4
5
3
6
19
11
17
0
1
0
0
0
0
0
0
1
0
0
0
0
0
1
0
2
1
2
6
4
8
12
15
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
4
0
1
3
8
15
10
7
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
1
5
4
6
13
8
10
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
3
2
7
12
10
11
0
0
0
0
0
0
0
0
0
0
0
0
0
1
2
1
1
2
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7
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6
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0
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0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
:&12
Channel Data Report

801:
5/1/2013
Sample Title:
Page
5:01:32 AM
0
01
Channell------l-------l-------l-------1-------l-------l-------l-------l
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1121
pex-Aipha
BLANK
1304106A-UU
02
Shelf 2
u iso
Detector Name:
Alpha_014
Sample Description:
Spectrum File:
Sample Geometry:

Env. Background:
Reagent Blank:
14
System Bkgd 55739
<not performed>
1. OOOE+OOO +/-
O.OOOE+OOO liter
4/30/2013
7:18:03 AM
4/30/2013
2:35:22 PM
170.0 minutes
Sample Size:
Sample Date/Time:

170.0 minutes
U232 UU-10A
0.603 mL
0.2314 +/- 0.0122
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
1.2536 +/- 0.0699
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.275
4.672
4.461
4.149
Net
Pk Area
450.28
2.32
1.66
2.81
AREA
REPORT
Pk Area
Ambient
Error %
Backgnd
2.72
0.68
0.34
1.19
9.27
149.13
169.38
142.99
FWHM
Reagent
Backgnd
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
20.9
2.9
2.9
2.9

Nuclide
U-232
U-234
U-235
U-238
Id
Conf.
Energy
(keV)
0.995
0.944
5302.50*
4761.50*
4385.50*
4184.40*
0. 960
0.991
Activity
(pCi/liter )
5.17E+OOO
2.66E-002
2.35E-002
3.21E-002
+I+I+I+I-
5.33E-001
3.98E-002
3.99E-002
4.60E-002
AG
.:i/tjt!J
MDA
(pCi/liter
9.84E-002
6.47E-002
6.77E-002
7.53E-002
+I+I+I+I-
1. 01E-002
6.67E-003
6.98E-003
7.76E-003
0000056752.CNF
start:
1:3507. 9(kev)
stop : 1024:6512.2(kev)
Acq. Start :Tue Apr 30 14:35:22 2013
60
55
50
45
40
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35
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<=
8 30
25
20
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II
~.11:
15
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5000
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5500
6000
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6500
Channel Data Report
5/1/2013
Page
5:01:41 AM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
02
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Channel Data Report

369:
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il125
Channel Data Report

801:
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Sample Title:
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5:01:41 AM
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pex-AiphaTM
c_
PZ-102R-SS TOT-DUP
1304106A-UU
03
Shelf 2
u iso
Detector Name:
Env. Background:
Alpha_033
04026479A
91132
System Bkgd 55746
Sample Description:
Spectrum File:
Sample Geometry:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
1.000E+000 +/- O.OOOE+OOO liter

4/11/2013
7:18:03 AM
4/30/2013
2:42:51 PM
170.0 minutes

170.0 minutes
U232 UU-10A
0.601 mL
0.2447 +/- 0.0126
0.1825 +/- 0.0032 on 12/16/2012
1.3409 +/- 0.0728
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
Jl(t/7
5.290
4.745
4.400
4.168
Net
Pk Area
AREA
REPORT
Pk Area
Error %
474.49
429.00
14.83
327.00
5:49:18 PM
9.00
9.47
51.24
10.86
Ambient
Backgnd
0.51
0.00
0.17
0.00
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
39.7
13.4
3.0
8.6

Nuclide
Id
conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.999
0.998
0.998
0.998
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.15E+000
4.66E+000
1.99E-001
3.53E+000
+I+I+I+I-
5.19E-001
6.44E-001
1. 04E- 001
5.23E-001
MDA
(pCi/liter
5.70E-002
6.51E-002
5.59E-002
6.48E-002
+I+I+I+I-
5.74E-003
6.55E-003
5.63E-003
6.52E-003
AC.
5/t/t~
!ll127
0000056759.CNF
Start:
l:l465.6(kev)
stop : 1024:650l.l(kev)
Acq. start :rue Apr 30 14:42:51 2013
60
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5500
6000
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6500
Channel Data Report
5/1/2013
Page
5:01:'$4 .1M
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
03
Elapsed Live time:

Elapsed Real Time:
10200
10200
Channell------l-------l-------l-------1-------l-------l-------l------1:
9:
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25:
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57:
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fl129
Channel Data Report

369:
Page
5/1/2013
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Sample Title:
03
Channell------l-------l-------l-------l-------l-------l-------1------377:
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Channel Data Report

801:
5/1/2013
0
Sample Title:
5:01:~
Page
Mt
0
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833:
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i131
pex-AiphaTM
Spectrum File:
Sample Geometry:
PZ-111-KS TOT
1304106A-UU
04
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_034
04026479B
91136
System Bkgd 55747
Sample Description:
<not performed>
1. OOOE+OOO +/- O.OOOE+OOO liter

4/9/2013
7:18:03 AM
2:42:53 PM
4/30/2013
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
Tracer Quantity:
U232_UU-10A
0.598 mL
0.2326 +/- 0.0122
0.1856 +/- 0.0032 on 12/16/2012
1.2535 +/- 0.0694
0.150 MeV
Tracer Certificate:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.281
4.732
4.390
4.145
)ftto
Net
Pk Area
AREA
REPORT
Pk Area
Error %
448.83
619.83
21.66
272.66
5:49:43 PM
Ambient
Backgnd
9.25
7.87
42.50
11.88
0.17
0.17
0.34
0.34
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
25.1
51.4
4.5
30.1

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.994
1.000
0.989
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.13E+000
7.07E+000
3.05E-001
3.10E+000
+I+I+I+I-
5.28E-001
9.17E-001
1.33E-001
4.87E-001
MDA
(pCi/liter
4.77E-002
4.76E-002
6.73E-002
5.43E-002
+I+I+I+I-
4.91E-003
4.90E-003
6.93E-003
5.59E-003
p..G,
S/1/~
-3132
0000056760.CNF
start:
1:3439.l(kev)
stop : 1024:6479.9(kev)
Acq. Start :Tue Apr 30 14:42:53 2013
60
55
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5000
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6000
5500
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Channel Data Report
Page
5/1/2013
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
04
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Channel Data Report

369:
5/1/2013
0
Sample Title:
Page
5:02:6'2 1M
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04
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Channel Data Report

801:
Page
5/1/2013
0
Sample Title:
04
Channell------l-------l-------l-------l-------l-------l-------1------809:
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841:
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8136
(
Sample Description:
Spectrum File:
Sample Geometry:
PZ-111-KS DIS
1304106A-UU
OS
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_035
04026477A
58771
System Bkgd 55748
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:18:03 AM
4/30/2013
2:42:54 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.600 mL
0.2472 +/- 0.0127
0.1826 +/- 0.0032 on 12/16/2012
1.3537 +/- 0.0732
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.289
4.743
4.414
4.167
T
AREA
REPORT
Pk Area
Error %
Net
Pk Area
478.66
652.66
19.83
260.83
8.96
7.67
44.23
12.14
5:49:42 PM
Ambient
Backgnd
0.34
0.34
0.17
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
31.3
31.1
2.9
11.4
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.999
0.998
0.994
0.998
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.14E+000 +I- 5.16E-001
7.01E+000 +I- 8.86E-001
2.63E-001 +/- 1.19E- 001
2.79E+000 +I- 4.39E-00l
S/r(i!J
MDA
(pCi/liter
5.14E-002
5.14E-002
5.53E-002
4.46E-002
+I+I+I+I-
5.16E-003
5.15E-003
S.SSE-003
4.48E-003
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rue Apr 30 14:42:54 2013
55
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Channel Data Report
5/1/2013
Page
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Channel Data Report

801:
5/1/2013
Sample Title:
5:06:2S
0
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D-6 TOT
\\OR-AIPHA1\Canberra\ApexAlpha\Root\Data\00000567
1304106A-UU
06
Shelf 2
U iso
Detector Name:
Alpha_037
04026478A
91133
System Bkgd 55750
Sample Description:

Env. Background:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:18:03 AM
4/9/2013
4/30/2013
2:42:56 PM
170.0 minutes

170.0 minutes
U232 UU-10A
0.600 mL
0.1559 +/- 0.0097
0.1783 +/- 0.0033 on 1/26/2013
0.8744 +/- 0.0566
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.281
4.736
4.318
4.111
Net
Pk Area
AREA
REPORT
Pk Area
Error %
301.83
12.66
1. 00
6.83
3:28:25 PM
Ambient
Backgnd
11.29
55.94
277.19
76.08
0.17
0.34
0.00
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
53.3
3.7
2.9
2.9
NUCLIDE ANAIYSISRESULTS
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.995
0.968
0.963
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.14E+OOO
2.16E-001
2.10E-002
1.16E-001
+I+I+I+I-
6.25E-001
1. 23E-001
5.83E-002
8.92E-002
MDA
(pCi/liter
7.11E-002
8.14E-002
1.26E-001
7.08E-002
+I+I+I+I-
8.64E-003
9.90E-003
1.53E-002
8.60E-003
A-6
s/t/t3
.fQ142
0000056753.CNF
Live Time 10200.000 sec
Real Time 10200.400 sec
Start:
1 3463.5(kev)
Stop : 1024 6468.5(kev)
Acq. Start rue Apr 30 14:42:56 2013
wl
55
501
45
40
35
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Channel Data Report
5/1/2013
Page
5:06:40 AM
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li-145
Channel Data Report

801:
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Sample Title:
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5:06:46 AM
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1146
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:

Env. Background:
Reagent Blank:
D-6 DIS
1304106A-UU
07
Shelf 2
u iso
Alpha_040
06027396B
91135
System Bkgd 55752
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:18:03 AM
2:42:57 PM
4/30/2013
170.0 minutes
170.0 minutes

U232_UU-10A
0.598 mL
0.1890 +/- 0.0108
0.1900 +/- 0.0033 on 12/16/2012
0.9946 +/- 0.0595
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
Nuclide
U-232
U-234
U-235
U-238
(MeV)
T
5.281
4. 729
4.398
4.142
T
Net
Pk Area
364.83
17.83
-0.17
17.83
AREA
5:49:33 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
0.17
0.17
0.17
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
10.26
46.68
1169.4
46.68
FWHM
(keV)
20.0
3.0
0.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.993
0.999
0.987
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.13E+000
2.50E-001
-2.95E-003
2.49E-001
+I+I+I+I-
5.75E-001
1.20E-001
3.45E-002
1.20E-001
AA
.5/t//'!>
MDA
(pCi/liter
5.87E-002
5.86E-002
7.23E-002
5.84E-002
+I+1+I+!-
6.58E-003
6.57E-003
8.11E-003
6.55E-003
0000056754.CNF
Real Ti~ 10200.300 sec
start:
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stop : 1024 6497 .l(kev)
Acq. start Tue Apr 30 14:42:57 2013
60
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.....
<::
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111
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Channel Data Report
5/1/2013
Page
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*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
*****
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07
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801:
5/1/2013
0
Sample Title:
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Sample Description:
Spectrum File:
Sample Geometry:
D-83 TOT
1304106A-UU
08
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91087
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<not performed>
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4/9/2013
7:18:03 AM
2:42:59 PM
4/30/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.599 mL
0.0968 +/- 0.0074
0.1978 +/- 0.0034 on 12/16/2012
0.4893 +/- 0.0385
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.293
4.717
4.396
4.212
T
Net
Pk Area
187.00
1.15
-0.51
-1.91
AREA
5:49:31 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
14.37
249.59
400.63
167.51
0.00
0.85
0.51
3.91
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
18.1
3.0
0.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.999
0.986
0.999
0.994
5302.50*
4761.50*
4385.50*
4184.40*
Activity
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3.15E-002
-1. 73E-002
-5.22E-002
+!+I+I+I-
7.73E-001
7.89E-002
6.92E-002
8.77E-002
MDA
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1.64E-001
1.78E-001
2.66E-001
+I+I+I+I-
2.48E-002
2.47E-002
2.67E-002
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J\-4
5/1//3
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5/1/20l3
5:G$:U
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Page
*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
08
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Channel Data Report

369:
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-!155
Channel Data Report

801:
5/1/2013
0
Sample Title:
Page
5:06:5$ AM
0
08
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IH56
pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
D-83 DIS
1304106A-UU
09
Shelf 2
u iso
Alpha_042
05026930B
84185
System Bkgd 55754
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:18:03 AM
4/30/2013
2:43:01 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
U232_UU-10A
0.599 mL
0.0915 +/- 0.0072
0.1846 +/- 0.0032 on 12/16/2012
0.4957 +/- 0.0399
0.150 MeV
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.280
4. 719
4.442
4.136
T
Net
Pk Area
176.83
1.49
0.49
1.66
AREA
5:49:29 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
0.17
0.51
0.51
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
14.75
190.02
416.98
169.38
FWHM
(keV)
10.0
3.0
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.996
0.988
0.978
0.983
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.13E+000
4.32E-002
1.75E-002
4.79E-002
+I+I+I+I-
7.92E-001
8.24E-002
7.32E-002
8.16E-002
MDA
(pCi/liter
1.21E-001
l . 52E- 001
1.88E-001
l . 38E-001
+I+I+I+I-
l . 87E-002
2.35E-002
2.90E-002
2 .13E-002
6/1113
!1157
0000056756.CNF
60

Start:
1:3450.2(kev)
Stop : 1024:6505.5(kev)
Acq. Start :Tue Apr 30 14:43:01 2013
55 150
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6500
Channel Data Report
5/1/2013
5:07:~1'
Page
*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
09
Elapsed Live time:

Elapsed Real Time:
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Channel Data Report

369:
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Sample Title:
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I lEI
Channel Data Report

801:
5/1/2013
0
Sample Title:
Page
5:07:0fi 1\:M
0
09
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~1S1
Sample Description:
Spectrum File:
Sample Geometry:
DUP 05 TOT
1304106A-UU
10
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_044
040264818
84168
System Bkgd 55756
<not performed>
Sample Size:
Sample Date/Time:

7:18:03 AM
4/9/2013
4/30/2013
2:43:03 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.596 mL
0.1257 +/- 0.0086
0.1902 +/- 0.0033 on 12/16/2012
0.6612 +/- 0.0467
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.280
4.728
4.383
4.126
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
242.00
13.83
4.00
10.00
5:49:26 PM
12.63
53.08
109.57
65.01
Ambient
Backgnd
0.00
0.17
0.00
0.00
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
29.7
4.5
3.0
3.0

Nuclide
U-232
U-234
U-235
U-238
Id
Conf.
Energy
(keV)
0. 996
5302.50*
4761. 50*
4385.50*
4184.40*
0.992
1.000
0.976
Activity
(pCi/liter )
5.11E+000
2.92E-001
1.04E-001
2.10E-001
+/+/+/+/-
6.86E-001
1.60E-001
1.15E-001
1.40E-001
MDA
(pCi/liter
1.27E-001
8.81E-002
1.56E-001
1.26E-001
+/+/+/+/-
1.70E-002
1.18E-002
2.09E-002
1.69E-002
0000056757.CNF
Start:
1:3447. 9(kev)
stop : 1024:6485.9(kev)
Acq. Start :rue Apr 30 14:43:03 2013
6055
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6000
5500
ROI Type: 3
1!
Channel Data Report
5/1/2013
Page
5:07:13 AM
*******************************************************
*****
E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
10
Elapsed Live time:

Elapsed Real Time:
10200
10200
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ill164
Channel Data Report

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1155
Channel Data Report

801:
Page
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0
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u iso
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Env. Background:
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58762
System Bkgd 55757
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Spectrum File:
Sample Geometry:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:18:03 AM
4/30/2013
2:43:05 PM
170.0 minutes
170.0 minutes
U232 UU-10A
0.580 mL
0.1143 +/- 0.0083
0.1789 +/- 0.0031 on 12/16/2012
0.6389 +1- 0.0475
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
)/flO
5.266
4.692
4.383
4.133
Net
Pk Area
214.00
6.00
2.00
5.83
AREA
5:49:23 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
13.43
86.43
169.74
82.55
0.00
0.00
0.00
0.17
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
12.7
3.0
3.0
6.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0. 991
0.966
1.000
0.981
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
4.97E+000
1. 39E-001
5.73E-002
1. 35E-001
+I+I+I+I-
7.04E-001
1.22E-001
9.76E-002
1.13E-001
MDA
(pCi/liter
1. 39E-001
1. 39E-001
1. 72E-001
9.65E-002
+I+I+I+I-
1.97E-002
1.97E-002
2.43E-002
1. 37E-002
A4
S/t/13
tg167
0000056758.CNF
start:
1:3453./(kevl
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Acq. Start :Tue Apr 30 14:43:05 2013
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5500
6000
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6500
Channel Data Report
5/1/2013
5:0'?:!!
Mt
Page
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S P E C T R A L
DATA
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*****
*****
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Channel Data Report

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~178
Channel Data Report

801:
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Sample Title:
Page
5:07:22 AM
0
11
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Sample Geometry:
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12
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02030596A
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Sample Size:
Sample Date/Time:

4/11/2013
7:18:03 AM
4/30/2013
2:43:07 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.565 mL
0.2147 +/- 0. 0119
0.1822 +/- 0.0032 on 12/16/2012
1.1784 +/- 0.0687
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.274
4.726
4.415
4.142
T
Net
Pk Area
AREA
5:49:21 PM
REPORT
Pk Area
Error %
391.49
460.49
21.66
383.83
~Ito
Ambient
Backgnd
9.91
9.14
42.50
10.01
0.51
0.51
0.34
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
21.6
20.6
2.9
22.6

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.994
0.991
0.994
0.987
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
4.84E+OOO
5.70E+OOO
3.30E-001
4.73E+OOO
+I+I+I+I-
5.28E-001
8.10E-001
1. 45E-001
6.99E-001
MDA
(pCi/liter
6.49E-002
6.49E-002
7.29E-002
5.14E-002
+I+I+I+I-
7.07E-003
7.07E-003
7.94E-003
5.60E-003
~
.5/t/t)
~172
0000056762.CNF
start:
1:3457. 9(kev)
Stop : 1024:6467.7(kev)
Acq. Start :Tue Apr 30 14:43:07 2013
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Channel Data Report
5/1/2013
5:07:~!
Page
AM
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*****
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DATA
R E p 0 R T
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Channel Data Report

369:
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2
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l!l175
Channel Data Report

801:
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0
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8176
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-102-SS DIS
1304106A-UU
13
Shelf 2
U iso
Alpha_048
02030596B
83111
System Bkgd 55759
<not performed>

4/11/2013
7:18:03 AM
2:43:08 PM
4/30/2013
170.0 minutes
1. 7 o. 0 minutes
Sample Size:
Sample Date/Time:
U232_UU-10A
0.572 mL
0.1995 +/- 0.0114
0.1680 +/- 0.0030 on 12/16/2012
1.1878 +/- 0.0709
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.262
4.719
4.379
4.136
Net
Pk Area
AREA
REPORT
Pk Area
Error %
368.49
433.00
15.00
253.00
5:49:20 PM
10.22
9.43
52.27
12.35
Ambient
Backgnd
0.51
0.00
0.00
0.00
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
7.2
28.5
3.0
16.4
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.988
0.987
1. 000
0.983
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
4.91E+000
5.76E+000
2.46E-001
3.35E+000
+I+I+I+I-
5.48E-001
8.42E-001
1.32E-001
5.58E-001
MDA
(pCi/liter
6.99E-002
7.98E-002
9.84E-002
7.94E-002
+I+I+I+I-
7.80E-003
8.91E-003
1.10E-002
8.87E-003
JtG
5/ 1( C>
:m177
0000056763.CNF
start:
1:34Sl.O(kev)
stop : 1024:6472.1(kev)
Acq. Start :Tue Apr 30 14:43:08 2013
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Channel Data Report
5/1/2013
Page
5:07:41 AM
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*****
E C T R A L
DATA
R E P 0 R T
*****
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Sample Title:
13
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Channel Data Report

369:
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Channel Data Report

801:
5/1/2013
Sample Title:
5:07:4~
Page
AM
0
13
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1181
Sample Description:
Spectrum File:
Sample Geometry:
PZ-102R-SS TOT
1304106A-UU
14
Shelf 2
U iso
Detector Name:
Envo Background:
Reagent Blank:
Alpha_018
18
System Bkgd 55740
<not performed>
Sample Size:
Sample Date/Time:
1o000E+000 +/- OoOOOE+OOO liter

4/11/2013
7:18:03 AM
4:24:43 PM
4/30/2013
170o0 minutes
170o0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
Oo600 mL
Oo2305 +/Oo0121
Oo1776 +/- Oo0033 on 12/15/2012
1.2975 +/- 0 00725
Oo150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
50282
4o733
4o407
4o158
Net
Pk Area
AREA
REPORT
Pk Area
Error %
446o64
421.32
21.15
276o79
1:57:26 PM
9o29
9o56
43o61
11.84
Ambient
Backgnd
1.36
Oo68
Oo85
2o21
FWHM
(keV)
Reagent
Backgnd
OoOOE+OOO
OoOOE+OOO
OoOOE+OOO
OoOOE+OOO
21.1
26o3
3o1
6o9

Nuclide
Id
Confo
Energy
(keV)
U-232
U-234
U-235
U-238
Oo997
00994
Oo997
Oo995
5302o50*
4761o50*
4385o50*
4184o40*
Activity
(pCi/liter )
5o15E+OOO
4085E+000
3o01E-001
3o17E+OOO
+I+I+I+I-
5o32E-001
6o83E-001
1.35E-001
4o99E-001
MDA
(pCi/liter
7o90E-002
6o50E-002
8o51E-002
9o17E-002
+I+I+I+I-
8o16E-003
6 o71E- 003
8o79E-003
9o47E-003
1\{1
.S/t /13
N182
0000056764.CNF
Start:
1:3404.1(kev)
Stop : 1024:6604.2(kev)
Acq. Start :Tue Apr 30 16:24:43 2013
60
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5000
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5500
6000
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6500
Channel Data Report
5/1/2013
Page
5:07:49 AM
*******************************************************
*****
T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
14
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Elapsed Real Time:
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~184
Channel Data Report

369:
5/1/2013
2
Sample Title:
5:07-:,UI
0
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1
Page
1
14
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fi1S5
Channel Data Report

801:
5/1/2013
0
Sample Title:
5:07:4~
Page
M-t
0
14
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ill18E
pex-AiphaTM
PZ-102R-SS DIS
1304106A-UU
15
Shelf 2
u iso
Detector Name:
Alpha_022
Sample Description:
Spectrum File:
Sample Geometry:

Env. Background:
22
System Bkgd 55741
Reagent Blank:
<not performed>

4/11/2013
7:18:03 AM
4/30/2013
4:24:44 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.600 mL
0.2190 +/- 0.0118
0.1531 +/- 0.0029 on 12/15/2012
1.4302 +/- 0.0816
0.150 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.275
4.727
4.400
4.146
Net
Pk Area
AREA
REPORT
Pk Area
Error %
424.47
457.15
29.15
281.49
1:57:26 PM
9.53
9.18
36.92
11.69
FWHM
(keV)
Ambient
Reagent
Backgnd
Backgnd
1.53
0.85
0.85
0.51
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
20.5
4.9
4.7
24.9

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.992
0.999
0.990
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.15E+000
5.54E+OOO
4.36E-001
3.40E+000
+I+I+I+I-
5.43E-001
7.75E-001
1. 67E-001
5.35E-001
MDA
(pCi/liter
8.62E-002
7.26E-002
8.95E-002
6.33E-002
+I+I+I+I-
9.09E-003
7.65E-003
9.44E-003
6.68E-003
AG
s/r/o
-til187
0000056765.CNF
Live Time
Real Time
start:
I
Stop : 1024
Acq. start
60
10200.000 sec
10200.000 sec
J42!.5(kev)
6608.8(kev)
rue Apr 30 16:24:44 2013
55
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5500
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6500
Channel Data Report
5/1/2013
Page
5:07:59 AM
*******************************************************
S P E C T R A L
R E P 0 R T
DATA
*****
*****
*******************************************************
Sample Title:
15
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
9:
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41:
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1
lii18S
Channel Data Report

369:
5/1/2013
0
Sample Title:
Page
5:07:59 AM
0
15
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0
-mtsm
Channel Data Report

801:
Page
5/l/2013
Sample Title:
15
Channell------l-------l-------l-------l-------l-------l-------1------809:
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945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
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E191
pex-AiphaTM
Sample Description:
Spectrum File:
PZ-104-SD DIS
1304106A-UU
17
Shelf 2
u iso
Detector Name:
Alpha_025
Sample Geometry:

Env. Background:
25
System Bkgd 55743
Reagent Blank:
<not performed>
1. OOOE+OOO +/-
Sample Size:
O.OOOE+OOO liter
4/11/2013
7:18:03 AM
4:24:46 PM
4/30/2013
170.0 minutes
Sample Date/Time:
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.550 mL
0.0539 +/- 0.0057
0.1736 +/- 0.0032 on 12/15/2012
0.3107 +/- 0.0331
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
Net
Pk Area
5.282
4. 728
4.303
4.159
T
AREA
REPORT
Pk Area
Error %
95.66
5.32
0.83
4.66
1:57:27 PM
20.08
91.11
239.53
94.59
Ambient
Backgnd
0.34
0.68
0.17
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.5
3.1
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.992
0.953
0.995
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
4.71E+000
2.62E-001
5.04E-002
2.28E-001
+/+/+/+/-
9.70E-001
2.45E-001
1.21E-001
2.21E-001
MDA
(pCi/liter
2.36E-001
2.78E-001
2.53E-001
2.34E-001
+/+/+/+/-
4.85E-002
5.72E-002
5.22E-002
4.82E-002
5 Ut11
0000056767.CNF
60
55
50

Real rime :10200.000 sec
start:
l:l405.9(kev)
stop : 1024:6615.8(kev)
Acq. Start :rue Apr 30 16:24:46 2013
4540
35
.....,
V>
<::
:::>
8 30
25
201510-
5=
~
~
~
~
'
'
ii>j
3500
4000
4500
t!~
,_.
tJ~
t~~l
ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
6500
Channel Data Report
5/1/2013
Page
5:08:2'5 AM
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
17
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
9:
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10200
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G19A
Channel Data Report

369:
5/1/2013
0
Sample Title:
Page
5:08:!$ 1M
0
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~195
Channel Data Report

801:
5/1/2013
Sample Title:
5:08:25
Page
17
Channell------l-------l-------1-------l-------l-------l-------l------809:
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953:
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969:
977:
985:
993:
1001:
1009:
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B19S
ex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
PZ-104-SS TOT
1304106A-UU
18
Shelf 2
u iso
Alpha_027
27
System Bkgd 55744
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:18:03 AM
4/11/2013
4:24:47 PM
4/30/2013
170.0 minutes
170.0 minutes

U232_UU-10A
0.602 mL
0.2234 +/- 0.0119
0.1728 +/- 0.0032 on 12/15/2012
1.2930 +/- 0.0731
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.269
4.733
4.383
4.101
T
Net
Pk Area
433.81
18.15
0.66
7.32
AREA
2:27:41 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
1.19
0.85
0.34
0.68
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
9.43
47.25
305.43
76.28
FWHM
(keV)
33.3
6.4
3.2
4.8

Nuclide
Id
Con.
Energy
(keV)
U-232
U-234
U-235
U-238
0.992
0.994
1.000
0.952
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.16E+000
2.16E-001
9.68E-003
8.66E-002
+I+I+I+I-
5.39E-001
1.04E-001
2.96E-002
6.67E-002
-~
s/r/1})
MDA
(pCi/liter
7.83E-002
7.12E-002
7.01E-002
6.68E-002
+I+I+I+I-
8.19E-003
7.44E-003
7.33E-003
6.98E-003
0000056768.CNF
60
55-

start:
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Acq. start rue Apr 30 16:24:47 2013
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Channel Data Report
5/1/2013
Page
5:41:24 AM
*******************************************************
S P E C T R A L
DATA
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*****
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1211
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5/1/2013
Sample Title:
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1211
ex-AiphaTM
Sample Geometry:
PZ-104-SS DIS
1304106A-UU
19
Shelf 2
U iso
Detector Name:
Alpha_029
Sample Description:
Spectrum File:

Env. Background:
Reagent Blank:
29
System Bkgd 55745
<not performed>
O.OOOE+OOO liter
l . OOOE+OOO +/4/11/2013
7:18:03 AM
4:24:48 PM
4/30/2013
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
U232 UU-10A
0.603 mL
0.2575 +/- 0.0130
0.1945 +/- 0.0036 on 12/15/2012
1.3238 +/- 0.0709
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.284
4.731
4.430
4.151
T
AREA
REPORT
Pk Area
Net
Pk Area
Error %
500.81
12.98
1.49
16.83
2:30:02 PM
Ambient
Backgnd
1.19
l . 02
0.51
0.17
8.77
56.85
190.02
48.06
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.2
3.1
3.1
3.1

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.993
0.986
0.992
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.17E+OOO
1.34E-001
1.90E-002
l . 73E-001
+I+I+I+I-
5.09E-001
7.72E-002
3.61E-002
8.48E-002
P-.4
s/r/1)
MDA
(pCi/liter
6.80E-002
6.50E-002
6.67E-002
4.28E-002
+I+I+I+I-
6.70E-003
6.41E-003
6.58E-003
4.23E-003
0000056769.CNF
start:
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stop: 1024 6597.5(kev)
Acq. Start Tue Apr 30 16:24:48 2013
60
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Channel Data Report
5/1/2013
Page
5:08:39 AM
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DATA
R E P 0 R T
*****
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19
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0
0
0
0
0
0
0
0
0
0
8215
Channel Data Report

801:
Page
5/1/2013
Sample Title:
19
Channell------l-------l-------1-------l-------l-------l-------l------- I
809:
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0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
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Page 1 of 2
4/30/2013 5:44:34 AM
ha
QA SUMMARY REPORT
Review Of QA Results - Pulser Check
Date
Time
: 4/30/2013
: 5:44:34 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
A}Jlha 028
Al~ha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
A}Jlha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
21f
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AlM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst!OODC
Alpha Analyst I OODC
Alpha Analyst!OODC
Alpha Anal)'StiOODC
AljJha Analvst!OODC
Alpha Analyst!OODC
Alpha Analyst!OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
DATE
4/30/2013 5:21:25 AM
4/30/2013 5:21:26 AM
4/30/2013 5:21:27 AM
4/30/2013 5:21:28 AM
4/30/2013 5:21:29 AM
4/30/2013 5:21:30 AM
4/30/2013 5:21:30 AM
4/30/2013 5:21:31 AM
4/30/2013 5:21:32 AM
4/30/2013 5:21:33 AM
4/30/2013 5:21:34AM
4/30/2013 5:21:35 AM
4/30/2013
4/30/2013
4/30/2013
4/29/2013
4/30/2013
5:21:36 AM
5:21:38 AM
5:21:39 AM
5:29:59 AM
5:21:40 AM
4/29/2013
4/30/2013
4/30/2013
4/30/20!3
5:30:03 AM
5:21:42 AM
5:21:43 AM
5:21:45 AM
Page 2 of 2
Review of QA Results - Pulser Check

4/30/2013 5-44-34 AM
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Aloha 048
DEVICE
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Ana_IystlOODC
Al!>ha Ana_IystlOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
APPROVED BY:
APPROVAL DATE:
FLAG
Passed
Passed
Not Done
Passed
Passed
Passed
DATE
4/29/2013 5:30:09 AM
4/30/2013 5:21:47 AM
4/30/2013 5:21 :48 AM
4/30/2013 5:21:50 AM
4/30/2013 5:21:52 AM
Library Listing Report
6/12/12
Page
12:17:04 PM
*************************************************************************
*****
L I B R A R Y
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:
Uranium
Nuclide Library Description:

Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1.410E+017
* = key
TOTALS:
Energy
(keV )
U-232,-234,-235,-238
Energy
Uncert. (kev
5302.500*
4761.500*
4385.500*
4184.400*
0.000
0.000
0.000
0.000
line
4
Nuclides
Energy Lines
Yield
(%)
99.8000
99.8000
80.9000
100.2300
Yield
Uncert. (Abs. +-)
0. 0000
0.0000
0. 0000
0.0000
RUN2
Eberline Services
Analysis Sheet
UUISO
Run 2
Work Order
Internal
Analysis Code
01
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Lab
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Printed: 5/6/2013 5:36AM

Page 1 of3
13-04106
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Printed: 5/6/2013 5:36AM

Page 2 of3
13-04106
UUISO
Run 2
Tracer
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Tracer Total
ACT(dpm)
0.6107
11.7
Radiometric Grav Carrier

% Rec
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0.6022
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13-04106
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Date
Sample
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Rough Prep
By
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Date
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Date/Time
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Page 3 of 3
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Page 2 of 3
Sample
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Printed: 5/6/2013 1:15PM

Page 3 of 3
Nuclide
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01
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U-235
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Identification
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BLANK
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1.77E-01
pCi/1
3.35E-02
1.40E-02
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03
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Printed: 5/6/20131:15 PM
Page 3 of 3
02
0:
DUP
05/06/13 09:42
Detect
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U-Ba
35.240
5/2/2013
U-Sa
34.350
5/2/2013
fraction
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Date
Technician
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5/2/2013 9:51
JBARNARD
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. o.5147.
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Volume
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01
U-232
U-10a
19.090
5/2/2013
0.6107
0.6300
02
U-232
U-10a
19.090
5/2/2013
0.6074
0.6300
03
U-232
U-10a
19.090
5/2/2013
0.6022
0.6300
16
U-232
U-10a
19.090
5/212013
0.6037
0.6300
0.000
0.00
0.000
0.00
7.96(
0.287
0.00
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0.00
0.000
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Known
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0.294

Solution
Date
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8171
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Volume
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0.5147
0.500 1 <
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Page 1 of 1
Printed: 5/2/2013 9:52AM
Eberline Analytical
Work Ord
13-o41os
Lab
Fraction
01
02
03
16
R
1
Analysis Code
Rpt Units
Lab Deadline
Technician
UUISO
liters
5/7/2013
JBARNARD
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Sample
Client ID
Type
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Printed: 5/2/2013 9:52 AM

Page 1 of 1
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Technician:
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Date:
J]
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Water Added
H3 mst
(ml)
Aliq
Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1304106B-UU
01
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_041
05026930A
91087
System Bkgd 56377
<not performed>
Sample Size:
Sample Date/Time:

5/6/2013
7:38:46 AM
9:42:03 AM
5/6/2013
170.0 minutes
172.7 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.611 mL
0.2074 +/- 0.0113
0.1978 +/- 0.0034 on 12/16/2012
1.0482 +/- 0.0600
Control Certificate Name: NatU_U-8A

U-238
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.281
4.733
4.395
4.153
T
Net
Pk Area
0.904886 +/-
AREA
0.067800
REPORT
Pk Area
Error %
408.66
562.81
29.66
579.94
5:49:31 PM
Ambient
Backgnd
0.34
1.19
0.34
3.06
9.70
8.27
36.23
8.16
FWHM
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O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
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17.3
7.8
3.0
24.6

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.994
0.999
0.993
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.23E+000
7.21E+OOO
4.68E-001
7.39E+000
+/+/+/+/-
5.60E-001
9.74E-001
1.77E-001
9.95E-001
MDA
(pCi/liter
6.12E-002
8.43E-002
7.55E-002
1.14E-001
+/+/+/+/-
6.55E-003
9.02E-003
8.08E-003
1.22E-002
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5/6/2013
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Page
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*******************************************************
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369:
5/6/2013
1
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12:43:56 l!'M
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01
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0
0
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t:l229
Channel Data Report

801:
5/6/2013
0
Sample Title:
Page
12:43:56 PM
0
01
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ex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1304106B-UU
02
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_042
05026930B
84185
System Bkgd 56378
<not performed>
Sample Size:
Sample Date/Time:
l . OOOE+OOO +/-
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.607 mL
0.1948 +/- 0.0109
0.1846 +/- 0.0032 on 12/16/2012
1.0553 +/- 0.0620
0.150 MeV
O.OOOE+OOO liter
5/6/2013
7:38:46 AM
5/6/2013
9:42:05 AM
170.0 minutes
1.72.7 minutes
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.278
4.697
4.457
4.086
AREA
REPORT
Pk Area
Error %
Net
Pk Area
381.83
2.49
0.83
2.66
5:49:29 PM
10.03
138.29
239.53
128.85
Ambient
Backgnd
0.17
0.51
0.17
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
4.4
3.0
3.0
3.0

Id
Nuclide
Conf.
U-232
U-234
U-235
U-238
0. 996
0.970
0. 965
0.934
Energy
(keV)
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.20E+OOO
3.39E-002
1.40E-002
3.61E-002
+/+/+/+/-
5.72E-001
4.71E-002
3.35E-002
4.67E-002
MDA
(pCi/liter
5.69E-002
7.15E-002
7.02E-002
6.49E-002
+/+/+/+/-
6.26E-003
7.87E-003
7.72E-003
7.14E-003
~231
0000057212.CNF
Start:
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stop : 1024:6505.5(kev)
Acq. Start :Mon May 06 09:42:05 2013
60
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c:
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8 30
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!,;j
ROI Type: 1
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5000
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Channel Data Report
5/6/2013
12:44:05 PM
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*******************************************************
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p E
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*****
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1ll234
Channel Data Report

801:
5/6/2013
0
Sample Title:
12:44:05
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PM
1
Page
0
02
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!i!235
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-104-SD TOT-DUP
1304106B-UU
03
Shelf 2
U iso
Detector Name:
Env. Background:
Alpha_047
02030596A
91086
System Bkgd 56381
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
2.500E-001 +/- O.OOOE+OOO liter

4/11/2013
7:38:46 AM
5/6/2013
9:42:00 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.602 mL
0.0771 +/- 0.0065
0.1822 +/- 0.0032 on 12/16/2012
0.4233 +/- 0.0367
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.277
4.704
4.377
4.089
Net
Pk Area
149.83
4.00
1.49
1. 83
AREA
5:49:21 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
16.02
109.57
190.02
152.56
0.17
0.00
0.51
0.17
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
11.3
2.9
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.977
1. 000
0.937
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.07E+001
5.51E-001
2.53E-001
2.51E-001
+I+I+I+I-
3.44E+000
6.11E-001
4.83E-001
3.85E-001
MDA
(pCi/liter
5.75E-001
8.26E-001
8.92E-001
5. 72E-001
+I+I+I+I-
9.57E-002
1. 37E-001
1. 48E- 001
9.53E-002
AG
5/(11(0
-iil2 36
0000057209.CNF

start:
l:l457.9(kev)
Stop : 1024:6467. 7(kev)
60
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Acq. Start :Mon May 06 09:42:00 2013
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Channel Data Report
5/6/2013
12:44:14 PM
Page
*******************************************************
*****
p E
T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
03
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5238
Channel Data Report

369:
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~239
Channel Data Report

801:
5/6/2013
0
Sample Title:
12:44:14
0
PM
0
Page
0
03
Channelj------l-------l-------l-------l-------l-------l-------l-------1
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-104-SD TOT
1304106B-UU
16
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_048
02030596B
83111
System Bkgd 56382
<not performed>

2.500E-001 +/- O.OOOE+OOO liter

7:38:46 AM
4/11/2013
5/6/2013
9:42:02 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.604 mL
0.0860 +/- 0.0069
0.1680 +/- 0.0030 on 12/16/2012
0.5119 +/- 0.0423
0.150 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.283
4.778
4.407
4.152
Net
Pk Area
167.49
1.49
3.00
1.66
AREA
5:49:20 PM
REPORT
Pk Area
Ambient
Backgnd
Error %
15.17
190.02
130.67
169.38
0.51
0.51
0.00
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
24.8
3. 0
3.0
3.0

Nuclide
Id
Con.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.998
0.997
0.993
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.07E+001
1. 84E- 001
, 4.57E-001
2.04E-001
+I+I+I+I-
3.28E+000
3.51E-001
6.02E-001
3.47E-001
AG
S/&(tJ
MDA
(pCi/liter
6.49E-001 +I6.48E-001 +I9.14E-001 +I5.88E-001 +/-
1.03E-001
1.03E-001
1.45E-001
9.31E-002
0000057210.CNF

start:
1:345l.O(kev)
Stop : 1024:6472.1(kev)
Acq. Start :Mon May 06 09:42:02 2013
60 155-
50 145
40!
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1
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6000
5500
ROI Type: 3
_l___l_
Channel Data Report
5/6/2013
Page
12:44:23 PM
*******************************************************
*****
S P E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
16
Elapsed Live time:

Elapsed Real Time:
10200
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&2A4
Channel Data Report

801:
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0
Sample Title:
Page
12:44:23 PM
0
16
809:
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953:
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969:
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Page 1 of 2
5/6/2013
5:36:52 AM
ha
QA SUMMARY REPORT
Date
Time
: 5/6/2013
: 5:36:52 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 01 I
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2If
2If
2lf
2If
2If
2lf
2lf
2If
2lf
2lf
2If
2If
2If
2If
2lf
2If
A1M730
AIM730
AIM730
AIM730
AIM730
A1M730
A1M730
A1M730
AIM730
A1M730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst!OODC
Alpha Analyst! OODC
Alpha Analyst!OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Not Done
Passed
Not Done
Not Done
Passed
Passed
Passed
DATE
5/6/2013 5:21 :40 AM

5/6/20 I 3 5:21 :40 AM
5/6/2013 5:21:41 AM
5/6/2013 5:2 1:42 AM
5/6/2013 5:21:43 AM
51612013 5:2 I :44 AM
5/6/2013 5:21:45 AM
5/6/2013 5:21:45 AM
5/6/2013 5:21:46 AM
5/6/2013 5:21:47 AM
51612013 5:21 :48 AM
5/6/2013 5:21:49 AM
5/6/2013 5:2 I :50 AM

5/6/2013 5:21:51 AM
5/6/2013 5:21 :53 AM
5/6/2013 5:21:54 AM
5/6/2013 5:21:56 AM
5/6/2013 5:21:58 AM
5/6/2013 5:21:59 AM
Page 2 of 2
Review of QA Results - Pulser Check

5/6/2013
CHAMBER
Alj)ha
Alpha
Alpha
Alpha
Alpha
Alpha
043
044
045
046
047
048
DEVICE
Alpha Analvst!OODC
Alpha Analyst!OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
APPROVED BY:
APPROVAL DATE:
FLAG
Not Done
Passed
Not Done
Passed
Passed
Passed
5:36:52 AM
DATE
5/6/2013 5:22:01 AM
5/6/2013 5:22:02 AM
5/6/2013 5:22:04 AM
5/6/2013 5:22:06 AM
6/12/12
Page
12:17:04 PM
*************************************************************************
LIBRARY
*****
LISTING
REPORT
*****
*************************************************************************
Uranium
Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1.410E+017
U-232,-234,-235,-238
Energy
(keV )
Energy
Uncert. (keV
5302.500*
4761.500*
4385.500*
4184.400*
0.000
0.000
0.000
0.000
key line
TOTALS:
Nuclides
Energy Lines
Yield
( %)
99.8000
99.8000
80.9000
100.2300
Yield
Uncert. (Abs.+-)
0.0000
0.0000
0.0000
0.0000
SECTION IX
ANALYTICAL DATA (ISOTOPIC THORIUM)
Eberline Services
Analysis Sheet
13-04106
Printed: 5/1/2013 6:05AM

Page 1 of3
ThiSO
Run 1
Work Order
I Sample
Client
Login
Desc
ID
CPM
Analysis Code
LCS
LCS
Sample
Date
I
Run
02
MBL
BLANK
Date Received
03
DUP
PZ-111-KS TOT
1.0000E+OO
04/16/13 00:00
1.0000E+OO
i
04/09/13
15:35
____
____)_
1.0000E+OO
43
04/09/13 15:35
1.0000E+OO
43
04/09/13 15:35
1.0000E+OO
1---.,
----------
'
Lab Deadline
5/7/2013
04
05
DO
---
Client
PZ-111-KS TOT
TRG
PZ-111-KS DIS
--
Project
West Lake OU-1
06
, TRG
'
---
Activity Units
pCi
WA
Matrix
Method
Instrument Type
Alpha Spectroscopy
09
-
--
----
45
~----
04/09/13 15:45
45
--
D-83 TOT
~-
TRG
10
1.0000E+OO
---
---
-fs-frRGt-08
TRG
Aliquot Units
D-6 DIS
i
I
'
D-83 DIS
TRG
1
1~RG .
04/09/13 15:45
----
40
40
1.0000E+OO
f----------
04/09/1316:16
1.0000E+OO
04/09/13 16:16
1.0000E+OO
DUP o5 TOT
47
o4/09/13 oo:oo
1.ooooE+oo
DUP 05 DIS
47
04/09/13 00:00
1.0000E+OO
12
TRG
PZ-102-SS TOT
39
, 04/11/13 09:10
1.0000E+OO
14
TRG
PZ-102R-SS TOT
45
' 04/11/1311:30
1.0000E+OO
45-t;/1111311,30
1.0000E<OO
Th-229
Radiometric Tracer
---
Radiometric Sol#
---
Th-18a
--
Tracer Act (dpm/g)
22.467
-----
--
Carrier
15 _
i TR~
161

-------
D-6 TOT
Report Level
-----
Sample
Aliquot
II 04/16/13 00:00
--
-----------
TR~
PZ-~02R-SS_~~-1
PZ-104-SDTOT
~- 18 -1 TR~L--~~104-SS TOT
17
19 _
; TRG '
--
TRG
PZ-104-SD DIS
PZ-104-SS DIS
_j
-- .
::::
-~:
44
_I
04/11/1311:38
~:"''"*-t
1
1.0000E+OO
1.0000EOO
! -- 42- - i 0411_111312:59 ,
1.0000E+OO
1.0000E<OO
-42
] 04111113 12'59
1 - Ia
t~
q~
!l'll
Eberline Services
Analysis Sheet
Printed: 5/1/2013 6:05AM

Page 2 of3
13-04106
ThiSO
Run 1
Internal
Fraction
Sample
Desc
LCS
Tracer
Aliquot (g)
0.4745
Tracer Total
ACT(dpm)
Radiometric
Tracer (pCi)
I Radiometric [ Grav Carrier I

% Rec
10.7
5.3 I
0.2367
Added {ml)
Grav Filter
Tare (g)
Grav Filter
Final (g)
Grav Filter
Net (g)
Grav
%Rec
Mean
%Rec
SAF
SAF
1"
2"
0.00
I
0.00,
0.2361
0.2344
0.2321
--
0.2341
I
0.2327 '
0.2336
-
0.2321
--+---+---+--+---
0.232;;-1
0.2319
----'
TRG
o.2329
5.2
~~
M
(JI
,_,
'*"*Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Internal
Fraction
Printed: 5/1/2013 6:05AM

Page 3 of3
Rough Prep
Date
Sample
Desc
Rough Prep
Prep
Date
By
Sep tO
Date/Time
Sep tO
Sep t1
Date/Time
By
Sep t1
By
----------~---------
11
TRG
TRG
~~1--------t------i~~~~~~~~~A~R~D~I
----~-
12
I--
13
TRG
14
TRG
15
I TRG
~-i
17
;--
19
1-----
I TRG
I TRG
..
__
JBARNARD
04/25/13 08:59
'
~4/25/13 08:59 , JBARNA~----
04/25/13 08:59
---~~
i
--------r
JBARNA~1
-~-
+-----j
.l
--11
--
t--_. --
I
--
t~
1\:1
(Jil
"* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
t -
04/25/13 08:59
-----t-;4/25/13 08:5g . JBARNARD
04/25/13 08:59
+-__
TRG
TRG
-
18
~ARD
---1-
..., Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
~
&
.g
0
u
-~
0
~
~
<o:
~'
~
~
~
"'.s
Lab
Fraction
Identification
Activity
Units
Results
Error Estimate
MDA
LCS
Known
LCS
LCS
%R
Flag
121.36
OK
RPD
Flag
MDA
Flag
pCi/1
5.84E+OO
8.85E-01
1.17E-01
TH-228
MBL
BLANK
pCI/1
1.02E-02
5.54E-02
1.21E-01
03
TH-228
DUP
PZ-111-KS TOT
pCI/1
1.57E-01
9.80E-02
1.11E-01
04
TH-228
DO
PZ-111-KS TOT
pCI/1
1.11E-01
7.86E-02
8.69E-02
OK
05
TH-228
TRG
PZ-111-KS DIS
pCI/1
-8.59E-03
5.61E-02
1.42E-01
OK
06
TH-228
TRG
D-6 TOT
pCI/1
1.38E-01
1.DOE-01
1.25E-01
OK
07
TH-228
TRG
D-6 DIS
pCI/1
2.14E-02
4.92E-02
9.58E-02
OK
08
09
TH-228
TRG
D-83TOT
pCI/1
1.98E.01
1.26E.01
1.37E.Q1
OK
TH-228
TRG
D-83 DIS
pCUI
3.35E-02
7.00E-02
1.33E-01
OK
10
TH-228
TRG
DUPOSTOT
pCUI
4.50E-02
5.59E-02
8.48E-02
OK
11
12
TH-228
TRG
DUP 05 DIS
pCI/1
6.08E-02
8.01E-02
1.28E-01
OK
TH-228
TRG
PZ-102-55 TOT
pCI/1
3.24E+OO
7.14E-01
1.31E-01
OK
13
TH-228
TRG
PZ-102-5S DIS
pCI/1
9.66E-02
7.02E-02
G.SSE-02
OK
14
15
TH-228
TRG
PZ-102R-55 TOT
pCI/1
2.49E-01
1.23E-01
5.84E-02
OK
TH-228
TRG
PZ-102R-55 DIS
pCI/1
8.15E..Q3
2.49E-02
5.90E-02
OK
16
TH-228
TRG
PZ-104-5D TOT
pCUI
4.66E-02
5.67E-02
6.87E-02
OK
17
TH-228
TRG
PZ-104-SD DIS
pCJ/1
2.33E-02
3.96E-02
6.71E-02
OK
"'c
18
19
TH-228
TRG
PZ-104-55 TOT
pCI/1
4.81E-02
5.24E.02
6.28E..02
OK
TH-228
TRG
PZ-104-SS DIS
pCI/1
2.51E-02
5.98E-02
1.16E-01
OK
4.81E+OO
en
.c
1-
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"
..::;;."'
"
"c
;;,
c
w
Blank
Flag
OK
OK
Ul
(..,J
Client
Oaao
LCS
Q.
Q.
Sample
LCS
..:0
Work Order: 13-04106-ThiS0-1
TH-228
..;
.5
Printed: 5/2/2013 9:17AM

Page 1 of 3
01
02
ill
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Nuclide
NA
OK
OK
Eberline Services
Printed: 5/2/2013 9:17 AM

Page 2 of 3

F.'.
,:
~
.g
0
.~
~
~
"
!
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Lab
Sample
Date
01
TH-228
LCS
04116/13 00:00
1.00E+OO
115.65
0.00
0.00
02
TH-228
MBL
04/16/13 00:00
1.00E+OO
103.18
0.00
0.00
03
TH-228
DUP
04/09/1315:35
1.00E+OO
122.51
0.00
0.00
04
TH-228
DO
04/09/13 15:35
1.00E+OO
123.12
0.00
0.00
en
05
TH-228
TRG
04/09/1315:35
1.00E+OO
96.26
0.00
0.00
. t:
06
TH228
TRG
04/09/1315:45
1.00E+OO
116.23
0.00
0.00
07
TH228
TRG
04/09/13 15:45
1.00E+OO
127.42
0.00
0.00
08
TH228
TRG
04109/1316:16
1.00E+OO
115.73
0.00
0.00
09
TH228
TRG
04109/1316:16
1.00E+OO
92.78
0.00
0.00
10
TH-228
TRG
04109/13 00:00
1.00E+OO
126.25
0.00
0.00
11
TH-228
TRG
04109/13 00:00
1.00E+OO
97.80
0.00
0.00
TH-228
TRG
04/11/13 09:10
1.00E+OO
87.06
0.00
0.00
.E
12
13
TH228
TRG
04/11/13 09:10
1.00E+OO
127.66
o.oo
0.00
t:
0
14
TH228
TRG
04/11/1311:30
1.00E+OO
104.21
0.00
0.00
15
TH228
TRG
04/11/1311:30
1.00E+OO
119.97
0.00
0.00
16
17
TH-228
TRG
04/11/1311:38
1.00E+OO
92.22
o.oo
o.oo
TH228
TRG
04/11/13 11:38
1.00E+OO
101.44
o.oo
0.00
c
c"'
18
TH228
TRG
04/11/13 12:59
1.00E+OO
104.03
o.oo
o.oo
"
;;,
c
w
19
TH228
TRG
04/11/1312:59
1.00E+OO
119.57
0.00
0.00
%Rec
Mean
%Rec
%Rec
SAF
Sep tO
Sep t1
DatefTime
Datemme
T""
1--
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Desc
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Aliquot
Radiometric
Nuclide
Fraction
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Fraction
Nucllde
Sample
Desc
Counting
Date/Time
01
02
TH-228
LCS
TH-228
03
Halfllfe
(days)
Count
Time
Bkg
Canier
05/01/13 12:48
A_Spec
Alpha_003
170 4.45 E+02
1.80 E-02
17.5
MBL
05/01/13 12:48
A_Spec
Alpha_004
170 7.70 E-01
1.90 E-02
19.4
TH-228
DUP
05/01/1312:48
A_Spec
Alpha_010
170 1.39 E+01
2.40 E-02
19.7
04
05
TH228
DO
05/01/13 12:48
A_Spec
Alpha_011
170 9.96 E+OO
1.20 E-02
19.7
TH-228
TRG
05/01/13 12:48
A_Spec
Alpha_013
170.02 5.70 E-01
2.10 E-02
18.7
06
TH-228
TRG
05/01/13 12:48
A_Spec
Alpha_014
170.02 1.09 E+01
2.40 E-02
18.5
07
TH-228
TRG
05/01/1312:49
A_Spec
Alpha_018
170 1.79 E+OO
1.30 E-02
17.8
08
TH-228
TRG
05/01/13 12:49
A_Spec
Alpha_022
170 1.29 E+01
1.80 E-02
15.3
09
TH-228
TRG
05/01/13 12:49
A_Spec
Alpha_024
170 1.96 E+OO
1.20 E-02
17.1
10
TH-228
TRG
05/01/1312:49
A_Spec
Alpha_025
170 3.64 E+OO
8.00 E-03
17.4
11
12
TH-228
TRG
05/01/13 12:49
A_Spec
Alpha_027
170 3.79 E+OO
1.30 E-02
17.3
TH-228
TRG
05/01/13 12:49
A_Spec
Alpha_029
170 2.03 E+02
1.40 E-02
19.5
..;
.5
t
13
TH-228
TRG
05/01/13 12:49
A_Spec
Alpha_033
170 8.32 E+OO
4.00 E-03
18.2
14
TH-228
TRG
05/01/13 12:49
A_Spec
Alpha_034
170 1.78 E+01
1.00 E-03
18.6
15
TH-228
TRG
05/01/1312:49
A_Spec
Alpha_035
170 6.60 E-01
2.00 E-03
18.3
....."'
16
TH-228
TRG
05/01/1312:49
A_Spec
Alpha_037
170 2.83 E+OO
1.00 E-03
17.8
17
TH-228
TRG
05/01/13 12:49
A_Spec
Alpha_040
170 1.66 E+OO
2.00 E-03
19
.."'c
18
TH-228
TRG
05/01/13 12:49
A_Spec
Alpha_041
170 3.66 E+OO
2.00 E-03
19.8
19
TH-228
TRG
05/01/1316:16
A_Spec
Alpha_003
170 1.94 E+OO
1.80 E-02
17.5
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Printed: 5/2/2013 9:17AM

Page 3 of 3
Detect
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CPM
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Nuclide
Printed: 5/2/2013 9:17AM

Page 1 of3
Sample
Client
Desc
Identification
Activity
Units
Results
Error Estimate
MDA
LCS
Known
LCS
%R
Flag
LCS
98.93
OK
RPD
Flag
MDA
Flag
01
TH-230
LCS
LCS
pCUI
5.38E+OO
8.28E-01
9.01E-02
02
TH-230
MBL
BLANK
pCUI
2.54E-01
1.23E-01
7.94E-02
03
04
TH-230
DUP
PZ-111-KS TOT
pCi/1
1.83E-01
9.60E-02
7.55E-02
TH-230
DO
PZ-111-KS TOT
pCI/1
2.04E-01
9.82E-02
5.22E-02
OK
5.44E+OO
Blank
Flag
OK
OK
NA
OK
OK
-.....
05
TH-230
TRG
PZ-111-KS DIS
pCI/1
1.40E-01
9.48E-02
7.74E-02
OK
.a-
en
J:
06
TH-230
TRG
D-6 TOT
pCI/1
1.28E-01
8.32E..02
6.98E-02
OK
07
TH-230
TRG
D-6 DIS
pCUI
6.81E-02
6.25E-02
7.73E-02
OK
08
TH-230
TRG
D-83TOT
pCI/1
4.74E-01
1.87E-01
1.03E-01
OK
09
10
TH-230
TRG
D-83 DIS
pCI/1
2.12E-01
1.24E-01
B.OOE-02
OK
TH-230
TRG
DUPOSTOT
pCUI
1.25E-01
8.14E-02
6.83E-02
OK
11
TH-230
TRG
DUP 05 DIS
pCI/1
9.40E-02
8.40E-02
9.90E-02
OK
12
13
TH-230
TRG
PZ-102-SS TOT
pCI/1
3.03E+OO
6.73E-01
9.38E-02
OK
TH-230
TRG
PZ-102-SS DIS
pCI/1
1.18E..01
7.65E-02
6.43E..02
OK
::
14
TH-230
TRG
PZ-102R-SS TOT
pCI/1
2.65E-01
1.28E-01
7.74E-02
OK
,,~
15
16
TH-230
TRG
PZ-1 02R-SS DIS
pCI/1
5.65E-02
5.41E-02
5.79E-02
OK
TH-230
TRG
PZ-104-50 TOT
pCI/1
1.72E..01
1.09E..01
7.72E-02
OK
"'
""
17
TH-230
TRG
PZ-104-SD DIS
pCI/1
1.61E-01
9.73E-02
6.58E-02
OK
".."'
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"
w
"
18
TH-230
TRG
PZ-104-SS TOT
pCI/1
1.57E-01
9.49E-02
7.72E-02
OK
19
TH-230
TRG
PZ-104-SS DIS
pCUI
8.44E-02
7.27E-02
8.72E-02
OK
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Radiometric
%Rec
Mean
Sample
Desc
Sample
Date
01
02
TH-230
LCS
04116/13 00:00
1.00E+OO
115.65
0.00
0.00
TH-230
MBL
04/16/13 00:00
1.00E+OO
103.18
0.00
0.00
03
TH-230
DUP
04109/13 15:35
1.00E+OO
122.51
0.00
0.00
04
05
TH-230
DO
04/09/13 15:35
1.00E+OO
123.12
0.00
0.00
TH-230
TRG
04/09/13 15:35
1.00E+OO
96.26
0.00
0.00
06
TH-230
TRG
04109/13 15:45
1.00E+OO
116.23
0.00
0.00
07
08
TH-230
TRG
04/09/13 15:45
1.00E+OO
127.42
0.00
0.00
TH-230
TRG
04/09/13 16:16
1.00E+OO
115.73
0.00
0.00
09
TH-230
TRG
04/09/1316:16
1.00E+OO
92.78
0.00
0.00
10
11
TH-230
TRG
04109/13 00:00
1.00E+OO
126.25
0.00
0.00
TH-230
TRG
04/09/13 00:00
1.00E+OO
97.80
0.00
0.00
12
TH-230
TRG
04/11/13 09:10
1.00E+OO
87.06
0.00
0.00
.;
.5
13
TH-230
TRG
04/11/13 09:10
1.00E+OO
127.66
0.00
0.00
t:
0
14
TH-230
TRG
04/11/1311:30
1.00E+OO
104.21
0.00
0.00
-..
15
TH-230
TRG
04/11/1311:30
1.00E+OO
119.97
0.00
0.00
16
TH-230
TRG
04/11/1311:38
1.00E+OO
92.22
0.00
0.00
17
TH-230
TRG
04/11/1311:38
1.00E+OO
101.44
0.00
0.00
18
TH-230
TRG
04111/1312:59
1.00E+OO
104.03
0.00
0.00
19
TH-230
TRG
04111/1312:59
1.00E+OO
119.57
0.00
0.00
Sample
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Printed: 5/2/2013 9:17AM

Page 2 of 3
Nuclide
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Page 3 of 3

Sample
Oesc
Counting
Date/Time
Halflife
(days)
Detect
Carrier
Count
Tim.
Counts
Bkg
CPM
Eff
01
TH-230
LCS
0510111312:48
A_Spec
Alpha_003
170 4.10 E+02
8.00 E-03
17.5
02
03
TH-230
MBL
05101113 12:48
A_Spec
Alpha_004
170 1.92 E+01
5.00 E-03
19.4
TH230
DUP
05/01/13 12:48
A_Spec
Alpha_010
170 1.66 E+01
8.00 E-03
19.7
04
TH-230
DO
0510111312:48
A_Spec
Alpha_011
170 1.87 E+01
2.00 E-03
19.7
~
[,
05
06
TH-230
TRG
0510111312:48
A_Spec
Alpha_013
170.02 9.49 E+OO
3.00 E-03
18.7
TH-230
TRG
05101113 12:48
A_ Spec
Alpha_014
170.02 1.03 E+01
4.00 E-03
18.5
07
TH-230
TRG
0510111312:49
A_Spec
Alpha_018
170 5.81 E+OO
7.00 E-03
17.8
08
09
TH-230
TRG
05101/1312:49
A_Spec
Alpha_022
170 3.16 E+01
8.00 E-03
15.3
TH-230
TRG
05/01113 12:49
A_Spec
Alpha_024
170 1.27 E+01
2.00 E-03
17.1
10
TH-230
TRG
05101113 12:49
A_Spec
Alpha_025
170 1.03 E+01
4.00 E-03
17.4
11
TH-230
TRG
0510111312:49
A_Spec
Alpha_027
170 5.98 E+OO
6.00 E-03
17.3
12
13
TH-230
TRG
05101/13 12:49
A_Spec
Alpha_029
170 1.93 E+02
5.00 E-03
19.5
TH-230
TRG
05101113 12:49
A_Spec
Alpha_033
170 1.03 E+01
4.00 E-03
18.2
14
TH-230
TRG
0510111312:49
A_Spec
Alpha_034
170 1.93 E+01
4.00 E-03
18.6
15
16
TH-230
TRG
0510111312:49
A_Spec
Alpha_035
170 4.66 E+OO
2.00 E-03
18.3
TH-230
TRG
05101113 12:49
A_Spec
Alpha_037
170 1.07 E+01
2.00 E-03
17.8
"""
0
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Nuclide
Fraction
"E
.."'
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TRG
05101113 12:49
A_Spec
Alpha_040
170 1.17 E+01
2.00 E-03
19
2"'
18
TH-230
TRG
05101/1312:49
A_Spec
Alpha_041
170 1.21 E+01
5.00 E-03
19.8
c
;;,
c
19
TH-230
TRG
05101113 16:16
A_ Spec
Alpha_003
170 6.64 E+OO
8.00 E-03
17.5
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Client
Activity
Identification
Units
01
TH-232
LCS
LCS
pCi/1
5.42E+OO
8.31E-01
8.64E-02
02
TH-232
MBL
BLANK
pCI/1
4.62E-02
5.29E-02
6.95E-02
03
TH-232
DUP
PZ-111-KS TOT
pCI/1
8.59E-02
6.66E-02
7.24E-02
04
TH-232
00
PZ-111-KS TOT
pCill
1.25E-01
7.66E-02
5.72E-02
OK
05
TH232
TRG
PZ-111-KS DIS
pCI/1
7.22E-03
3.01E-02
7.73E-02
OK
06
TH-232
TRG
0-6 TOT
pCI/1
3.89E-02
4.96E-02
7.39E-02
OK
07
TH232
TRG
0-6 DIS
pCI/1
1.72E-02
4.15E-02
8.32E-02
OK
08
TH-232
TRG
D-113 TOT
pCI/1
~5.38E..03
3.2SE-02
1.02E-01
OK
09
TH-232
TRG
0-113 DIS
pCI/1
-1.70E-02
3.56E-02
1.05E-01
OK
10
TH-232
TRG
DUPOSTOT
pCI/1
2.81E-02
4.21E-02
6.82E-02
OK
11
TH-232
TRG
CUP OS DIS
pCI/1
5.02E..03
3.25E-02
8.85E-02
OK
12
TH-232
TRG
PZ-102-SS TOT
pCUI
4.35E+OO
9.05E-01
9.38E-02
OK
13
TH-232
TRG
PZ-102-SS DIS
pCI/1
3.41E-02
4.49E-02
6.82E-02
OK
14
THw232
TRG
PZ-102R-SS TOT
pCI/1
3.63E-01
1.52E-01
7.19E-02
OK
"
c
"e
".."'
15
TH232
TRG
PZ-102R-SS DIS
pCI/1
1.00E-02
2.41E-02
5.05E-02
OK
16
TH-232
TRG
PZ-1 04-SD TOT
pCi/1
1.61E-02
4.4BE-02
9.66E-02
OK
c
::;;
..
17
TH-232
TRG
PZw104~SD
DIS
pCI/1
-4.67E-03
2.77E-02
6.57E-02
OK
"'
18
TH-232
TRG
PZ-104-SS TOT
pCI/1
-2.85E-02
2.99E-02
1.03E-01
OK
""c
s,
19 I
TH-232
! TRG
PZ-104-SS DIS
pCUI
-1.51E-02
2.74E-02
8.36E-02
OK
-.1-c
en
'i:
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Results
Error Estimate
MDA
LCS
LCS
Known
%R
LCS
Flag
112.51
OK
4.81E+OO
RPD
Flag
MDA
Flag
Blank
Flag
OK
OK
OK
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Sample
Desc
""-
Printed: 5/2/2013 9:18AM

Page 1 of 3
Nuclide
Lab
Fraction
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Preliminary Data Report & AnalytiCal Calculations
Printed: 5/2/2013 9:18AM

Page 2 of 3
Work Order: 13-041'06-ThiS0-1
,:
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Nucllde
Sample
Oesc
Sample
Sample
Date
Aliquot
01
TH-232
LCS
04/16/13 00:00
02
03
TH-232
MBL
04116113 00:00
1.00E+OO
103.18
0.00
0.00
TH-232
DUP
04/09/13 15:35
1.00E+OO
122.51
0.00
0.00
04
TH-232
DO
04/09/1315:35
1.00E+OO
123.12
0.00
0.00
05
06
TH-232
TRG
04109113 15:35
1.00E+OO
96.26
0.00
0.00
TH232
TRG
04109113 15:45
1.00E+OO
116.23
0.00
0.00
07
TH-232
TRG
04109/1315:45
1.00E+OO
127.42
0.00
0.00
08
TH-232
TRG
04109113 16:16
1.00E+OO
115.73
0.00
0.00
09
TH232
TRG
04109113 16:16
1.00E+OO
92.78
0.00
o.oo
10
TH-232
TRG
04109113 00:00
1.00E+OO
126.25
0.00
0.00
11
TH-232
TRG
04/09/13 00:00
1.00E+OO
97.80
o.oo
0.00
TH232
TRG
04/11/13 09:10
1.00E+OO
87.06
0.00
0.00
12
13
TH-232
TRG
04111/13 09:10
1.00E+OO
127.56
0.00
0.00
t:0
14
TH-232
TRG
04111/1311:30
1.00E+OO
104.21
0.00
0.00
-..
15
TH-232
TRG
0411111311:30
1.00E+OO
119.97
0.00
0.00
16
TH-232
TRG
04/1111311:38
1.00E+OO
92.22
0.00
0.00
17
TH-232
TRG
04/11/1311:38
1.00E+OO
101.44
0.00
0.00
18
19
TH-232
TRG
0411111312:59
1.00E+OO
104.03
0.00
0.00
TH-232
TRG
0411111312:59
1.00E+OO
119.57
0.00
0.00
Lob
Fraction
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Cl
"..
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1.00E+OO
Radiometric
%Rec
115.65
Mean
%Rec
Gm
%Rec
0.00
SAF
SeptO
Date/Time
Sep t1
DatefTime
0.00
;;
'
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Counting
Halnife
Oesc
Datemme
(days)
TH-232
LCS
TH-232
03
Nuclide
01
02
Count
Bkg
Carrier
05/01/13 12:48
A_Spec
Alpha_003
170 4.13 E+D2
7.00
E~3
17.5
MBL
05/01/1312:48
A_Spec
Alpha_004
170 3.49 E+OO
3.00 E-03
19.4
TH-232
DUP
05/01/13 12:48
A_ Spec
Alpha_010
170 7.81 E+OO
7.00 E-03
19.7
04
TH-232
DO
05/01/13 12:48
A_Spec
Alpha_011
170 1.15 E+01
3.00 E-03
19.7
en
-1-
05
TH-232
TRG
05/01/1312:48
A_Spec
Alpha_013
170.02 4.90 E-01
3.00 E-03
18.7
J:
06
TH-232
TRG
05/01/1312:48
A_Spec
Alpha_014
170.02 3.15 E+OO
5.00 E-03
18.5
07
TH-232
TRG
05101/13 12:49
A_Spec
Alpha_018
170 1.47 E+O~
9.00 E-03
17.8
08
TH-232
TRG
05/01/1312:49
A_Spec
Alpha_022
170 -3.60
E-0~
8.00 E-03
15.3
09
TH-232
TRG
05/01/1312:49
A_Spec
Alpha_024
170 -1.02 E+OO
6.00 E-03
17.1
10
TH-232
TRG
06101/13 12:49
A_Spec
Alpha_025
170 2.32 E+OO
4.00 E-D3
17.4
11
TH-232
TRG
05/01/1312:49
A._Spec
Alpha_027
170 3.20 E-01
4.00 E-03
17.3
12
TH-232
TRG
05/01/1312:49
A_Spec
Alpha_029
170 2.78 E+02
0.00 E+OO
19.5
13
TH-232
TRG
05/01/1312:49
A._Spec
Alpha_033
170 3.00 E+OO
0.00 E+OO
18.2
t:
0
14
TH-232
TRG
05/01/13 12:49
A_Spec
Alpha_034
170 2.65 E+01
3.00 E-03
18.6
"'.c:
-.
15
TH-232
TRG
05/01/13 12:49
A_Spec
Alpha_035
170 8.30 E-01
1.00 E-03
18.3
...."'
:;;
16
TH-232
TRG
05/01/1312:49
A._Spec
Alpha_037
170 1.00 E+OO
0.00 E+OO
17.8
c:
17
TH-232
TRG
06/01/13 12:49
A_Spec
Alpha_040
170 -3.40 E-01
2.00 E-D3
19
"'c:
18
TH-232
TRG
05/01/1312:49
A_ Spec
Alpha_041
170 -2.21 E+OO
1.30 E-02
19.8
,.
1
"
a."cc:
19
TH-232
TRG
05/01/13 16:16
A_Spec
Alpha_003
170 -1.19 E+OO
7.00 E-03
17.5
If\~;
Time
Counts
CPM
Eff
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Lob
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Printed: 5/2/2013 9:18AM

Page 3 of 3
Detect
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Count Room Report

13-04106-ThiS0-1 (pCi/1) in WA
Tracer 10: Th-18a
('
1'-)
Internal
Fraction
Sample
Desc
Client
ID
Sample
Date
Sample
Aliquot
01
LCS
LCS
04/16/1300:00
1.0000
0.4745
10.6606
0.00
MBL
BLANK
04/16/13 00:00
1.0000
0.2367
5.3179
0.00
PZ-111-KSTOT
04/09/1315:35
02
'
03
DUP ,
1.0000
'
--~
Tracer
Aliquot (g)
04
[t
\0
PZ-111-KS TOT
04/09/1315:35
PZ-111-KSDIS
04/09/1315:35:
1.0000 __
0.2321
5.~146
0.0~~--t-----t----l
0.00
D-6TOT
04/09/1315:45
1.000~-
0.2341
5.2595
07
i TRG
D-6 DIS
04/09/1315:45
1.0000
0.2327
5.2281
08
TRG
D-83TOT
04/09/1316:16
0.2336
5.2483
09
TRG
D-83 DIS
04/09/13 16:16
1.0000
0.2321
5.2146
10
TRG
DUP 05 TOT
04/09/13 00:00
!"- 1.0000
0.2324
5.22~3
11
T~
DUP05DIS
04/09/1300:00
1.0000
0.2319
5.2101
0.00
1.0000
0.2329
5.2326
0.00
1.0000
0.2338
5.2528 -
1.0000
0.2322
5.2168
TRGI~PZ-102-SSTOT
04/11/1309:10
PZ-102-SS DIS
04/11/13 09:10
14
TRG
PZ-102R-SS TOT
04/11/1311:30
~-
TRG_
_PZ-104-SDTOT _
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18
TRG
19
TRG
PZ-104-SSTOT
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PZ~1-04-SSDIS-
0.00
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SAF
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5.2663
TRG
t:ll
_5.3045
SAF
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0.2344
13
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Radiometric
% Rec
1.0000
Radiometric
Tracer (pCi)
05
12
r-
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Tracer
ACT (dpm)
0.2361 I
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Printed: 5!1/2013 6:05AM

Page 1 of 1
'
1.0000
04/11/1311:3+-~.:_()~325____
04/11/1312:59
04/11/131-2:59tl
1.0000
0.2326
~~~00~0-r--omi
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5.2236
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0.00
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Page 1 of 1
Printed: 4/25/2013 8:59AM
Internal Work Order
Run
Analysis Code
Date
Technician
13-04106
ThiSO
4/25/2013 8:59
JBARNARD
LCS & Matrix Spikes

Isotope
Sol#
Th-228
Th-Bb
Activity
dpmlg
103.560
Solution
Date
1
4/25/2013
Approx
Addition
0.100
LCS
MS
LCSD
MSD
Volume
Used(g}
Volume
Used(g}
Volume
Used(g)
Volume
Used(g}
0.1032
Witness Initials
LCS
Known
pCi
MS
Error
Estimate
0.173
4.81
Added
pCi
0.00
LCSD
Error
Estimate
oool
'
. ~~~L
Th-1b
23.525
4/25/2013
0.500
0.5136
5.44
0.147
0.00
0.000
Th-232
Th-Bb
103.560
4/25/2013
0.100
0.1032
4.81
0.173
0.00
0.000
Tracers
traction
Isotope
Sol#
Activity
dpmlg
Volume
Used(g}
Approx
Addition
I Th-229
Th-1Ba
22.467 4/25/2013
0.4745
0.2200
02
Th-229
Th-18a
22.467 4/25/2013
0.2367
0.2200
03
Th-229
Th-18a
22.467 4/25/2013
0.2361
0.2200
04
I Th-229
Th-18a
22.467
4/25/2013
0.2344
0.2200
05
Th-229
Th-18a
22.467 4/25/2013
0.2321
0.2200
Th-229
Th-1Ba
22.467 4/25/2013
0.2341
0.2200
Th-229
Th-18a
22.467 4/25/2013
0.2327
0.2200
--
08
'
Th-229
Th-18a
22.467 4/25/2013
0.2336
0.2200
-rnh-229
Th-18a
22.467 4/25/2013
0.2321
0.2200
Th-229
Th-18a
22.467 4/25/2013
0.2324
0.2200
--~h-229
Th-1Ba
22.467 4/25/2013
0.2319
0.2200
10
12
Th-229
Th-18a
22.467 4/25/2013
0.2329
0.2200
13
Th-229
Th-18a
22.467 4/25/2013
0.2338
0.2200
14
Th-229
Th-18a
22.4671 4/25/2013
0.2322
0.2200
15
Th-229
Th-1Ba
22.467 4/25/2013
0.2317
0.2200
16
Th-229
Th-18a
22.467 4/25/2013
0.2325
0.2200
17
Th-229
Th-1Ba
22.467 4/25/2013
0.2316
0.2200
Th-229
Th-18a
22.467
4/25/2013
0.2326
0.2200
Th-229
Th-18a
22.467 4/25/2013
0.2307
0.2200
'
IJ::-1
til
i,,,,Jf
Version 2.0 08/99
o.oo'
Tracer
-0.2361
-1n2344
-~3. 2321
-0.2341
-[1.2327
0.000
0.000
ooof
0.000
0.000
o.ool
0.000
LCS
'3
'j
'3
'3
0.5136 '3
(1.
W32 '3
-0:2336 q
-0.2321 9
-~3. :2324 '3
-0. 231'3 g
-(1. 2329 g
-0,233E: g
-0.2322
-0.2317
-0.2325
-0.2316
-0.2326
-[1. 2307
'3
'3
'3
'3
'3
g
Error
Estimate
0.00
0.4745 9
~3.2367
Added
pCi
0.000

Solution
Date
01
MSD
Error
Estimate
0.000
Th-230
Known
pCi
Matrix Spike
Eberline Analytical
Work Order
Analysis Code
Rpt Units
Lab Deadline
Technician
ThiSO
liters
5/7/2013
JBARNARD
Sample
Muffle Data
Client ID
Type
Ratio
Post/Pre
LCS
BLANK
PZ-111-KS TOT
PZ-111-KS TOT
PZ-111-KS DIS
D-6 TOT
D-6 DIS
D-83 TOT
D-83 DIS
DUP OS TOT
DUP OS DIS
PZ-1 02-SS TOT
PZ-102-SS DIS
PZ-102R-SS TOT
PZ-102R-SS DIS
PZ-104-SD TOT
PZ-104-SD DIS
PZ-1 04-SS TOT
LCS
MBL
DUP
DO
TRG
TRG
TRG
TRG
TRG
TRG
.. TRG
TRG
TRG
TRG
TRG
TRG
13-041os
Lab
Fraction
01
02
03
04
OS
06
07
08
09
10
11
12
13
14
1S
16
17
18
19
--
PZ-104-SS DIS
en
~~.
Comments
Technician:
Dilution Data
Dil Factor
No of Oils
.
.:
I
_:_
/
._
..
TRG
TRG
TRG
-
Printed: 4/25/2013 8:59AM

Page 1 of 1
Aliquot Worksheet
--
..
..
Aliquot Data
Ratio
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
1.00E+OO
Aliquot
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
.
Net Equiv
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E>OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
.
MS Aliquot Data
Aliquot
H-3 Solids Only

H3 Dist
Water Added
(ml)
Net Equiv
Aliq
..
..
j.
-
---
~--
--li
~=l=
.
....
:
=+=---
... _
--- f------
Date
J../ JS~
pex-AiphaTM
Spectrum File:
Sample Geometry:
SPIKE
1304106A-TH
01
Shelf 2
Th iso
Detector Name:
Alpha_003
Sample Description:

Env. Background:
System Bkgd 55734
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:33:34 AM
5/1/2013
12:48:31 PM
5/1/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.475 mL
0.2020 +/- 0.0123
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM
1.1565 +/- 0.0736
Control Certificate Name: NatTh_Th-8

TH-232
0.175 MeV
PEAK
Energy
Nuclide
(MeV)
TH-227
TH-228
TH-229
TH-230
TH-232
5.779
5.377
4.883
4.641
3.959
1.125063 +/-
AREA
REPORT
Pk Area
Net
Pk Area
Error %
11.79
444.94
365.98
409.64
412.81
0.094350
Ambient
Backgnd
2.21
3.06
1.02
1.36
1.19
63.03
9.33
10.26
9.70
9.66
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
4.5
19.6
4.4
26.8
62.3
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.974
0.997
0.999
0.995
0.993
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1. 59E-001
5.84E+000
4.82E+000
5.38E+000
5.42E+000
+I+I+I+I+I-
1.02E-001
8.85E-001
5.75E-001
8.28E-001
8.31E-001
MDA
(pCi/liter
1.08E-001
l.17E-001
8.31E-002
9.01E-002
8.64E-002
+I+I+I+I+I-
1. 28E-002
1.40E-002
9.91E-003
1. 07E-002
1. 03E-002
5/d'll :!>
8265
0000056825.CNF
start:
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Channel Data Report
5/2/2013
Page
5:10:49 AM
*******************************************************
s p E C T R A L DATA R E P 0 R T
*****
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
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~2-67
Channel Data Report

369:
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7
Sample Title:
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6
11
12
13
1
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1
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1
1
1
3
3
1
0
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1
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3
10
14
5
1
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1
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8
1
3
3
3
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2
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1
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0
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3
7
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20
9
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0
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2
6
4
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16
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5
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9
11
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0
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6
10
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6
0
1
3
4
5
10
6
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1
1
2
4
2
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1
0
0
1
0
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9
9
16
21
4
1
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18
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3
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1
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1
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12
14
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1
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1
1
0
1
0
0
1
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1
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3
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11
17
0
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1
1
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0
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lll268
Channel Data Report

801:
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0
Sample Title:
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5:10:49 AM
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1
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1
0
0
0
0
0
0
0
0
0
0
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1
0
0
1
0
0
0
0
0
2
0
1
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
2
1
0
0
0
0
0
0
0
0
0
0
0
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1
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1
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1
2
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0
ID2E9
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
BLANK
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000568
1304106A-TH
02
Shelf 2
Th iso
Alpha_004
4
System Bkgd 55735
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

5/1/2013
7:33:34 AM
5/1/2013
12:48:32 PM
170.0 minutes

170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.237 mL
0.2002 +/- 0.0162
0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM
1.0318 +/- 0.0855
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.826
5.392
4.858
4.660
3.906
Net
Pk Area
AREA
REPORT
Pk Area
Error %
1.62
0.77
180.98
19.15
3.49
253.91
542.87
14.62
45.94
113.53
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
2.38
3.23
1. 02
0.85
0.51
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
4.9
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.997
1.000
0.999
0.999
0.958
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.20E-002
1. 02E- 002
2.41E+000
2.54E-001
4.62E-002
+I+I+I+I+I-
5.59E-002
5.54E-002
3.81E-001
1.23E-001
5.29E-002
~
5/~t?
MDA
(pCi/liter
l.llE-001
1.21E-001
8.38E-002
7.94E-002
6.95E-002
+I+I+I+I+I-
1. 76E-002
1. 91E-002
1.33E-002
1.26E-002
l.lOE-002
0000056826.CNF
start:
l:l49l.l(kev)
stop : 1024:6486.9(kev)
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6500
Channel Data Report
5/2/2013
?:tllU
Page
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
02
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Elapsed Real Time:
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10200
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-m-27:3
Channel Data Report

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~l27A
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
PZ-111-KS TOT-DUP
1304106A-TH
03
Shelf 2
Th iso
Alpha_010
10
System Bkgd 55736
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:33:34 AM
5/1/2013
12:48:27 PM
170.0 minutes

170.0 minutes
Th229 TH-18A
0.236 mL
0.2410 +/- 0.0180
0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM
1.2251 +/- 0.0944
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.896
5.360
4.877
4.636
3.959
Net
Pk Area
AREA
REPORT
Pk Area
Ambient
Backgnd
Error %
0.11
13.92
217.30
16.64
7.81
3327.8
60.88
13.36
50.29
76.13
2.89
4.08
1. 70
1.36
1.19
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
6.2
2.9
2.9

Nuclide
Id
Con.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.989
0.992
1.000
0.993
0.992
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1. 24E- 003
1.57E-001
2.40E+OOO
1. 83E-001
8.59E-002
+I+I+I+I+I-
4.14E-002
9.80E-002
3.52E-001
9.60E-002
6.66E-002
MDA
(pCi/liter
9.89E-002
1.11E-001
8.12E-002
7.55E-002
7.24E-002
+I+I+I+I+I-
1.45E-002
1.63E-002
1.19E-002
1.11E-002
1. 06E- 002
AG
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8275
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Acq. start :wed May 0112:48:27 2013
60
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8 30-
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I.
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1,
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4000
4500
;!!)
fi'1~
~ ~
ROI Type: 1
5000
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5500
6000
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6500
Channel Data Report
5/2/2013
5::1;:!;:~
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Channel Data Report

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Jll278
Channel Data Report

801:
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-111-KS TOT
1304106A-TH
04
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_Oll
11
System Bkgd 55737

<not performed>
Sample Size:
Sample Date/Time:
1.000E+000 +I- O.OOOE+OOO liter

4/9/2013
7:33:34 AM
5/1/2013
12:48:28 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.234 mL
0.2429 +/- 0.0182
0.1973 +/- 0.0042 on 12/15/2012 11:28:06 AM
1.2312 +/- 0.0957
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.742
5.347
4.873
4.629
3.969
Net
Pk Area
AREA
REPORT
Pk Area
Error %
0.13
9.96
217.47
18.66
11.49
2294.8
69.15
13.35
45.85
59.30
Ambient
Backgnd
1.87
2.04
1.53
0.34
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.7
2.7
2.9
2.7
2.7
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0. 941
0.985
1.000
0.990
0.996
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1.46E-003
l.llE-001
2.38E+000
2.04E-001
1.25E-001
+I+I+I+I+I-
3.34E-002
7.86E-002
3.50E-001
9.82E-002
7.66E-002
f(4
s(.;;-/t3
MDA
(pCi/liter
8.49E-002
8.69E-002
7.79E-002
5.22E-002
5.72E-002
+I+I+I+I+I-
1. 24E-002
1.27E-002
1.14E- 002
7.66E-003
8.39E-003
0000056822.CNF
60-

start:
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~283
Channel Data Report

801:
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1
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-111-KS DIS
1304106A-TH
05
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_013
13
System Bkgd 55738
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:33:34 AM
5/1/2013
12:48:29 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.232 mL
0.1799 +/- 0.0153
0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM
0.9626 +/- 0.0839
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.821
5.343
4.855
4. 614
4.070
Net
Pk Area
2. 94
-0.57
159.49
9.49
0.49
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
170.25
652.66
15.55
65.59
417.03
3.06
3.57
0.51
0.51
0.51
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
0.0
2.8
6.4
2.8
2.8
T = Tracer Peak used for Effective Efficiency

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.996
0.983
0.999
0.983
0.972
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.45E-002
-8.59E-003
2.36E+OOO
1.40E-001
7.22E-003
+I+I+I+I+I-
7.61E-002
5.61E-002
3.94E-001
9.48E-002
3.01E-002
1/4
5/:>-/13
MDA
(pCi/liter
1.35E-001
1. 42E- 001
7.77E-002
7.74E-002
7.73E-002
+I+I+I+I+I-
2.26E-002
2.37E-002
1.30E-002
1.29E-002
1.29E-002
0000056823.CNF
start:
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Channel Data Report
Page
5/2/2013
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6289
pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
D-6 TOT
1304106A-TH
06
Shelf 2
Th iso
Alpha_014
14
System Bkgd 55739
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:33:34 AM
12:48:30 PM
5/1/2013
170.0 minutes
l70.0 minutes
Th229 TH-18A
0.234 mL
0.2145 +/- 0.0169
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
1.1623 +/- 0.0941
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.800
5.367
4.864
4.641
3.956
Net
Pk Area
AREA
REPORT
Pk Area
Error %'
0.09
10.92
191. 81
10.32
3.15
4723.7
71.11
14.20
63.32
126.68
Ambient
Backgnd
3.91
4.08
1.19
0.68
0.85
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.9
2.9
9.8
2.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.987
0.994
1. 000
0.995
0.991
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi I liter )
1.14E- 003
1.38E-001
2.38E+000
1.28E-001
3.89E-002
+!+I+I+I+I-
5.37E-002
1.00E-001
3.68E-001
8.32E-002
4.96E-002
16
5'(~/I?J
MDA
(pCi/liter
1.24E-001
1.25E-001
8.18E-002
6.98E-002
7.39E-002
+I+I+I+I+I-
1. 91E-002
1.93E-002
1. 26E- 002
1. 08E-002
1.14E-002
0000056824.CNF
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4500
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~, ...11.
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5500
6000
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Channel Data Report
5/2/2013
5:11:3tt
MJ
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801:
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Sample Description:
Spectrum File:
Sample Geometry:
D-6 DIS
1304106A-TH
07
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_018
18
System Bkgd 55740
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:33:34 AM
12:49:00 PM
5/1/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.233 mL
0.2263 +/- 0.0175
0.1776 +/- 0.0033 on 12/15/2012
1.2742 +/- 0.1012
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.786
5.345
4.885
4.616
3.888
Net
Pk Area
AREA
REPORT
Pk Area
Error %
0.94
1. 79
201.15
5.81
1.47
1:57:26 PM
Ambient
Backgnd
443.31
229.05
13.85
90.53
240.74
3.06
2.21
0.85
1.19
1. 53
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
7.9
3.1
3.1

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.979
0.984
0.999
0.984
0.940
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1.13E-002 +I- 5.02E-002

2.14E-002 +I- 4.92E-002
2.37E+000 +/- 3.58E-001
6.81E-002 +I- 6.25E-002
1. 72E-002 +I- 4.15E-002
1\-G
S/<Y/t3
MDA
(pCi/liter
1. 07E-001
9.58E-002
7.04E-002
7.73E-002
8.32E-002
+I+I+I+I+I-
1. 63E- 002
1.45E-002
1. 07E-002
1.17E-002
1.26E-002
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ROI Type: 1
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Channel Data Report

801:
5/2/2013
0
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5: ll!.itl
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D-83 TOT
1304106A-TH
08
Shelf 2
Th iso
Detector Name:
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22
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<not performed>
Sample Size:
Sample Date/Time:

7:33:34 AM
4/9/2013
12:49:01 PM
5/1/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.234 mL
0.1772 +/- 0.0152
0.1531 +/- 0.0029 on 12/15/2012
1.1573 +/- 0.1018
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.818
5.334
4.862
4.636
4.023
Net
Pk Area
4.98
12.94
158.13
31.64
-0.36
AREA
1:57:26 PM
REPORT
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Error %
Ambient
Backgnd
97.79
61.56
15.69
35.71
604.11
1.02
3.06
1.87
1.36
1.36
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Reagent
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O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
4.2
4.7
3.1
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.995
0.978
0.999
0. 993
0.997
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
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7.65E-002
1. 98E- 001
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4.74E-001
-5.38E-003
+I+I+I+I+I-
7.59E-002
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4.00E-001
1. 87E- 001
3.25E-002
1+(4
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MDA
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9.68E-002
1.37E-001
1.14E-001
1. 03E- 001
1.02E-001
+I+I+I+I+I-
1.63E-002
2.30E-002
1. 91E-002
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5/2/2013
S:Utii-
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Channel Data Report

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Spectrum File:
Sample Geometry:
D-83 DIS
1304106A-TH
09
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Th iso
Detector Name:
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Alpha_024
24
System Bkgd 55742
<not performed>
Sample Size:
Sample Date/Time:

7:33:34 AM
4/9/2013
5/1/2013
12:49:03 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.232 mL
0.1587 +/- 0.0143
0.1710 +/- 0.0032 on 12/15/2012
0.9278 +/- 0.0852
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.875
5.302
4.846
4.662
3.947
Net
Pk Area
2.11
1.96
140.66
12.66
-1.02
AREA
2:02:15 PM
REPORT
Pk Area
Error %
217.68
208.49
16.55
55.94
208.15
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
2.89
2.04
0.34
0.34
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O.OOE+OOO
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3.1
3.1
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Nuclide
Id
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Energy
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TH-228
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TH-230
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0.997
0.951
0.996
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5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
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2.36E+000
2.12E-001
-1.70E-002
+I+I+I+I+I-
7.91E-002
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MDA
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1. 05E- 001
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2.65E-002
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Channel Data Report
5/2/2013
Page
5:12:01 11M
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
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Sample Title:
09
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ill3ili7
Channel Data Report

369:
5/2/2013
0
Sample Title:
5::!,~~~$
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l!.13i.\l8
Channel Data Report

801:
5/2/2013
0
Sample Title:
5:1~-t
.w
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
DUP 05 TOT
1304106A-TH
10
Shelf 2
Th iso
Detector Name:
Alpha_025

Env. Background:
Reagent Blank:
25
System Bkgd 55743
<not performed>
Sample Size:
Sample Date/Time:
l . OOOE+OOO +/O.OOOE+OOO liter

7:33:34 AM
4/9/2013
5/1/2013
12:49:04 PM
170.0 minutes
170. 0 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.232 mL
0.2191 +/- 0.0171
0.1736 +/- 0.0032 on 12/15/2012
1.2625 +/- 0.1015
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.743
5.356
4.869
4.632
3.947
Net
Pk Area
2.98
3.64
194.49
10.32
2.32
AREA
1:57:27 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
134.36
123.16
14.08
63.32
149.12
l . 02
l. 36
0.51
0.68
0.68
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
13.6
6.3
3.1
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.942
0.990
1.000
0.992
0.987
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
3.70E-002
4.50E-002
2.36E+OOO
l.25E-001
2.81E-002
+I+I+I+I+I-
5.01E-002
5.59E-002
3.62E-001
8.14E-002
4.21E-002
MDA
(pCi/liter
7.83E-002
8.48E-002
6.38E-002
6.83E-002
6.82E-002
+I+I+I+I+I-
l.20E-002
1.30E-002
9.78E-003
l. 05E- 002
l. 05E-002
,A4
5(>/f3
t!l3Hl
0000056831.CNF
Start:
1:3405. 9(kev)
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Channel Data Report
5/2/2013
5:12:!99
.w
Page
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*****
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Channel Data Report

369:
5/2/20B
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Sample Title:
5:12:<&4
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mJ13
Channel Data Report

801:
5/2/2013
0
Sample Title:
Page
5:l2:8Jt.
0
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pex-AiphaTM
Sample Geometry:
DUP 05 DIS
1304106A-TH
11
Shelf 2
Th iso
Detector Name:
Alpha_027
Sample Description:
Spectrum File:
Env. Background:
Reagent Blank:
27
System Bkgd 55744
<not performed>

4/9/2013
7:33:34 AM
12:49:05 PM
5/1/2013
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
Th229 TH-18A
0.232 mL
0.1690 +/- 0.0148
0.1728 +/- 0.0032 on 12/15/2012
0.9780 +/- 0.0878
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.763
5.372
4.866
4.628
3. 896
AREA
REPORT
Pk Area
Error %
Net
Pk Area
5.15
3.79
149.64
5.98
0.32
2:27:41 PM
94.34
130.58
16.11
87.78
646. 93
Ambient
Reagent
Backgnd
Backgnd
0.85
2.21
1.36
1. 02
0.68
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.2
3.2
5.7
3.2
3.2
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.961
0.996
1. 000
0.990
0.948
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
8.30E-002
6.08E-002
2.36E+000
9.40E-002
5.02E-003
+I+I+!+I+I-
7.96E-002
8.01E-002
4.06E-001
8.40E-002
3.25E-002
MDA
(pCi/liter
9.65E-002
1. 28E-001
1. 08E-001
9.90E-002
8.85E-002
+I+I+I+I+I-
1. 66E- 002
2.21E-002
1. 86E-002
1.70E-002
1.52E-002
1'G
6/d-fo
iti315
0000056832.CNF
start:
1:3402 .4(kev)
Stop : 1024:66SB.l(keV)
60+
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6500
1,
Channel Data Report
5/2/2013
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-102-SS TOT
1304106A-TH
12
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_029
29
System Bkgd 55745
<not performed>
Sample Size:
Sample Date/Time:

7:33:34 AM
4/11/2013
5/1/2013
12:49:06 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.233 mL
0.1694 +/- 0.0148
0.1945 +/- 0.0036 on 12/15/2012
0.8706 +/- 0.0779
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.842
5.384
4.878
4. 631
3.958
Net
Pk Area
AREA
REPORT
Pk Area
Error %
10.64
202.62
150.64
193.15
278.00
2:30:02 PM
Ambient
Backgnd
64.42
13.86
16.05
14.14
11.78
1. 36
2.38
1.36
0.85
0.00
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
10.5
7.8
15.8
20.9
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
1. 000
0.999
1.000
0.991
0.992
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1.71E-001
3.24E+000
2.37E+000
3.03E+000
4. 35E+000
+I+I+I+I+I-
1.14E-001
7.14E-001
4.07E-001
6.73E-001
9.05E-001
I}G
.5/..).jr3
MDA
(pCi/liter
1.10E-001
1. 31E-001
1.08E-001
9.38E-002
9.38E-002
+I+I+I+I+I-
1.89E-002
2.25E-002
1. 85E-002
1. 61E- 002
1. 61E-002
0000056833.CNF
start:
1:3413.S(kev)
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Channel Data Report
5/2/2013
Page
5:12:2'1' .f6l
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S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
12
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Channel Data Report

369:
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-i]323
Channel Data Report

801:
5/2/2013
0
Sample Title:
Page
5:12:27 AM
0
12
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1324
Sample Description:
Spectrum File:
Sample Geometry:
PZ-102-SS DIS
1304106A-TH
13
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_033
04026479A
91132
System Bkgd 55746
<not performed>
Sample Size:
Sample Date/Time:

4/11/2013
7:33:34 AM
5/1/2013
12:49:46 PM
170. 0 minutes
170.1 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.234 mL
0.2329 +/- 0.0177
0.1825 +/- 0.0032 on 12/16/2012
1.2766 +/- 0.0997
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.970
5.334
4.883
4.630
3.890
Net
Pk Area
AREA
REPORT
Pk Area
Error %
1.66
8.32
208.00
10.32
3.00
5:49:18 PM
169.38
71.13
13.62
63.32
130.67
Ambient
Backgnd
0.34
0.68
0.00
0.68
0.00
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
6.5
4.5
5.9

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.927
0.977
0.999
0. 991
0.942
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1. 94E- 002
9.66E-002
2.38E+OOO
1.18E-001
3.41E-002
+I+I+I+I+I-
3.30E-002
7.02E-002
3.55E-001
7.65E-002
4.49E-002
MDA
(pCi/liter
5.59E-002
6.55E-002
6.85E-002
6.43E-002
6.82E-002
+I+I+I+I+I-
8.33E-003
9.77E-003
1. 02E-002
9.59E-003
1.02E-002
ALi
6/afr!:.
t!l325
0000056835.CNF
start:
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stop : 1024:650l.l(kev)
Acq. Start :wed May 0!12:49:46 2013
6055
501
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+-'
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!1
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ROI Type: 1
ill
!I
6000
5500
WI
tJ
ROI Type: 3
6500
Channel Data Report
5/2/2013
Page
5:12:35 AM
*******************************************************
*****
E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
13
Elapsed Live time:

Elapsed Real Time:
10200
10206
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~m-327
Channel Data Report

369:
5/2/2013
0
Sample Title:
Page
5:12:35 AM
0
13
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E328
Channel Data Report

801:
5/2/2013
0
Sample Title:
Page
5:12:3!0 .Mf
0
13
809:
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1
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-102R-SS TOT
1304106A-TH
14
Shelf 2
Th iso
Alpha_034
04026479B
91136
System Bkgd 55747
<not performed>

4/11/2013
7:33:34 AM
5/1/2013
12:49:49 PM
Sample Size:
Sample Date/Time:
170.0 minutes
170.1 minutes
Th229 TH-18A
0.232 mL
0.1934 +/- 0.0160
0.1856 +/- 0.0032 on 12/16/2012
1.0421 +/- 0.0879
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.752
5.373
4.893
4.633
3.972
Net
Pk Area
0.66
17.83
171.49
19.32
26.49
AREA
5:49:43 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
305.43
46.68
14.99
45.50
38.51
0.34
0.17
0.51
0.68
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
8.1
3.0
8.9

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.951
0.996
0.998
0.992
0.997
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
9.29E-003
2.49E-001
2.36E+000
2.65E-001
3.63E-001
+I+I+I+I+I-
2.84E-002
1.23E-001
3.82E-001
1.28E-001
1. 52E-001
.5'/dlrJ
MDA
(pCi/liter
6.73E-002
5.84E-002
7.22E-002
7.74E-002
7.19E-002
+I+I+I+I+I-
1. 09E-002
9.44E-003
1.17E- 002
1.25E-002
1.16E-002
0000056836.CNF
start:
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60 155
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401
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8 30
1-
25+
r
20
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5
~
~
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3500
4000
4500
I<W
t~~
(;.ll
.....
ROI Type: 1
5000
Energy(kev)
I.
5500
6000
ROI Type: 3
Channel Data Report
5/2/2013
?:J;~~t
Page
*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
14
Elapsed Live time:

Elapsed Real Time:
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10206
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!Y332
Channel Data Report

369:
5/2/2013
0
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8333
Channel Data Report

801:
5/2/2013
0
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-102R-SS DIS
1304106A-TH
'15
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_035
04026477A
58771
System Bkgd 55748
<not performed>
Sample Size:
Sample Date/Time:

4/11/2013
7:33:34 AM
5/1/2013
12:49:43 PM
170.0 minutes

170.1 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.232 mL
0.2190 +/- 0.0171
0.1826 +/- 0.0032 on 12/16/2012
1.1997 +/- 0.0962
0.175 MeV
PEAK
Energy
Nuclide
(MeV)
TH-227
TH-228
TH-229
TH-230
TH-232
5.792
5.347
4.908
4.630
3.866
Net
Pk Area
3.32
0.66
193.83
4.66
0.83
AREA
5:49:42 PM
REPORT
FWHM
(keV)
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
0.68
0.34
0.17
0.34
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
119.77
305.43
14.09
94.59
239.53
2.9
2.9
7.3
2.9
2.9

Nuclide
Id
Con.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.983
0.985
0.993
0.991
0.915
5850.00*
5400.00*
4872.00*
4672. 00*
3997.00*
Activity
(pCi/ liter )
4 .13E-002
8.15E-003
2.36E+OOO
5.65E-002
1. OOE-002
+I+I+I+I+I-
4.98E-002
2.49E-002
3.61E-001
5.41E-002
2.41E-002
/}(;
S(~(j
MDA
(pCi/liter
7.01E-002
5.90E-002
5.07E-002
5.79E-002
5.05E-002
+I+I+I+I+I-
1. 08E-002
9.06E-003
7.78E-003
8.89E-003
7.74E-003
0000056837.CNF
start:
1:3463.4(kev}
Stop : 1024:6473.5(kev}
60
55
50
45
40
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6000
ROI Type: 3
II
II I
Channel Data Report
5/2/2013
Page
5:12:5:2 AM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
15
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Elapsed Real Time:
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Channel Data Report

369:
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lfi3.38
Channel Data Report

801:
5/2/2013
1
Sample Title:
Page
5:12:52 AM
0
15
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pex-AiphaTM
Sample Description:
Spectrum File:
c__
PZ-104-SD TOT
\\OR-ALPHA1\Canberra\ApexA1pha\Root\Data\00000568
1304106A-TH
16
Shelf 2
Sample Geometry:
Th iso
Detector Name:
Env. Background:
A1pha_037
04026478A
91133
System Bkgd 55750
Reagent Blank:
<not performed>
1.000E+000 +/O.OOOE+OOO liter

4/11/2013
7:33:34 AM
5/1/2013
12:49:45 PM
170.0 minutes
Sample Size:
Sample Date/Time:
170.1 minutes
Th229 TH-18A
0.233 mL
0.1644 +/- 0.0146
0.1783 +/- 0.0033 on 1/26/2013
0.9222 +1- 0.0835
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.790
5.312
4.875
4.618
3.834
Net
Pk Area
0. 32
2.83
146.00
10.66
1. 00
AREA
3:28:25 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
646.93
120.53
16.28
61.14
277.19
0.68
0.17
0.00
0.34
0.00
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
4.6
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.981
0.960
1.000
0.985
0.870
5850.00*
5400.00*
4872. 00*
4672.00*
3997.00*
Activity
(pCi/liter )
5.30E-003
4.66E-002
2.36E+OOO
1. 72E-001
1. 61E-002
+I+I+I+I+I-
3.43E-002
5.67E-002
4.11E-001
1. 09E- 001
4.48E-002
S/:/!0
MDA
(pCi/liter
9.34E-002
6.87E-002
9.71E-002
7.72E-002
9.66E-002
+I+I+I+I+I-
1. 62E- 002
1.19E- 002
1. 69E-002
1.34E-002
1.68E-002
)7'-Mr;
0000056838.CNF
start:
13463.5(kev)
Stop : 1024 6468.5(kev)
Acq. start wed May 0112:49:45 2013
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Channel Data Report
5/2/2013
5:13: (I!
J?age
~'
*******************************************************
S P E C T R A L
R E P 0 R T
DATA
*****
*****
*******************************************************
Sample Title:
16
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Channel Data Report

369:
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ill343
Channel Data Report

801:
5/2/2013
0
Sample Title:
5:131.,
0
w
0
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0
16
Channel[------1-------[-------[-------[-------l-------[-------l-------[
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:

Env. Background:
PZ-104-SD DIS
1304106A-TH
17
Shelf 2
Th iso
Alpha_040
06027396B
91135
System Bkgd 55752
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
l. OOOE+OOO +/- O.OOOE+OOO liter

4/11/2013
7:33:34 AM
12:49:54 PM
5/1/2013
170.0 minutes
170.1 minutes
Th229_TH-18A
0.232 mL
0.1927 +/- 0.0159
0.1900 +/- 0.0033 on 12/16/2012
1.0144 +/- 0.0858
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.874
5.409
4.857
4.675
3.946
Net
Pk Area
-0.34
1.66
170.49
11.66
-0.34
AREA
5:49:33 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
592.90
169.38
15.04
58.37
592.90
0.34
0.34
0.51
0.34
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
0.0
3.0
8.9
3.0
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.997
1.000
0.999
l. 000
0.987
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
-4.80E-003
2.33E-002
2.36E+OOO
l. 61E-001
-4.67E-003
+I+I+I+I+I-
2.85E-002
3.96E-002
3.82E-001
9.73E-002
2.77E-002
lfG
5/J-/0
MDA
(pCi/liter
6.75E-002
6.71E-002
7.25E-002
6.58E-002
6.57E-002
+I+I+I+I+I-
1.10E-002
l. 09E-002
l.18E- 002
l. 07E-002
l. 07E-002
0000056839.CNF
start:
1:3459.0(kev)
stop : 1024:6497.3(kev)
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Channel Data Report
5/2/2013
Page
5:13::!;1;
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
17
Elapsed Live time:

Elapsed Real Time:
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-CJ347
Channel Data Report

369:
5/2/2013
1
Sample Title:
5:13
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Channel Data Report

801:
5/2/2013
0
Sample Title:
5:13:3,:1,
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-104-SS TOT
1304106A-TH
18
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_041
05026930A
91087
System Bkgd 55753
<not performed::>
Sample Size:
Sample Date/Time:
l. OOOE+OOO +/- O.OOOE+OOO liter

4/11/2013
7:33:34 AM
12:49:51 PM
5/1/2013
170.0 minutes
170.1 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.233 mL
0.2058 +/- 0.0165
0.1978 +/- 0.0034 on 12/16/2012
1.0403 +!- 0.0854
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.784
5. 375
4.879
4.671
3. 948
Net
Pk Area
3.15
3.66
182.83
12.15
-2.21
AREA
5:49:31 PM
REPORT
Pk Area
Error %
126.67
107.87
14.50
58.49
104.02
Ambient
Backgnd
0.85
0.34
0.17
0.85
2.21
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
6.0
6.7
3.7
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.978
0.997
l. 000
l. 000
0.988
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.17E-002
4.81E-002
2.37E+000
l.57E-001
-2.85E-002
+I+I+I+I+I-
5.32E-002
5.24E-002
3. 72E-001
9.49E-002
2.99E-002
5'"/.J./(J
MDA
(pCi/liter
7.92E-002
6.28E-002
5.40E-002
7.72E-002
1.03E-001
+I+I+I+I+I-
l. 25E- 002
9.88E-003
8.49E-003
l.21E-002
l. 62E- 002
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Channel Data Report
5/2/2013
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369:
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Channel Data Report

801:
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Sample Title:
5:13:!4!1
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-104-SS DIS
1304106A-TH
19
Shelf 2
Th iso
Detector Name:
Env. Background:
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Alpha_003
3
System Bkgd 55734

<not performed>
Sample Size:
Sample Date/Time:

4/11/2013
7:33:34 AM
5/1/2013
4:16:51 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.231 mL
0.2088 +/- 0.0167
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM
1.1957 +/- 0.0985
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.779
5.308
4.875
4.680
3.949
Net
Pk Area
4.79
1.94
183.98
6.64
-1.19
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
111.13
237.37
14.50
84.69
180.60
2.21
3.06
1. 02
1. 36
1.19
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
10.9
3.0
0.0

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.974
0.956
1.000
1.000
0.988
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
6.25E-002
2.51E-002
2.35E+OOO
8.44E-002
-1.51E-002
+I+I+I+I+I-
7.01E-002
5.98E-002
3.69E-001
7.27E-002
2.74E-002
lt{j
S(<J/tJ
MDA
(pCi/liter
1. 04E-001
1.16E-001
8.03E-002
8.72E-002
8.36E-002
+I+I+I+I+I-
1. 64E-002
1.82E-002
1.26E-002
1. 37E-002
1.31E-002
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6500
Channel Data Report
5/2/2013
s:13n
Page
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
19
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
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41:
49:
57:
65:
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0
0
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0
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0
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0
0
0
0
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0
0
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0
0
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0
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0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
ID357
Channel Data Report

369:
5/2/2013
0
Sample Title:
Page
5:13:28 AM
0
19
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1
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0
1
1
0
2
2
3
5
2
3
1
0
0
3
2
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
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2
2
0
4
1
1
4
0
3
2
1
0
1
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
3
0
1
4
1
2
2
2
1
2
0
2
0
0
0
0
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1
0
0
0
0
0
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0
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1
0
0
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0
2
3
2
2
5
2
5
2
0
0
3
1
2
1
2
0
1
0
0
0
0
0
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3
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2
1
2
2
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t!l358
Channel Data Report

801:
5/2/2013
0
Sample Title:
5:13:
0
! w
0
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0
0
0
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0
0
0
0
0
0
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0
0
0
0
0
0
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0
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0
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0
0
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0
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0
0
0
0
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0
0
0
0
0
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0
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0
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0
0
0
0
0
0
0
0
0
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0
0
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1
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0
0
0
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0
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0
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0
0
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0
0
0
0
1
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0
0
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0
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Page 1 of 2
5/1/2013
5:42:12 AM
QA SUMMARY REPORT
Date
Time
: 5/1/2013
: 5:42:12 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Ah>ha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
A_ljJha 028
Ah>ha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
A_ljJha 038
A_ljJha 039
AlJlha 040
Alpha 041
Alpha 042
DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst 1OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Aljl_ha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst!OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
DATE
511/2013 5:26:43 AM
511/2013 5:26:44 AM
5/1/2013 5:26:45 AM
511/2013 5:26:45 AM
5/1/2013 5:26:46 AM
5/1/2013 5:26:47 AM
5/1/2013 5:26:48 AM
511/2013 5:26:49 AM
5/1/2013 5:26:50 AM
5/1/2013 5:26:51 AM
5/1/2013 5:26:51 AM
511/2013 5:26:52 AM
5/1/2013 5:26:53 AM
511/2013 5:26:55 AM
5/1/2013 5:26:56 AM
4/29/2013 5:29:59 AM
511/2013 5:26:58 AM
4/29/2013 5:30:03 AM
5/1/2013 5:26:59 AM
511/2013 5:27:01 AM
511/2013 5:27:02 AM
Page 2 of 2
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
Review of QA Results - Pulser Chttik
DEVICE
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha Analyst! OODC
Al]Jha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Passed
Passed
Not Done
Passed
Passed
Passed
5/1/2013 54212 AM
DATE
4/29/2013 5:30:09 AM
5/l/2013 5::27:04 AM
5/l/2013 5:27:06 AM
5/l/2013 5:27:08 AM
5/1/2013 5:27:09 AM
APPROVED BY:
APPROVAL DATE:
,[{/II?
8361
6/12/12
Page
12:16:29 PM
*************************************************************************
*****
L I B R A R Y
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Thorium

Nuclide
Name
Half-Life
(Seconds)
Energy
(keV )
TH-227
TH-228
TH-229
TH-230
TH-232
6.873E+008
6.034E+007
2.487E+011
2.379E+012
4.434E+017
5850.000*
5400.000*
4872.000*
4672.000*
3997.000*
Th-227,-228,-229,-230,-232
Energy
Uncert. (keV
0.000
0.000
0.00{)
0.000
0.000
* = key line
TOTALS:
Nuclides
Energy Lines
Yield
( %)
97.5000
99.9400
99.5200
99.8200
100.0000
Yield
Uncert. (Abs. +-)
0-0000
0.0000
0. 0000
0.0000
0.0000
SECTION X
ANALYTICAL DATA (RADIUM-226)
E363
Eberline Services
Analysis Sheet
Work Order
Analysis Code
Ra226
Run 1
I '
Ra226
Run
Date Received
Lab Deadline
Client
Printed: 5/2/2013 6:13 PM

Page 1 of 3
13-04106
4/16/2013
Internal
Fraction
Sample
Desc
Client
Login
ID
CPM
01
LCS
LCS
04/16/13 00:00
02
MBL
BLANK
04/16/13 00:00
1.5000E+OO I
03
DUP
PZ-111-KS TOT
43
04/09/13 15:35
1.5000E+OOI
PZ-111-KS TOT
43
04/09/13 15:35
1.5000E+OO
PZ-111-KS DIS
43
04/09/13 15:35
1.5000E+OOI
Sample
Date
Sample
Aliquot
I
1.0000E+OO
5/7/2013
04
DO
05
TRG
!
Project
West Lake OU-1
06
TRG
D-6 TOT
45
04/09/13 15:45
1.5000E+OO
Report Level
07
TRG
D-6 DIS
45
04/09/13 15:45
1.5000E+OO
Activity Units
pCi
08
TRG
D-83 TOT
40
04/09/13 16:16
1.5000E+OO
Aliquot Units
09
TRG
D-83 DIS
40
04/09/13 16:16
1.5000E+OO
WA
10
TRG
DUP05TOT
47
04/09/13 00:00
1.5000E+OO
Method
EPA 903.0 Modified
11
TRG
DUP 05 DIS
47
04/09/13 00:00
1.5000E+OO
Instrument Type
Alpha Spectroscopy
12
TRG
PZ-102-SS TOT
39
04/11/13 09:10
1.5000E+OO
Radiometric Tracer
Ba-133
13
TRG
PZ-102-SS DIS
39
04/11/13 09:10
1.5000E+OO
Radiometric Sol#
Ba-6a
14
TRG
PZ-102R-SS TOT
45
04/11/1311:30
1.5000E+OO
Tracer Act (dpmlg)
1009.047
15
TRG
PZ-1 02R-SS DIS
45
04/11/13 11:30
1.5000E+OO
Carrier
16
TRG
PZ-104-SD TOT
44
04/11/1311:38
1.5000E+OO
17
TRG
PZ-104-SD DIS
44
04/11/13 11 :38
1.5000E+OO
18
TRG
PZ-1 04-SS TOT
42
04/11/13 12:59
1.5000E+OO
19
TRG
PZ-104-SS DIS
42
04/11/13 12:59
1.5000E+OO
Matrix
- -
~.!D
lrc.
~~ : __:,. ,-. .. SAF1
""
is used for Gross Alpha and all othep.ra'dionuclides.-.S.AF2 is used for Gross Beta only.
"*Actual niasS:.exceeded.tl")e:calibration curve range. Results should be qi.iaiifi"ed as a(ipropriate.
Eberline Services
Analysis Sheet
Printed: 5/212013 6:13PM

Page 2 of 3
13-04106
Ra226
Run 1
Internal
Fraction
Sample
Desc
01
LCS
0.9115
919.7
404.3
97.59
0.0224
0.0278
0.0054
02
MBL
0.9097
917.9
399.5
96.62
0.0225
0.0281
03
DUP
0.9069
915.1
370.1
89.78
0.0224
04
DO
0.9027
910.9
376.3
91.71
05
TRG
0.8995
907.6
362.5
06
TRG
0.9010
909.2
07
TRG
0.8735
08
TRG
09
Tracer
Aliquot (g)
Tracer Total
Radiometric
ACT(dpm)
Tracer(pCQ
Radiometric Grav Carrier

%Rec
Added(ml)
Grav Filter
Grav Filter
Grav Filter
Tare (g)
Final (g)
Net(g)
Grav
%Rec
Mean
%Rec
SAF
1'
SAF
2'
97.59
1.91
1.00
0.0056
96.62
2.00
1.00
0.0281
0.0057
89.78
2.04
1.00
0.0223
0.0283
0.0060
91.71
2.16
1.00
88.66
0.0223
0.0281
0.0058
88.66
2.08
1.00
337.4
82.39
0.0222
0.0305
0.0083
82.39
2.84
1.00
881.4
339.2
85.43
0.0224
0.0302
0.0078
85.43
2.72
1.00
0.9031
911.3
359.6
87.60
0.0226
0.0319
0.0093
87.60
3.09
1.00
TRG
0.8786
886.5
365.2
91.45
0.0225
0.0313
0.0088
91.45
2.96
1.00
10
TRG
0.9011
909.3
315.6
77.06
0.0227
0.0310
0.0083
77.06
2.84
1.00
11
TRG
0.8694
877.3
344.1
87.08
0.0223
0.0302
0.0079
87.08
2.74
1.00
12
TRG
0.9020
910.2
217.8
53.12
0.0225
0.0272
0.0047
53.12
1.55
1.00
13
TRG
0.9038
912.0
343.9
83.71
0.0229
0.0286
0.0057
83.71
2.04
1.00
14
TRG
0.9034
911.6
162.8
39.65
0.0231
0.0390
0.0159
39.65
7.64
1.00
15
TRG
0.9002
908.3
326.1
79.70
0.0224
0.0280
0.0056
79.70
2.00
1.00
16
TRG
0.8050
812.3
256.5
70.10
0.0226
0.0292
0.0066
70.10
2.37
1.00
17
TRG
0.9010
909.2
365.4
89.22
0.0226
0.0296
0.0070
89.22
2.50
1.00
18
TRG
0.9107
918.9
386.7
93.42
0.0225
0.0287
0.0062
93.42
2.23
1.00
19
TRG
0.9016
909.8
424.9
103.68
0.0225
0.0290
0.0065
103.68
2.34
1.00
Ia
!.il
..(fl
Ul
* SAF1 is used for Gross Alpha and alt:othe'fir.adionuclides. SAF2 is used for Gross Beta only.
** Actlllaftnass exceed"',d the calibration curve range. Results should-be.,qualified as,appropriate.
Eberline Services
Analysis Sheet
Printed: 5/2/2013 6:13PM
13-04106
Page 3 of 3
Ra226
Run 1
Internal
Fraction
Sample
Desc
01
Rough Prep
Prep
SepiO
Sep If
Date
Prep
By
SepW
By
Date/Time
By
Date/Time
LCS
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
02
MBL
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
03
DUP
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
04
DO
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
05
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
06
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
07
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
08
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
09
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
10
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
11
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
12
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
13
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
14
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
15
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
16
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
17
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
18
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
19
TRG
04/25/13 09:06
JBARNARD
05/02/13 13:37
LWALKER
Rough Prep
Date
Sep If
By
I
I'
t.1l~
. , :-,~...
~
!l1
* SAF1 is used for Gross Alpha and. aJUother radio-nuclides. SAF2 is used for Gross Beta only.
**~ActUaLmass exceeded the calibration curve range.
Results
should~be~qualified as appropriate.
Eberline Services
Lb
Fraction
1
i
01
~
0:
""" I I
02
Work Order: 13-041 06-Ra226-1

1
Nuclide
Sample
Desc
RA-226
-
LCS
RA-226
MBL
RA-226
-------
Client
Activity
Identification
Unlts
LCS
------ .
!I Error Estimate1
1.16E+OO
'
BLANK
DUP
Results
1.04E+01:
------
8.86E-03i
-
03
Printed: 5/3/2013 12:01 PM

Page 1 of 3
----~
PZ-111-KS TOT
2.04E01
5.55E-02i
--1
1.67E~01
2.95E-01
MDA
LCS
LCS
Known
%R
1.02E+01
LCS
Flag
(.)
-!!'! ,I
~;
00:
CD
N
N
ca
0::
04
RA-226
--- --
05
06
RA-226
D-6 TOT
1.71E01
08
RA-226
TRG
~--1 09
RA-226
TRG
OK
OK
3.48E-01
1.71E01:
1.11E-01
pCi/1
3.14E...Q1
1.70E-01:
1.33E-01
pCi/1
1.91E+OO,
5.02E-01
2.08E-01
OK
OK
i--
1.75E+OO
4.74E-01:
2.40E-01
OK
D-83 TOT
pCi/1
3.17E+OO:
7.25E-01
3.17E-01
OK
D-83 DIS
pCi/1
1.79E+OO
4.86E-01
1.60E-01
OK
D-6 DIS
10'
RA-226
TRG
DUP 05 TOT
pCi/1
1.27E+OO
4.39E01
2.36E-01
OK
"'
:E
11
RA-226
TRG
DUP 05 DIS
pCi/1
8.52E-01
3.37E-01
2.29E-01
OK
12
RA-226
TRG
PZ-102-SS TOT
pCI/1
8.05E+OO
9.52ED1
1.82E01
.;
.E
t:0
c.
c.
~
13
14
RA-226
TRG
'
RA-226
TRG
15
RA-226
TRG
"E
""'
c"
16
RA-226
TRG
17
RA-226
TRG
"'c
~
"c
c;,
18
RA-226
19
RA-226
(/)
~
(.)
:;;"
UJ
I:!!R
1:,\Jr
(!11
~~~
OK
.. ,.. -
.I
I
I
OK
pCi/1
-~
'"
'(
... !~
--------
pCi/1
TRG
J:
OK
'
I
RA-226
--- --------- r-
TRG
PZ-102-SS DIS
pCi/1
4.58E+OO
6.65E-01
1.33E-01
PZ-102R-SS TOT
pCi/1
3.18E+OO
1.11E+OO
5. 75E-01
OK
'
I
'.
Blank
Flag
OK I
1.34E-01
'
RA-226
Flag
---
PZ-111-KS DIS
TRG
1'
07
~IIIII
PZ-111-KS TOT
DO
---.
MDA
Flag
OK
102.12
. ......
~
0
RPD
OK
PZ-102R-SS DIS
pCi/1
1.88E+OO
4.25E-01
1.27E-01
OK
PZ-104-SD TOT
pCi/1
5.72E+OO
8.84E-01
1.60E-01
OK
PZ-104-SD DIS
pCi/1
3.76E+OO
6.28E-01
1.37E-01
OK
TRG
I
I
PZ-104-SS TOT
pCi/1
1.19E+OO-
3.18E-01
1.40E-01
OK
TRG
PZ-104-SS DIS
pCi/1
8.06E-01
2.69E-01
1.41E-01
OK
'
'
OK
Eberline Services
La~
Work Order: 13-04106-Ra226-1
Nuclide
Fraction
01
'=
II
02
RA226
RA-226
Sample
Sample
Sample
Oesc
Date
Aliquot
LCS
04/16/13 00:00
MBL
04/16/13 00:00
Radiometric
Grav
Mean
% Rec
% Rec
% Rec
1.00E+OO]
-r-
I
1.50E+OO[
97.59
96.62
O.ooi
r
I
0.001
I
1
----
-; -------
03
RA-226
DUP
04/09/13 15:35
1.50E+OO:
04
RA-226
oo
04/09/1315:35
-1J
05
RA-226
TRG
-~
ll)
. '"'
06
RA226
a:::
-a7--
RA-226
c.o
N
N...a'
..
SAF
97.59[
1
5/2/2013 13:37j
96.62l
5/2/201313:371
'
--+ -
I
~--i
-~---
89.781
1.50E+ool
91.71
o.oo1
91.7~T
04/09/1315:35
1.50E+OOI
88.66
0.001
88.661
- ..--i-
5/2/201313:371
TRG
04/09/1315:45
1.50E+OO;
82.39
0.00 1
82.391
5/2/2013 13:371
. : TRG
04/09/1315:45
'-
--+------I
1.50E+O~r-- --------~5.43
o.oo!
08
RA-226
TRG
04/09/1316:16
1.50E+OOI
09
RA-226
TRG
04/09/1316:16
-~
~
10
RA-226
TRG
11
RA-226
12
5/2/2013 13:371
j
5/2/201~ 13;~;1
+---
8~~~~~
5/212013-1~:37!'
. . . . ,.
87.60
0.00
87.60:
5/2/201313:371
1.50E+OOI
91.45
0.00
91.45:
5/2/201313:371
04/09/13 00:00
1.50E+OO
77.06
0.00
77.06!
5/212013 13:37'
TRG
04/09/13 00:00
1.50E+OOI
87.08
0.00
87.08
5/2/201313:37:
RA-226
TRG
04/11/13 09:10
53.12
0.00
53.12
5/2/2013 13:371
13
RA-226
TRG
04/11/13 09:10
1.50E+OO'
'.
1.50E+OO:
83.71
0.00
83.71
5/2/201313:371
14
RA-226
TRG
04/11/1311:30
1.50E+OOi
39.65
0.00
39.65
5/2/201313:37:
15
RA-226
TRG
0411111311:30
1.50E+OO,
79.70
0.00
79.70
5/2/201313:37;
16
RA-226
TRG
0411111311:38
1.50E+oo:
70.10
0.00
70.10
5/2/201313:37
17
RA-226
TRG
0411111311:38
1.50E+OO:
89.22
0.00
89.22
5/2/2013 13:37
18
RA-226
TRG
93.42
0.00
93.42
5/2/201313:37
19
RA-226
TRG
100.00
0.00
103.68
5/2/201313:37
0-
-~--i
'
--
.E
~
c
~
"en
~
l
I
.
"
.,
:.::
..
~c
'i I I
;;,
c
w
Ia
t,..)
t1'l
(:1)
I
I
04/1111312:59
1.50E+O~:.
0411111312:59
1.50E+OO
Sep t1
OatefTime
,
+
--
0.00:
--'I.
Sep tQ
Date/Time
89.78
Printed: 5/3/2013 12:01 PM

Page 2 of 3
Eberline Services
"('""
II
01
RA226
--------
. RA~226
02
.:i
0::
RA226
05
ca
06
I 08
Counting
DatefTime
Halflife
(days)
Detect
.
Carner
Alpha_003
170 3.52 E+02 18.00 E-03

....... i. -
17.5
Alpha_004
170:4.70 E-01 . :9.00 E-03
19.4
LCS
05/03/13 05:44
A_Spec
MBL
05/03/13 05:44
A_Spec
DUP
05/03/13 05:44
A_Spec
DO
05/03/13 05:44
A_Spec
RA-226
TRG
05/03/13 05:44
A_Spec
...........
)Aipha_010
Count
Time
RA-226
TRG
--j -
A_Spec
Eff
.
170.02,1.44 E+01
i1.50 E-02
19.7
!Aipha_011
iAipha_013
/Aipha_014
170.021.65 E+01
j3.00 E-03
,..
'
170;1.41 E+01 15.00 E-03

...... ;
170.02:5.80 E+01
19.7
18.7
16.00 E-03
18.5
TRG
05/03/13 05:44
A_Spec
jAipha_018
170 5.51 E+01
i1.1o E-02
17.8
RA-226
TRG
05/03/13 05:44
A_Spec
!Aipha_022
170 7.80 E+01
!1.20 E-02
15,3
RA-226
TRG
05/03/13 05:44
A_Spec
jA1pha_024
170 5.37 E+01
2.00 E-03
17.1
170 3.40 E+01
'6.00 E-03
17.4
170 2.65 E+01
:9.00 E-03
17.3
RA-226
-
05/03/13 05:44
Bkg
CPM
Counts
1- - --
07 :
~
1 Sample
Oesc
RA-226
Printed: 5/3/2013 12:01 PM

Page 3 of 3
Work Order: 13-04106-Ra226-1
04
.......
,_ "'IIII
-~
N l"d
uc 1 e
03
~CD
Lab
Fraction
- --
0
~
09 ,
:::.:
j_-
11
05/03/13 05:44
A_Spec
Aipha_025
i
RA-226
TRG
05103/13 05:44
A_Spec
IA1pha_027
RA-226
TRG
05/03/13 05:44
A_Spec
/Aipha_029
1703.04 E+02
'8.00 E-03
19.5
13
RA-226
TRG
05/03/13 08:20
A_Spec
iAipha_033
170 1.94 E+02
4.00 E-03
18.2
-g
14
RA-226
TRG
05/03/13 08:20
A_ Spec
:Alpha_034
170 3.32 E+01
5.00 E-03
18.6
Aipha_035
170:7.75 E+01
3.00 E..03
18.3
Q.
a.
i'
15
RA-226
TRG
16
RA-226
TRG
I 17
RA-226
g> I I 18
'E
TRG
12
ifl
1:!
RA-226
[
::::
'
10
.~
i .
----- --
C)
~I
05/03/13 08:20
A_Spec
05/03/1308:20
A_Spec
;Aipha_037
170.1.71 E+02
,2.00E-03
17.8
TRG
05/03/13 08:20
A_Spec
:Aipha_040
170 1.44 E+02
3.00 E-03
19
RA-226
TRG
05/03/13 08:20
A_Spec
'Alpha_041
170 5.58 E+01
7.00 E-03
19.8
RA-226
TRG
05/03/13 08:20
A_Spec
Alpha_042
170 3.60 E+01
6.00 E-03
18.5
~:
~ I I
;;,
c
UJ
Iilli
t.~~
r.n
l!l
19
Count Room Report

Printed: 5/2/2013 6:13 PM

Page 1 of 1
13-04106-Ra226-1 (pCi/1) in WA
Tracer ID: Ba-6a
~.~
I
f
Internal
Sample
Fraction
~c
Client
ID
Sample
Date
Sample
Aliquot
01.....,<
LCS
LCS
04/16/13 00:00
1.0000
o.9115
02
MBL
BLANK
04/16/13 00:00
1.5000
/ 03
DUP.
P.Z-111-KS TOT
04/09/13 15:35
04
DO
PZ-111-KS TOT
05
TRG
II
Radiometric
Tracer (pCi)
SAF
2.
97.59
1.91
1.00
0.9097
917.9301
399.5000
96.62
2.00
1.00
1.5000
0.9069
915.1047
370.1000
89.78
2.04
1.00
04/09/13 15:35
1.5000
0.9027
910.8667
376.3000
91.71
2.16
1.00
PZ-111-KS DIS
04/09/13 15:35
1.5000
0.8995
907.6378
362.5000
88.66
2.08
1.00
06 _yc rTRG
D-6 TOT
04/09/13 15:45
1.5000
0.9010
909.1513
337.4000
82.39
2.84
1.00
07
!.>. YTRG
D-6 DIS
04/09/13 15:45
1.5000
0.8735
881.4026
339.2000
85.43
2.72
1.00
l~8
TRG
D-83 TOT
04/09/13 16:16
1.5000
0.9031
911.2703
359.6000
87.60
3.09
1.00
09
TRG
D-83 DIS
04/09/13 16:16
1.5000
0.8786
886.5487
365.2000
91.45
2.96
1.00
10
TRG
DUP 05TOT
04/09/13 00:00
1.5000
0.9011
909.2523
315.6000
77.06
2.84
1.00
11
TRG
DUP 05 DIS
04/09/13 00:00
1.5000
0.8694
877.2655
344.1000
87.08
2.74
1.00
12-,;A,rTRG
PZ-102-SS TOT
04/11/13 09:10
1.5000
0.9020
910.1604
217.8000
53.12
1.55
1.00
13'7 )TRG
PZ-102-SS DIS
04/11/13 09:10
1.5000
0.9038
911.9767
343.9000
83.71
2.04
1.00
14
TRG
PZ-102R-SS TOT
04/11/13 11:30
1.5000
0.9034
911.5731
162.8000
39.65
7.64
1.00
15
TRG
PZ-102R-SS DIS
04/11/1311:30
1.5000
0.9002
908.3441
326.1000
79.70
2.00
1.00
16
TRG
PZ-104-SD TOT
04/11/13 11:38
1.5000
0.8050
812.2828 '
256.5000
70.10
2.37
1.00
17
TRG
PZ-104-SD DIS
04/11/13 11:38
1.5000
0.9010
909.1513
365.4000
89.22
2.50
1.00
18
TRG
PZ-104-SS TOT
04/11/13 12:59
1.5000
0.9107
918.9391
386.7000
93.42
2.23
1.00
19 t hTRG
PZ-104-SS DIS
04/11/1312:59
1.5000
0.9016
909.7568
424.9000
103.68
2.34
~~
'~.'
~!&
SAF
1.
404.3000
-,
.,I,.JI
Radiometric
%Rec
919.7463
~"'
J
Tracer
ACT(dpm)
Tracer
Aliquot (g)
'><;
.-.;./
f\~;:.O')At
1.00
Eberline Services
Page 1 of 1
Printed: 4/25/2013 9:06AM
Internal Work Order
Run
Analysis Code
Date
Technician
13-04106
Ra226
4/25/2013 9:05
JBARNARD
LCS & Matrix Spikes

Isotope
Sol#
Ra-226
Ra-Sb
Activity
dpm!g
Solution
Date
44.071
4/25/2013
Approx
Addition
0.500
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
LCS
I
Known
pCi
10.23
0.5151
Witness Initials
MS
Error
Estimate
0.470
Added
pCi
0.00
MSD
Error
Estimate
0.000
Known
pCi
Error
I
0.00!
Added
pCi
0.000
Error
Estimate
0.00(
0.00
---
------
I
I
Tracers
Activity
dpmlg
Solution
Date
Volume
Used(g)
Approx
Addition
fraction
Isotope
Sol#
01
Ba-133
Ba-6a
1009.047 4/25/2013
. 0.9115
1.0000
02
Ba-133
Ba-6a
1009.047 4/25/2013
0.9097
1.0000
03
Ba-133
Ba-6a
1009.047 4/25/2013
0.9069
1.0000
0.9027
1.0000
04
t~
,_,
"<!
Ba-133
05
Ba-133
06
1009.047 4/25/2013
Ba-6a
LCS
Tracer
0~
'3115 ':!
0.90'37 9
-~3:9069
'3
-0u 9027 '3

-0.8995 9
-0. ';J110 ;3
Ba-6a
1009.047 4/25/2013
0.8995
1.0000
Ba-133
Ba-6a
1009.047 4/25/2013
0.9010
1.0000
07
Ba-133
Ba-6a
1009.047 4/25/2013
0.8735
1.0000
08
Ba-133
Ba-6a
1009.047 4/25/2013
0.9031
1.0000
9
-0.9031 9
-0.8786 s
09
Ba-133
Ba-6a
1009.047 4/25/2013
0.8786
1.0000
-0:9gl1 =j
10
Ba-133
Ba-6a
1009.047 4/25/2013
0.9011
1.0000
11
Ba-133
Ba-6a
1009.047! 4/25/2013
0.8694
1.0000
-0.9038 9
12
Ba-133
Ba-6a
1009.047 4/2512013
0.9020
1.0000
13
Ba-133
Ba-6a
1009.047 4/25/2013
0.9038
1.0000
-0. 9134 9
-0. 9002 '3
14
Ba-133
Ba-6a
1009.047 4/25/2013
0.9034
1.0000
15
Ba-133
Ba-6a
1009.047 4/25/2013
0.9002
1.0000
16
Ba-133
Ba-6a
1009.047 4/25/2013
0.8050
1.0000
17
Ba-133
Ba-6a
1009.047 4/25/2013
0.9010
1.0000
18
Ba-133
Ba-6a
1009.047 4/25/2013
0.9107
1.0000
19
Ba-133
Ba-6a
1009.047 4/25/2013
0.9016
1.0000
--
..!I
Version 2.0 08/99
'
'
0~5151.
-0~8735
-0~8694
g
-0. 912(1 g
-0.8050 s
-0.901.0 'l
-0. '3H;:J7 '3
-0. 9016~ s
'3
0. 5108 '3
Matrix Spike
Eberline Analytical
Work Order
13-o41os
Lab
Lab Deadline
Technician
Ra226
liters
5/7/2013
JBARNARD
Type
03
LCS
BLANK
PZ-111-KS TOT
LCS
MBL
DUP
04
05
PZ-111-KS TOT
PZ-111-KS DIS
DO
TRG
D-6 TOT
D-6 DIS
D-83 TOT
D-83 DIS
TRG
TRG
TRG
TRG
10
11
12
13
DUP 05 TOT
DUP 05DIS
PZ-102-SS TOT
PZ-102-SS DIS
15
PZ-102R-SS TOT
PZ-102R-SS DIS
TRG
TRG
TRG
TRG
TRG
...
06
07 ...
08
----
09
~
17
18
19
Rpt Units
--
PZ-104-SD TOT
...
PZ-104-SD DIS
PZ-1 04-SS TOT
PZ-1 04-SS DIS
Dilution Data
Muffle Data
Sample
Client 10
116
Analysis Code
I 1
Fraction
01
02
PosUPre
Aliquot Data
.. ..
Rcitio
No of Oils
Oil Fa-ctor
Ratio
Aliquot
I
.
:.:
..
I
.
TRG
TRG
TRG
TRG
TRG
.
..
.
..
.
----
Comments
t!l
(;I
Technician:
Printed: 4/25/2013 9:08 AM

Page 1 of 1
Aliquot Worksheet
Jl j
Date:
.J. _i_olJ_
~2...
_1
iJ!./--2..-
..
.
'NetEquiv
1.0000E+OO
1.5000E+OO
1.5000E+OO
1.0000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1:5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
f.SOOOE+OO
.. 1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
MS Aliquot Data
Aliquot
H-3 Solids Only

Water Added
(ml)
Net Equiv
H3 Oist
Aliq
..
--
...
..
Eberline Services - Oak Ridge

Version 1.0 9/1999
Printed: 5/2/2013 4:01 PM

Page 1 of 1
Gravimetric Worksheet
Analysis
Code
Work Order
Gravimetric
Carrier
Carrier Cone
-------j _
Technician
(mg/ml)
Ra226
TRetec
::.:---_- ---
Sample ~ar!ier[)ata
Carrier Added
Type
(ml)
__MBL
LCS
Du
-~~
.
.. ___ -=--
--
--' '"'
~~~
-::~~~:~~
-- -
-::__:-- ::____
--
- -- -
- -. -- --
~
l>l
-..JI
'~"""""c:A ~
~-- ~~-
---
LWALKER
.,-------. _l___
Filter Data
___ ,
Filter Tare
(g)
-- - - ---
Filter Final
(g)
~~~83
~ ~ "-='
"""' '
+--
""""
'''"'~+--
~.0225
-: ~~=
Date
___,2__,
(3
1- -o-o2~~
-- . ---- ----1
Gravimetric
%
Recovery
2 .
o.no2<!'7;tJ8+---- n.,u.u
.o_nos4
-....
0.02_4 I'. ----- . ()- -=-:
0281 ,_
_---;:
II
0 m)56
0 0225 :_
. 81 I
u.u057
0
0223 0 0281 I
::
___ II
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TM
Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1304106A-RA
01
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_003
3
System Bkgd 55734

<not performed>
Sample Size:
Generic Mult. Factor:
Sample Date/Time:

1. 910E+000
Generic Div. Factor:
1:37:25 PM
5/3/2013
5:44:14 AM
5/3/2013
170.0 minutes
170.0 minutes
0.9759 +/0.1746 +/0.1704 +/-

0.0000
0.0033 on 12/15/2012 11:26:47 AM
0.0032
Control Certificate Name: Ra226 Ra-5b

RA-226
0.534636 +/Peak Match Tolerance:
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5.530
4.590
Net
Pk Area
AREA
8.74
10.48
0.034258
REPORT
Pk Area
Error %
505.62
351.64
1.000E+000
Ambient
Backgnd
2.38
1.36
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
4.8
11.7
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.969
0.951
5685.50*
4785.00*
Activity
(pCi/liter )
1.48E+001 +/- 1.26E+003
1.04E+001 +/- 1.16E+OOO
MDA
(pCi/liter
2.40E-001 +/- 2.05E+001
2.04E-001 +/- 7.46E-003
0000057030.CNF
Start:
1 3498.4(kev)
stop : 1024 6549.5(kev)
Acq. start Fri May 03 05:44:14 2013
55
45
35
....,
V>
<=
:=s
25
15
3500
!l:~
(,,JJ
~J
U11
ROI Type: 1
4000
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/3/2013
Page
11:17:50 AM
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
9:
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33:
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Channel Data Report

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l!l317
Channel Data Report

801:
5/3/2013
3
Sample Title:
Page
11:17:50 AM
4
01
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pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
BLANK
1304106A-RA
02
Shelf 2
Ra
Alpha_004
4
System Bkgd 55735
Reagent Blank:
<not performed>

2.000E+000
1:37:25 PM
5/3/2013
5/3/2013
5:44:15 AM
170.0 minutes
Sample Size:
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170.0 minutes
0.9662 +/0.1940 +/0.1875 +/-
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5.491
4.613
l.OOOE+OOO
0.0000
0.0036 on 12/15/2012 11:26:46 AM
0.0034
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REPORT
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Net
Pk Area
Error %
0.11
0.47
3327.8
626.90
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Backgnd
2.89
53
1.
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(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
2.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.952
0. 962
5685.50*
4785.00*
Activity
(pCi/liter )
2.05E-003 +/- 1.87E-001
8.86E-003 +/- 5.55E-002
MDA
(pCi/liter
1.63E-001 +/- 1.39E+001
1.34E-001 +/- 4.82E-003
5379
0000057009.CNF
start:
l:l49l.l(kev)
Stop : 1024:6486.9(kev)
Acq. Start :Fri May 03 05:44:15 2013
60 155
50
4540
35
....c::
V)
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25-
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3500
~JI
t ...~
00
l:\1ll
ROI Type: 1
',/,
4000
4500
5000
Energy(kev)
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Channel Data Report
5/3/2013
Page
11:18:02 AM
*******************************************************
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p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
02
Elapsed Live time:

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Channel Data Report

369:
5/3/2013
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Sample Title:
11:18:0!
Page
02
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~382
Channel Data Report

801:
5/3/2013
0
Sample Title:
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Spectrum File:
Sample Geometry:
PZ-111-KS TOT-DUP
1304106A-RA
03
Shelf 2
Ra
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Alpha_010
10
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<not performed>
Sample Size:
Sample Date/Time:

2.040E+000
5/2/2013
1:37:25 PM
5:44:09 AM
5/3/2013
170.0 minutes
170.0 minutes

0.8978 +/0.1967 +/0.1766 +/-
Energy
(MeV)
RA-224
RA-226
0.0000
0.0036 on 12/15/2012 11:26:40 AM
0.0032
0.350 MeV
PEAK
Nuclide
1.000E+000
Net
Pk Area
5.557
4.597
AREA
REPORT
Pk Area
Error %
4.26
14.45
135.22
56.64
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
3.74
2.55
O.OOE+OOO
O.OOE+OOO
2.9
4.4

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.978
0.955
5685.50*
4785.00*
Activity
(pCi/liter )
1.04E-001 +/- 1.81E+001
2.95E-001 +/- 1.67E-001
MDA
(pCi/liter
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1.71E-001 +/- 6.12E-003
0000057004.CNF
Live Time lOlOl.OOO sec
start:
1 3505./(kev)
stop : 1024 6498.0(kev)
Acq. Start Fri May 03 05:44:09 2013
60!
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5/3/2013
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Sample Title:
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Channel Data Report

801:
5/3/2013
0
Sample Title:
Page
11:11!:1! ~
0
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lll388
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
PZ-111-KS TOT
1304106A-RA
04
Shelf 2
Ra
Alpha_Oll
11
System Bkgd 55737
Reagent Blank:
<not performed>
Sample Size:

2.160E+000
5/2/2013
1:37:25 PM
5:44:10 AM
5/3/2013
170.0 minutes
170.0 minutes
Sample Date/Time:

0.9171 +/0.1973 +/0.1810 +/-
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
Net
Pk Area
5.483
4.559
OOOE+OOO
0.0000
0.0042 on 12/15/2012 11:28:06 AM
0.0038
AREA
REPORT
Pk Area
Error %
5.60
16.49
1.
Ambient
Backgnd
108.33
49.13
3.40
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
2.7
2.7

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0. 948
0.935
5685.50*
4785.00*
Activity
(pCi/liter )
1.41E-001 +/- 2.45E+001
3.48E-001 +/- 1.71E-001
MDA
(pCi/liter
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1.11E-001 +/- 4.57E-003
0000057005.CNF
Start:
1:3645.8(keV)
stop : 1024:6374.2(kev)
60 If-
Acq. start :Fri May 03 05:44:10 2013
55
50
45 If40 If-
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Channel Data Report
5/3/2013
1l: ;jc.l
N1
Page
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*****
p E C T R A L
DATA
R E P 0 R T
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Sample Title:
04
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tr!3'91
Channel Data Report

369:
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Sample Title:
11:1$1J,f;
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Channel Data Report

801:
5/3/2013
0
Sample Title:
11:18:21
0
Page
04
ChannelJ------I-------1-------J-------I-------I-------I-------I-------J
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
PZ-111-KS DIS
1304106A-RA
05
Shelf 2
Ra
Alpha_013
13
System Bkgd 55738
Reagent Blank:
<not performed>
l . 500E+000 +/O.OOOE+OOO liter
2.080E+000
5/2/2013
1:37:25 PM
5:44:11 AM
5/3/2013
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.8866 +/0.1869 +/0.1657 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
Net
Pk Area
5.448
4.566
0.0000
0.0035 on 12/15/2012 11:26:45 AM
0.0031
AREA
REPORT
Pk Area
Error %
5.43
14.15
1.000E+000
111.88
53.90
Backgnd
Reagent
Backgnd
3.57
0.85
O.OOE+OOO
O.OOE+OOO
Ambient
FWHM
(keV)
2.8
2.8
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.929
0.939
5685.50*
4785.00*
Activity
(pCi/liter )
1.44E-001 +/- 2.50E+001
3.14E-001 +/- 1.70E-001
MDA
(pCi/liter
2.50E-001 +/- 4.35E+001
1.33E-001 +/- 4.81E-003
0000057006.CNF
start:
1 3547.5(kevl
stop : 1024 6438.1(kev
60
55
It-
50
It
45
401
35V)
+-'
<=
::::s
8 30
2J
20 It
1J
10
5
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1 l l ll
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1
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4000
a
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4500
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5000
Energy(kev)
~
l,,l_fijfJ
I I,
5500
II l
I I I II
6000
l!
Channel Data Report
Page
5/3/2013
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
05
Elapsed Live time:

Elapsed Real Time:
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10200
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Channel Data Report

369:
5/3/2013
0
Sample Title:
11:~e~n
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0
l!lage
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Channel Data Report

801:
5/3/201.3
0
Sample Title:
11:18:st
0
.,.
0
Page
0
05
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817:
825:
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
D-6 TOT
1304106A-RA
06
Shelf 2
Ra
Alpha_014
14
System Bkgd 55739
<not performed>
Sample Size:

2.840E+000
1:37:25 PM
5/2/2013
5/3/2013
5:44:13 AM
170.0 minutes
170.0 minutes
Sample Date/Time:
0.8239 +/0.1846 +/0.1521 +/-

Energy
(MeV)
RA-224
RA-226
5.508
4.567
0.0000
0.0034 on 12/15/2012 11:26:44 AM
0.0028
0.350 MeV
PEAK
Nuclide
1.000E+000
Net
Pk Area
AREA
REPORT
Pk Area
Error %
10.43
57.98
71.82
26.00
Ambient
Backgnd
Backgnd
FWHM
(keV)
3.57
1. 02
O.OOE+OOO
O.OOE+OOO
Reagent
2.9
3.7
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0. 960
0.940
5685.50*
4785.00*
Activity
(pCi/liter )
4.11E-001 +/- 7.15E+001
1.91E+OOO +/- 5.02E-001
MDA
(pCi/liter
3.71E-001 +/- 6.47E+001
2.08E-001 +/- 7.55E-003
0000057007.CNF
Live Time
10201.000 sec

start:
I 3507. 9(kev)
Stop : 1024 6512.2(kev)
60+
55
50
45
40
35
Vl
+-'
<=
8 30
25
20
15
10
5
0
4000
t!~
t~
!lil
1~1
ROI
Type: 1
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
Page
5/3/2013
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
06
Elapsed Live time:

Elapsed Real Time:
10201
10201
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
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137:
145:
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257:
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369:
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1
llltilil2
Channel Data Report

801:
5/3/2013
Fage
1 1 :''H
' :. U -..'.'
Sample Title:
06
809:
817:
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fiL483
Sample Description:
Spectrum File:
Sample Geometry:
D-6 DIS
\\OR-AIPHA1\Canberra\ApexAlpha\Root\Data\00000570
1304106A-RA
07
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_018
18
System Bkgd 55740
<not performed>
Sample Size:
Sample Date/Time:

2. 720E+000
5/2/2013
1:37:25 PM
5:44:51 AM
5/3/2013
170.0 minutes
170.0 minutes
0.8543 +/0.1776 +/0.1518 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
1:57:26 PM
0.350 MeV
Nuclide
0.0000
0.0033 on 12/15/2012
0.0028
1. OOOE+OOO
REPORT
Pk Area
Error %
Net
Pk Area
5.537
4.574
AREA
16.30
55.13
51.42
26.92
Ambient
Backgnd
1. 70
1.87
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.1
3.1
NDCLIDE ANALYSIS RESULTS
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.972
0.943
5685.50*
4785.00*
Activity
(pCi/liter )
6.16E-001 +/- 1.07E+002

1.75E+OOO +/- 4.74E-001
MDA
(pCi/liter
2.78E-001 +/- 4.84E+001
2.40E-001 +/- 8.74E-003
0000057010.CNF
Start:
l:l404.1(kev)
Stop: 1024:6604.2(kev)
Acq. start :Fri May 03 05:44:51 2013
60+
55
II ~
50
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+-'
c::
8 30
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,f.::t.
!i!!l
(,)1
ROI Type: 1
'
4000
4500
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Energy(kev)
5500
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Channel Data Report
Page
5/3/2013
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
07
Elapsed Live time:

Elapsed Real Time:
10200
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Channel Data Report

369:
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Channel Data Report

801:
5/3/2013
0
Sample Title:
11:1i:!Hi
0
w,
0
Page
0
07
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961:
969:
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993:
1001:
1009:
1017:
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0
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0
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
D-83 TOT
1304106A-RA
08
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_022
22
System Bkgd 55741
<not performed>

3.090E+000
1:37:25 PM
5/2/2013
5/3/2013
5:44:52 AM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.8760 +/0.1531 +/0.1342 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
1:57:26 PM
0.350 MeV
Nuclide
0.0000
0.0029 on 12/15/2012
0.0026
1.000E+000
Net
Pk Area
REPORT
Pk Area
Error %
14.45
77.96
5.507
4.561
AREA
56.63
22.54
Ambient
Backgnd
2.55
2.04
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.1
3.6
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.959
0.936
5685.50*
4785.00*
Activity
(pCi/liter )
7.02E-001 +/- 1.22E+002

3.17E+OOO +/- 7.25E-001
MDA
(pCi/liter
4.08E-001 +/- 7.10E+001
3.17E-001 +/- 1.18E-002
0000057011.CNF
start:
1:3421.5(kev)
stop : 1024:6608.8(kev)
Acq. start :Fri May 03 05:44:52 2013
60+
55
II
50
45
40
...
35
V>
r:::
8 30
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5
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lli!i
$.~
~"t>!l'
ell
ROI Type: 1
4000
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/3/2013
11:19 :.(!V'
Page
*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
08
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
9:
17:
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33:
41:
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57:
65:
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81:
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m411
Channel Data Report

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Sample Title:
Page
11:19:0'1 1\M
0
08
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0
nl412
Channel Data Report

801:
Page
5/3/2013
0
Sample Title:
08
Channeli------I-------I-------I-------I-------I-------1-------I-------J
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0
0
1
0
0
U13
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
D-83 DIS
1304106A-RA
09
Shelf 2
Ra
Alpha_024
24
System Bkgd 55742
<not performed>
2.960E+000
5/2/2013
1:37:25 PM
5:44:54 AM
5/3/2013
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.9145 +/0.1710 +/0.1564 +/-
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
Net
Pk Area
5.534
4.565
0.0000
0.0032 on 12/15/2012
0.0029
AREA
2:02:15 PM
REPORT
Pk Area
Error %
9.43
53.66
1.000E+OOO
Ambient
Backgnd
76.67
26.86
3.57
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.1
3.9

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.970
0.938
5685.50*
4785.00*
Activity
(pCi/liter )
3.76E-00l +/- 6.56E+001
1.79E+000 +/- 4.86E-001
MDA
(pCi/liter
3.76E-00l +/- 6.56E+001
1.60E-001 +/- 5.85E-003
0000057012.CNF
start:
1 l411.6(kev)
Stop : 1024 6597 .O(kev)
60+
55
II
50
45
40
35
Vl
+-'
<=
8 30
25
20
15
10
5
0
'
3500
~
t~~.
""'
Ul
ROI Type: 1
4000
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/3/2013
11:19; J,i'
Page
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
09
Elapsed Live time:

Elapsed Real Time:
10200
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1
_fi!-lt16
Channel Data Report

369:
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:6417
Channel Data Report

801:
5/3/2013
0
Sample Title:
Page
11:19:1'1'1 !AM
0
09
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921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
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l!l418
pex-Aipha
TM
Sample Description:
Spectrum File:
Sample Geometry:
Procedure Description:.
DUP 05 TOT
1304106A-RA
10
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_025
25
System Bkgd 55743
<not performed>
Sample Size:
Sample Date/Time:

2.840E+000
1:37:25 PM
5/2/2013
5:44:55 AM
5/3/2013
170.0 minutes
170.0 minutes
0.7706 +/0.1736 +/0.1337 +/-
Chern. RecoverY Factor:

PEAK
Energy
(MeV)
RA-224
RA-226
5.543
4.606
1:57:27 PM
0.350 MeV
Nuclide
0.0000
0.0032 on 12/15/2012
0.0025
1. OOOE+OOO
AREA
Pk Area
Error %"
Net
Pk Area
13.13
33.98
58.42
34.21
REPORT
Ambient
Backgnd
1.87
1. 02
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.1
4.7
Nuclide
Id
Con.
Energy
(keV)
RA-224
RA-226
0.974
0. 959
5685.50*
4785.00*
Activity
(pCi/liter )
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1.27E+OOO +/- 4.39E-001
MDA
(pCi/liter
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2.36E-001 +/- 8.63E-003
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Channel Data Report
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Channel Data Report

801:
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0
Sample Title:
11; l!Ot '"

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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
DUP 05 DIS
1304106A-RA
11
Shelf 2
Ra
Alpha_027
27
System Bkgd 55744
<not performed>
Sample Size:
Sample Date/Time:

2.740E+000
5/2/2013
1:37:25 PM
5:44:56 AM
5/3/2013
170.0 minutes
170.0 minutes

0.8708 +/0.1728 +/0.1504 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
0.0000
0.0032 on 12/15/2012
0.0028
AREA
Net
Pk Area
Ambient
Error %
Backgnd
9.30
26.47
70.81
39.36
2:27:41 PM
REPORT
Pk Area
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4.566
1.000E+000
1. 70
1.53
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Reagent
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O.OOE+OOO
O.OOE+OOO
3.2
3.2
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.969
0.939
5685.50*
4785.00*
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3.57E-001 +/- 6.23E+001
8.52E-001 +/- 3.37E-001
MDA
(pCi/liter
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2.29E-001 +/- 8.40E-003
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Channel Data Report
5/3/2013
11:1;~Jjf
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p E C T R A L
DATA
R E P 0 R T
*****
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Elapsed Live time:

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0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-102-SS TOT
1304106A-RA
12
Shelf 2
Ra
Alpha_029
29
System Bkgd 55745
<not performed>
Sample Size:

1.550E+000
1:37:25 PM
5/2/2013
5/3/2013
5:44:57 AM
170.0 minutes
l70. 0 minutes
Sample Date/Time:
0.5312 +/0.1945 +/0.1033 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5.523
4.589
Net
Pk Area
0.0000
0.0036 on 12/15/2012
0.0019
AREA
23.77
11.28
2:30:02 PM
REPORT
Pk Area
Error %
70.13
303.64
1.000E+000
Ambient
Backgnd
1.87
1.36
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
7.0
3.7

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.966
0.951
5685.50*
4785.00*
Activity
(pCi/liter )
2.22E+OOO +/- 3.87E+002
8.05E+OOO +/- 9.52E-001
MDA
(pCi/liter
2.40E-001 +/- 4.17E+001
1.82E-001 +/- 6.54E-003
0000057015.CNF
start:
13413.5(kev)
Stop : 1024 6597.5(kev)
60
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5/3/2013
11 : ;a4 : ,@f
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*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
12
Elapsed Live time:

Elapsed Real Time:
10200
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Channel Data Report

801:
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1
1
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0
2
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3
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0
2
0
1
1
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0
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0
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0
0
1
1
0
0
1
0
0
pex-Aipha
PZ-102-SS DIS
1304106A-RA
13
Shelf 2
Ra
Detector Name:
Env. Background:
Alpha_033
04026479A
91132
System Bkgd 55746
Sample Description:
Spectrum File:
Sample Geometry:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.040E+000
5/2/2013
1:37:25 PM
8:20:23 AM
5/3/2013
170.0 minutes
170.1 minutes
0.8371 +/0.1825 +/0.1527 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5. 521
4. 593
1. OOOE+OOO
Net
Pk Area
48.66
194.32
0.0000
0.0032 on 12/16/2012
0.0027
AREA
5:49:18 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
28.21
14.09
0.34
0.68
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
4.5
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.965
0.953
5685.50*
4785.00*
Activity
(pCi/liter )
1.40E+OOO +/- 2.83E+002

4.58E+000 +/- 6.65E-001
MDA
(pCi/liter
1.37E-001 +/- 2.78E+001
1.33E-001 +/- 4.58E-003
0000057025.CNF
start:
1 3465.6(kev)
stop : 1024 6503.3(kev)
60+
55
50
45
40
35
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.....
c:
8 30
25
20
15
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ROI Type: 1
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4000
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Energy(kev)
5500
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5/3/2013
11:20::1~
Page
AM
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
13
Elapsed Live time:

Elapsed Real Time:
10200
10205
1:
9:
17:
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41:
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~L437
Channel Data Report

801:
5/3/2013
0
Sample Title:
Page
u~~~U:j!i
13
ChannelJ------I-------I-------I-------I-------1-------I-------I-------J
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pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-102R-SS TOT
1304106A-RA
14
Shelf 2
Ra
Alpha_034
04026479B
91136
System Bkgd 55747
<not performed>

4.000E+000
5/2/2013
1:37:25 PM
8:20:24 AM
5/3/2013
170.0 minutes
170.1 minutes
Sample Size:
Sample Date/Time:
0.3965 +/0.1856 +/0.0736 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
AREA
6.83
33.15
76.08
34.55
5:49:43 PM
REPORT
Pk Area
Error %
Net
Pk Area
5.544
4.624
0.0000
0.0032 on 12/16/2012
0.0013
1. OOOE+OOO
Ambient
Backgnd
0.17
0.85
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.0
4.5

Nuclide
RA-224
RA-226
Id
Conf.
Energy
(keV)
0.974
5685.50*
4785.00*
0. 967
Activity
(pCi/liter )
7.99E-001 +/- 1.62E+002
3.18E+OOO +/- 1.11E+000
MDA
(pCi/liter
4.88E-001 +/- 9.88E+001
5.75E-001 +/- 1.96E-002
0000057026.CNF
Real rime 10205.000 sec
start:
1 3439.1(kev)
stop : 1024 6479.9(kev)
60
55
50
45
40
35
Vl
+-'
<::
::::s
8 30
25
20
15
10
5
0
3500
tl!i
t':~
f,;it,,
I~
ROI Type: 1
4000
4500
5000
Energy(kev)
5500
6000
Channel Data Report
5/3/2013
:11 ' 2{>-t ~'~
Page
1.
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
14
Elapsed Live time:

Elapsed Real Time:
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BA.41
Channel Data Report

369:
5/3/2013
0
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11 : 2.0 l
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mliit2
Channel Data Report

801:
5/3/2013
0
Sample Title:
Page
11:20:38 AM
0
14
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-102R-SS DIS
1304106A-RA
15
Shelf 2
Ra
Alpha_035
04026477A
58771
System Bkgd 55748
<not performed>
Sample Size:

2.000E+000
5/2/2013
1:37:25 PM
8:20:19 AM
5/3/2013
170.0 minutes
Sample Date/Time:
170.1 minutes
0.7970 +/0.1826 +/0.1455 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
1.000E+000
0.0000
0.0032 on 12/16/2012
0.0025
AREA
REPORT
Net
Pk Area
Pk Area
Error %
5. 499
4.598
19.66
77.49
5:49:42 PM
Ambient
Backgnd
44.65
22.35
0.34
0.51
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
2.9
3. 9

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.955
0.956
5685.50*
4785.00*
Activity
(pCi I liter )
5.82E-001 +/- 1.18E+002
1.88E+OOO +/- 4.25E-001
MDA
(pCi/liter
1.41E-001 +/- 2.86E+001
1.27E-001 +/- 4.36E-003
0000057027.CNF
Live Time
Real rime
start:
I
stop : 1024
Acq. Start
60
10200.000 sec
10205.000 sec
3463 .4(kev)
6473.5(kev)
Fri May 03 08:20:19 2013
55
50
45
40
35
V>
......
s::
8 30
25
20
15
10
5
I
ur1 1,
0
'
3500
Ia
'~~~.
t'.28,
IJ'n
ROI Type: 1
4000
4500
5000
Energy(kev)
5500
6000
Channel Data Report
5/3/2013
Page
11:20:4"'.
*******************************************************
*****
T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
15
Elapsed Live time:

Elapsed Real Time:
10200
10205
1:
9:
17:
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33:
41:
49:
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i\l<U'S
Channel Data Report

369:
5/3/2013
1
Sample Title:
Bage
H2(;);~ '"'A.. ,, , .1
15
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'ntitt17
Channel Data Report

801:
5/3/2013
1
Sample Title:
11::2CI~It
.w
0
Page
0
15
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pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-104-SD TOT
1304106A-RA
16
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_037
04026478A
91133
System Bkgd 55750
<not performed>
Sample Size:
Sample Date/Time:

2.370E+000
5/2/2013
1:37:25 PM
8:20:21 AM
5/3/2013
170.0 minutes
170.1 minutes
0.7010 +/0.1783 +/0.1250 +/-

Energy
(MeV)
RA-224
RA-226
5.539
4.592
3:28:25 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0033 on 1/26/2013
0.0023
1.000E+OOO
Net
Pk Area
32.83
170.66
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
34.31
15.02
0.17
0.34
O.OOE+OOO
O.OOE+OOO
2.9
3.7

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.972
0.952
5685.50*
4785.00*
Activity
(pCi/liter )
1.34E+OOO +/- 2.71E+002
5.72E+000 +/- 8.84E-001
MDA
(pCi/liter
1.70E-001 +/- 3.45E+001
1.60E-001 +/- 5.83E-003
0000057028.CNF
start:
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stop : 1024 6468.5(kev)
60
55
50
45
40
35
...,c:
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8 30
25
20
15
10
5
0
'
3500
11101
g~~
Ul
~!1;1
ROI Type: 1
'
4000
4500
5000
Energy(kev)
5500
6000
Channel Data Report
5/3/2013
11:21:1S
Page
*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
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EA52
Channel Data Report

801:
5/3/2013
0
Sample Title:
11:2l:Jrt
1
Page
0
16
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0
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-104-SD DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000570
1304106A-RA
17
Shelf 2
Ra
Alpha_040
06027396B
91135
System Bkgd 55752
<not performed>
Sample Size:

2.500E+000
1:37:25 PM
5/2/2013
8:20:30 AM
5/3/2013
170.0 minutes
170.1 minutes
Sample Date/Time:
0.8922 +/0.1900 +/0.1695 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
5. 490
4.587
5:49:33 PM
0.350 MeV
Nuclide
0.0000
0.0033 on 12/16/2012
0.0029
1. OOOE+OOO
Net
Pk Area
AREA
REPORT
Pk Area
Error %
33.32
144.49
34.36
16.34
Backgnd
Reagent
Backgnd
0.68
0.51
O.OOE+OOO
O.OOE+OOO
Ambient
FWHM
(keV)
3.7
3.3
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.951
0.950
5685.50*
4785.00*
Activity
(pCi/liter )
1.06E+000 +/- 2.14E+002
3.76E+000 +/- 6.28E-001
MDA
(pCi/liter
1.79E-001 +/- 3.62E+001
1.37E-001 +/- 4.65E-003
0000057029.CNF
start:
1 3459.0(kev~
Stop : 1024 6497 .l(kev
60+
55
50
45
40
35
...,c
Vl
8 30
25
20
15
10
5
0
'
3500
ti!lJ
....
Ul
Uli
ROI Type: 1
'
4000
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/3/20B
il:2lt~
Page
*******************************************************
*****
*******************************************************
Sample Title:
17
Elapsed Live time:

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mltss
Channel Data Report

369:
5/3/2013
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Sample Title:
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U57
Channel Data Report

801:
5/3/2013
0
Sample Title:
11: ~;!; t~
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Channelf------l-------l-------f-------f-------l-------f-------1-------l
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Spectrum File:
Sample Geometry:
PZ-104-SS TOT
1304106A-RA
18
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_041
05026930A
91087
System Bkgd 55753
<not performed>
Sample Size:
Sample Date/Time:

2.230E+000
1:37:25 PM
5/2/2013
5/3/2013
8:20:26 AM
170.0 minutes
170.1 minutes
0.9342 +/0.1978 +/0.1848 +/-

Energy
(MeV)
Net
Pk Area
5.494
4.587
RA-224
RA-226
5:49:31 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0034 on 12/16/2012
0.0032
1. OOOE+OOO
9.66
55.81
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
64.35
26.56
0.34
1.19
O.OOE+OOO
O.OOE+OOO
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.953
0.950
5685.50*
4785.00*
Activity
(pCi/liter )
2.51E-001 +/- 5.07E+001
1.19E+000 +/- 3.18E-001
MDA
(pCi/liter
1.24E-001 +/- 2.51E+001
1.40E-001 +/- 4.75E-003
U59
0000057023.CNF
start:
ll452.7(kev)
stop : 1024 6506.6(kev)
60
55
50
45
40
35
V>
......
s:::
:::s
8 30
25
20
15
10
5
0
'
3500
~I
~~
0'1
illl
ROI Type: 1
'
4000
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/3/2013
Page
11:2l~U ~
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
18
Elapsed Live time:

Elapsed Real Time:
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1:
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:m&s1
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Wi!E2
Channel Data Report

801:
5/3/2013
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Sample Title:
11: 2:f :U
0
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0
Page
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18
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-104-SS DIS
1304106A-RA
19
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_042
050269308
84185
System Bkgd 55754
<not performed>
Sample Size:
Sample Date/Time:

2.340E+000
1:37:25 PM
5/2/2013
8:20:28 AM
5/3/2013
170.0 minutes
170 .l minutes
1.0000 +/0.1846 +/0.1846 +/-

Energy
(MeV)
Net
Pk Area
5.519
4.558
RA-224
RA-226
5:49:29 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/16/2012
0.0032
1.000E+000
AREA
REPORT
Pk Area
Error %
11.15
35.98
61.26
33.21
Ambient
Backgnd
0.85
l . 02
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
6.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.964
0.935
5685.50*
4785.00*
Activity
(pCi/liter )
3.04E-001 +/- 6.15E+001
8.06E-001 +/- 2.69E-001
MDA
(pCi/liter
1.63E-001 +/- 3.30E+001
1.41E-001 +/- 4.81E-003
0000057024.CNF
Start:
ll450.2(kev)
stop : 1024 6505.5(kev)
.
60+
55
50
45
40
35
Vl
"'-'
c::
8 30
25
20
15
10
5
0
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3500
~
~~.
tn
t'J1!
ROI Type: 1
'
4000
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4500
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5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/3/2013
11:21:4'~ ~
Page
*******************************************************
*****
P E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
19
Elapsed Live time:

Elapsed Real Time:
10200
10205
1:
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0
0
0
0
1
0
0
0
0
0
0
1
1
0
0
0
0
1
2
1
1
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
2
0
1
1
0
1
0
1
1
1
0
0
0
0
0
0
0
0
1
0
1
0
0
2
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
1
0
1
0
1
0
0
0
0
0
0
1
0
1
0
0
0
1
0
1
0
0
0
0
0
0
1
0
0
0
l
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
3
1
0
0
0
0
0
~AG-6
Channel Data Report

369:
5/3/2013
0
Sample Title:
11: :ill. I~~

0
w
0
Page
1
19
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
1
1
0
1
0
0
0
0
0
0
1
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
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0
0
0
0
0
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0
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0
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0
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0
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0
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0
0
0
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0
0
0
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0
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0
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0
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0
0
0
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0
0
0
0
0
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
2
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
ffl467
Channel Data Report

801:
5/3/2013
0
Sample Title:
Page
11:21:42 AM
0
19
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
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0
0
0
0
0
0
0
0
0
0
~.468
Page 1 of 2
5/3/2013
5:43:48 AM
ex-AI ha
QA SUMMARY REPORT
Date
Time
: 5/3/2013
: 5:43:48 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
2lf
2lf
21f
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
21f
2lf
2lf
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystiOODC
Alpha Analyst] OODC
Alpha Analyst! OODC
Alpha AnalystiOODC
Alpha AnalystiOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
DATE
5/3/2013 5:20:28 AM
5!3120 13 5:20:29 AM
5/3/2013 5:20:30 AM
5!312013 5:20:31 AM
5/3/2013 5:20:32 AM
5/3/2013 5:20:33 AM
5/3/2013 5:20:33 AM
5!3120 13 5:20:34 AM
5/3/2013 5:20:35 AM
5/3/2013 5:20:36 AM
5/3/2013 5:20:37 AM
5/3/2013 5:20:38 AM
5/3/2013 5:20:39 AM
5/3/2013 5:20:40 AM
5/3/2013 5:20:42 AM
4/29/2013 5:29:59 AM
5/3/2013 5:20:43 AM
4/29/2013 5:30:03 AM
5/3/2013 5:20:45 AM
5/3/2013 5:20:46 AM
5/3/2013 5:20:48 AM
Page 2 of 2
Review of QA Results- Pulser Cheek

5/3/2013
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst! OODC
Alpha Analyst!OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
APPROVED BY:
APPROVAL DATE:
FLAG
Passed
Passed
Not Done
Passed
Passed
Passed
5"4348 AM
DATE
4/29/2013 5:30:09 AM
5/3/2013 5:20:50 AM
5/3/2013 5:20:51 AM
5/3/2013 5:20:53 AM
5/3/2013 5:20:55 AM
6/12/12
Page
12:16:17 PM
*************************************************************************
LIBRARY
*****
LISTING
REPORT
*****
*************************************************************************
Radium
Nuclide
Name
Half-Life
(Seconds)
Energy
(keV )
P0-218
RN-222
RA-226
5.049E+010
5.049E+010
5.049E+010
6003.000*
5490.000*
4785.000*
Ra-226, Po-218, Rn-222

Energy
Uncert. (keV
0.000
0.000
0.000
Yield
(%)
99.9800
99.9200
100.0000
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0.0000
key line
TOTALS:
Nuclides
Energy Lines
~L471
SECTION XI
ANALYTICAL DATA (RADIUM-228)
t!l472
Eberline Services
Analysis Sheet
Printed: 5/14/2013 2:10PM

Page1 of3
13-04106
Ra228
Run 1
Sample
Desc
Work Order
Client
ID
Login
Sample
Date
CPM
LCS
02
4/16/2013
Date Received
Client
~--
04
05
Project
West Lake OU-1
i ---
DO
PZ-111-KS DIS
06
Activity Units
07
_,______
TRG
___________
D-6
,,_
TOT
----------
--
D-6 DIS
04/16/13 00:00
1.5000E+OO
1S:~5
1.5oaaE-:aa
04/09/13
------ ---------1
04/09/13 15:35
D-83
--
--+
43
~--45
!
45
__ _)___ ______ _
-------------
TRG
pCi
1.0000E+OO
1.5000E+OO
1 ---
-----
--
Report Level
TOT
PZ-111-KS
. -- __ _j_-- ----
----j-----c-- ----- . -----~---~~---

03
i
DUP i
PZ-111-KS TOT
,
43
5/7/2013
Lab Deadline
04/16/13 00:00
BLANK____,
MBL
Sample
Aliquot
TOT
04/09/13 15:35
04/09/1315:45
1.5000E+OO
04f09/1~1_5~~~~5~~a~:o;;
.
16:1~tl_
---
- - "" ..
1.5000E+OO
----~-----------
40
04/09/13
40
04/09/13 16:16
---
.. -
-------
1.5000E+OO
--
TRG
Aliquot Units
Matrix
WA
10
D-83 DIS
TRG
1----
TOT
47
DUP 05 DIS
DUP 05
EPA 904.0 Modified
11
TRG
---
- -------- ... ------
Instrument Ty~~--Radiometric Tracer
Alpha/B~t<J-~PC
12
'
47
. ----. - . .. i--- .
04/09/13~~~~~-L _1.~oooE+oo
39
04/11/13 09:1 0
Ba-133
13
PZ-102-SS DIS
39
1.5000E+OO
PZ-102R-SS TOT
45
04/11/1309:10 I
--T-04/11/1311:30 i
1.5000E+OO
-----------
-----
PZ-102-SS TOT
TRG
---------
TRG
Ba-6a
14
TRG
Carrier
ICarrier Cone (mg/ml)
-- ---
-------
1009.047
15
TRG
PZ-102R-SS DIS
45
04/11/1311:30
Yttirum
16
TRG
PZ-104-SD
TOT
44
04/11/13 11 :38
------
35
17
TRG
1.5000E+OO
-- ---------
------------
Tracer Act (dpm/g)
1.5000E+OO
! ------
Radiometric Sol#
04/09/13 00:00
-----
Method
1.5000E+OO
--t------- .
-- -
----------
---
PZ-104-SD DIS
-+'
--------
1.5000E+OO
1.5000E+OO
- - - - - - - -
------
44
04/11/1311:38
1.5000E+OO
42
04/11/1312:59
1.5000E+OO
42
04/11/13 12:59
1.5000E+OO
--------
18
TRG
PZ-104-SS
TOT
--
19
TRG
--
PZ-104-SS DIS
Ia
!;:;.
...,_~
(..)
" SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
""Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
13-04106
Ra228
Printed: 5114/2013 2:10 PM

Page 2 of 3
Run 1
Internal I Sample
Fraction ' Desc
Tracer Total
Tracer
Aliquot (g)
~-Radiometric ,
Radiometric
Tracer (pCi)
ACT(dpm}
%Rec
-- --[--1
~~
-~
-~
Grav
%Rec
Mean
%Rec
SAF
SAF
2.
:::
01
LCS
02
MBL
03
DUP
04
DO
05
TRG
77.77[1.aa 11.00
06
TRG
41.9of1-.oo . 1.oo
07
TRG
72.25~-~~?l_~o_o
08
TRG
73.96! 1.00
09
TRG
59.44. 1.oo
10
TRG
65.2~_1:00
I ~00.
11
TRG
12
TRG
~-::t I ::
4f~O~??
72_.3____
81.62,
1.00~00
,_ t---
1.00
+- ----
--- +
344.1
0.9020
910.2
51.62! 1.00 1.00
21.62r1.oo l1.oo
53.12
217.8
1.oo
---t---
13
TRG
0.9038
912.0
343.9
83.71
60.87r-1.oo-l1.00
14
TRG
0.9034
911.6
162.8
39.65i
16.GOr1.ooT
79.70!
36.89[1~~iL 1.00
---- _j_ __ --- ---
-----
15
TRG
0.9002
16
TRG
17
TRG
- -
------
812.3
0.8050
----
-----
326.1
908.3
. ----
---
0.9010
--------
;--
70.10
256.5
!
52.29.
36.65r 1.00
~--
i- --
-------j
1-~oo
909.2
365.4
89.22
85.57,
918.9
386.7
93.42
87.00
424.9
103.68
63.00
1.00
--
76.3~L 1.oo
---
18
TRG
0.9107
'
81.28
1.00
- -- - --------
19
TRG
0.9016
909.8
65.32
1.00
IIi
~
~;::..
**Actual mass exceeded the calibration cwve range. Results should be qualified as appropriate.
1.00
Eberline Services
Analysis Sheet
Run 1
I Sample
Internal
Fraction
Desc
01
Rough Prep
Date
Rough Prep
Prep
Date
By
LCS
02
MBL
03
DUP
-----
---+---- --i
LWALKER
-~-~----~--1
---:
------~
JBARNARD
---- ----t
Sept1
Date/Time
Sep t1
05/14/13 05:59
RMARTZ
~~~--------+--. --~~-~~ ~- -~
I
05/02/1313:37
By
~-
~~--
LWALKER ! 05/14/13 05:59
RMARTZ
~~-------~ ----
-~--~
RMARTZ
08
TRG
09
TRG
----:-
10
TRG
11
TRG
12
TRG
~--+'--~~~~~~------~-~~
---
' ----
04/25/13 09:07
------------
TRG
---
--
--------.-.---:-- . .
-------------~:
JBARNARD
05/02/13 13:37
--
-------------- - - - - - - - .
__ _L__~
04/25/13 09:07
TRG
------:----------------;-----------------
--------
-.
RMARTZ
' 05/14/13 05:59
RMARTZ
05/02/13 13:37 ' LWALKER
05/14/13 05:59
RMARTZ
JBARNARD+~ 05/02t13 13:3-lrLWALKER
05/14/13 05:59
RMARTZ
JBARNARD
05/14/13 05:59
RMARTZ
05/14/13 05:59
RMARTZ
LWALKER l 05/14/13 05:59
RMARTZ
JBARNARD
-. o4tZSf13-o9:Cl7
I
05/02/1313:37
..
----
05/02/13 13:37
04/25/13 09:07 JBARNARD
--_~_~,
LWALKER
-----;---
---------
LWALKER
------------------
----------
04/25/13 09:07
05/02/13 13:37
JBARNARD
- ------ -----------
RMARTZ
04/25/13 09:07 i JBARNARD . 05/02/13 13:37

----------
[___
04/25/13 09:07
JBARNARD
--
-- ------- ----- ---
04/25/13 09:07
______
04/25/13 09:07
JBARNARD
..
RMARTZ
05/02/13 13:37
- - - - - - - - - - - - - --
05/02/13 13:37
LWALKER
05/14/13 05:59
RMARTZ
LWALKER
05/14/13 05:59
RMARTZ
LWALKER
05/14/13 05:59
RMARTZ
------------
-- ---------
TRG
RMARTZ
. 04/25/13 09:07
1=-
RMARTZ
05/14/13 05:59
I
I
~~- ~-- ~~ ~~
05/14/13 05:59
--------.
TRG
--------
'
:
TRG
-----
LWALKER
___ j____ ___ 04/~~~3-~9:07 I JBARNARD 05/0~~!_1~~3!1L_WJ~LKER
TRG
04/25~~3-~fj:07_j_JBARNARD _ 05/02!~1~:~7 ]__L\f\/~L_K:~
____ j _ _
TRG
14
---+
--- ---+-LWALKER
---- +-05/14/13 05:59
~
I 04/25/13 09:07 I JBARNARD . 05/02/1313:37
-----------
13
--
JBARNARD
- -------- -- --------- ------+-- - - ---------
19
JBARNARD
04/25/13 09:07
TRG
-----~~~~~
04/25/13 09:07
~ ~ ~ ~~~
TRG
07
17
i JBARNARD
TRG
16
04/25/13 09:07
06
15
SeptO
By
JBARNARD! 05/02/13 13:37
---~~-->~-~-~~--
I 04/25/13 09:07
---
--
04/25/13 09:07
-- ------
SeptO
Date/Time
By
DO
05
Prep
--------
'I
04
18
Printed: 5/14/2013 2:10PM

Page 3 of 3
13-04106
Ra228
JBARNARD
05/02/13 13:37
--
--------
04/25/13 09:07 , JBARNARD ; 05/02/13 13:37
G,i~l
.~,
''"~
tn
.. SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
"*Actual mass exceeded the calibration cwve range. Results should be qualified as appropriate.
Eberline Services
Lab
1
Fraction
01
; Sample
RA-228
Desc
Identification
Client
Activity
Units
LCS
LCS
pCI/1
IError Estimate
Results
~
~
- II 03
~--L-----.
_
QO
ca
~ 0::
DUP
__
TRG
PZ111-KS DIS
RA-228
TRG
07
RA-228
TRG
08
RA-228
TRG
09
RA-228
TRG
. --1~---
*l-~
---+-
13
"g"
li
Jl
_ i
a;
:.:::
t.>
(1)
C)
~
~
RA-228
i-15
I
--------------D-83 DIS
. -+-~-
----
19
1
I
--!----
I
--1--
TRG
-
--.--
., ..
-+-
pCi/1
'
- ..
PZ-102-SS DIS
-------------
~----
PZ-102R-SS TOT
...
--
TRG
TRG
TRG
--
---
1.05E+00j
'
' ..
1.66E+OOI
,
I
pCill
!
1
1.79E+OO[
7.98E+ooi
----+~~~
pCi/1
, 2.35E+OO
7.39E~1 i
1.20E+ooi
6.40E~1 !
1.12E+OO
-____ ,i___ .
'
7.07E-01 [
--t
---~--+
1.61E+ool
2.67E+oo
--
s.s3E~1 1
. ---+-----~---,---------~~---~-;-.
PZ-104-SD TOT
pCi/1
------
.... --+------+--- . - ~----------~------

1
pCI/1
1.90E+oo[ 4.97E~1~ 8.50E~1 l
----- ---- -----
---
PZ-1 04-SS TOT

. ---
1.02E+OO[
pCill
8.04E-011
1.88E+OOj
4.61E~1L8.99E~1,
---L----------+-----!
pCI/1
1.58E+OOj
6.25E~1j
_______ ; ......-..
1.17E+OO'
-'- -- -+-- --- .;..
0_"< +-
j__
OK
. ----~ -----
.!:~.~~.
'-I
1111
--1
-----+----
OK
----- -- ---'
-j-----~~
OK
1---
INV
'
- ----r------r-------------1-.-----
-i
.
-------t--~~--1
INV
C .
-----1-------t
OK
---- -!...
'
--+-~~
OK -r- -I
f-- L
~ --------+----------t---
--~~KI
'
OK--~
-~--
I<~
'
i
--+------------~
1.87E+oo,
- ... ------~-------------- --------1------------+- - -i

I
;
i
---
PZ1 04-SS DIS
2.72E+OO[
OK
--+----
~----+-
pcitl
-------
OK
--
PZ102R-5S DIS
, 1.soE+OO!
OK
-1-------
1.31E+00i
-
------'--6.11 E-~ 1.04E+OO;
I
OK
- -+------1-
p~l/;- -~01 E-01 ;~~~~~0 ~--~~;~:~~~

---t----r-----------r---------: - !
+--
----;-.
____ ,__
'
I
------;-----~-----.,.....
-1---J~~K~l_--------
"'"-------l-
9.45E~1:
Blank
Flag
OK
--------;--
1-------------i-----. ----.J...---
3.78E+Oo['
2.45E+OO
NA
-- ---.
PZ1 04-5D DIS
TRG
TRG
pCi/1
--
PZ-102-5S TOT
TRG
--
----- ------ ----- ------
TRG
-
---------
9.77E~1!
---~r------t--~---- ---~--------
-----r---
DUP 05 DIS
.....-----------
--
-- --
RA-228
4.79E~1~
7.29E01
------------.
TRG
--
RA228
--------------------- .
RA-228
pCi/1
1srRA-228
17 I
! 1.08E+OO
pCi/1
DUPOSTOT
... -
---------L--- ------- -
'i:
D-83 TOT
--. --------
18
c.
Jl
RA228
-----------------------
TRG
---+-- ----L---r~K
:::;;-~f-::::::::1_-~~:_:-_:~_~H;s~I;~[~_-- _:
D-6 DIS
-----------
------
RA228
-f--- ....
14 ,
01
'
-~
pCi/1
5.89E+OO
---+-
-------------------
--
3.74E~11 7.1~=~1-.
4.71E~1~
D-6 TOT
pCi/1
---f
-----------------
os
6.99E011
4.;;E.o11--;:~~~~~1r~+----+--- ----\--- -----'---
------------------------
'
'
Flag
OK
pCitl---1-- 2.62E01
------
PZ-111-KS TOT
DO
RA-228
f.. ~~-j_~RA228
-~-+--
PZ,111-KS TOT
-----------
1'' ---
pCi/1
----------------------
-------
-t--rv:-228
04 I
BLANK
MBL
RA-228
MDA
Flag
RPD
MDA
7.23E+OO
------ -------------
02 I
I-'M
Page 1 of 3
5/14/~U1~ ~:11
Work Order: 13-04106-Ra228-1
Nuclide
Printed:
--
~-----
.. --
Eberline Services
Lab
'
Fraction !
01
&
02
II-- - -
or-
o3
f
.~
RA-228
i Sample
'
Oesc
Sample
Date
LCS
04/16/13 oo:oo
Sample
Aliquot
o5 .-
Radiometric
% Rec
1.ooe+oo'
- ----+---
96.621
RA-228
1 MBL
1
04116/13 oo:oo
1.50E+oo:
----------+------ --
oup
04/09/1315:35
1.5oe+oo
04/09/1315:35
1 DO
- .
1.50E+OO'
RA:;;;--t;~~- -~~~9/1; 15:3;--t-1.50~:~~

RA-228 ____: TRG
~:
: : : : :
09
RA-228
_o4~09/~~~~-~:~JE:oo_
:::I
TRG
Grav
% Rec
97.591
-- --
---~------------1 -----------~--------'--------
06
I'
------,------ --------------+----
RA-228
rd
1 8
-------:- ----- -------------L--
04
10
RA-228
11
RA-228
TRG
86.29
89.78
80.57
89.00
88.66;
----~
87.71
RA-228
13
RA-228--
'g
14
RA-228
uO-
TRG
04/11/13 09:10
TRG
04/11/13_0~:~0--
TRG
j
15
RA-228
16
RA-228
TRG
.~
17
;.;._~;;~
TRG
: TRG
-- :.
:;;
18
li!
19
Cl
-
~
J::;~~,
~~.JI
'"~
53.12
.. 1:=0E+OO
83.71.
--
1.50E+OO
39.65
04/11/1311:30
; -
04/11/1311:38
RA-228
70.10
j-
------RA-228
--------------
1.50E+OO
------TRG
04/11/1312:59
-
41_!1~1_ __
::~
----;;~~-
103.68
-
5/14/2013 5:59
5/14/2013 5:59
_512/20~~3:~t
:: - ~~:;.;:
1.00
___
1.00:
5/2/201313:37
' ------ --
59.291
51.62j
52.00j
27.62,
m~"""
5/14/2013 5:59
------ .... ---------------
1.00 1
5/2/201313:371
5/14/2013 5:59
1.00
5/2/201313:37
5/14/2013 5:59
n=--~-71 I ----~~~~-8~[-~1:0~1
5/212013 13:37'
5/14/2013 5:59
5/2/2013 13:37:
5/14/2013 5:59
5/2/201313:37
5/14/2013 5:59
89.22--
- --1.50E+OO
51212013 13:371
----r------- --"--- --
16.60 i
1 ____ ,___ _j
52.291
93.42'
5/14/2013 5:59
---------------------------1------
1.00._;___
46.29j
c-
5/21201313:37
-;~_n;-- ~:~~: ----;/2/2;1;;;,-~;\
1.00
-- -
36.89j
36.651
'
1.00:
------------j--------------~-----
~~;;;/;;~-1~38 --~-;:;~~:~0
TRG
1.00,
84.7~---:~~28 ___
41.86~
1.50E+OO
-----------------. ---j ------
1.oo:
81.62i
:1
___
79.70;
5/14/2013 5:59
--~14~0~=-~~
1.50E+OO
5121201313:371'
--~21201313:~7:
--------
1.50E+OO
5/14/2013 5:59
----------------t----------------
'
87.08
--------
Cl
72.341
50.86
65.00
1.50E+OO
+----
04/11/13 11:30
-- --
,jl
-~
--
---------
1.oo:
-t--
82.39~
77.06
5/21201313:371
91.71 I
1.50E+OO
Sep t1
Datefflme
------+----- - . ---------------+ -----
91.45
. ------
Sep to
Date/Time
1.oot
83.37:
+ -
rlVI
------------------j
----+-----------:-- ------
04/09/1316:16
04/09/13 00:00
-----
83.09!
+-:
:-
04/09/1300:00
TRG
-j-
12
SAF
'
::::~~;~;:: -i ~~;~:
-r--1.50~;~~--
Mean
85.14
I I
Page 2 of3
% Rec
---------- ----+-- . ------
:5:
t-'flntea: '0/1"+/..!:U IV,
Work Order: 13-04106-Ra228-1
RA-228
.-
~ ~
Nuc
---- -
' -- --------
1.00
--~~;II-------;~.;~r------1.00:
------,----------+' ----
5/2/201313:37
5/14/2013 5:59
5/2/201313:37
5/14/2013 5:59
------
---
--------------
87.00!
81.28!
1.00'
5/21201313:37
5/14/2013 5:59
63.00)
65.32!
1.001
5/2/201313:37;
5/14/2013 5:59
--------~-------------+---- .
I
------------r-----------+------ --- -----.
Eberline Services
Lab
Fraction
&
-1:
8
-~
1;
~
""'
co
Nuclide
Sample
Counting
Halflife
Oesc
Date!Time
{days)
RA-228
LCS
02
RA-228
03
RA-228
04
RA-228
--tI
05/14/13 09:50
LB4110R
MBL
05/14113 09:50
LB4110R
A2 -
DUP
05/14/13 09:50
LB4110R
A3
------- +-------i---
.. ; __
A1
DO
05/14/13 09:50
RA-228
TRG
05/14/13 09:53
LB4110A
-t---------
RA-228
TRG
05/14/13 09:53
B1
--~--
I LB4110A
---- ----------------- ..L_~--------__;--.
~
c
.,.,"'
.:
c
c
c,
w
!:!~
"'"
Oll
-l-
120
179t.966666667i _0.4699
120
195/
TRG
05/14/13 09:53
LB4110A
B3
RA-228
TRG
05/14/13 09:53
LB4110A
64
RA-228
TRG
05/14/13 09:53
LB4110A
C2
. 2~~
120
TRG
05/14/13 09:53
LB4110A
C3
120[
RA-228
TRG
05/14/13 09:53
LB4110A
C4
12
RA-228
TRG
05/14/13 09:53
LB4110A
02
13
RA-228
TRG
05/14/13 09:53
LB4110A
o4
14
RA-228
TRG
05/14/1310:11
LB4110R
B1
RA-228
16
RA-228
TRG
05/14/1310:11
LB4110R
B3
17
RA-228
TRG
05/14/1310:11
LB4110R
B4
TRG
05/14/1310:11
LB4110R
B2
....1....
I
120
568i1.133333333.
120
393[1.316666667
------ ___l
I
'
--!-------- ----
120
05/14/1310:11
LB4110R
RA-228
TRG
05/14/1310:11
LB4110R
0.4578
0.4699
:
120/
2491
1.25' 0.4692
----~----+------t---- ----------;--- .. .
1201
41411.483333333)
0.4682
_l_-~_12_o~--~~---2-89~~~~~6~~~~_a"7~_-_-o:47~1
i
'
120[
1751
----------+-- 1201
1.4,
0.4754
--+--
199!1.183333333,:
--~
250!1.216666667
1
0.4658
12oi
2asl
0.4773
'
'
120[
-,-------1---------t--
TRG
0.4619
+----
-----t-- -----:-
RA-228
0.4691
-~---
34811.466666667 i
-----+ -- -
--
-- - I
0.4713
-----------1-
1.1
. -- . . . ,..
C1
120]
232/1.366666667;
.. - + ----: ---------1---- - -C2
120'
28511.483333333:
-~---1
19
0.4732
423[1.316666667:
----r------~-----t-----
18
1.051
358T1.~~~6~~~~;r 0.449
----+----+ ' . ----
-r
15
0.4809
--120
-+---
11
1.45i
-:=1---2-_3f-~3~;33;;;__ o.~~~-~
--+--
RA-228
0.4776
B2
RA-228
a.
- e~
~
--+-- __ [._________
576/1.133333333'
. !--
__ j_
"'"E"
Eff
120
A4 --
LB4110R
______ ,. _____________ ,_!...~-------- ------
cu
-t:
g_
Counts
Time
N
N
Count
Carrier
Detect
Oti'+J~u
1v
rv
Page 3 of3
Work Order: 13-04106-Ra228-1
01
10
r-nnrea:
0.4705
. --+-.
0.4676
Count Room Report

Internal
Fraction
Sample
Desc
01
LCS
Client
02
MBL
03
Dl
04
Sample
Sample
Date
ID
LCS
. ----------
04/16/13 00:00
------~~
--
Tracer
Aliquot (g)
-Aliquot
1.0000
BLANK
PZ-111-KSTOT
04/09/1315:35 :
: 04/09/13 15:35 i 1.5000

.
-------+
. . ----- 1----- . .
PZ-111-KS DIS
04/09/13 15:35 ' 1.5000
0.9027
PZ-111-KS TOT
05
D-6 TOT
06
r-O~JQg/131SAS_.L 1~5000
D-6 DIS
--+
08
TRG
D-83 TOT
09
TRG
D-83 DIS
10
TRG
DUP 05TOT
1.5000
0.9031
1.5000
0.8786
1.5000
0.9011
915.1047
907
- -+
i
o4to9t13 oo:oo
399.5ooo
96.62
1.00
1.00
370.1000
89.78
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
881.4026
81;
85.43
1.00
1.00
8~_6()
1.00
1.00
91.45
1.00
1.00
1.00
1.00
337.4ooo
--
1.00
88.66
------
--[--
339.2000 '
2703-~ -359~6()()()
886.5487
-- ----------f---
362.5000
909.1513 .
SAF
2.
1.00
I---------------~-
----------,--
SAF
1*
97.59
. ~1 0.8~~71 ~6.3000 : _:~71
0.9010
. 04/09/1316:16
04/09/13 16:16
-.----
0.8735
917.9301
0.8995
1.5000
I --
404.3000
----+--- -
-----------~;-------
04/09/13_1545
; Radiometric i
% Rec
-------+------------- _, _______ _
--j----- ---- -
.-~-------
07
0.9097
0.9069
Radiometric
Tracer (pCi)
919.7463
- t ----
----- --+--------- --------'--------
1.5000
Tracer
ACT(dpm)
0.9115
-----~--------j-
04/16/13 00:00
1.5000
------ ---- ----+----. -------- -t---------1
DO
Printed: 5/14/2013 2:11PM

Page 1 of 1
13-04106-Ra228-1 (pCi/1) in WA
Tracer ID: Ba-6a
----- --+-----
909.2523
----------
11
TRG
DUP 05 DIS
12
TRG
PZ-102-SS TOT
13
TRG
PZ-102-SS DIS
, 04/09/13 00:00
_____ _)_________
I
04/11/13 09:10
04/11/13 09:10
_________
-
14
TRG
PZ-102R-SS TOT
15
TRG
PZ-102R-SS DIS
04/11/1311:30
TRG
-----
877.2655
1.00
1.00
1.5000
0.9020
910.1604
1.00
1.00
;___
1.5000
0.9038
04/11/1311:30
1.5000
PZ-104-SD DIS
1.5000
______
,,
---------
!!~
t:j;.
<.J
to
19
TRG
PZ-104-SS DIS
0.9002
1.5000
0.8050
911.5731
908.3441
04/11/13 11 :38
04/11/13 12:59
812.2828
---------
---~--------
83.71
1.00
1.00
162.8000
39.65
1.00
1.00
326.1000
79.70
1.00
1.00
..
256.5000
70.10
1.00
1.00
89.22
1.00
1.00
- ---------.
1.5000
0.9010
909.1513
365.4000
1.5000
0.9107
918.9391
386.7000
93.42
1.00
1.00
1.5000
0.9016
909.7568
424.9000
103.68
1.00
1.00
TRG
0.9034
343.9000
-----------
~----
04/11/13 11:38
PZ-104-SD TOT
TRG
18
911.9767
.
--------!---- -----------_ _;_
17
0.8694
----!-- ------
16
1.5000
-----------
Eberline Services
Date
Code
Ra228
--~~
Isotope
Ra-228
I
I
r---ccs
LCS & Matrix Spikes-~~

Sol#
Ra~11
Page 1 of 1
Printed: 4/25/2013 9:07AM
Activity
dpmlg
38~94~
Solution
Date
4/25/2013
Approx
Addition
Volume
Used(g)
0.510
Initials
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
LCS
Known
pCi
I
j
89~
0.5108
JBARNARD
4/25/2013 9:06
MS
Error
Estimate
0.457
Added
pCi
oool
LCSD
Error
Estimate
0.000
Known
pCJ
oool
MSD
Error
Estimate
0.000
-'-
Tracers
fraction
Activity
dpm!g
I Solution
Date
Volume
Used(g)
Approx
Addition
Isotope
Sol#
01
Ba-133
BaBa
1009.047 4/25/2013
... 0.9115
1.0000
02
Ba-133
Ba~6a
1009.047 4/25/2013
0.9097
1.0000
03
Ba-133
Ba-6a
1009.047 4/25/2013
0.9069
1.0000
04
Ba-133
Ba~6a
1009.047 4/25/2013
0.9027
1.0000
05
Ba-133
Ba~6a
1009.047 4/25/2013
0.8995
1.0000
06
Ba-133
Ba-6a
0.9010
1.0000
07
Ba-133
Ba~6a
1009.047 4/25/2013
'1009.047 4/25/2013
. 0.8735
1.0000
08
Ba-133
Ba-6a
1009.047 4/25/2013
0.9031
1.0000
09
Ba-133
Ba-6a
1009.047 4/25/2013
0.8786
1.0000
10
Ba-133
Ba6a
1009.047 4/25/2013 I
0.9011
1.0000
11
Ba-133
Ba-6a
1009.047 4/25/2013
0.8694
1.0000
12
Ba-133
Ba-6a
1009.047" 4/25/2013
0.9020
1.0000
o:9o38
1.0000
13
Ba-133
Ba-6a
1009.047 4/25/2013
14
Ba-133
Ba-6a
1009.047 4/25/2013
0.9034
1.0000
15
Ba-133
Ba~6a
1009.047! 4/25/2013
0.9002
1.0000
16
Ba-133
Ba~6a
1009.047 4/25/2013
.. 0.8050
1.0000
17
Ba-133
Ba-6a
1009.047 4/25/2013
0.9010
1.0000
18
Ba-133
Ba~6a
1009.047 4/25/2013
0.9107
1.0000
19
Ba-133 _j
Ba-6a
1009.047 4/25/2013
0.9016
1.0000
m
t~
Version 2.0 08/99
LCS
~
~~.
Tracer
.~
Matrix Spike
Added
pCi
0.00
Error
Estimate
0.00(
Eberline Analytical
Work Order
Run
13-o41os
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
Client ID
LCS
BLANK
PZ-111-KS TOT
PZ-111-KS TOT
PZ-111-KS DIS
D-6 TOT
D-6 DIS
D-83 TOT
D-83 DIS
DUP 05 TOT
DUP 05DIS
PZ-102-SS TOT
PZ-102-SS DIS
PZ-102R-SS TOT
PZ-102R-SS DIS
PZ-104-SD TOT
PZ-104-SD DIS
PZ-104-SS TOT
PZ-104-SS DIS
Analysis Code
Rpt Units
Lab Deadline
Technician
Ra228
liters
5/7/2013
JBARNARD
I 1
Lab
Sample
Type
LCS
MBL
DUP
TRG
TRG
>.. Oil Factor
No ofDils
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
-~-
Dilution Data
Muffle Data
Ratio
-.
POstfPre<>'>:.
..
..
.
.
.
..
...
$t~
();)
'""'
Technician:
.s%>l
Date
Aliquot Data
Ratio
Aliquot
1.0000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO I
1.5000E+OO
1 .5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
---
..
Comments
lll.l
Printed: 4/25/2013 9:09AM

Page 1 of 1
Aliquot Worksheet
J-ff~
N~tEquiv
MS Aliquot Data
.-
1.0000E+OO
1.5000E+OO
1.5000E+OO
1.5000Et00
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.SOOOE+OO
1.5000E+OO
1.5000E+OO
1:5000E+OO
1.5000E+OO
1 .5000E+OO
1.5000E+OO
Aliquot
H-3 Solids Only

Water Added
(ml)
Net Equiv
H3 Dist
Aliq
I
~~==t=---
<
$----
-
..
--f-
~-
.=:J.
=+-=--=
---~---
Eberline Services - Oak Ridge

Version 1.0 9/1999
Printed: 5/14/2013 2:09PM

Page 1 of 1
Gravimetric Worksheet
Gravimetric
Carrier
Analysis
Work Order
Code
Carrier Cone
(mglml)
-------------
Yttirum
Ra228
TRetec I Engineering Management Support, Inc. I Sample
Fraction
Client ID
Type
(g)
-~~~I=
--------------- - - - - - - - -
18
_19_+
~~~
0;1
'""
N
Technician:
PZ-104-SS TOT
----
TRG
1Q4~~-!)1_s_~- rR_<>
}>z..
--
---------------.
(g)
----~~~~2.o6_oo.
--o-.1489
--------------------
.K~~~ri ----- ~ ~~~~ I
-----0:0926.[::::~-~- g, 1282
9.:.0923 !_
__(l:."l_515
0.0911
0.1502
---.------------
~~~~~6
~:~~~~+
-------------
0.0
. 0.0
-- ' ... _0.:_0~:21_1_ . ___0.1430 I
_0,0907 -- .... 0.1200 '
0.0921
0.1245
-----------
-- ----0.0923
0.1289
___O.o!Jo2 T __ o:15o1
-~
------- - - - - - - - - - - - - - - -
2.0000
MMCDOUGALL
0.0921
__
:O:a91:-
t . ,...-;z.
Date:_/_/~
-------
0.1530
-~Jii3~s
-- %----
Filter Net
(g)
- ~:~~~-h-! . . ~:~~~~ I
PZ-111-KS
TO
-- ---------- -----PZ-111-KS DIS
TRG
----D-6
TOT
TRG
- ---------------07
D-6
DIS
TRG -. __
---- ----- - ----n " TOT TRG
1
1
U-HJ DIS
2.0000
09
----------------10
DUP OS TOT
2.0000
11
DUP
05
DIS
TRG
2.00001
I ... -- ..... ------- . - ---
12
PZ-102-SS TOT
TRG
-------
. ---- 2.0000
- -13
_PZ-102:~S Dl~. --- _I~G
2.0000
14 ____ I'_Z.::~02R-SST()T____.. TRG .
2,0000
15
PZ-102R-SS
DIS
TRG
2.0000
. -----------------------------
16
PZ-1 04-SD TOT
TRG
2.0000
-iT -- Pz-1o4:sD-i:lls -- - -TRG- -2.oooo
--:::~~--
Gravimetric
Filter Tare-----, Fnte-r Final
Carrier Added
(ml)
-0.0925
os_
Technician
Filter Data
Carrier Data
35.0000
Recovery
nna::.as
85.14
86.29
--
0.0564 - - - - - -80.57
--n na.?-:t
89.00
:::::
I
U.UO"I'+
87.71
n.
n"la::.a. .
50.86
.. - - - - - - ..~.~::: . - - -84.57
-:.:--
84.43
~~-~-~
11 ruil:;;l:;,
65.00
----84.71
U.U0::7.3 1----------0.0415
59.29
----52.00
. 0.0364 t- -------..: . : : : : ~--- ----- 72.71
..~.~:::I
41.86
---46.29
- ---
52.29
85.57
0.0609
87.00
---
n-~n...t.d1
63.00
::::
u.uttu4
~--
-~
.:=~==
~-~ ~
j -
Sheet1
Detector ID Sample ID Alpha Beta Count Time Voltage

TOD
1304106-01
19
576
120
1400 5/14/13 11:50
A1
1304106-02 18
179
120
1400 5/14/13 11 :50
A2
1304106-03 19
195
120
1400 5/14/1311:50
A3
1304106-04 13
222
120
1400 5/14/13 11 :50
A4
~!
~~II<
((I
1/..t.j!
Page 1
\~\.0
6l~
Sheet1
TOO
1304106-05 23
232
1400 5/14/13 11:53
120
B1
1304106-06 20
423
1400 5/14/1311:53
B2
120
1304106-07 16
358
120
1400 5/14/13 11 :53
B3
568
1400 5/14/1311:53
1304106-08 21
120
B4
1400 5/14/13 11:53
1304106-09 16
393
120
C2
1304106-10 17
348
1400 5/14/1311:53
120
C3
1304106-11
249
1400 5/14/13 11:53
9
120
C4
1304106-12 30
414
120
1400 5/14/13 11:53
02
1304106-13 17
289
1400 5/14/1311:53
120
04
!iii~
!>;.
(10
t,.,,
Page 1
~\\)
51
IW
Sheet1

TOO
1304106-18 18
1400 5/14/1312:11
232
120
C1
1400 5/14/13 12:11
285
120
C2
1304106-19 21
1304106-14 12
1400 5/14/13 12:11
B1
175
120
1304106-15 13
1400 5/14/13 12:11
B2
199
120
1304106-16 12
250
1400 5/14/1312:11
120
B3
1400 5/14/13 12:11
285
120
B4
1304106-17 21
!i~
.t~
00
U1t
Page 1
~,o
'5\\~
Eberline Analytical
GPC Detector Report
g,.
l;):li
Ill)
Detector
Alpha/Beta
Calibration Date
Count Date
Bkg CPM
PFW
LCL
Mean
UCL
LB4110A- A1
Alpha
11/18/2007
5/14/2013
6.67E-02
-2.18E+01
2.93E-01
2.24E+01
LB4110A- A2
Alpha
11/18/2007
5/14/2013
1.67E-02
-1.85E+01
2.62E-01
1.90E+01
LB4110A- A3
Alpha
11/18/2007
5/14/2013
5.00E-02
-1.80E+01
2.23E-01
1.84E+01
LB4110A- A4
Alpha
11/18/2007
5/14/2013
8.33E-02
-1.91E+01
2.44E-01
1.96E+01
LB4110A- 81
Alpha
11/18/2007
5/14/2013
5.00E-02
-9.87E-02
7.50E-02
2.49E-01
LB4110A- 82
Alpha
11/18/2007
5/14/2013
6.67E-02
-7.93E-02
7.28E-02
2.25E-01
LB4110A- 83
Alpha
11/18/2007
5/14/2013
1.33E-01
-6.40E-02
5.32E-02
1.70E-01
LB4110A- 84
Alpha
11/18/2007
5/14/2013
8.33E-02
-1.43E-01
7.92E-02
3.02E-01
LB4110A- C1
Alpha
11/18/2007
5/14/2013
2.17E-01
-1.52E-01
8.93E-02
3.31E-01
LB4110A- C2
Alpha
11/18/2007
5/14/2013
8.33E-02
-1.80E-01
8.81E-02
3.56E-01
LB4110A- C3
Alpha
11/18/2007
5/14/2013
6.67E-02
-1.76E-01
l.01E-01
3.78E-01
LB4110A- C4
Alpha
11/18/2007
5/14/2013
6.67E-02
-6.26E-02
6.88E-02
2.00E-01
LB4110A- D1
Alpha
11/18/2007
5/14/2013
1.67E-02
-5.36E-02
8.40E-02
2.22E-01
LB4110A- D2
Alpha
11/18/2007
5/14/2013
1.50E-01
-7.02E-02
6.05E-02
1.91E-01
1.91E-01
LB4110A- D3
Alpha
11/18/2007
5/14/2013
3.33E-02
-4.76E-02
7.18E-02
LB4110A- D4
Alpha
11/18/2007
5/14/2013
5.00E-02
-5.74E-02
7.09E-02
1.99E-01
LB4110R- A1
Alpha
11/24/2006
5/14/2013
1.17E-01
-1.01E-01
1.01E-01
3.03E-01
LB4110R- A2
Alpha
11/24/2006
5/14/2013
1.17E-01
-9.00E-02
7.75E-02
2.45E-01
LB4110R- A3
Alpha
11/24/2006
5/14/2013
1.33E-01
-7.34E-02
7.68E-02
2.27E-01
LB4110R- A4
Alpha
11/24/2006
5/14/2013
3.33E-02
-5.29E-02
7.17E-02
1.96E-01
LB4110R- 81
Alpha
11/24/2006
5/14/2013
l.OOE-01
-9.57E-02
6.20E-02
2.20E-01
LB4110R- 82
Alpha
11/24/2006
5/14/2013
8.33E-02
-6.95E-02
6.43E-02
1.98E-01
LB4110R- 83
Alpha
11/24/2006
5/14/2013
1.17E-01
-6.52E-02
7.01E-02
2.05E-01
LB4110R- 84
Alpha
11/24/2006
5/14/2013
5.00E-02
-6.47E-02
7.08E-02
2.06E-01
LB4110R- C1
Alpha
11/24/2006
5/14/2013
1.17E-01
-7.79E-02
7.43E-02
2.27E-01
2.20E-01
LB4110R- C2
Alpha
11/24/2006
5/14/2013
1.67E-02
-7.54E-02
7.21E-02
LB4110R- C3
Alpha
11/24/2006
5/14/2013
6.67E-02
-8.90E-02
8.47E-02
2.58E-01
LB4110R- C4
Alpha
11/24/2006
5/14/2013
8.33E-02
-6.23E-02
8.20E-02
2.26E-01
LB4110R- D1
Alpha
11/24/2006
5/14/2013
O.OOE+OO
-9.95E-02
7.29E-02
2.45E-01
-7.36E-02
7.23E-02
2.18E-01
7.20E-02
2.23E-01
LB4110R- D2
Alpha
11/24/2006
5/14/2013
O.OOE+OO
LB4110R- D3
Alpha
11/24/2006
5/14/2013
O.OOE+OO
-7.89E-02
-7.04E-02
7. 70E-02
2.24E-01
-1.56E-02
9.58E-02
2.07E-01
LB4110R- D4
Alpha
LB5100 - 1
Alpha
------
--
Printed: 5/14/2013 6:52AM

Page 1 of 1
(ALL Backgrounds)
------
.....
11/24/2006
5/14/2013
O.OOE+OO
7/10/2006
10/26/2007
5.00E-02
.:.-.-
-.<.
Jltl.f(t?
Eberline Analytical
GPC Detector Report
Printed: 5/14/2013 6:52AM

Page 1 of 1
(ALL Backgrounds)
C---
t,~,
!>;,
(10
~ ... JI
Detector
Alpha/Beta
LB4110A- A1
Beta
Calibration Date
11/18/2007
Count Date
Bkg CPM
PFW
LCL
Mean
UCL
5/14/2013
8.106+00
-2.966+02
7.636+00
3.116+02
LB4110A - A2
Beta
11/18/2007
5/14/2013
3.25E+OO
-3.116+01
2.55E+OO
3.626+01
L84110A- A3
Beta
11/18/2007
5/14/2013
L256+00
. -5.136+01
2.67E+OO
5.66E+01
L84110A- A4
Beta
11/18/2007
5/14/2013
7.176+00
-3.33E+01
3.046+00
3.946+01
LB4110A- 81
Beta
11/18/2007
5/14/2013
L43E+00.
-L04E+01
3.25E+00
L69E+01
L84110A- B2
Beta
11/18/2007
5/14/2013
L326+00
-7.546+00
L99E+00
L15E+01
2.626+00
LB4110A- B3
Beta
11/18/2007
5/14/2013
L32E+OO
L06E-01
L36E+00
LB4110A- 84
Beta
11/18/2007
5/14/2013
L13E+00,
-7.60E+OO
L97E+00
L15E+01
LB4110A- C1
Beta
11/18/2007
5/14/2013
L476+00.
-5.50E+OO
2.15E+OO
9.80E+00
L84110A- C2
Beta
11/18/2007
5/14/2013
L326+00
3. 79E-01
L27E+OO
2.16E+OO
LB4110A- C3
Beta
11/18/2007
5/14/2013
L47E+00.
4.696-01
1.476+00
2.46E+OO
LB4110A- C4
Beta
11/18/2007
5/14/2013
L256+00.
-L 77E+OO
2.146+00
6.056+00
-2.386+00
2.58E+OO
7.556+00
-6. 79E-01
L576+00
3.816+00
LB4110A- D1
Beta
11/18/2007
5/14/2013
L976+00
L84110A- D2
Beta
11/18/2007
5/14/2013
L486+00
LB4110A- D3
Beta
11/18/2007
5/14/2013
4.276+00
L23E+OO
4.476+00
7.726+00
-4.496-01
L376+00
3.206+00
L84110A- D4
Beta
11/18/2007
5/14/2013
1.126+00
L84110R- A1
Beta
11/24/2006
5/14/2013
L136+00
-6.196+01
3.776+00
6.956+01
5.336+01
L84110R- A2
Beta
11/24/2006
5/14/2013
9.676-01 '
-4.926+01
2.056+00
LB4110R- A3
Beta
11/24/2006
5/14/2013
1.456+00.
-4.556+01
2.796+00
5.116+01
LB4110R- A4
Beta
11/24/2006
5/14/2013
1.056+00
-4.546+01
2.026+00
4.956+01
LB4110R- 81
Beta
11/24/2006
5/14/2013
L40E+OO.
-4. 786+01
2.056+00
5.196+01
L84110R- B2
Beta
11/24/2006
5/14/2013
1.186+00.
-4. 786+01
2.086+00
5.206+01
LB4110R- 83
Beta
11/24/2006
5/14/2013
L22E+OO.
-4.766+01
2.716+00
5.306+01
LB4110R- B4
Beta
11/24/2006
5/14/2013
L106+00"
-4. 796+01
L956+00
5.186+01
LB4110R- C1
Beta
11/24/2006
5/14/2013
L376+00
-4.776+01
3.036+00
5.38E+01
L84110R- C2
Beta
11/24/2006
5/14/2013
1.486+00'
-4.776+01
2.756+00
5.326+01
LB4110R- C3
Beta
11/24/2006
5/14/2013
L406+00
-4.826+01
2.566+00
5.336+01
LB4110R- C4
Beta
11/24/2006
5/14/2013
L336+00
-5.436+01
2.986+00
6.036+01
LB4110R- D1
Beta
11/24/2006
5/14/2013
0.006+00
-4.516+01
5.776+00
5.666+01
LB4110R- D2
Beta
11/24/2006
5/14/2013
O.OOE+OO
-4.866+01
L956+00
5.256+01
LB4110R- D3
Beta
11/24/2006
5/14/2013
0.006+00
-5.196+01
5.746+00
6.346+01
LB4110R- D4
Beta
11/24/2006
5/14/2013
0.006+00
-4.836+01
2.326+00
5.296+01
LB5100 - 1
Beta
7/10/2006
10/26/2007
4.526+00
-3.19E-01
L586+00
3.486+00
J(f'fli)
Eberline Analytical
GPC Detector Report

(ALL Efficiencies)
Alpha/Beta
Calibration Date
Count Date
Elf
PFW
LCL
Mean
UCL
LB4110A- A1
Alpha
11/18/2007
5/14/2013
0.2446
-0.0186
0.2147
0.4480
LB4110A- A2
Alpha
11/18/2007
5/14/2013
0.2101
-0.0560
0.1726
0.4012
LB4110A- A3
Alpha
Alpha
11/18/2007
5/14/2013
0.2022
-0.0796
0.1615
0.4026
11/18/2007
5/14/2013
0.2155
-0.0580
0.1804
0.4188
0.2203
0.1943
0.2246
0.2549
0.1929
0.2218
0.2506
LB4110A- B1
5/14/2013
Alpha
11/18/2007
5/14/2013
0.2063
LB4110A- B3
Alpha
11/18/2007
5/14/2013
0.2432
0.1294
0.2326
0.3358
LB4110A- B4
Alpha
11/18/2007
5/14/2013
0.2260
0.2090
0.2367
0.2644
LB4110A- C1
Alpha
11/18/2007
5/14/2013
0.2192
0.1973
0.2208
0.2443
LB4110A- C2
Alpha
11/18/2007
5/14/2013
0.2266
0.1966
0.2252
0.2538
LB4110A- C3
Alpha
11/18/2007
5/14/2013
0.2552
0.2228
0.2494
0.2759
0.2215
0.1965
0.2258
0.2550
Alpha
11/18/2007
5/14/2013
LB4110A- D1
Alpha
11/18/2007
5/14/2013
0.2224
0.2036
0.2334
0.2632
LB4110A- D2
Alpha
11/18/2007
5/14/2013
0.2478
0.2278
0.2584
0.2890
LB4110A- D3
Alpha
11/18/2007
5/14/2013
0.2565
0.2314
0.2639
0.2963
0.1819
0.1650
0.1999
0.2347
Alpha
11/18/2007
5/14/2013
LB4110R- A1
Alpha
11/24/2006
5/14/2013
0.2415
0.2031
0.2389
0.2747
LB4110R- A2
Alpha
11/24/2006
5/14/2013
0.2170
0.1899
0.2206
0.2514
LB4110R- A3
Alpha
11/24/2006
5/14/2013
0.2193
0.1964
0.2249
0.2534
fll'f{l)
LB4110R- A4
Alpha
11/24/2006
5/14/2013
0.2483
0.2160
0.2457
0.2755
LB4110R- B1
Alpha
11/24/2006
5/14/2013
0.2194
0.1878
0.2261
0.2644
LB4110R- B2
Alpha
11/24/2006
5/14/2013
0.2075
0.1801
0.2176
0.2490
0.2068
0.2440
0.2550
0.2813
LB4110R- B3
Alpha
11(24/2006
5/14/2013
LB4110R- B4
Alpha
11/24/2006
5/14/2013
0.2226
0.1938
0.2320
0.2702
LB4110R- C1
Alpha
11/24/2006
5/14/2013
0.2119
0.1861
0.2153
0.2445
LB4110R- C2
Alpha
11/24/2006
5/14/2013
0.2202
0.1963
0.2340
0.2064
0.2248
0.2397
0.2533
0.2731
LB4110R- C3
0~
11/18/2007
LB4110A- B2
LB4110A- D4
~"'
Alpha
LB4110A- C4
0:11
(.._.
Detector
LB4110A- A4
4':.'\1;
Printed: 5/14/2013 6:53AM

Page 1 of 1
Alpha
11/24/2006
5/14/2013
LB4110R- C4
Alpha
11/24/2006
5/14/2013
0.2057
0.1858
0.2229
0.2600
LB4110R- D1
Alpha
11/24/2006
5/14/2013
0.0000
0.0366
0.2070
0.3774
LB4110R- D2
Alpha
11/24/2006
5/14/2013
0.0000
0.0424
0.2354
0.4284
LB4110R- D3
Alpha
11/24/2006
5/14/2013
0.0000
0.0417
0.2312
0.4207
LB4110R- D4
Alpha
11/24/2006
5/14/2013
0.0000
0.0319
0.1864
0.3408
LB5100- 1
Alpha
7/10/2006
10/26/2007
0.3368
0.3332
0.3455
0.3578
Eber!ine Analytical
GPC Detector Report

(ALL Efficiencies)
Detector
Alpha/Beta
Calibration Date
Count Date
Eff
PFW
LCL
Mean
UCL
LB4110A- A1
Beta
11/18/2007
5/14/2013
0.5495
0.2037
0.5628
0.9218
LB4110A- A2
Beta
11/18/2007
5/14/2013
0.4894
0.1545
0.4633
0.7722
0.4622
0.0819
0.4571
0.8322
5/14/2013
0.5197
0.1343
0.4878
0.8413
0.4637
0.5306
0.5974
LB4110A- A3
LB4110A- A4
11/18/2007
5/14/2013
LB4110A- B2
Beta
11/18/2007
5/14/2013
0.5036
0.4639
0.5276
0.5913
0.5525
0.3192
0.5321
0.7449
Beta
11/18/2007
5/14/2013
LB4110A- B4
Beta
11/18/2007
5/14/2013
0.5376
0.4922
0.5546
0.6170
LB4110A- C1
Beta
11/18/2007
5/14/2013
0.5048
0.4502
0.5027
0.5552
LB4110A- C2
Beta
11/18/2007
5/14/2013
0.4992
0.4280
0.5011
0.5743
0.6020
0.5277
0.5902
0.6526
Beta
11/18/2007
5/14/2013
LB4110A- C4
Beta
11/18/2007
5/14/2013
0.5229
0.4568
0.5251
0.5933
LB4110A- D1
Beta
11/18/2007
5/14/2013
0.5365
0.4798
0.5542
0.6287
LB4110A- D2
Beta
11/18/2007
5/14/2013
0.5443
0.4904
0.5887
0.6871
LB4110A- D3
Beta
11/18/2007
5/14/2013
0.5964
0.5368
0.6155
0.6942
LB4110A- D4
Beta
11/18/2007
5/14/2013
0.4313
0.3863
0.4734
0.5605
LB4110R- A1
Beta
11/24/2006
5/14/2013
0.5648
0.4814
0.5680
0.6545
LB4110R- A2
Beta
11/24/2006
5/14/2013
0.5153
0.4209
0.5089
0.5968
LB4110R- A3
Beta
11/24/2006
5/14/2013
0.5301
0.4580
0.5398
0.6215
LB4110R- A4
Beta
11/24/2006
5/14/2013
0.6001
0.5101
0.5918
0.6734
LB4110R- B1
Beta
11/24/2006
5/14/2013
0.5255
0.4535
0.5428
0.6320
0.5088
0.4313
0.5202
0.6092
Beta
11/24/2006
5/14/2013
LB4110R- B3
Beta
11/24/2006
5/14/2013
0.6004
0.5016
0.5913
0.6810
LB4110R- B4
Beta
11/24/2006
5/14/2013
0.5275
0.4623
0.5500
0.6376
LB4110R- C1
Beta
11/24/2006
5/14/2013
0.4595
0.4241
0.5032
0.5824
0.5133
0.4503
0.5292
0.6081
LB4110R- C2
t!.l
11/18/2007
5/14/2013
Beta
LB4110R- B2
00
Beta
11/18/2007
0.5144
LB4110A- C3
iJ::;.
Beta
LB4110A- B1
LB4110A- B3
tli:l1
Printed: 5/14/2013 6:53AM

Page 1 of 1
Beta
11/24/2006
5/14/2013
LB4110R- C3
Beta
11/24/2006
5/14/2013
0.5580
0.4814
0.5713
0.6612
LB4110R- C4
Beta
11/24/2006
5/14/2013
0.4923
0.4324
0.5265
0.6206
LB4110R- D1
Beta
11/24/2006
5/14/2013
0.0000
0.0866
0.4950
0.9033
LB4110R- D2
Beta
11/24/2006
5/14/2013
0.0000
0.0981
0.5562
1.0143
LB4110R- D3
Beta
11/24/2006
5/14/2013
0.0000
0.0952
0.5402
0.9852
LB4110R- D4
Beta
11/24/2006
5/14/2013
0.0000
0.0749
0.4447
0.8144
LB5100- 1
Beta
7/10/2006
10/26/2007
0.4428
0.4555
0.4731
0.4906
c....'Jil'fm
SECTION XII
BARIUM-133 ANALYTICAL TRACER DATA
~)P
VAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMAoSCUSRoARCHIVE]SMP_l30410601 GEl BAFIL 191239oCN

PEAK Vl6o9 PE,AKEFF V2o2
SPIKE
2-MAY-2013 00:00:000
1304106-01
FILTER
GEl
0 00:15:00000
25
3o00000
No
Pk It
Energy
Area
Bkgnd
4
4
4
0
2
2
0
0
4
4
0
1
1
2
2
2
2
0
0
4
4
4
3
3
3
0
1
1
0
0
27o90
30o97
34o87
52o63
61.86
65o73
81.33
92o75
112023
116 027
160o54
273o94
276o69
303o0l
307o8l
334o07
337o90
356042
377o50
383o75
387o04
391.60
4l5o06
418093
422022
437o4l
467o93
472 062
5110 31
678ol5
33
1885
536
58
257
81
872
31
221
50
19
17
69
171
34
58
24
564
23
86
247
58
29
23
8
125
23
9
29
9
70
80
91
83
81
106
151
108
84
69
79
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
2-MAY-2013 17:00:33o64
20
29
27
18
20
25
12
16
12
4
13
16
17
9
12
3
7
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
lo5l
lo 39
2o03
2o66
1. 73
1. 74
1. 90
lol6
2002
2007
1. 22
1. 80
1. 80
lo58
2o0l
1. 70
2003
lo74
4o35
1. 83
2008
2005
2013
2o30
2o30
2o00
1. 93
1. 93
1.40
1. 92
28ol4
3lo20
35ol0
52o86
62ol0
65 096
81.56
92o97
ll2o45
116 050
160076
274ol6
276o91
303o22
308002
334o28
338 011
356o63
377 071
383096
387o24
39lo8l
4l5o26
419014
422043
437062
468ol3
472o82
5110 51
678033
Left
Pw
27
27
27
50
57
57
76
89
108
108
159
272
272
299
299
330
330
352
375
381
381
381
409
409
409
434
465
465
508
675
13
13
13
7
13
13
12
8
16
16
7
9
9
14
14
15
15
10
7
14
14
14
24
24
24
7
12
12
9
7
2-MAY-2013 16:45:150
loOOOOOE+OO filter
0
BAFIL
0 00:15:00028 0.0%
4096
lOoOOOOO
Cts/Sec %Err
3o65E-02
2o09E+00
5o95E-01
6o44E-02
2o85E-Ol
8o99E-02
9o69E-01
3o4lE-02
2o46E-01
5o6lE-02
2 ol3E-02
lo89E-02
7o62E-02
1. 89E-01
3o77E-02
6o39E-02
2o67E-02
6o27E-01
2o57l;i:-02
9o5lE-02
2o75E-01
6o48E-02
3o26E-02
2o53E-02
9o03E-03
1. 39E-Ol
2o50E-02
9 o72E-03
3o21E-02
1. OOE-02
38o7
2o4
6o6
29ol
8o3
23o3
4o4
61.5
9o2
36o9
79o6
31.6
l5o5
806
3004
l8o5
4402
4o5
32o4
l3o5
7o6
1602
2600
3902
99o6
9o8
30o0
63ol
24o8
33o3
Fit
6o84E+Ol
8o82E+00
2o2lE+00
lo09E+Ol
6o06E+00
3o96E+00
lo94E+01
2o03E+00
1. 63E+00
Summary of Nuclide Activity

Sample ID : 1304106-01
Acquisition date
Total number of lines in spectrum

Number of unidentified lines
Number of lines tentatively identified by NID
30
26
4
Page :
2
2-MAY-2013 16:45:15
13.33%
Nuclide Type : FISSION

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 4.042E+02
Total Activity
4.042E+02
Wtd Mean
Decay Corr
pCi/filter
4.043E+02
Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.771E+02
19.06
4.043E+02
Nuclide Type : NATURAL

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.462E+02
Total Activity
Grand Total Activity :
Wtd Mean
Decay Corr
pCi/filter
3.462E+02
3.462E+02
3.462E+02
7.504E+02
7.504E+02
Flags: "K" ; Keyline not found

"E" ; Manually edited
Decay Corr
2-Sigma
0.601E+02
17.35
"M" ; Manually accepted

"A" ; Nuclide specific abn. limit
Nuclide Line Activity Report

Sample ID : 1304106-01
Acquisition date
Page :
3
2-MAY-2013 16:45:15
Nuclide Type: FISSION

Nuclide
BA-133
Energy
81.00
302.84
356.01
%-Abn
33.00*
17.80
60.00
Final Mean for
Uncorrected Decay Corr 2-Sigma

%-Eff
pCi/filter pCi/filter %Error
1.963E+01 4.042E+02
4.043E+02 19.06
5.855E+02 33.89
4.915E+00 5.854E+02
4.054E+02 17.65
6.963E+00 4.054E+02
3 Valid Peaks =
Status
OK
OK
OK
4.043E+02+/- 7.707E+01 ( 19. 06%-)
Nuclide Type: NATURAL

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
* 11 = Key line

%Eff
5.865E+01 3.462E+02
3.462E+02 17.35
1 Valid Peaks =
Status
OK
3.462E+02+/- 6.007E+01 ( 17.35%)
Combined Activity-MDA Report

Sample ID : 1304106-01
Acquisition date
4
Page :
2-MAY-2013 16:45:15
---- Identified Nuclides

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
4.043E+02
3.462E+02
Act error
7.707E+01
6.007E+01
MDA
(pCi/filter)
1. 833E+01
6.368E+01
MDA error
Act/MDA
3.009E+00
2.040E+00
22.052
5.436
MDA error
Act/MDA
6.533E+00
2.769E+01
3.632E-03
6.910E-02
7.625E+00
1.627E-01
-0.319
-0.441
0.000
2.545
-0.235
1.448
Non-Identified Nuclides
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-6.665E+00
-9.447E+01
O.OOOE+OO
9.359E+OO
-1.475E+01
1.004E+01
Act error
1.418E+01
1.681E+02
O.OOOE+OO
1.766E+OO
4.718E+01
3.755E+00
MDA
(pCi/filter)
2.093E+01
2.140E+02
1. 933E-01
3.677E+00
6.263E+01
6.933E+00
\~v\\?
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l304l0602 GE2 BAFIL l9l240.CN

PEAK Vl6.9 PEAKEFF V2.2
BLANK
2-MAY-2013 00:00:00.
l304l06-02
FILTER
GE2
0 OO:l5:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
l1
12
13
l4
l5
l6
l7
l8
l9
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
30.98
35.23
52.82
6l.85
65.88
Sl. 09
93.28
l11.85
16l. Ol
21l. 25
223.70
276.60
302.98
307.l9
333.95
338.78
356.07
365.2l
384 .ll
387.05
39l.ll
394.73
414.53
417.87
428.52
436.98
468.72
484.07
495.99
507.90
5l2.90
53l.18
539.23
609.24
676.35
731.26
2036
486
74
219
93
789
42
l76
27
15
23
60
159
32
139
l26
l44
68
72
130
l06
123
76
43
36
19
10
10
17
24
l5
l5
l8
l2
7
7
l3
14
5
9
5
1
3
1
1
4
1
l
0
5
3
3
0
1
l
0
0
0
0
0
0
0
3
3
6
6
0
0
8
8
8
8
2
2
0
0
0
0
0
l
1
0
0
0
0
0
2-MAY-20l3 l7:00:54.20
72
36
552
lO
7l
l92
49
10
32
2l
l2
85
28
7
9
9
7
7
7
9
9
6
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
l. 32
l. 68
2.03
1.46
1.47
l.45
l. 57
l. 26
l. 60
2.46
3.4l
1.82
1.52
2.16
l. 87
2.93
l.47
l. 59
2.32
l. 89
2.08
3.64
2.07
2.08
2.83
l. 60
1.75
l. 06
2.28
l. 78
l. 78
l. 89
2. 71
l. 65
l. 66
2.72
3l.10
35.34
52.94
6l.96
66.00
Sl. 20
93.39
l11. 96
l61.l2
2l1.36
223.81
276.71
303.08
307.30
334.05
338.89
356.18
365.31
384.21
387.l6
39l.2l
394.84
414.64
4l7.98
428.62
437.09
468.82
484.l7
496 .lO
508.00
5l3. 00
53l. 29
539.33
609.35
676.44
73l. 36
Left
Pw
27
27
50
58
58
76
89
lOS
l57
208
221
275
299
299
329
329
35l
362
38l
38l
38l
381
410
410
426
433
464
481
493
507
507
529
537
605
673
727
13
13
8
12
12
8
9
7
8
6
7
6
l5
15
17
17
lO
8
17
17
17
17
l1
l1
7
9
10
7
7
lO
10
7
5
7
7
9
2-MAY-2013 16:45:37.
l. OOOOOE+OO filter
0
BAFIL
0 OO:l5:00.29 0.0%
4096
lO.OOOOO
Cts/Sec %Err
2.26E+00
5.40E-Ol
8.24E-02
2.43E-Ol
l. 03E-01
8.77E-01
4.67E-02
1.95E-Ol
3.02E-02
l. 64E- 02
2.6lE-02
6.65E-02
l.76E-Ol
3.59E-02
8.05E-02
3.99E-02
6 .l3E-Ol
l. l6E- 02
7.89E-02
2.l4E-Ol
5.49E-02
l. 10E- 02
3.50E-02
2.28E-02
l. 37E-02
9.40E-02
3.l1E-02
7.36E-03
l. 04E- 02
9.62E-03
8.29E-03
7.78E-03
7.71E-03
9.50E-03
l.OOE-02
6.97E-03
2.4
5.9
30.6
8.8
l6.5
4.3
46.7
l2.9
58.8
75.l
46.8
l7.2
8.4
31.6
15.7
37.9
4.5
69.9
23.2
9.l
23.l
93.7
27.2
41.l
4l. 6
l2.6
24.l
50.2
45.6
2.9
65.0
59.l
44.6
42.3
33.3
73.3
Fit
4.27E+00
l.l5E+00
2.48E+00
2.58E+00
7.67E+00
1.88E+00
3.82E+00

Sample ID : 1304106-02
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.995E+02
Total Activity
:
11.11%
FISSION
Hlife
10.50Y
Nuclide Type
36
32
4
Page :
2
2-MAY-2013 16:45:37
---------
3.995E+02
Wtd Mean
Decay Corr
pCi/filter
3.995E+02
---------
Decay Corr
2-Sigma
0.780E+02
19.51
3.995E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.511E+02
Total Activity
---------
Wtd Mean
Decay Corr
pCi/filter
7.511E+02
---------
7.511E+02
7.511E+02
1.151E+03
1.151E+03
Flags: "K" = Keyline not found

"E" = Manually edited
Decay Corr
2-Sigma
19.80
1.487E+02
"M" = Manually accepted

"A" = Nuclide specific abn. limit

Sample ID : 1304106-02
Acquisition date
Page :
3
2-MAY-2013 16:45:37

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%-Eff
1.799E+01 3.995E+02
3.995E+02 19.51
3.541E+02 34.34
7.560E+00 3.540E+02
3.854E+02 17.57
7.170E+00 3.853E+02
3 Valid Peaks =
Status
OK
OK
OK
3.995E+02+/- 7. 796E+01 ( 19.5 1%-)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" = Keyline

%-Eff
7.511E+02 19.80
2.305E+01 7.511E+02
1 Valid Peaks=
Status
OK
7.511E+02+/- 1.487E+02 ( 19.80%-)

Sample ID : 1304106-02
Acquisition date
Page :
4
2-MAY-2013 16:45:37

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.995E+02
7.511E+02
Act error
7.796E+01
1.487E+02
MDA
(pCi/ filter)
2.181E+01
1.562E+02
MDA error
Act/MDA
3.714E+00
1.291E+01
18.316
4.807
MDA error
Act/MDA
1.453E+00
2.124E+01
1.835E-01
6.949E-02
6.283E+00
1.461E+00
-0.080
-0.351
3.851
1. 005
-0.028
0.804
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-7.557E-01
-6.500E+01
3.710E+01
3.384E+00
-1.570E+00
1.518E+01
Act error
5.472E+00
1.215E+02
4.937E+00
1.764E+00
3.920E+01
1.063E+01
MDA
(pCi/ filter)
9.464E+00
1.850E+02
9.634E+00
3.369E+00
5.564E+01
1.888E+01
S498
~\0
~

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30410603 GE3 BAFIL 19124l.CN

PZ-111-KS TOT
2-MAY-2013 00:00:00.
1304106-03
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
3
3
0
3
3
0
0
4
4
4
4
0
1
1
0
5
5
5
2
2
0
1
1
1
1
1
1
0
0
0
0
30.90
35.11
52.33
61.84
65.75
81.13
93.40
108.75
112.03
116.25
122.67
142.69
182.84
185.84
277.38
302.98
307.38
311.67
334.04
338.66
356.30
383.65
386.79
3 91. 53
411.64
414.87
417.87
437.47
467.92
510.56
609.49
1880
435
91
262
93
772
31
18
225
88
14
29
12
29
42
143
40
16
77
22
418
103
177
46
8
42
17
84
21
14
5
98
73
122
90
123
175
49
50
48
41
29
33
19
26
34
8
7
5
17
16
28
12
12
12
3
3
3
13
10
7
5
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
2-MAY-2013 17:01:37.98
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.41
1. 75
3.04
1.82
1. 83
1.93
1. 35
2.11
1. 81
2.06
2.14
2.66
1.68
1. 69
1.24
1. 72
2.65
2.65
1. 95
2.02
1. 80
1.87
1. 87
1. 88
1.89
1.89
1. 90
1.90
1.19
3.14
2.01
31.22
35.43
52.65
62.15
66.06
81.45
93.72
109.07
112.34
116.56
122.98
143.01
183.15
186.15
277.69
303.29
307.68
311.97
334.35
338.96
356.60
383.95
387.10
391.83
411.94
415.17
418.17
437.78
468.22
510.86
609.78
Left
Pw
27
27
49
58
58
77
92
107
107
107
107
140
182
182
274
298
298
298
331
331
352
381
381
381
409
409
409
434
464
507
606
14
14
9
12
12
10
5
19
19
19
19
8
8
8
8
18
18
18
18
18
10
16
16
16
16
16
16
10
8
9
6
2-MAY-2013 16:45:57.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.70 0. 4%
4096
10.00000
Cts/Sec %Err
2.09E+00
4.84E-Ol
l.OlE-01
2.91E-Ol
1.04E-01
8.58E-01
3.41E-02
1.98E-02
2.51E-Ol
9.81E-02
1.60E-02
3.26E-02
1.37E-02
3.21E-02
4.70E-02
1.59E-Ol
4.49E-02
1.74E-02
8.60E-02
2.47E-02
4.64E-01
1.15E-Ol
1.97E-Ol
5.07E-02
9.01E-03
4. 72E-02
1.91E-02
9.33E-02
2.28E-02
1. 52E- 02
6.06E-03
2.4
5.9
24.1
8.1
23.0
4.8
39.7
55.8
8.0
19.5
79.0
38.3
52.4
32.8
28.4
8.8
28.2
54.6
14.0
36.2
5.4
11.8
9.9
20.7
55.8
17.9
46.8
13.5
34.8
44.1
75.1
Fit
2.39E+00
3.11E+00
1.98E+00
3.75E+00
1.63E+00
2.67E+00
1.98E+Ol
2.59E+00

Sample ID : 1304106-03
Acquisition date

Nuclide Type
Nuclide
C0-57
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.255E+00
1. 00
3.701E+02
---------
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.810E+02
Grand Total Activity

;
;
---------
3.743E+02
---------
Total Activity
nE"
Wtd Mean
Decay Corr
pCi/filter
4.262E+00
3.701E+02
Decay Corr
2-Sigma
6.750E+00
158.37
0.686E+02
18.53
3.744E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
16.13%
FISSION
Hlife
270.90D
10.50Y
Nuclide Type
31
26
5
Page :
2
2-MAY-2013 16:45:57
Wtd Mean
Decay Corr
pCi/filter
7.810E+02
---------
7.810E+02
7.810E+02
1.155E+03
1.155E+03
Key line not found

Manually edited
"M"
II
All
Decay Corr
2-Sigma
1.368E+02
17.52
Manually accepted
Nuclide specific abn. limit

Sample ID : 1304106-03
Acquisition date
Page :
3
2-MAY-2013 16:45:57

Nuclide
C0-57
Energy
122.06
136.48
%Abn
85.51*
10.60
Final Mean for

BA-133
81.00
302.84
356.01
1 Valid Peaks =
33.00*
17.80
60.00
Final Mean for

%Eff
4.262E+00 158.37
1.191E+01 4.255E+00
1.069E+01 ----- Line Not Found -----
1.899E+01
6.222E+00
5.860E+00
4.262E+00+/- 6.750E+00 (158.37%)
3.701E+02
3.868E+02
3.569E+02
3 Valid Peaks =
Status
OK
Absent
3.701E+02
3.869E+02
3.570E+02
18.53
27.16
17.44
OK
OK
OK
3.701E+02+/- 6.857E+01 ( 18.53%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

%Eff
2.648E+01 7.810E+02
7.810E+02 17.52
1 Valid Peaks=
Status
OK
7.810E+02+/- 1.368E+02 ( 17.52%)
Flag: "*" = Keyline
til5flJ1

Sample ID : 1304106-03
Acquisition date
Page :
4
2-MAY-2013 16:45:57

Nuclide
C0-57
BA-133
TH-234
Activity
(pCi/filter)
Act error
4.262E+00
3.701E+02
7.810E+02
6.750E+00
6.857E+01
1.368E+02
MDA
(pCi/filter)
9.891E+00
2.029E+01
1.372E+02
MDA error
Act/MDA
1.130E+00
3.102E+00
7.367E+00
0.431
18.246
5.695
MDA error
Act/MDA
1.647E+01
4.858E-02
3.791E-02
4.651E+00
8.995E-01
-0.188
0.841
0.970
-0.161
1.320
Nuclide
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-3.763E+01
2.873E+00
2.585E+00
-9.252E+00
2.415E+01
Act error
1.473E+02
1.719E+00
1.376E+00
3.695E+01
9.922E+00
MDA
(pCi/filter)
1.998E+02
3.416E+00
2.666E+00
5.753E+01
1.829E+01
1(')1\\')
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410604 - GE3 BAFIL 191242.CN

PEAK V16.9 PEAKEFF V2.2
PZ-111-KS TOT
2-MAY-2013 00:00:00.
1304106-04
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
30.88
35.13
53.05
61.93
66.23
81.15
84.14
111.74
115.74
233.63
276.71
298.67
303.03
307.57
333.81
338.09
356.18
365.00
383.77
387.09
391.55
417.57
437.30
467.67
472.29
510.98
1894
512
44
253
112
785
24
200
50
24
31
11
138
30
81
66
4
4
0
3
3
7
7
2
2
0
0
0
2
2
3
3
0
0
7
7
7
0
0
0
0
0
2-MAY-2013 17:16:57.44
72
16
451
15
58
200
41
65
95
17
12
25
96
92
108
77
58
63
68
42
38
24
17
16
18
27
19
16
17
12
10
20
5
16
3
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.46
1.62
1.48
1. 82
1. 84
1.60
1. 47
1.75
1. 76
3.14
1. 09
2.96
1.71
1.99
1. 80
2.22
1. 97
1. 37
1.90
1.75
1. 82
4.20
1.96
1.95
1.89
3.66
31.20
35.45
53.37
62.25
66.54
81.47
84.46
112.05
116.06
233.94
277.02
298.98
303.34
307.88
334.11
338.39
356.49
365.30
384.08
387.39
391.86
417.88
437.61
467.97
472.59
511.28
Left
Pw
27
27
50
58
58
76
76
107
107
230
275
294
300
300
330
330
351
362
381
381
381
412
433
463
471
507
15
15
6
12
12
11
11
13
13
8
6
7
11
11
13
13
11
7
15
15
15
13
10
9
5
10
2-MAY-2013 17:01:35.
1. OOOOOE+OO filter
0
BAFIL
0 00:15:03.42 0.4%
4096
10.00000
Cts/Sec %Err
2.10E+00
5.69E-01
4.92E-02
2.81E-01
1. 24E- 01
8.72E-01
2.62E-02
2.22E-01
5.51E-02
2.66E-02
3.45E-02
1.18E-02
1. 53E-01
3.31E-02
8.01E-02
1.73E-02
5.01E-01
1.66E-02
6.48E-02
2.22E-01
4.57E-02
7.25E-02
1.06E-01
1.86E-02
1.30E-02
2.78E-02
2.4
5.2
38.1
8.4
17.9
3.9
94.9
9.7
33.5
51.1
36.0
83.0
9.2
29.1
14.8
65.9
5.1
51.2
21.1
8.1
21.3
19.3
11.2
51.2
40.9
20.0
Fit
8.23E+00
6.11E+00
7.74E+00
3.59E+00
4.83E+00
1.87E+00
1.64E+01

Sample ID : 1304106-04
Acquisition date

26
22
4
Page :
2
2-MAY-2013 17:01:35
15.38%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3. 762E+02
Total Activity
3.762E+02
Wtd Mean
Decay Corr
pCi/filter
3.763E+02
Decay Corr
2-Sigma
0.663E+02
17.63
3.763E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.557E+02
Total Activity
Wtd Mean
Decay Corr
pCi/filter
7.557E+02
7.557E+02
7.557E+02
1.132E+03
1.132E+03

Decay Corr
2-Sigma
1.365E+02
18.06


Sample ID : 1304106-04
Acquisition date
Page :
3
2-MAY-2013 17:01:35

Nuclide
BA-133
Energy
81.00
302.84
356.01
%-Abn
33.00*
17.80
60.00
Final Mean for

%-Eff
3.763E+02 17.63
1.899E+01 3.762E+02
3.731E+02 27.66
6.222E+00 3.731E+02
3.850E+02 17.00
5.860E+00 3.850E+02
3 Valid Peaks =
Status
OK
OK
OK
3.763E+02+/- 6.633E+01 ( 17.63%-)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" = Keyline

%Eff
2.648E+01 7.557E+02
7.557E+02 18.06
1 Valid Peaks=
Status
OK
7.557E+02+/- 1.365E+02 ( 18.06%-)

Sample ID : 1304106-04
Acquisition date
Page :
4
2-MAY-2013 17:01:35

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.763E+02
7.557E+02
6.633E+01
1.365E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
2.109E+01
1.424E+02
3.226E+OO
7.650E+00
17.837
5.306
MDA
(pCi/filter)
MDA error
Act/MDA
1.266E+00
1.729E+01
4.408E-02
3.983E-02
4.804E+OO
8.556E-01
-0.063
0.158
0.565
1. 221
0.222
0.988
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
-6.944E-01
3.323E+01
1.752E+00
3.420E+00
1.319E+01
1.720E+01
7.026E+00
1.282E+02
1.597E+00
1.417E+00
3.586E+01
9.180E+00
1.108E+01
2.097E+02
3.099E+00
2.800E+00
5.943E+01
1.740E+01
~~\v)
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30410605 GEl BAFIL 191243.CN

PZ-111-KS DIS
2-MAY-2013 00:00:00.
1304106-05
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
27.90
30.95
34.88
52.63
61.94
65.72
81.37
84.63
93.67
111.87
161.49
184.91
276.79
303.55
334.34
338.69
356.39
360.57
365.12
384.79
391.78
415.16
418.54
421.43
437.39
468.06
579.31
23
1880
467
49
252
112
782
23
52
192
18
24
65
125
57
31
488
8
24
106
59
37
26
12
117
30
6
62
69
74
85
61
63
46
49
77
95
55
77
28
49
40
18
15
15
10
1
6
13
9
7
3
3
0
3
3
3
0
2
2
3
3
0
0
0
0
0
0
0
0
4
4
4
1
1
2
2
2
0
0
0
2-MAY-2013 17:17:21.43
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 51
1. 37
1. 85
1.51
1.73
1. 74
1.63
1.95
1.11
1. 72
2.16
3.72
1.28
1. 71
1. 31
2.59
1.44
2.47
2.48
1.71
1. 88
2. 08
2.09
2.09
1.82
1.97
1.16
28.14
31.18
35.11
52.87
62.17
65.95
81.60
84.86
93.90
112.10
161.72
185.13
277.01
303.77
334.55
338.90
356.60
360.78
365.33
385.00
391.99
415.36
418.74
421.64
437.60
468.27
579.50
2-MAY-2013 17:02:02.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.25 0.0%
4096
10.00000
Left
Pw
Cts/Sec %Err
27
27
27
50
58
58
77
77
90
107
158
182
273
300
331
338
352
352
352
381
381
411
411
411
432
465
576
14
14
14
8
12
12
11
11
8
8
6
8
8
7
7
5
16
16
16
16
16
14
14
14
12
6
6
2.60E-02 49.0
2.09E+00 2.4
5.18E-01 7.2
5.41E-02 35.7
2.80E-Ol 7.9
1.25E-01 16.1
8.69E-Ol 3.7
2.50E-02105.8
5.75E-02 32.8
2.13E-01 11.4
1.97E-02 70.7
2.62E-02 67.6
7.22E-02 18.8
1.39E-Ol 12.9
6.28E-02 22.5
3.46E-02 28.7
5.42E-01 4.5
9.24E-03219.7
2.68E-02 27.9
1.18E-01 11.3
6.59E-02 14.7
4.15E-02 21.9
2.83E-02 34.3
1.39E-02 58.1
1.30E-01 9.7
3.33E-02 20.4
6.67E-03 40.8
Fit
7.23E+01
4.43E+00
2.33E+Ol
6.83E+00
2.40E+Ol
4.85E+00

Sample ID : 1304106-05
Acquisition date

27
22
5
Page :
2
2-MAY-2013 17:02:02
18.52%

Nuclide
Hlife
BA-133
10.50Y
NP-237 2.14E+06Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.625E+02
1.00 3.502E+Ol
Total Activity
3.975E+02
Wtd Mean
Decay Corr
pCi/filter
3.625E+02
3.502E+01
Decay Corr
2-Sigma
0.670E+02
18.47
7.422E+01
211. 95
3.975E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
l . 00
3.390E+02
Total Activity
Flags: "K"
"E"
= Keyline
=
Wtd Mean
Decay Corr
pCi/filter
3.390E+02
3.390E+02
3.390E+02
7.365E+02
7.365E+02
not found
Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
0.564E+02
16.64
Manually accepted

Sample ID : 1304106-05
Acquisition date
Page :
3
2-MAY-2013 17:02:02

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

NP-237
86.50
3 Valid Peaks =
12.60*
Final Mean for
Uncorrected Decay Carr 2-Sigma

%Eff
1. 963E+Ol 3.625E+02
3.625E+02 18.47
4.915E+00 4.281E+02
4.282E+02 39.02
6.963E+00 3.504E+02
3.505E+02 17.65
1.532E+Ol
3.625E+02+/- 6. 696E+Ol ( 18.47%)
3.502E+01
1 Valid Peaks=
Status
OK
OK
OK
3.502E+01 211.95
OK
3.502E+01+/- 7.422E+Ol (211.95%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" = Key line

%Eff
5.865E+01 3.390E+02
3.390E+02 16.64
1 Valid Peaks =
Status
OK
3.390E+02+/- 5.641E+01 ( 16.64%)

Sample ID : 1304106-05
Acquisition date
4
Page :
2-MAY-2013 17:02:02
Identified Nuclides
Nuclide
BA-133
TH-234
NP-237
Activity
(pCi/ filter)
3.625E+02
3.390E+02
3.502E+01
Act error
6.696E+01
5.641E+01
7.422E+01
MDA
(pCi/ filter)
1.655E+01
5.170E+01
4.842E+01
MDA error
Act/MDA
2.717E+00
1.656E+00
5.895E+00
21.901
6.558
0.723
MDA error
Act/MDA
7.017E+00
2.380E+01
3.632E-03
6.743E-02
1.504E-01
0.231
-0.135
0.000
2.329
1. 640
Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241
Key-Line
Activity K.r.,.
(pCi/filter)Ided
5.197E+00
-2.478E+01
O.OOOE+OO
8.358E+00
1.051E+01
Act error
1.260E+01
1.346E+02
O.OOOE+OO
1.743E+00
3.292E+00
MDA
(pCi/filter)
2.248E+01
1.840E+02
1.933E-01
3.588E+00
6.410E+00
\&
\\'3
~\[ll
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk I t
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
3
3
0
2
2
1
1
0
0
0
0
0
0
0
0
0
6
6
6
1
1
0
0
0
0
0
2-MAY-2013 17:17:48.74
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30410606 GE2 BAFIL 191244.CN

D-6 TOT
2-MAY-2013 00:00:00.
1304106-06
FILTER
GE2
0 00:15:00.00
25
3.00000
No
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
2-MAY-2013 17:02:29.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Energy
Area
Bkgnd
FWHM Channel
Left
Pw
Cts/Sec %Err
30.95
35.25
52.66
61.82
65.89
80.99
83.75
93.40
111.39
186.95
276.11
302.82
307.51
333.90
338.40
356.09
383.77
387.09
391.23
414.74
418.07
437.25
511.95
518.29
584.40
1237.47
1857
449
54
191
84
667
19
22
125
34
69
142
27
57
29
488
103
169
43
30
12
83
27
11
5
6
119
126
91
74
80
51
67
68
116
81
20
24
29
32
18
12
13
9
8
13
14
16
9
1
3
2
1.34
31.06
1. 63
35.36
1.66
52.78
1.60
61.94
1.61
66.00
1. 50
81.10
1. 50
83.86
1.63
93.52
1.40 111.50
1.71 187.06
1.69 276.21
1.27 302.93
1.80 307.62
1. 35 334.01
1.57 338.51
1.51 356.20
2.26 383.88
2.02 387.19
2.36 391.33
1.88 414.85
1. 89 418.17
1.74 437.35
1. 96 512.06
1.83 518.39
1. 28 584.50
2.55 1237.55
27
27
50
57
57
77
77
91
108
183
272
299
306
330
337
354
380
380
380
410
410
433
508
516
581
1233
14
14
6
13
13
15
15
6
8
9
8
7
6
7
6
7
15
15
15
16
16
9
8
6
6
2.5
6.1
31.3
9.9
18.7
4.2
94.2
62.1
17.3
50.7
16.5
10.2
36.8
21.2
30.8
4.7
13.2
9.9
26.4
27.6
71.3
14.0
27.9
34.7
70.7
54.3
2.06E+OO
4.99E-01
6.00E-02
2.13E-Ol
9.29E-02
7.41E-01
2.16E-02
2.47E-02
1.39E-01
3.78E-02
7.67E-02
1. SSE- 01
3.00E-02
6.28E-02
3.20E-02
5.43E-01
1.14E-01
l.SSE-01
4.75E-02
3.35E-02
1.33E-02
9.23E-02
2.98E-02
1.21E-02
5.56E-03
7 6.81E-03
Fit
2.77E+00
2.61E+00
1.09E+01
2.46E+00
7.76E-01
f!J511

Sample ID : 1304106-06
Acquisition date

26
22
4
Page :
2
2-MAY-2013 17:02:29
15.38%

Hlife
10.50Y
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.374E+02
Total Activity
3.374E+02
Wtd Mean
Decay Corr
pCi/filter
3.374E+02
Decay Corr
2-Sigma
0.654E+02
19.38
3.374E+02

Hlife
Nuclide
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 6.560E+02
Total Activity
Flags: "K"
"E"
= Keyline
=
Wtd Mean
Decay Corr
pCi/filter
6.560E+02
6.560E+02
6.560E+02
9.934E+02
9.935E+02
not found
Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
21.85
1.433E+02
Manually accepted
~512

Sample ID : 1304106-06
Acquisition date
Page :
3
2-MAY-2013 17:02:29

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.374E+02 19.38
1.799E+01 3.374E+02
3.172E+02 36.16
7.560E+00 3.171E+02
7.170E+00 3.409E+02
3.410E+02 17.80
3 Valid Peaks
Status
OK
OK
OK
3.374E+02+/- 6.541E+01 ( 19.38%)

Nuclide
TH-234
Energy
63.29
3.80*
Final Mean for

Flag: "*"

2.305E+01 6.560E+02
6.560E+02 21.85
%Eff
%Abn
1 Valid Peaks
Status
OK
6.560E+02+/- 1.433E+02 ( 21.85%)
Key line
19513

Sample ID : 1304106-06
Acquisition date
4
Page :
2-MAY-2013 17:02:29

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.374E+02
6.560E+02
Act error
MDA
(pCi/filter)
6.541E+01
2.058E+01
1. 433E+02
1. 468E+02
MDA error
Act/MDA
3.504E+00
1.213E+01
16.399
4.470
MDA error
Act/MDA
1. 4 01E+00
1.868E+01
1.877E-01
6.543E-02
5.444E+00
1.443E+00
0.105
-0.696
3.897
0.955
-0.619
0.944
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
9.552E-01
-1.133E+02
3.841E+01
3.029E+00
-2.985E+01
1.759E+01
Act error
5.070E+00
1.141E+02
5.071E+OO
1.654E+00
3.328E+01
1.027E+01
MDA
(pCi/ filter)
9.125E+00
1.627E+02
9.857E+OO
3.172E+00
4.822E+01
1.864E+01
~rv\l)
6

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

D-6 DIS
2-MAY-2013 00:00:00.
1304106-07
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
21.25
28.38
31.06
35.17
36.23
53.37
61.96
65.72
66.25
79.54
80.07
81.17
112.06
116.69
276.23
276.75
302.70
303.32
333.60
356.00
356.59
383.46
384.11
387.04
77
23
1856
372
57
25
269
45
90
32
23
672
168
35
29
24
29
118
49
314
21
30
51
114
31
39
117
17
2
20
19
13
14
35
36
28
39
27
5
5
3
0
6
14
0
0
0
2
2
0
0
2
2
3
3
3
0
0
1
1
1
1
0
7
7
4
4
0
2-MAY-2013 17:18:11.11
13
6
9
18
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
2-MAY-2013 17:02:50.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:01.18 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
0.49
0.14
0.79
0.68
0.57
0.54
0.96
0.66
0.76
0.92
0.76
0.65
0.87
0.52
1. 03
1. 03
1. 06
1. 06
0.32
0.82
0.94
1.16
1.04
0.67
201
269
293
332
332
509
586
628
628
758
758
758
1070
1111
2644
2644
2896
2896
3190
3406
3406
3673
3673
3705
18
16
30
29
29
14
29
26
26
41
41
41
20
22
24
24
26
26
28
28
28
28
28
25
8.55E-02 21.3
2.50E-02 66.2
2.06E+00 3.0
4.13E-Ol 6.2
6.37E-02 27.3
2.77E-02 43.7
2.99E-01 7.3
4.94E-02 26.6
9.95E-02 15.0
3.53E-02 44.5
2.59E-02102.3
7.46E-01 4.3
1.86E-Ol 11.0
3.84E-02 37.7
3.21E-02 28.4
2.62E-02 29.7
3.20E-02 37.9
1.32E-Ol 7.5
5.49E-02 17.0
3.49E-01 6.4
2.30E-02 79.7
3.36E-02 32.5
5.63E-02 18.9
1.27E-Ol 11.6
209.26
277.70
303.42
342.91
353.00
517.55
599.96
636.00
641.06
768.59
773.67
784.27
1080.66
1125.14
2656.00
2661.00
2910.00
2916.00
3206.54
3421.48
3427.08
3685.00
3691.23
3719.31
Fit
1.73E+00
1.48E+00
1.74E+00
6.15E-01
4.92E+00
1.15E+00
1.08E+00
tl515

Sample ID : 1304106-07
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.391E+02
---------
Total Activity
:
25.00%
FISSION
Hlife
10.50Y
Nuclide Type
24
18
6
Page :
2
2-MAY-2013 17:02:50
3.391E+02
Wtd Mean
Decay Corr
pCi/filter
3.392E+02
---------
2-Sigma
Decay Corr
17.47
0.592E+02
3.392E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.431E+02
---------
Total Activity
Wtd Mean
Decay Corr
pCi/filter
2.431E+02
---------
2.431E+02
2.431E+02
5.823E+02
5.823E+02
Flags: "K" = Key line not found

HEll
= Manually edited
Decay Corr
2-Sigma
0.367E+02
15.11
"Mu = Manually accepted

= Nuclide specific abn.
"A"
limit
lli51E

Sample ID : 1304106-07
Acquisition date
Page :
3
2-MAY-2013 17:02:50

Nuclide
BA-133
Energy
81.00
302.84
356.01
%-Abn
33.00*
17.80
60.00
Final Mean for

%-Eff
l.802E+Ol 3.391E+02
3.392E+02 17.47
2.575E+00 1.889E+02
1.889E+02 80.21
3.642E+02 19.34
4.312E+00 3.642E+02
3 Valid Peaks =
Status
OK
OK
OK
3. 392E+02+/- 5.925E+01 ( 17.47%-)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" = Keyline

%Eff
8.750E+01 2.431E+02
2.431E+02 15.11
1 Valid Peaks =
Status
OK
2.431E+02+/- 3.673E+01 ( 15.11%-)

Sample ID : 1304106-07
Acquisition date
Page :
4
2-MAY-2013 17:02:50

Nuclide
BA-133
TH-234
Activity
(pCi/ filter)
Act error
3.392E+02
2.431E+02
MDA
(pCi/filter)
MDA error
Act/MDA
5.925E+01
3.673E+01
1.264E+01
2.472E+01
1.862E+00
3.181E-01
26.825
9.834
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
8.114E+00
1.533E+01
2.089E-02
2.228E-02
3.977E+00
2.809E-02
0.228
0.048
0.436
1. 800
-0.074
0.274
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/ filter) Ided
5.447E+00
7.585E+00
8.101E-01
3.562E+00
-3.330E+00
6.850E-01
1.184E+01
8.468E+01
8.983E-01
1.528E+00
2.498E+01
1.513E+00
2.394E+01
1.593E+02
1. 856E+00
1.979E+00
4.509E+01
2.496E+00
ms1s
~)\{/
.:;\""'
VAX/VM$ Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
D~lOO:
[GAMMA.SCUSR.ARCHIVE]SMP 130410608 - GEl BAFIL 191246.CN

D-83 TOT
2-MAY-2013 00:00:00.
1304106-08
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk l t
Energy
Area
Bkgnd
3
3
0
3
3
0
1
1
2
2
0
0
0
0
0
0
3
3
0
1
1
4
4
4
0
0
0
4
4
0
0
30.90
35.15
52.39
61.93
65.84
81.27
92.69
96.62
111.97
116.46
161.71
186.19
252.45
276.84
303.10
307.70
333.87
338.34
356.48
384.96
391.62
415.25
418.50
422.37
437.17
445.87
468.67
507.62
511.22
599.71
610.62
1988
493
57
250
113
776
43
14
214
32
27
47
22
59
157
24
77
24
533
152
43
37
31
14
111
8
25
5
14
5
7
76
55
93
71
82
116
46
42
46
51
43
69
29
20
24
32
19
21
24
3
3
14
7
6
6
9
11
8
7
3
4
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
2-MAY-2013 17:33:36.36
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 52
1. 65
2. 71
1.91
1. 91
1. 89
1. 62
1. 63
1. 81
1.82
1. 08
4.12
2.50
1.34
1. 71
1.18
1.70
2.23
1. 81
1.88
1.88
2.52
2.02
2.30
1. 92
2.66
2.05
1. 95
2.60
2.79
1.82
31.13
35.39
52.62
62.16
66.07
81.50
92.92
96.85
112.19
116.68
161.94
186.41
252.66
277.05
303.31
307.91
334.08
338.55
356.69
385.17
391.83
415.45
418.70
422.57
437.37
446.07
468.88
507.82
511.42
599.90
610.82
Left
Pw
27
27
49
58
58
76
88
88
106
106
159
183
249
273
300
307
329
329
352
381
381
411
411
411
431
442
465
505
505
596
607
13
13
8
12
12
11
12
12
14
14
6
9
8
8
6
5
17
17
10
16
16
19
19
19
10
7
10
11
11
6
6
2-MAY-2013 17:18:19.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.27 0.0%
4096
10.00000
Cts/Sec %Err
2.21E+00
5.48E-01
6.36E-02
2.78E-01
1.26E-01
8.62E-01
4.83E-02
1.52E-02
2.38E-01
3.57E-02
2.98E-02
5.17E-02
2.45E-02
6.54E-02
1.75E-01
2.69E-02
8.51E-02
2.72E-02
5.92E-01
1.69E-01
4.74E-02
4.12E-02
3.48E-02
1.57E-02
1.23E-01
8.92E-03
2.80E-02
5.65E-03
1. 55E- 02
5.56E-03
7.68E-03
2.3
5.2
31.9
8.4
17.3
4.5
29.6
83.9
8.5
38.2
43.8
35.1
48.6
18.5
9.4
42.5
14.3
44.6
4.7
10.5
20.8
28.0
26.4
54.1
10.3
70.8
31.0
92.2
47.1
70.7
61.0
Fit
2.82E+01
3.91E+00
2.15E+00
1.37E+00
1.53E+00
2.43E+01
1.28E+00
l.lOE+OO

Sample ID : 1304106-08
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.596E+02
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.371E+02
Total Activity
=
=
---------
3.596E+02
Wtd Mean
Decay Corr
pCi/filter
3. 596E+02
---------
Decay Corr
2-Sigma
0.688E+02
19.13
3.596E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
12.90%
FISSION
Hlife
10.50Y
Nuclide Type
31
27
4
Page :
2
2-MAY-2013 17:18:19
---------
Wtd Mean
Decay Corr
pCi/filter
3.371E+02
---------
3.371E+02
3.371E+02
6.967E+02
6.967E+02
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
0.591E+02
17.54
Manually accepted
l!l52lil

Sample ID : 1304106-08
Acquisition date
Page :
3
2-MAY-2013 17:18:19

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.963E+01 3.596E+02
3. 596E+02 19.13
5.404E+02 34.72
4.915E+OO 5.403E+02
3.833E+02 17.80
6.963E+00 3.832E+02
3 Valid Peaks
Status
OK
OK
OK
3.596E+02+/- 6.879E+01 ( 19.13%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

%Eff
5.865E+01 3.371E+02
3.371E+02 17.54
1 Valid Peaks;
Status
OK
3.371E+02+/- 5.914E+01 ( 17.54%)
Flag: "*" ; Key line
~l521

Sample ID : 1304106-08
Acquisition date
Page :
4
2-MAY-2013 17:18:19

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.596E+02
3.371E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.879E+01
5.914E+01
1.576E+01
5.724E+01
2.586E+00
1.834E+00
22.826
5.889
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.696E+00
2.705E+01
3.632E-03
6.866E-02
6.865E+00
1.450E-01
0.281
0.299
0.000
2.594
0.223
1.263
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
6.019E+00
6.248E+01
O.OOOE+OO
9.477E+00
1.259E+01
7.807E+00
1.275E+01
1.387E+02
O.OOOE+OO
1.743E+00
3.797E+01
3.334E+00
2.145E+01
2.091E+02
1.933E-01
3.654E+00
5.639E+01
6.182E+00
~522
~\\'7
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP- 130410609 - GE2 - BAFIL 191247.CN

D-83 DIS
2-MAY-2013 00:00:00.
1304106-09
FILTER
GE2
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
28.01
30.99
35.02
37.76
46.30
52.42
61.95
65.75
77.02
81.02
111.72
116.73
186.54
276.56
292.89
302.98
306.97
333.73
337.73
356.06
365.83
383.72
386.96
391.06
415.07
421.89
437.10
511.59
584.30
31
1771
424
28
12
44
164
87
16
722
108
36
28
67
9
165
19
48
24
522
9
102
154
34
30
9
80
33
10
65
114
115
88
126
125
50
47
19
35
131
50
50
17
12
10
8
19
12
32
15
15
9
5
8
5
7
6
4
3
3
3
3
0
0
1
1
1
1
0
0
0
0
1
1
1
1
1
0
0
1
1
1
1
1
0
0
0
2-MAY-2013 17:33:59.30
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
2-MAY-2013 17:18:44.
1.00000E+00 filter
0
BAFIL
0 00:15:00.27 0.0%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
28.12
31.11
35.13
37.87
46.41
52.54
62.07
65.87
77.14
81.13
111.83
116.84
186.65
276.66
293.00
303.09
307.07
333.84
337.83
356.17
365.94
383.83
387.07
391.17
415.17
422.00
437.21
511.69
584.40
27
27
27
27
44
50
58
58
76
76
108
115
185
273
290
290
290
330
330
351
363
381
381
381
412
412
432
507
580
15
15
15
15
6
8
11
11
11
11
8
6
6
8
28
28
28
14
14
10
7
19
19
19
15
15
10
11
8
3.39E-02 35.1
1.97E+00 2.5
4. 71E-01 6.3
3.12E-02 67.6
1.32E-02152.3
4.87E-02 47.5
1.82E-01 10.7
9.62E-02 16.0
1.79E-02 37.7
8.02E-01 3.9
1.20E-01 20.6
4.01E-02 35.1
3.12E-02 44.3
7.42E-02 16.4
1.06E-02 61.8
1.84E-01 7.8
2.15E-02 39.5
5.37E-02 19.0
2.70E-02 31.4
5.80E-01 4.8
1.04E-02 74.6
1.14E-01 12.2
1.71E-01 10.3
3.73E-02 28.7
3.33E-02 25.7
1.00E-02 60.4
8.84E-02 12.9
3.61E-02 22.4
1.11E-02 46.9
1. 37
1.40
1. 68
1.40
1. 08
1.42
1.46
1. 47
1.49
1. 50
1.42
1. 75
1.11
1.96
1.61
1. 78
1.79
1.81
1. 82
1. 41
1.50
1.86
1.86
1. 86
1.88
1.72
1.45
2.00
3.79
Fit
2.48E+01
5.30E+00
5.50E+00
4.49E+00
2.24E+00
2.10E+00
4.32E+00
:fil523

Sample ID : 1304106-09
Acquisition date

29
24
5
Page :
2
2-MAY-2013 17:18:44
17.24%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.652E+02
Total Activity
3.652E+02
Wtd Mean
Decay Corr
pCi/filter
3.652E+02
Decay Corr
2-Sigma
0.700E+02
19.16
3.652E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 5.607E+02
Total Activity
Wtd Mean
Decay Corr
pCi/filter
5.607E+02
5.607E+02
5.607E+02
9.259E+02
9.259E+02
Flags: "K" = Keyline not found

"E" = Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.304E+02
23.25
Manually accepted

Sample ID : 1304106-09
Acquisition date
Page :
3
2-MAY-2013 17:18:44

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.799E+01 3.652E+02
3.652E+02 19.16
7.560E+00 3.689E+02
3.690E+02 33.71
3.641E+02 17.97
7.170E+00 3.641E+02
3 Valid Peaks =
Status
OK
OK
OK
3.652E+02+/- 6.997E+01 ( 19.16%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for


%Eff
2.305E+01 5.607E+02
5.607E+02 23.25
1 Valid Peaks =
Status
OK
5.607E+02+/- 1.304E+02 ( 23.25%)

Sample ID : 1304106-09
Acquisition date
Page :
4
2-MAY-2013 17:18:44

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.652E+02
5.607E+02
6.997E+01
1.304E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
1.766E+01
1.283E+02
3.007E+00
1.061E+01
20.681
4.369
MDA
(pCi/filter)
MDA error
Act/MDA
1.130E+00
1.859E+01
1.815E-01
6.576E-02
5.356E+00
1.397E+00
-0.575
-0.385
3.558
0.920
-0.067
1.168
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
-4.230E+00
-6.228E+01
3.392E+01
2.935E+00
-3.159E+00
2.109E+01
5.171E+00
1.069E+02
4.906E+00
1.669E+00
2.931E+01
9.566E+00
7.361E+00
1.619E+02
9.533E+00
3.188E+00
4.744E+01
1.805E+01
,u7
s \r"U\(J
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP- 130410610 - GE3 - BAFIL- 191248.CN

DUP 05 TOT
2-MAY-2013 00:00:00.
1304106-10
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
30.81
34.81
52.22
61.82
66.54
81.03
93.37
111.74
276.68
302.95
307.53
333.94
338.01
352.25
356.22
366.41
369.75
384.26
386.99
391.42
414.87
418.53
422.72
437.12
468.18
511.48
599.79
924.56
1455
324
44
224
63
658
16
192
43
133
44
63
25
11
431
8
12
131
148
30
21
19
13
97
18
20
5
6
55
59
101
85
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
1
1
0
1
1
0
0
0
0
2
2
4
4
6
6
0
0
5
5
0
1
1
0
0
0
0
0
0
2-MAY-2013 17:34:27.22
92
159
102
140
19
16
26
17
13
5
10
22
11
22
10
17
19
20
7
3
3
5
7
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.44
1.45
2.55
1. 51
1. 52
1.92
1.13
1.84
1.38
1.69
1.99
2.12
2.44
2.23
1.59
1. 76
1.84
2.66
1. 59
2.51
1.89
1.90
1.79
1.92
1. 61
2.33
2.44
2.74
31.13
35.13
52.54
62.14
66.86
81.35
93.69
112.06
276.99
303.25
307.84
334.24
338.31
352.55
356.52
366.71
370.06
384.56
387.29
391.72
415.17
418.83
423.02
437.42
468.48
511.78
600.08
924.83
2-MAY-2013 17:19:09.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.30 0.4%
4096
10.00000
Left
Pw
Cts/Sec %Err
26
26
50
57
57
77
91
108
274
300
300
329
329
351
351
362
368
381
381
391
412
412
421
432
465
509
595
921
13
13
7
16
16
10
7
8
7
11
11
18
18
10
10
7
6
9
9
5
10
10
6
9
6
7
7
7
1.62E+00 2.9
3.60E-Ol 6.9
4.87E-02 40.8
2.48E-Ol 9.3
7.04E-02 26.3
7.31E-01 5.3
1.73E-02110.4
2.13E-Ol 12.9
4.78E-02 22.7
1.48E-01 9.6
4.85E-02 22.2
6.97E-02 16.6
2.73E-02 38.6
1. 24E-02 39.5
4.79E-01 4.9
9.33E-03 97.3
1.34E-02 51.5
1. 45E- 01 13.3
1. 64E-01 9.9
3.30E-02 31.8
2.38E-02 38.3
2.12E-02 44.6
1. 45E- 02 42.8
1.08E-01 10.5
1.98E-02 28.3
2.24E-02 28.9
5.65E-03 96.9
6.67E-03 40.8
Fit
3.52E+Ol
2.01E+00
7.85E+00
2.00E+00
5.02E-01
2.27E+01
6.79E+00
B5:27

Sample ID : 1304106-10
Acquisition date

28
24
4
Page :
2
2-MAY-2013 17:19:09
14.29%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.155E+02
Total Activity
3.155E+02
Wtd Mean
Decay Corr
pCi/filter
3.156E+02
Decay Corr
2-Sigma
19.00
0.600E+02
3.156E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 6.671E+02
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
6.671E+02
6.671E+02
6.671E+02
9.826E+02
9.826E+02
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.322E+02
19.82
Manually accepted

Sample ID : 1304106-10
Acquisition date
Page :
3
2-MAY-2013 17:19:09

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.155E+02
3.156E+02 19.00
6.222E+00 3.618E+02
3.619E+02 28.11
5.860E+00 3.684E+02
3.684E+02 16.86
3 Valid Peaks
Status
OK
OK
OK
3.156E+02+/- 5.996E+01 ( 19.00%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
* 11

2.648E+01 6.671E+02
6.671E+02 19.82
%Eff
1 Valid Peaks
Status
OK
6.671E+02+/- 1.322E+02 ( 19.82%)
Key line
-f!l529

Sample ID : 1304106-10
Acquisition date
Page :
4
2-MAY-2013 17:19:09

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.156E+02
6.671E+02
5.996E+01
1.322E+02
Act error
MDA error
Act/MDA
2.015E+01
1.219E+02
3.081E+OO
6.548E+00
15.662
5.472
MDA
(pCi/filter)
MDA error
Act/MDA
1.239E+OO
1.678E+01
6.068E-02
3.781E-02
4.821E+OO
8.987E-01
0.204
0.178
1.040
1.321
-0.201
1. 619
MDA
(pCi/filter)
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
2.208E+00
3.616E+01
4.438E+00
3.511E+00
-1.200E+01
2. 960E+01
6.028E+00
1.399E+02
2.185E+00
1.378E+00
4.410E+01
9.528E+00
1.084E+01
2.035E+02
4.267E+00
2.659E+00
5.964E+01
1.828E+01
\~\~/
'6

Configuration
Analyses by
Client IP
Deposition Pate
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130410611 - GE5 - BAFIL- 191249.CN

DUP 05 DIS
2-MAY-2013 00:00:00.
1304106-11
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
11.33
21.19
31.05
35.18
36.02
37.74
53.52
61.92
66.20
79.71
81.21
112.06
116.18
168.40
276.53
302.98
307.50
333.87
338.03
338.55
355.84
356.41
383.55
384.30
386.38
387.22
10
92
1699
348
62
9
46
209
158
65
681
138
41
6
43
109
21
59
11
41
174
106
51
68
22
166
2
15
107
17
3
6
13
38
25
16
12
53
21
11
3
5
6
11
6
2
14
14
15
11
11
13
0
0
0
2
2
0
0
0
0
2
2
0
0
0
0
0
0
0
1
1
6
6
6
6
1
1
2-MAY-2013 17:35:24.32
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
2-MAY-2013 17:19:39.
1. OOOOOE+OO filter
0
BAFIL
0 00:15:01.10 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
0.31
0.41
0.78
0.68
0.57
0.73
0.29
0.70
0.78
0.84
0.68
0.77
0. 72
0.43
0.39
0.70
0.75
1. 20
1.10
1.11
1. 08
0. 71
1.12
1.16
1.16
1.16
110
198
291
333
333
360
509
586
629
758
758
1070
1111
1605
2645
2896
2943
3192
3241
3241
3404
3404
3672
3672
3705
3705
9
21
28
28
28
11
21
25
29
36
36
21
18
18
25
27
21
27
19
19
30
30
29
29
27
27
1. 12E- 02 40.8
1.02E-Ol 15.0
1.89E+00 3.0
3.87E-01 6.4
6.88E-02 29.2
9.44E-03 63.5
5.09E-02 22.7
2.33E-01 9.6
1.76E-01 11.0
7.17E-02 23.5
7.57E-01 4.0
1. 54E-01 14.0
4.57E-02 27.2
6.54E-03110.6
4.80E-02 17.3
1. 21E-01 10.4
2.28E-02 30.8
6.58E-02 16.8
1.25E-02 44.2
4.55E-02 11.0
1.93E-01 10.9
1.18E-01 16.5
5.63E-02 22.7
7.51E-02 14.4
2.48E-02 40.5
1. 84E- 01 7.6
114.10
208.72
303.36
342.95
351.00
367.53
518.92
599.54
640.57
770.30
784.61
1080.72
1120.24
1621.27
2658.87
2912.68
2956.02
3209.12
3249.00
3254.00
3419.92
3425.39
3685.84
3693.00
3713.00
3721.00
Fit
7.11E-01
1.57E+00
1.14E+00
8.15E-01
2.30E+00
5.20E+00

Sample ID : 1304106-11
Acquisition date

26
19
7
Page :
2
2-MAY-2013 17:19:39
26.92%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.440E+02
Total Activity
3.440E+02
Wtd Mean
Decay Corr
pCi/filter
3.441E+02
Decay Corr
2-Sigrna
0.592E+02
17.19
3.441E+02

Nuclide
Hlife
PA-234 4.47E+09Y
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 4.259E+00
1. 00
1.891E+02
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
4.259E+00
1.891E+02
1.933E+02
1.933E+02
5.374E+02
5.374E+02
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.287E+00
30.21
0.371E+02
19.64
Manually accepted
~532

Sample ID : 1304106-11
Acquisition date
Page :
3
2-MAY-2013 17:19:39

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.802E+01 3.440E+02
3.441E+02 17.19
2.575E+00 7.114E+02
7.115E+02 33.66
4.312E+00 2.017E+02
2.017E+02 26.18
3 Valid Peaks
Status
OK
OK
OK
3.441E+02+/- 5.916E+01 ( 17.19%)

Nuclide
PA-234
Energy
9.89
21.72
37.93
131.42
%Abn
89.00
64.90*
23.75
20.40
Final Mean for

TH-234
63.29
Flag: "*"
3 Valid Peaks
3.80*
Final Mean for

%Eff
1.000E+02 3.416E-01
3.416E-01 81.70
1. OOOE+02
4.259E+00
4.259E+00 30.21
1.000E+02 1.075E+00
1.075E+00 127.05
2.473E+00 ----- Line Not Found -----
8.750E+01
1 Valid
4.259E+00+/- 1.287E+00 ( 30.21%)
1.891E+02
Peaks~
Status
OK
OK
OK
Absent
1.891E+02
19.64
OK
1.891E+02+/- 3.713E+01 ( 19.64%)
Key line
ms:n

Sample ID : 1304106-11
Acquisition date
Page :
4
2-MAY-2013 17:19:39

Nuclide
BA-133
PA-234
TH-234
Activity
(pCi/filter)
Act error
3.441E+02
4.259E+00
1.891E+02
5.916E+01
1.287E+00
3.713E+01
Act error
MDA error
Act/MDA
1.188E+01
7.073E-01
2.189E+01
1.750E+00
7. 962E- 03
2.816E-01
28.956
6.021
8.637
MDA
(pCi/filter)
MDA error
Act/MDA
8.114E+00
1.611E+01
1. 927E-02
4.111E+00
2. 714E-02
0.029
-0.078
-0.184
0.035
0.646
MDA
(pCi/filter)
Nuclide
C0-57
CD-109
PA-231
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
6.925E-01
-1.308E+01
-3.144E-01
1.627E+00
1.558E+00
1.262E+01
9.295E+01
9.850E-01
2.513E+01
1.247E+00
2.394E+01
1.674E+02
1.712E+00
4.660E+01
2.411E+00
\~,)0
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130410612 - GE1_BAFIL_191250.CN

PZ-102-SS TOT
2-MAY-2013 00:00:00.
1304106-12
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
30.94
35.28
52.91
61.91
65.63
81.39
93.34
109.77
116.62
161.41
186.45
276.78
302.98
307.62
333.93
337.96
356.43
386.29
416.06
430.71
437.40
470.27
510.90
517.89
1232
221
48
156
55
470
40
22
35
26
25
51
79
22
45
12
325
177
37
10
62
30
25
11
101
98
82
50
50
107
49
24
34
57
56
30
13
13
12
7
22
39
15
4
10
3
2
0
14
15
16
17
18
19
20
21
22
23
24
0
0
0
1
1
0
0
1
1
0
0
0
2
2
1
1
0
0
0
0
0
0
0
0
2-MAY-2013 17:50.:24.10
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.36
2.43
3.56
1. 58
1. 58
1.70
1.34
1.49
1.65
1.89
1.15
1.31
1.66
2.01
1.84
1.84
1. 78
4.48
1.63
2.82
1. 98
6.77
3.38
2.92
31.17
35.51
53.15
62.14
65.86
81.61
93.57
110.00
116.85
161.63
186.67
277.00
303.19
307.83
334.15
338.17
356.64
386.49
416.27
430.92
437.60
470.47
511.10
518.09
Left
Pw
27
35
50
58
58
77
90
108
108
157
184
274
299
299
331
331
352
382
411
428
434
466
507
516
7
5
8
12
12
10
7
14
14
8
7
7
13
13
11
11
8
8
10
6
9
11
9
6
2-MAY-2013 17:35:05.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.20 0.0%
4096
10.00000
Cts/Sec %Err
1.37E+00
2.45E-01
5.37E-02
1.74E-01
6.12E-02
5.22E-01
4.43E-02
2.44E-02
3.87E-02
2.86E-02
2.76E-02
5.67E-02
8.79E-02
2.48E-02
4.97E-02
1. 33E-02
3.61E-Ol
1.97E-01
4 .11E-02
1.15E-02
6.85E-02
3.31E-02
2.78E-02
1. 22E-02
3.1
11.3
35.5
11.0
27.7
6.2
33.5
41.2
32.3
54.2
53.4
22.6
13.6
31.5
19.2
61.1
6.1
9.7
25.6
44.0
15.6
21.4
22.6
30.2
Fit
4.42E+00
1.61E+Ol
5.94E+00
1. 63E+00
ty535

Sample ID : 1304106-12
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
2.178E+02
1. 00
---------
Total Activity
:
2.178E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.106E+02
--------Total Activity
;
"Eu
Wtd Mean
Decay Corr
pCi/filter
2.178E+02
---------
Decay Corr
2-Sigma
0.457E+02
20.98
2.178E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "Ku
16.67%
FISSION
Hlife
10.50Y
Nuclide Type
24
20
4
Page :
2
2-MAY-2013 17:35:05
Wtd Mean
Decay Corr
pCi/filter
2.106E+02
---------
2.106E+02
2.106E+02
4.284E+02
4.284E+02
Key line not found

Manually edited
"M"
"An
2-Sigma
Decay Corr
0.476E+02
22.62
Manually accepted
til5.36

Sample ID : 1304106-12
Acquisition date
Page :
3
2-MAY-2013 17:35:05

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.963E+01 2.178E+02
2.178E+02 20.98
2.717E+02 40.00
4.915E+00 2.716E+02
6. 963E+00 2.338E+02
2.338E+02 19.43
3 Valid Peaks
Status
OK
OK
OK
2.178E+02+/- 4.568E+01 ( 20.98%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
5.865E+Ol 2.106E+02
2.106E+02 22.62
1 Valid Peaks
Status
OK
2.106E+02+/- 4.764E+01 ( 22.62%)

Sample ID : 1304106-12
Acquisition date
Page :
4
2-MAY-2013 17:35:05

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
2.178E+02
2.106E+02
4.568E+01
4.764E+01
Act error
MDA error
Act/MDA
1.570E+01
5.509E+01
2.577E+00
1.765E+00
13.875
3.824
MDA
(pCi/filter)
MOA error
Act/MDA
6.010E+00
2.354E+01
3.632E-03
6.544E-02
6.436E+00
1. 241E- 01
0. 235
-0.167
0.000
2.355
0.232
0.774
MDA
(pCi/filter)
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
4.532E+00
-3.038E+01
O.OOOE+OO
8.202E+00
1.228E+01
4.095E+00
1.134E+01
1.342E+02
O.OOOE+OO
1.672E+00
3.515E+01
2.977E+00
1.925E+01
1.820E+02
1.933E-01
3.482E+00
5.286E+01
5.291E+00
-8538
,cJ?,v\\'7
-s
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30410613 - GE2 - BAFIL- 191251.CN

PZ-102-SS DIS
2-MAY-2013 00:00:00.
1304106-13
FILTER
GE2
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
31.01
35.15
52.90
61.88
65.75
81.04
92.47
111.60
116.48
161.87
276.40
302.95
307.35
312.85
333.94
337.88
356.11
383.72
387.00
391.06
399.04
415.85
419.89
436.73
510.94
593.09
912.16
1755
369
58
151
128
125
109
56
60
129
73
82
58
55
34
23
34
13
14
8
30
5
4
3
1
12
2
2
7
2
3
2
2
0
1
1
0
0
0
0
0
0
3
3
0
1
1
0
1
1
1
0
9
9
0
0
0
0
2-MAY-2013 17:50:50.20
71
680
37
147
31
25
51
134
29
8
84
23
453
115
157
28
12
39
10
95
29
6
8
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.43
1. 53
1. 39
1.46
1.47
1.43
1.17
1. 56
2.03
1. 88
2.05
1.51
2.16
0.96
1. 81
1. 82
1. 53
1. 86
1.86
1.86
1. 66
4.04
1.72
1. 93
4.27
1.19
2.05
31.12
35.27
53.02
62.00
65.87
81.15
92.58
111.72
116.60
161.98
276.51
303.06
307.46
312.96
334.05
337.99
356.21
383.83
387.10
391.17
399.15
415.96
420.00
436.83
511.05
593.19
912.25
Left
Pw
26
26
50
57
57
76
89
107
115
159
274
299
299
311
330
330
351
380
380
380
396
411
411
431
506
590
909
14
14
7
13
13
10
8
8
5
7
10
13
13
5
16
16
9
16
16
16
7
14
14
10
10
6
6
2-MAY-2013 17:35:35.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Cts/Sec %Err
1.95E+00
4.10E-01
6.39E-02
1.68E-01
7.84E-02
7.55E-Ol
4.16E-02
1.63E-01
3.50E-02
2.82E-02
5.72E-02
1.49E-Ol
3.17E-02
8.57E-03
9.39E-02
2.53E-02
5.03E-01
1. 28E- 01
1.74E-Ol
3.16E-02
1. 28E-02
4.31E-02
1.15E-02
1.05E-01
3.25E-02
6.11E-03
8.89E-03
2.5
7.2
33.2
11.0
20.0
5.0
42.5
13.5
38.3
51.7
25.0
10.1
39.1
78.5
12.0
35.7
5.2
10.4
10.1
32.5
34.7
24.3
56.6
10.7
25.3
55.3
49.2
Fit
5.16E+00
3.60E+00
8.59E+00
2.02E+00
6.42E+00
2.12E+00

Sample ID : 1304106-13
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.439E+02
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 5.180E+02
Total Activity
=
=
---------
3.439E+02
Wtd Mean
Decay Corr
pCi/filter
3.439E+02
---------
Decay Corr
2-Sigma
Error
%Error Flags
2-Sigma
0.691E+02
20.10
3.439E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
14.81%
FISSION
Hlife
10.50Y
Nuclide Type
27
23
4
Page :
2
2-MAY-2013 17:35:35
---------
Wtd Mean
Decay Corr
pCi/filter
5.180E+02
---------
5.180E+02
5.180E+02
8.619E+02
8.619E+02
Keyline not found

Manually edited
"M"
"A"
Decay Corr
2-Sigma
1.238E+02
23.91
= Manually
=
accepted

Sample ID : 1304106-13
Acquisition date
Page :
3
2-MAY-2013 17:35:35

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1. 799E+01
3.439E+02
3.439E+02 20.10
7.560E+00 2.988E+02
2.989E+02 36.14
3.162E+02 18.34
7.170E+00 3.161E+02
3 Valid Peaks
3.439E+02+/- 6.913E+01
Status
OK
OK
OK
20. 10%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" ; Key line

%Eff
2.305E+01 5.180E+02
5.180E+02 23.91
1 Valid Peaks;
Status
OK
5.180E+02+/- 1.238E+02 ( 23.91%)

Sample ID : 1304106-13
Acquisition date
Page :
4
2-MAY-2013 17:35:35

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.439E+02
5.180E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.913E+01
1.238E+02
1.677E+01
1.443E+02
2.855E+00
1.192E+01
20.507
3.590
Act error
MDA
(pCi/filter)
MDA error
Act/MOA
1.395E+00
1.766E+01
1.916E-01
6.541E-02
5.582E+00
1.399E+00
0.179
-0.399
3.705
0.397
0.094
0.876
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
1.627E+00
-6.135E+01
3.728E+01
1.259E+00
4.625E+00
1.585E+01
5.348E+00
1.171E+02
5.218E+00
1.868E+00
3.351E+01
9.996E+00
9.082E+00
1.538E+02
1. 006E+01
3.171E+00
4.943E+01
1.808E+01
\~
\{'1
6:vVAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
critical level

PZ-102R-SS TOT
2-MAY-2013 00:00:00.
1304106-14
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
30.96
35.32
46.60
53.34
58.97
61.97
66.39
69.75
81.31
93.58
111.97
115.66
187.89
198.59
267.11
276.63
302.94
308.38
324.27
333.80
337.86
356.32
383.82
386.66
414.58
418.72
437.29
470.50
511.41
582.82
663.23
930
217
34
36
15
96
30
14
340
28
89
29
20
25
13
23
64
10
14
29
10
209
23
39
16
10
39
17
17
7
8
53
47
65
75
35
52
45
41
112
72
51
52
36
30
4
11
14
11
7
7
6
16
20
24
7
4
3
7
0
2
2
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
4
4
0
0
2
2
2
2
0
0
5
5
0
0
0
0
0
0
0
1
1
0
2
2
1
1
0
0
0
0
0
2-MAY-2013 17:51:28.73
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 59
1. 93
2.99
1.99
1.65
1.66
1.67
1.68
1.90
1.47
1.90
2.34
3.37
1. 92
2.94
1.36
1.65
1.26
2.89
1.83
1.83
1. 66
2.06
2.06
1.89
1. 90
1. 58
6.03
2.48
1.38
3.50
31.28
35.64
46.92
53.66
59.29
62.29
66.71
70.07
81.63
93.89
112.28
115.97
188.20
198.90
267.42
276.94
303.25
308.69
324.57
334.11
338.17
356.62
384.12
386.96
414.88
419.02
437.59
470.80
511.71
583.12
663.52
Left
Pw
26
26
43
51
58
58
58
58
77
89
108
108
183
195
264
274
299
307
321
330
330
352
381
381
412
412
434
465
509
579
660
17
17
8
7
15
15
15
15
11
8
14
14
9
8
8
7
8
6
7
14
14
9
10
10
10
10
6
10
8
7
7
2-MAY-2013 17:36:09.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.96 0.4%
4096
10.00000
Cts/Sec %Err
1.03E+00
2.42E-01
3.82E-02
4.00E-02
1. 64E- 02
1.06E-Ol
3.39E-02
1.56E-02
3.77E-01
3 .11E-02
9.88E-02
3.24E-02
2.22E-02
2.82E-02
1.44E-02
2.56E-02
7 .11E-02
1.11E-02
1. 56E-02
3.24E-02
1.14E-02
2.32E-01
2.55E-02
4.30E-02
1.82E-02
1. 09E-02
4.29E-02
1.87E-02
1.89E-02
8.02E-03
9.11E-03
3.5
9.1
43.8
43.0
55.6
15.5
41.0
78.2
8.1
55.8
16.6
55.4
58.5
43.8
38.5
31.4
16.1
60.6
41.2
20.5
52.3
7.7
38.9
28.2
32.9
47.7
17.7
38.7
24.3
48.1
44.1
Fit
5.02E+00
3.31E+00
1.59E+00
1.70E+00
3.21E+00
1.19E+00

Sample ID : 1304106-14
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 1.628E+02
--------Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.851E+02
1.00 4.271E+00
Total Activity
=
=
1.628E+02
Wtd Mean
Decay Corr
pCi/filter
1.628E+02
---------
Decay Corr
2-Sigma
0.369E+02
22.67
1.628E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
AM-241
432.20Y
Flags: "K"
"E"
16.13%
FISSION
Hlife
10.50Y
Nuclide Type
31
26
5
Page :
2
2-MAY-2013 17:36:09
---------
Wtd Mean
Decay Corr
pCi/filter
2.851E+02
4.271E+00
---------
2.894E+02
2.894E+02
4.522E+02
4.522E+02
Keyline not found

Manually edited
"M"
"A"
=
=
2-Sigma
Decay Corr
0.907E+02
31.80
4.759E+00
111.42
Manually accepted

Sample ID : 1304106-14
Acquisition date
Page :
3
2-MAY-2013 17:36:09

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 1.628E+02
1.628E+02 22.67
1.736E+02 38.19
6.222E+00 1.736E+02
5.860E+00 1.787E+02
1.787E+02 20.60
3 Valid Peaks
1.628E+02+/- 3.692E+01
Status
OK
OK
OK
22. 67%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
Flag: "*"
1 Valid Peaks
35.90*
Final Mean for

%Eff
2.648E+01 2.851E+02
2.851E+02 31.80
2.893E+01
1 Valid Peaks
2.851E+02+/- 9.067E+01 ( 31.80%)
4.271E+00
=
Status
OK
4.271E+00 111.42
OK
4.271E+00+/- 4.759E+00 (111.42%)
Key line
-fil..S-i!-5

Sample ID : 1304106-14
Acquisition date
Page :
4
17:36:09
2-MAY-2013

Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filter)
1.628E+02
2.851E+02
4.271E+00
Act error
3.692E+01
9.067E+01
4.759E+00
MDA
(pCi/filter)
1.757E+01
1.070E+02
1.034E+01
MDA error
Act/MDA
2.687E+00
5.747E+00
5.086E-01
9.268
2.665
0.413
MDA error
Act/MDA
9.837E-01
1.234E+01
3.862E-02
2.866E-02
3.820E+00
-0.093
-0.646
0.222
0.772
-0.345
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/filter)Ided
-8.025E-01
-9.667E+01
6.018E-01
1.556E+00
-1.632E+01
Act error
5.401E+00
1.215E+02
1.452E+00
1.069E+00
3.585E+01
MDA
(pCi/filter)
8.611E+00
1.496E+02
2.715E+00
2.015E+00
4.725E+01
,uC\.J.O
-5
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410615 GE5 BAFIL 191253.CN

PZ-102R-DIS
2-MAY-2013 00:00:00.
1304106-15
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
3.93
10.94
21.24
31.05
35.15
36.17
53.39
61.90
65.82
66.55
81.23
112.13
118.29
276.57
302.90
303.32
333.44
333.96
356.27
356.68
383.45
384.22
386.70
387.32
13
8
97
1788
391
73
43
207
78
29
646
185
8
52
91
11
30
26
388
22
26
36
77
32
16
5
21
87
10
9
17
39
22
9
74
35
13
3
0
0
3
3
11
9
4
5
17
9
0
0
0
0
2
2
0
0
1
1
0
0
0
0
2
2
1
1
3
3
2
2
4
4
2-MAY-2013 17:51:56.65
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
2-MAY-2013 17:36:37.
1.00000E+00 filter
0
BAFIL
0 00:15:01.14 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
0.31
0.18
1.02
0.74
0.65
0.62
0.43
0.85
0.66
0.66
0.60
0.83
1.27
0.55
1.29
1.06
1.10
1.10
1.25
1.13
1.15
1. 27
1.16
0.76
40
105
200
291
332
332
510
588
627
627
773
1071
1129
2646
2896
2896
3195
3195
3406
3406
3671
3671
3703
3703
7
10
17
23
29
29
15
21
25
25
26
22
15
22
28
28
22
22
31
31
30
30
25
25
1.45E-02 62.2
8.89E-03 63.1
1.08E-01 14.9
1.99E+00 2.7
4.35E-01 5.6
8.15E-02 25.3
4.79E-02 23.7
2.30E-01 9.4
8.65E-02 17.2
3.22E-02 44.1
7.18E-01 5.1
2.06E-01 10.4
8.52E-03105.0
5.76E-02 15.3
1.01E-01 9.6
1.20E-02 69.9
3.33E-02 23.3
2.84E-02 26.3
4.31E-01 4.9
2.43E-02 79.0
2.91E-02 33.4
3.99E-02 22.1
8.52E-02 16.8
3.57E-02 30.5
43.07
110.37
209.23
303.35
342.69
352.46
517.72
599.34
637.00
644.00
784.88
1081.36
1140.43
2659.24
2911. 90
2916.00
3205.00
3210.00
3424.03
3428.00
3684.89
3692.23
3716.00
3722.02
Fit
2.12E+OO
3.17E+00
1.13E+00
1.76E+00
8.09E+00
8.54E-01
7.90E-01

Sample ID : 1304106-15
Acquisition date

24
17
7
Page :
2
2-MAY-2013 17:36:37
29.17%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.260E+02
Total Activity
Wtd Mean
Decay Corr
pCi/filter
3.261E+02
3.260E+02
3.261E+02
Wtd Mean
Uncorrected
pCi/filter
5.720E-01
4.493E+00
1.873E+02
Wtd Mean
Decay Corr
pCi/filter
5.720E-01
4.493E+00
1.873E+02
1.924E+02
1.924E+02
5.184E+02
5.184E+02
2-Sigma
Decay Corr
0.598E+02
18.33

Nuclide
Hlife
PA-231 3.28E+04Y
PA-234 4.47E+09Y
TH-234 4.47E+09Y
Decay
1. 00
1.00
1.00
Total Activity
Flags: "K"
"E"
=
=
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
7.225E-01
126.31
1.349E+00
30.01
0.361E+02
19.28
Manually accepted

Sample ID : 1304106-15
Acquisition date
Page :
3
2-MAY-2013 17:36:37

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.261E+02 18.33
1.802E+01 3.260E+02
5.970E+02 32.61
2.575E+00 5.969E+02
4.312E+00 4.504E+02
4.504E+02 17.49
3 Valid Peaks =
Status
OK
OK
OK
3.261E+02+/- 5.977E+01 ( 18.33%)

Nuclide
PA-231
Energy
9.28
10.11
283.67
302.67
%Abn
42.00*
20.20
1.60
2.30
Final Mean for

PA-234
9.89
21.72
37.93
131.42
TH-234
63.29
3 Valid Peaks =
89.00
64.90*
23.75
20.40
Final Mean for
1.000E+02
1.000E+02
1.000E+02
2.473E+00
8.750E+01
2.699E-01 126.31
4.493E+00 30.01
9.275E+00 50.86
Not Found -----
4.493E+00+/- 1.349E+00
1.873E+02
1 Valid Peaks =
Status
OK
OK
Absent
OK
5.720E-01+/- 7.225E-01 (126.31%)
2.699E-01
4.493E+00
9.275E+00
----- Line
3 Valid Peaks =
3.80*
Final Mean for

%Eff
5.720E-01 126.31
1.000E+02 5.720E-01
1.000E+02 1.189E+00
1.189E+00 126.31
2.191E+00 ----- Line Not Found ----2.572E+00 4.626E+03
4.626E+03 31.04
1.873E+02
19.28
OK
OK
OK
Absent
30.01%)
OK
1.873E+02+/- 3.612E+01 ( 19.28%)
-t515.49

Sample ID : 1304106-15
Acquisition date
Page :
4
2-MAY-2013 17:36:37

Nuclide
BA-133
PA-231
PA-234
TH-234
Activity
(pCi/filter)
3.261E+02
5.720E-01
4.493E+00
1.873E+02
Act error
5.977E+01
7.225E-01
1.349E+00
3.612E+01
MDA
(pCi/filter)
1.783E+01
1.558E+00
9.485E-01
2.685E+01
MDA error
Act/MDA
2.625E+00
1.753E-02
1.068E-02
3.454E-01
18.289
0. 367
4.737
6.975
MDA error
Act/MDA
9.091E+00
1.643E+01
3.866E+00
2.946E-02
-0.581
0.215
-0.307
0.381
Nuclide
C0-57
CD-109
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-1. 557E+01
3.673E+01
-1.347E+01
9.979E-01
Act error
1.769E+01
8.714E+01
2.582E+01
1.548E+00
MDA
(pCi/filter)
2.682E+01
1.707E+02
4.383E+01
2.617E+00
~\t..\,v7
Configuration
Analyses by
Client ID
peposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130410616 GEl BAFIL 191254.CN

PZ-104-SD TOT
2-MAY-2013 00:00:00.
1304106-16
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
27.90
30.97
34.95
46.45
53.11
62.10
66.25
81.36
93.29
112.15
116.57
160.93
166.93
186.68
215.06
276.60
303.94
331.79
338.14
356.40
376.87
384.55
387.19
391.39
414.62
418.84
437.29
448.15
468.30
473.68
511.00
17
1436
344
23
61
202
103
553
50
184
51
29
18
26
14
58
139
12
27
411
13
113
177
36
22
22
95
4
22
9
13
55
57
53
51
71
60
74
119
84
45
33
40
35
66
38
23
17
3
22
15
10
9
4
4
4
7
9
7
1
3
11
3
3
3
0
0
5
5
0
0
4
4
1
1
0
0
0
0
3
3
0
4
4
4
4
5
5
0
0
5
5
0
2-MAY-2013 18:05:48.54
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
Left
28.14
31.21
35.18
46.68
53.34
62.33
66.48
81.59
93.52
112.37
116.80
161.15
167.15
186.90
215.28
276.81
304.15
332.00
338.35
356.61
377.08
384.76
387.40
391.59
414.83
419.05
437.50
448.35
468.50
473.88
511.20
27
27
27
43
50
58
58
77
89
107
107
157
157
182
210
272
300
330
330
351
373
373
373
373
411
411
433
443
466
466
508
1.51
1.38
1. 85
1.16
1.99
1.95
2.17
1.83
1. 79
2.19
2.20
1.70
1. 70
2.30
2.08
1.47
1.95
1. 67
2.23
1.90
2.49
2.50
1. 68
2.50
1.89
2.75
1.96
1. 83
2.51
2.83
1.14
Pw
2-MAY-2013 17:50:31.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.22 0.0%
4096
10.00000
Cts/Sec %Err
13 1.89E-02 61.3
2.7
13 1.60E+00
13 3.82E-01 8.7
7 2.52E-02 56.4
8 6.79E-02 27.0
17 2.25E-01 9.4
17 1.14E-01 18.6
10 6.14E-01 5.7
8 5.60E-02 34.5
18 2.04E-01 9.6
18 5.68E-02 26.5
20 3.27E-02 35.2
20 1.98E-02 57.9
8 2.91E-02 57.2
8 1.53E-02 81.9
10 6.45E-02 20.2
10 1.55E-01 10.0
15 1.32E-02 35.3
15 3.03E-02 34.5
12 4.57E-01 5.3
23 1.49E-02 46.1
23 1.26E-01 12.8
23 1.96E-01 8.5
23 3.95E-02 33.6
15 2.47E-02 30.0
15 2.47E-02 36.5
9 1. 06E- 01 11.7
7 4.29E-03124.8
11 2.44E-02 24.2
11 1.02E-02 42.7
7 1.39E-02 51.5
Fit
1.94E+01
2.65E+00
2.58E+00
1. 48E+00
6.13E+00
7.40E+00
1.68E+00
5.23E-01
1!1551

Sample ID : 1304106-16
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.564E+02
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.725E+02
Total Activity
= Keyline
=
---------
2.564E+02
Wtd Mean
Decay Corr
pCi/filter
2.565E+02
---------
Decay Corr
2-Sigma
20.33
0.521E+02
2.565E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
12.90%
FISSION
Hlife
10.50Y
Nuclide Type
31
27
4
Page :
2
2-MAY-2013 17:50:31
---------
Wtd Mean
Decay Corr
pCi/filter
2.725E+02
---------
2.725E+02
2.725E+02
5.289E+02
5.290E+02
not found
Manually edited
"M"
"A"
2-Sigma
Decay Corr
0.529E+02
19.41
= Manually
=
accepted
B55_2

Sample ID : 1304106-16
Acquisition date
Page :
3
2-MAY-2013 17:50:31

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Ef
1.963E+01 2.564E+02
2.565E+02 20.33
4.915E+00 4.780E+02
4.781E+02 35.41
2.956E+02 18.47
6.963E+OO 2.956E+02
3 Valid Peaks =
Status
OK
OK
OK
2.565E+02+/- 5.214E+01 ( 20. 33%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" = Keyline

%Eff
5.865E+01 2.725E+02
2.725E+02 19.41
1 Valid Peaks =
Status
OK
2.725E+02+/- 5.288E+01 ( 19.41%)

Sample ID : 1304106-16
Acquisition date
Page :
4
2-MAY-2013 17:50:31

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
2.565E+02
2.725E+02
Act error
5.214E+01
5.288E+01
MDA
(pCi/filter)
1.767E+01
5.111E+01
MDA error
Act/MDA
2.901E+00
1.638E+00
14.510
5.332
MDA error
Act/MDA
5.674E+00
2.501E+01
3.632E-03
6.326E-02
6.640E+00
1.277E-01
-0.055
-0.119
0.000
2.139
-0.061
1.069
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-1.007E+00
-2.295E+01
O.OOOE+OO
7.199E+00
-3.309E+00
5.818E+00
Act error
1.141E+01
1.412E+02
O.OOOE+OO
1.633E+00
3.930E+01
2.926E+00
MDA
(pCi/filter)
1.818E+01
1.933E+02
1.933E-01
3.366E+00
5.454E+01
5.441E+00
)fyv)rl
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130410617 GE2 BAFIL 191255.CN

PZ-104-SD DIS
2-MAY-2013 00:00:00.
1304106-17
FILTER
GE2
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
31.03
35.25
46.00
52.67
60.74
66.27
81.02
83.75
93.88
111.54
116.40
160.63
185.71
276.84
302.91
307.35
333.93
338.34
356.10
364.17
376.73
383.81
387.03
391.53
414.94
418.25
421.91
437.33
468.20
511.39
525.52
1862
478
54
67
137
71
722
27
28
140
37
16
26
80
126
42
71
21
519
15
14
112
174
28
41
24
8
85
12
25
6
127
3
3
0
0
0
0
1
1
0
0
0
0
0
0
3
3
4
4
0
0
0
1
1
0
2
2
2
0
0
0
0
2-MAY-2013 18:06:30.51
96
98
95
244
86
54
49
75
128
70
74
44
29
9
8
10
19
18
11
7
16
34
16
7
8
8
8
9
7
4
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 32
1. 68
3.21
2.05
1. 51
1.32
1. 50
1. 50
1.91
1. 32
1.55
1.13
2.92
1.84
1.56
2.16
1.83
2.42
1.49
1.46
1. 82
1. 86
1.83
1.88
2.07
2.08
2.08
1.79
1. 20
2.05
1.74
31.14
35.36
46.11
52.78
60.85
66.38
81.14
83.86
94.00
111.65
116.52
160.74
185.83
276.95
303.02
307.46
334.04
338.45
356.21
364.28
376.84
383.92
387.13
391.63
415.04
418.36
422.02
437.44
468.30
511.50
525.62
Left
Pw
26
26
44
50
58
65
77
77
91
108
115
158
183
271
299
299
330
330
352
361
373
380
380
390
412
412
412
433
465
506
522
18
18
6
6
8
5
10
10
7
8
6
7
6
12
15
15
13
13
8
7
8
11
11
6
20
20
20
8
7
10
6
2-MAY-2013 17:51:11.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Cts/Sec %Err
2.07E+00
5.31E-01
5.95E-02
7.43E-02
1.52E-01
7.86E-02
8.02E-01
2.97E-02
3.09E-02
1.56E-01
4.13E-02
1. 72E-02
2.84E-02
8.89E-02
1.40E-01
4.62E-02
7.94E-02
2.30E-02
5.76E-01
1. 61E- 02
1.53E-02
1.25E-01
1.93E-01
3.09E-02
4.51E-02
2. 71E-02
9.07E-03
9.40E-02
1.34E-02
2.73E-02
6.28E-03
2.5
5.8
32.2
26.2
21.4
23.6
4.0
72.4
55.8
16.2
39.9
95.2
45.9
17.6
9.5
22.9
14.1
44.2
4.6
45.4
44.2
12.7
10.1
30.7
18.1
35.1
73.7
12.3
49.9
29.0
72.4
Fit
2.60E+00
1.22E+Ol
4.45E+00
1.58E+00
l.llE+Ol
1.84E+00

Sample ID : 1304106-17
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.654E+02
---------
Total Activity
Nuclide
AM-241
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.657E+Ol

;
---------
2-Sigma
Decay Corr
19.27
0.704E+02
3.654E+02
3.654E+02
---------
Total Activity
Wtd Mean
Decay Corr
pCi/filter
3.654E+02
NATURAL
Hlife
432.20Y
Flags: nK"
"E"
12.90%
FISSION
Hlife
10.50Y
Nuclide Type
31
27
4
Page :
2
2-MAY-2013 17:51:11
Wtd Mean
Decay Corr
pCi/filter
4.657E+01
---------
4.657E+Ol
4.657E+Ol
4.119E+02
4.120E+02
Key line not found

Manually edited
"Mn
All
II
2-Sigma
Decay Corr
2.031E+Ol
43.62
Manually accepted
8556

Sample ID : 1304106-17
Acquisition date
Page :
3
2-MAY-2013 17:51:11

Energy
81.00
302.84
356.01
Nuclide
BA-133
%Abn
33.00*
17.80
60.00
Final Mean for

1.799E+01 3.654E+02
3.654E+02 19.27
2.814E+02 35.44
7.560E+00 2.814E+02
3.620E+02 17.74
7.170E+00 3.620E+02
%Eff
3 Valid Peaks
Status
OK
OK
OK
3.654E+02+/- 7.041E+01 ( 19.27%)

Nuclide
AM-241
Energy
59.54
%Abn
35.90*
Final Mean for

Flag:
11
* 11

2.461E+01 4.657E+01
4.657E+01 43.62
%Eff
1 Valid Peaks
Status
OK
4.657E+01+/- 2.031E+01 ( 43.62%)
Key line
=Ji557

Sample ID : 1304106-17
Acquisition date
Page :
4
2-MAY-2013 17:51:11

Nuclide
BA-133
AM-241
Activity
(pCi/filter)
Act error
3.654E+02
4.657E+01
7.041E+01
2.031E+01
MDA
(pCi/filter)
2.023E+01
1.871E+01
MDA error
Act/MDA
3.445E+00
1.448E+00
18.062
2.488
MDA error
Act/MDA
1.458E+00
2.124E+01
1.942E-01
6.997E-02
2.143E+01
6.045E+00
0.086
0.387
3.702
1.057
1. 567
0.110
Nuclide
C0-57
CD-109
PA-231
PA-234
TH-234
NP-237
Key-Line
Activity K.L.
(pCi/filter)Ided
8. 119E- 01
7.157E+01
3.775E+01
3.587E+00
4.065E+02
5.895E+00
Act error
5.743E+00
1.180E+02
5.302E+00
1.874E+00
1.446E+02
3.646E+01
MDA
(pCi/filter)
9.493E+00
1.850E+02
1.020E+01
3.392E+00
2.594E+02
5.354E+01
IJ!55S
\~,~.--\l)
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410618 GE3 BAFIL 191256.CN

PZ-104-SS TOT
2-MAY-2013 00:00:00.
1304106-18
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
30.92
35.40
53.23
61.80
65.64
71.14
81.13
84.54
93.07
101.50
111.93
116.40
136.50
153.85
162.30
249.04
276.79
303.08
308.18
333.58
338.39
356.34
366.22
383.87
386.87
414.72
418.06
437.40
468.16
512.38
615.22
2004
459
46
243
131
25
807
25
53
14
224
63
27
40
50
13
50
141
30
63
34
463
30
106
199
34
14
119
22
19
6
104
81
89
87
101
99
75
90
110
81
68
67
75
50
52
27
20
10
16
16
6
32
18
26
40
20
35
11
7
6
1
2
2
3
3
3
3
3
3
0
0
3
3
0
0
0
0
0
5
5
5
5
0
0
1
1
2
2
0
0
0
0
2-MAY-2013 18:07:11.45
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.58
1.59
1. 80
1.82
1.83
1. 85
1.58
1. 87
1.54
1. 57
1. 72
1. 93
2.54
2.74
5.26
1.25
1.13
1.67
2.65
1. 87
2.68
1. 82
5.07
1.87
1.79
2.08
2.09
1. 92
1.93
2.27
2.81
31.24
35.72
:j3.55
62.12
65.96
71.46
81.45
84.85
93.39
101.82
112.25
116.72
136.81
154.17
162.61
249.35
277.09
303.39
308.49
333.89
338.69
356.64
366.53
384.17
387.17
415.02
418.36
437.70
468.45
512.68
615.51
Left
Pw
27
27
50
50
50
50
76
76
89
100
108
108
133
151
158
246
276
300
300
330
330
352
362
381
381
410
410
432
464
506
612
14
14
25
25
25
25
13
13
9
6
12
12
8
8
9
6
5
18
18
12
12
11
11
10
10
12
12
10
2-MAY-2013 17:51:49.
1.00000E+00 filter
0
BAFIL
0 00:15:04.29 0. 5%
4096
10.00000
Cts/Sec %Err
2.23E+00 2.3
5.10E-01 5.8
5.13E-02 34.2
2.70E-01 8.6
1.46E-01 16.4
2.76E-02 66.0
8.96E-01 3.8
2.74E-02100.7
5.94E-02 38.1
1.56E-02105.1
2.49E-01 8.6
7.05E-02 25.3
3.01E-02 58.9
4.40E-02 35.6
5.60E-02 29.3
1.44E-02 69.0
5.53E-02 20.7
1.56E-01 8.8
3.35E-02 31.6
7.03E-02 16.2
3.81E-02 22.6
5.14E-01 5.3
3.32E-02 32.3
1.18E-01 13.9
2.21E-01 9.6
3.77E-02 28.8
1. 52E- 02 78.1
1.33E-0110.4
7 2.44E-02 29.2
13 2.14E-02 35.2
6 6.19E-03 54.6
Fit
1.88E+01
3.97E+00
4.83E+00
1.23E+00
3.06E+00
6.32E+00
1.73E+01
2.52E+00
1!l559

Sample ID : 1304106-18
Acquisition date

31
25
6
Page :
2
2-MAY-2013 17:51:49
19.35%

Nuclide
Hlife
BA-133
10.50Y
NP-237 2.14E+06Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 3.866E+02
1. 00 3.356E+01
Total Activity
4.202E+02
Wtd Mean
Decay Corr
pCi/filter
3.867E+02
3.356E+01
Decay Corr
2-Sigma
0.680E+02
17.57
6.765E+01
201. 61
4.202E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.245E+02
Total Activity
Wtd Mean
Decay Corr
pCi/filter
7.245E+02
7.245E+02
7.245E+02
1.145E+03
1.145E+03

Decay Corr
2-Sigma
1.342E+02
18.53


Sample ID : 1304106-18
Acquisition date
Page :
3
2-MAY-2013 17:51:49

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

NP-237
86.50
3 Valid Peaks
12.60*
Final Mean for

1.899E+01 3.866E+02
3.867E+02 17.57
3.818E+02 27.09
6.222E+00 3.817E+02
5.860E+00 3.952E+02
3.952E+02 17.24
%-Eff
1.749E+01
3.867E+02+/- 6.795E+01
3.356E+01
1 Valid Peaks;
Status
OK
OK
OK
17.57%)
3.356E+01 201.61
OK
3.356E+01+/- 6.765E+01 (201.61%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

%Eff
2.648E+01 7.245E+02
7.245E+02 18.53
1 Valid Peaks ;
Status
OK
7.245E+02+/- 1.342E+02 ( 18.53%)
Flag: "*'' ; Keyline
.Et561

Sample ID : 1304106-18
Acquisition date
Page :
4
2-MAY-2013 17:51:49

Nuclide
BA-133
TH-234
NP-237
Activity
(pCi/ filter)
3.867E+02
7.245E+02
3.356E+01
Act error
6.795E+01
1.342E+02
6.765E+01
MDA
(pCi/filter)
2.015E+01
1.319E+02
5.417E+01
MDA error
Act/MDA
3.081E+00
7.086E+00
4.379E+00
19.192
5.491
0.619
MDA error
Act/MDA
1.307E+00
1.539E+01
4.585E-02
3.908E-02
9.014E-01
0.569
-0.022
0.692
0.997
1.437
Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
6.505E+00
-4.023E+00
2.229E+00
2.740E+00
2.635E+01
Act error
6.397E+00
1.327E+02
1.640E+00
1.422E+00
9.799E+00
MDA
(pCi/filter)
1.144E+01
1.866E+02
3.224E+00
2.748E+00
1.833E+01
ii156_2
~
\l'(
6\,v
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample IP
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30410619 _GE5_BAFIL_l91257.CN

PZ-104-SS DIS
2-MAY-2013 00:00:00.
1304106-19
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
12.30
20.96
27.49
31.04
35.15
35.95
53.32
53.73
61.90
65.82
66.70
70.43
79.69
81.19
112.10
116.47
276.61
303.01
333.34
333.96
356.10
383.46
384.09
386.06
386.93
390.45
391.19
414.77
5
100
20
2014
383
141
35
7
32
15
114
31
23
17
9
12
25
20
9
45
28
51
20
13
10
7
4
13
3
4
5
15
5
5
7
0
0
0
0
6
6
1
1
0
5
5
0
1
1
0
0
0
0
1
1
0
1
1
3
3
1
1
0
2-MAY-2013 18:08:00.27
13
263
37
58
17
40
842
177
53
38
97
14
94
392
19
83
15
130
12
53
26
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
2-MAY-2013 17:52:24.
l.QOOOOE+OO filter
0
BAFIL
0 00:15:01.17 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
0.10
0.84
1.01
0.72
0.61
0.91
0.62
0.62
0.88
0.66
1.07
0.28
0.76
0.68
0.75
0.52
0.62
0.76
1.10
1.10
0. 71
1.16
1.16
1.28
1.16
1.16
1. 28
0.62
118
191
261
290
333
333
506
506
587
627
627
673
760
760
1070
1112
2644
2899
3191
3191
3405
3676
3676
3702
3702
3745
3745
3970
9
26
16
25
30
30
23
23
25
29
29
14
37
37
25
24
24
24
30
30
33
24
24
29
29
27
27
24
5.09E-03123.9
1. 12E- 01 18.5
2.18E-02 50.7
2.24E+00 2.6
4.26E-01 6.5
1.56E-01 20.3
3.84E-02 32.5
1.49E-02 78.5
2.92E-Ol 6.9
4.16E-02 36.7
6.43E-02 25.3
1.89E-02 40.5
4.44E-02 34.7
9.35E-01 3.7
1.97E-01 12.3
5.85E-02 23.5
4.20E-02 25.9
l.OSE-01 11.8
1.56E-02 63.2
1.04E-Ol 9.3
4.36E-Ol 5.4
2.16E-02 44.1
9.24E-02 11.6
1.61E-02 65.8
1.44E-Ol 10.4
1.32E-02 37.7
5.84E-02 13.5
2.83E-02 27.8
123.36
206.50
269.15
303.26
342.63
350.39
517.00
521.00
599.34
637.00
645.39
681.17
770.10
784.48
1081.10
1122.96
2659.62
2913.02
3204.00
3210.00
3422.42
3685.00
3 691. 00
3709.89
3718.27
3752.00
3759.12
3985.41
Fit
l.OOE+OO
9.75E-01
9.05E-01
8.52E-Ol
3.62E+00
1.63E+00
8.93E-Ol
9.86E-01

Sample ID : 1304106-19
Acquisition date

28
22
6
Page :
2
2-MAY-2013 17:52:24
21.43%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 4. 249E+02
Total Activity
4.249E+02
Wtd Mean
Decay Corr
pCi/filter
4.249E+02
Decay Corr
2-Sigma
0.720E+02
16.95
4.249E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.375E+02
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
2.375E+02
2.375E+02
2.375E+02
6.623E+02
6.624E+02
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
0.342E+02
14.38
Manually accepted

Sample ID : 1304106-19
Acquisition date
Page :
3
2-MAY-2013 17:52:24

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

pCi/filter pCi/filter ~Error
4.249E+02 16.95
1.802E+01 4.249E+02
6.343E+02 35.38
2.575E+00 6.342E+02
4.312E+00 4.552E+02
4.553E+02 18.05
~Eff
3 Valid Peaks =
4.249E+02+/- 7.201E+01 (
Status
OK
OK
OK
16.95~)

Nuclide
TH-234
Energy
63.29
3.80*
Final Mean for

pCi/filter pCi/filter %'Error
2.375E+02 14.38
8.750E+01 2.375E+02
~Eff
%Abn
1 Valid Peaks
2.375E+02+/- 3.416E+01 (
Status
OK
14.38~)
Flag: "*" = Keyline
lll5S5

Sample ID : 1304106-19
----
Acquisition date
Page :
4
2-MAY-2013 17:52:24
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
4.249E+02
2.375E+02
7.201E+Ol
3.416E+01
MDA
(pCi/filter)
1.264E+01
2.397E+Ol
MDA error
Act/MDA
1.862E+00
3.083E-01
33.604
9.908
MDA error
Act/MDA
9.408E+00
1.740E+Ol
1. 541E-02
2.265E-02
3.261E+00
3.189E-02
0.146
0.558
-0.666
2.308
-0.685
0.835
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
4.061E+00
1.010E+02
-9.ll9E-01
4.644E+00
-2.534E+01
2.367E+00
Act error
1.450E+01
8.387E+Ol
8.948E-01
1. 725E+00
2.411E+01
1.458E+00
MDA
(pCi/filter)
2.775E+01
1.809E+02
1.369E+00
2.012E+00
3.697E+01
2.833E+00
!15.56

Engineering Management Inc.: Support

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ENGINEERING MANAGEMENT SUPPORT, INC.

West Lake OU-1

Chain of Custody & pH Check Sheet

Analytical Results Summary

Quality Control Sample Results Summary

Laboratory Technician's Notes

Analytical Data (Isotopic Uranium)

Analytical Data (Isotopic Thorium)

Analytical Data (Radium-226)

Analytical Data (Radium-228)

Barium-133 Analytical Tracer Data

Last Page Number

STANDARD OPERATING PROCEDURE

Eberline Services - Oak Ridge Laboratory

Eberline Services Work Order # _ _ _

K13s 'I 1! .. /t'!> K<:.

Second Technical Data Review

Data Entry/Electronic Deliverable

Electronic Deliverable Proof

Client in Possession of Data

Technical/Clerical Corrections, Signatures Needed, Problems, Etc

Chain of Custody Record

!J-.\2-:;t LAl;: 00' J

Send Report To:l\J

601 Scarboro Road

1865)4S1-o683 Photle. (BS5} 483-4821 Fax

Sampler (Print Name):

.j~ \::) ~/\\-)

Sampler {Print Name):

fY'=G- to~- '5 '2

I Xl I~ IhI 'f' IXll .i4

.I~MJ3T 111..,- I&~I::::l

f>c, <::;ciA.-5-s --P6--~A-s~

I Xllt<\ IXll ~ !'XJhlQ

I \ I Xl/ XJ /A l'ili'Xl 1Jj

Received by: (Signature)

Relinquished by: (SiQri-Bture)

J.><ll 'AI !t:l 1.x1

Received Containers Intact?

REC'D APR i 6 2013

Chain of Custody Record

Sampler (Print Name):

elinquished by: (Signature)

Aelinqufshed tJy: (Signature}

<. r<" ,).! I J-.i'.

Leo somple 111

X! ).() I)C 'A XI XI

Pt:- !d-e -'5 ~

14f7/J3 IEti!IIR cf1to

Sample Custodian Remarks (Completed By Laboratory):

Receiued by: (Signature)

Received by: (Signature)

Oak Ridge Laboratory

Pl.O ... ~--

Location circle one)

---- ..--...... ___ .,,

------- ---- ------------------.. --..------------ .. ------------- ---- --- ----- -------------.

--------------------------------------------------------- -----------!---------- --------Sample Storage

Printed: 4/16/2013 12:37PM:mmm7

Oak Ridge Laboratory

Original Lab Deadline: 05/14/13

Location (circle one)

Received by rSample Storage

-----~pie Star--~:;;:Sample Storage

flo~s:I=;CD-~8D;:;Tro~I-T;=========~I~1~~~~~~~~~WAP1.. 0--90-:o. ~--~~~4~

[;lll;~I~[D~lU;P,~OS:D~):I~S/========~1 ~~~~~~~~~~:V~:~~~P~-~0o 0