and titrate with silver standard solution using your indicator. Make three trials. Laboratory Exercise No. 7 Theoretical Framework
Group No. 5 Trinidad, Sharla Jay S. Sayenga, Jershwin Hermel B.
A. Preparation of Reagents
Chlorine Standard Solution: Weigh 1.648g NaCl and dilute to 1L.
B. Analysis of Unknown
Silver standard solution: Dissolve 30g AgNO3 with 950mL distilled water. Take 100mL of this solution and dilute to 1L. Store in light proof container. 3. Indicator: Weigh 5g K2CrO4 and add 100mL distilled water. Add drops of your silver standard until small amount of red precipitate appears. Stand for 2 hours and filter. Take 50mL of your unknown sample and put in evaporating dish. Check pH. Adjust by adding H2SO4 or CaCO3 to pH 7-10.
Add 1mL of indicator. Titrate with standard silver solution until pink-red silver chromate persists for 10-15 seconds. Make three trials.