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  • Iv. Data Dan Pembahasan 4.1 Data T (S) V Campuran V Naoh: Naoh Terpakai Asam Oksalat Oksalat Naoh

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    Retno Anjasari
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    This document presents the data and discussion of an experiment on determining concentration of a mixture over time. It includes: 1) Time and volume data of the NaOH solution and mixture. 2) Calculations of preparing standard solutions of NaOH, oxalic acid, ethyl acetate, and HCl. 3) Determining the concentration of the mixture at different times by titrating with NaOH. 4) Regression analysis to obtain the equation relating concentration of the mixture to time. 5) Graphs of time vs volume, concentration, and rate constant which are fitted to linear equations.

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    Perhitungan 5 Kk

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    This document presents the data and discussion of an experiment on determining concentration of a mixture over time. It includes: 1) Time and volume data of the NaOH solution and mixture. 2) Calculations of preparing standard solutions of NaOH, oxalic acid, ethyl acetate, and HCl. 3) Determining the concentration of the mixture at different times by titrating with NaOH. 4) Regression analysis to obtain the equation relating concentration of the mixture to time. 5) Graphs of time vs volume, concentration, and rate constant which are fitted to linear equations.

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    20 views7 pages

    Iv. Data Dan Pembahasan 4.1 Data T (S) V Campuran V Naoh: Naoh Terpakai Asam Oksalat Oksalat Naoh

    Uploaded by

    Retno Anjasari
    This document presents the data and discussion of an experiment on determining concentration of a mixture over time. It includes: 1) Time and volume data of the NaOH solution and mixture. 2) Calculations of preparing standard solutions of NaOH, oxalic acid, ethyl acetate, and HCl. 3) Determining the concentration of the mixture at different times by titrating with NaOH. 4) Regression analysis to obtain the equation relating concentration of the mixture to time. 5) Graphs of time vs volume, concentration, and rate constant which are fitted to linear equations.

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    of 7

    IV.

    DATA DAN PEMBAHASAN


    4.1 Data
    t (s) V campuran V NaOH
    600 30 13.1
    1200 30 13.1
    1800 30 13.4
    2400 30 13.5
    t 30 13.7

    4.2 Perhitungan
    A. Pembuatan NaOH 0,02 N



    g = 0,2 gram
    B. Pembuatan asam oksalat 0,02 M



    g = 0,126 gram
    C. Standarisasi NaOH dengan asam oksalat
    V
    NaOH terpakai
    = 9.4 mL
    V
    asam oksalat
    = 10 mL
    (V.N)
    oksalat
    = (V.N)
    NaOH
    10 mL . 0,02 N = 9.4 mL . N
    M = 0,021 N
    D. Pembuatan etil asetat 0,02 N
    N =



    N =



    N = 9,81 N

    V
    1
    .N
    1
    = V
    2
    . N
    2
    V . 9,8 N = 250 mL . 0,021 N
    V = 0,535 mL

    Massa = . V
    = 0,9 g/mL . 0,535 mL
    = 0,4815 gram
    E. Pengenceran HCl 4 N menjadi 0,02 N
    V
    1
    .N
    1
    = V
    2
    . N
    2
    V
    1
    . 4 N = 100 mL . 0,02 N
    V = 0,5 mL
    F. Penentuan Konsentrasi campuran
    (V.N)
    NaOH
    = (V.N)
    Campuran
    a. t = 10
    13,1 mL . 0,021 N = 30 mL . N
    N = 0,00917 N
    b. t = 20
    13,1 mL . 0,021 N = 30 mL . N
    N = 0,00917 N
    c. t = 30
    13,4 mL . 0,021 N = 30 mL . N
    N = 0,00938 N
    d. t = 40
    13,5 mL. 0,021 N = 30 mL. N
    N = 0,00945 N

    e. t =
    13,7 mL . 0,021 N = 30 mL . N
    N = 0,00959 N
    G. Menghitung nilai y



    x = konsentrasi campuran
    a = konsentrasi NaOH
    a. t = 10




    b. t = 20




    c. t = 30




    d. t = 40




    e. t =




    H. Menentukan nilai k



    a. t = 10


    b. t = 10


    c. t = 30


    d. t = 40

    = 0,03535
    I. Persamaan Regresi
    x = t (s)
    y =



    X Y xy x
    2

    600
    22147,2 360000
    1200
    44294,4 1440000
    1800
    69190.2 3240000
    2400
    93506,4 5760000
    = 6000
    151,224 229138,2 10800000






    =



    = 0,0012

    A = -
    = 37,806 (0,0012 . 1500)
    = 36,006
    Y = 36,006 + 0,0012x
    4.3 Grafik
    Grafik t vs Volume NaOH

    Grafik t vs y





    y = 0.0003x + 12.9
    R = 0.8824
    13
    13.05
    13.1
    13.15
    13.2
    13.25
    13.3
    13.35
    13.4
    13.45
    13.5
    13.55
    0 1000 2000 3000
    V
    o
    l
    u
    m
    e

    N
    a
    O
    H

    (
    m
    L
    )

    Waktu (s)
    WAKTU VS VOLUME NaOH
    volume NaOH
    Linear (volume NaOH)
    y = 0.0013x + 35.91
    R = 0.8796
    36.5
    37
    37.5
    38
    38.5
    39
    39.5
    0 500 1000 1500 2000 2500 3000
    N
    i
    l
    a
    i

    y

    waktu (s)
    WAKTU VS Y
    y
    Linear (y)
    Grafik t vs k


    y = -2E-05x + 0.0688
    R = 0.8545
    0
    0.01
    0.02
    0.03
    0.04
    0.05
    0.06
    0.07
    0 500 1000 1500 2000 2500 3000
    N
    i
    l
    a
    i

    k

    Waktu (s)
    WAKTU VS K
    k
    Linear (k)
    4.4 Foto
    FOTO Keterangan

    Dilarutkan 0,126 gram asam oksalat, lalu
    diencerkan dengan akuades

    Diencerkan 0,4815 gram etil asetat diencerkan
    dengan akuades dalam labu ukur 250 mL

    Dicampurkan 10 mL etil asetat dengan 20 mL
    HCl di dalam erlenmeyer. Kemudian
    erlenmeyer ditutup dengan alumunium foil
    untuk mencegah penguapan

    Larutan dititrasi dengan NaOH sampai
    terbentuk larutan berwarna merah muda yang
    tidak hilang dengan pengocokan

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