Central Laboratory

REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Petroleum products distillation apparatus

Work Instruction: KRC/CL-WI-3-1-64
Instrument No.: CL-M-132-1
Location: Room132
Model: BSZY-2b
Manufacture: Jinghua electronic instrument factory xian China
Serial No.:: SD-008

Range: 0 ~ 4C 1C
1. Calibration References:
Use the standard thermometer check and set the bath temp.

2. Calibration data:
Ref. Thermometer

Display temperature
Tolerance

0
0

3. Conclusion: Pass
4. Calibration date:

2011.9.25

5. Re Calibration date: 2012.9.24

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Petroleum products distillation apparatus

Work Instruction: KRC/CL-WI-3-1-64
Instrument No.: CL-M-132-2
Location: Room132
Model: BSZY-2b
Manufacture: Jinghua electronic instrument factory xian China
Serial No.:: SD-006

Range: 0 ~ 4C 1C
1. Calibration References:
Use the standard thermometer check and set the bath temp.

2. Calibration data:
Ref. Thermometer
Display temperature
Tolerance

0
0
0

3. Conclusion: Pass
4. Calibration date:
2011.9.25
5. Re Calibration date: 2012.9.24

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Petroleum products distillation apparatus
Work Instruction: KRC/CL-WI-3-1-64
Instrument No.: CL-M-133-1
Location: Room133
Model: BSZR-2b
Manufacture: Jinghua electronic instrument factory xian China
Serial No.:: SD-009

1. Calibration References:
Use standard thermometer check and set the bath temperature.

Range: 30601
2. Calibration data:
Ref. Thermometer
Display temperature
Tolerance

40
39
1

3. Conclusion: Pass
4. Calibration date:

2012.6.6

5. Re Calibration date: 2013.6.5

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Petroleum products distillation apparatus

Work Instruction: KRC/CL-WI-3-1-64
Instrument No.:: CL-M-133-2
Location: Room133
Model: BSZR-2b
Manufacture: Jinghua electronic instrument factory xian China
Serial No.:: SD-012

1. Calibration References:
Use standard thermometer check and set the bath temperature.

Range: 30601

2. Calibration data:
Ref. Thermometer
Display temperature
Tolerance

45
46
1

3. Conclusion: Pass
4. Calibration date:

2012.6.6

5. Re Calibration date: 2013.6.5

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

InstrumentName: Freezing point apparatus

Work Instruction: KRC/CL-WI-3-1-66
Instrument No.: CL-M-127-1
Location: Room127
Model: PZB(Y.B)-2
Manufacture: Jinghua electronic instrument factory xian China
Serial No.: SD-032

1. Calibration References:
Use standard thermometer check and set the bath temp. .

Range: -60

2. Calibration data:
Ref. Thermometer
Display Temp.
Tolerance

-65
-65
0

3. Conclusion: pass
4. Calibration date:

2011.11.6

5. Re Calibration date: 2012.11.5

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

InstrumentName: Freezing ,cloud & crystal point apparatus

Work Instruction: KRC/CL-WI-3-1-60
Instrument No.: CL-M-127-8
Location: Room127
Model: DSY-021A
Manufacture: Dalian Rigo instrument CO. Ltd. China
Serial No.: 031005004

1. Calibration References:
Use standard thermometer check and set the bath temp. .

Range: -60

2. Calibration data:
Ref. Thermometer
Display Temp.
Tolerance

-70
-70
0

3. Conclusion: Pass
4. Calibration date:

2011.11.6

5. Re Calibration date: 2012.11.5

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

InstrumentName: Cloud and pour point apparatus

Work Instruction: KRC/CL-WI-3-1-60
Instrument No.: CL-M-127-4
Location: Room127
Model: YLQ-4D8K
Manufacture: Jinghua electronic instrument factory xian China
Serial No.: SD-031

1. Calibration References:
Use standard thermometer check and set the bath temp. .

Range: Control point temp.-1

2. Calibration data:
Ref. Thermometer
Display temp.
Tolerance

-17

-34

-51

0
0

-17
0

-35
0

-51
0

3. Conclusion: Pass
4. Calibration date:
2011.11.6
5. Re Calibration date: 2012.11.5

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Aniline point apparatus

Work Instruction: KRC/CL-WI-3-1-9
Instrument No.: CL-M-254-10
Location: Room254
Model: JZY-262A
Manufacture: Dalianjinzhou intellect petroleum analysis instrument factory China
Serial No.: 200610012

1. Calibration References:
Used standard thermometer check the test temp.

Range: 69.30.2
2. Verification data:
Standard Thermometer

69.3

Selected Temp. Range

69.3

Tolerance

3. Conclusion: Pass
4. Verification date:

2011.12.20

5. Re Verification date: 2012.12.19

Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Kinematic viscosity apparatus

Work Instruction: KRC/CL-WI-3-1-58
Instrument No.: CL-M-252-17
Location: Room252
Model: HVU482A
Manufacture: Herzog
Serial No.: 084820092

1. Calibration References:

2. Calibration data:
Standard Thermometer
Selected Temp. Range
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Kinematic viscosity apparatus

Work Instruction: KRC/CL-WI-3-1-58
Instrument No.: CL-M-252-2
Location: Room252
Model: DSY-004A
Manufacture: Dalian Rigo instrument CO. LTD. China
Serial No.: 99210

1. Calibration References:
Use standard thermometer check and set the bath temperature.

Range:400.1
Standard thermometer No. 15

2. Calibration data:
Standard Thermometer

40

Selected Temp. Range

Tolerance

40
0

3. Conclusion: Pass
4. Calibration date:

2012.2.7

5. Re Calibration: date: 2013.2.6

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Kinematic viscosity apparatus

Work Instruction: KRC/CL-WI-3-1-58
Instrument No.: CL-M-252-3
Location: Room252
Model: DSY-004A
Manufacture: Dalian Rigo instrument CO. LTD. China
Serial No.: 99203

1. Calibration References:
Use standard thermometer check and set the bath temperature.

Range: 1000.1

2. Calibration data:
Standard Thermometer
Selected Temp. Range
Tolerance

100
100
0

3. Conclusion: Pass
4. Calibration date:

2012.6.13

5. Re Calibration: date: 2013.6.12

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Low temperature kinematic viscosity apparatus

Work Instruction: KRC/CL-WI-3-1-58
Instrument No.: CL-M-252-4
Location: Room252
Model: DSY-019A
Manufacture: Dalian Rigo instrument CO. LTD. China
Serial No.: 99204

1. Calibration References:
Use standard thermometer check and set the bath temperature.

Range: -201

2. Calibration data:
Standard Thermometer
Selected Temp. Range
Tolerance

-20
-20
0

3. Conclusion: Pass
4. Calibration date:

2011.6.13

5. Re Calibration: date: 2012.6.12

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Engine fuels existent gum apparatus

Work Instruction: KRC/CL-WI-3-1-51
Instrument No.: CL-M-252-5
Location: Room252
Model: FRJ-2
Manufacture: Jinghua electronic instrument factory xian China
Serial No.: SD-023

1. Calibration References:
Use standard thermometer check and set the bath temp.

Range: 2503
2. Calibration data:
Standard Thermometer
Selected Temp. Range
Tolerance

250
251
1

3. Conclusion: Pass
4. Calibration date:

2011.9.19

5. Re Calibration date: 2012.9.18

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Gasoline existent gum apparatus
Work Instruction: KRC/CL-WI-3-1-51
Instrument No.: CL-M-252-6
Location: Room252
Model: DSY-311
Manufacture: Dalian Rigo instrument CO. LTD. China
Serial No.: 021005005

1. Verification References:
Use standard thermometer check and set the bath temp..
Range: 162.52.5

2. Verification data:
Standard Thermometer
Set temperature
Display temperature
Tolerance

162.5
162
163
1

3. Conclusion: Pass
4. Verification date:

2011.7.21

5. Re Verification date: 2012.7.20

Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Existent gum solid block bath apparatus

Work Instruction: KRC/CL-WI-3-1-51
Instrument No.: CL-M-342-2
Location: Room342
Model: 12200
Manufacture: SETA-England
Serial No.: 440

1. Calibration References:

2. Calibration data:

Standard Thermometer
Selected Temp. Range
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Flash point apparatus-closed cup method

Work Instruction: KRC/CL-WI-3-1-63
Instrument No.: CL-M-254-1
Location: Room254
Model: DSY-002A
Manufacture: Dalian Rigo instrument CO. LTD. China
Serial No.: 99218

1. Calibration References:
For verification:
According to this testing method that check and calibration the sample cup.

2. Calibration data:
It is up to the mustard.
3. Conclusion: pass
4. Calibration date:

2011.9.14

5. Re Calibration date: 2012.9.13

Calibration By:

Instrument Calibration Record

Instrument Name: Flash point apparatus-closed cup method

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Work Instruction: KRC/CL-WI-3-1-63

Instrument No.: CL-M-254-2
Location: Room254
Model: DSY-002A
Manufacture: Dalian Rigo instrument CO. LTD. China
Serial No.: 021015005

1. Calibration References:
According to testing method that check and calibration the sample cup.

2. Calibration data: for verification

It is up to the mustard.
3. Conclusion: Pass
4. Calibration date:
2011.9.14
5. Re Calibration date: 2012.9.13

Ver./Calibration By:

Instrument Calibration Record

Instrument Name: Flash and fire point apparatus

Work Instruction: KRC/CL-WI-3-1-54
Instrument No.: CL-M-254-3
Location: Room254
Model: DSY-001A

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Manufacture: Dalian Rigo instrument CO. LTD. China

Serial No.: 99137

1. Calibration References:
According to testing method check and calibration the sample cup

2. Calibration data: for verification

It is up to the mustard.
3. Conclusion:
4. Calibration date:

2011.9.14

5. Re Calibration date: 2012.9.13

Ver./Calibration By:

Instrument Calibration Record

Instrument Name: Automatic flash point apparatus

Work Instruction: KRC/CL-WI-3-1- 63
Instrument No.: CL-M-254-4
Location: Room254
Model: 70000-0
Manufacture: SETA-England
Serial No.: V226

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

1. Calibration References:
Check and Checks the instruments running program.

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: petroleum products carbon residue apparatus

Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-249-1
Location: Room249
Model: TSY-1116
Manufacture: Dalian Tianyuan petroleum testers CO. LTD. China
Serial No.: 15014

1. Calibration References:
Use standard UJ33a MV meter check and set the bath temp. .

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Room temp. :25,

Range: 5205
2. Calibration data:
Input mV
Display temp

21.19mv
522

Tolerance

3. Conclusion: Pass
4. Calibration date:
2011.11.8
5. Re Calibration date: 2012.11.7

Calibration By:

Instrument Calibration Record

Instrument Name: CFR-engine

Work Instruction: KRC/CL-WI-3-1-14
Instrument No.: CL-M-134-1
Location: Room134
Model: CFR-F2U
Manufacture: CFR-USA
Serial No.: FAS004545

1. Calibration References:
2. Calibration data:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Standard sample
composev/v
toluene
n-heptane

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Allowable error
academic
octane number

test
octane number

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Condensing point apparatus

Work Instruction: KRC/CL-WI-3-1-60
Instrument No.: CL-M-127-5
Location: Room127
Model: BSN(S)-3
Manufacture: Jinshi petrochemical instrument CO. LTD. China
Serial No.: 318

1. Calibration References:
Use standard thermometer check and set the bath temp.
Range:-171

2. Calibration data:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Standard Thermometer

Instrument Calibration Record

Page: 12 of

-17

Display
Tolerance

-17.5
0.5

3. Conclusion: Pass
4. Calibration date:

2012.5.9

5. Re Calibration: date: 2013.5.10

Calibration By:

Instrument Calibration Record

Instrument Name: Condensing point apparatus

Work Instruction: KRC/CL-WI-3-1-60
Instrument No.: CL-M-127-3
Location: Room127
Model: JH011205
Manufacture: Jinshi petrochemical instrument CO. LTD. China
Serial No.: 709111

1. Calibration References:
Use standard thermometer check and set the bath temp.
Range:0/-171

2. Calibration data:
1

Standard Thermometer

-17

Display

-17

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Tolerance

Instrument Calibration Record

Page: 12 of

3. Conclusion: Pass
4. Calibration date:

2012.5.9

5. Re Calibration: date: 2013.5.10

Calibration By:

Instrument Calibration Record

Instrument Name: Jet fuel thermal oxidation stability apparatus

Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-342-3
Location: Room342
Model: JFTOT-
Manufacture: USA
Serial No.: 318-9935

1. Calibration References:

2. Calibration data:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Jet fuel silver strip corrosion apparatus

Work Instruction: KRC/CL-WI-3-1-59
Instrument No.: CL-M-254-5
Location: Room254
Model: SYF-1
Manufacture: Jinghua electronic instrument factory xian China
Serial No.: SD-020

1. Calibration References:
Use standard thermometer check and set the bath temp. .
Range : 501

2. Calibration data:
Ref. Thermometer
Display
Tolerance

50
50
0

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

3. Conclusion: Pass
4. Calibration date:
2011.11.8
5. Re Calibration date: 2012.11.7

Calibration By:

Instrument Calibration Record

Instrument Name: Copper strip corrosion apparatus
Work Instruction: KRC/CL-WI-3-1-59
Instrument No.: CL-M-254-6
Location: Room254
Model: FTF-1
Manufacture: Jinghua electronic instrument factory xian China
Serial No.: SD-022

1. Calibration References:
Use standard thermometer check the bath temp. and set temp.
Range:1001

2. Calibration data:
Ref. Thermometer

100

Display
Tolerance

100
0

3. Conclusion: Pass
4. Calibration date: 2012.5.6

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

5. Re Calibration: date: 2013.5.5

Calibration By:

Instrument Calibration Record

Instrument Name: LPG Copper strip corrosion apparatus

Work Instruction: KRC/CL-WI-3-1-52
Instrument No.: CL-M-248-3
Location: Room248
Model: TSY-3001
Manufacture: Dalian Tianyuan petroleum testers CO. LTD. China
Serial No.: 067003

1. Calibration References:
Use standard thermometer check the bath temp. and set temp.
Range:37.80.1 thermomter no 200301

2. Calibration data:
Ref. Thermometer
Display
Tolerance

37.8
37.9
0.1

3. Conclusion: Pass
4. Calibration date:

2012.6.27

5. Re Calibration date: 2013.6.26

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Calibration By:

Instrument Calibration Record

Instrument Name: Petroleum color test apparatus

Work Instruction: KRC/CL-WI-3-1-11
Instrument No.: CL-M-254-8
Location: Room254
Model: AF650
Manufacture: SETA-England
Serial No.: 1662

1. Calibration References:

2. Calibration data:
Standard liquied
Color disc

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Calibration By:

Instrument Calibration Record

Instrument Name: Saybolt color test apparatus

Work Instruction: Method ASTM D156
Instrument No.: CL-M-254-9
Location: Room254
Model: 15311-2
Manufacture: SETA-England
Serial No.: 00078586

1. Calibration References:

1.

Calibration data:

3. Conclusion:
4. Verification date:
5. Re Verification date:

Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Auto mercaptan test apparatus

Work Instruction: KRC/CL-WI-3-1-30
Instrument No.: CL-M-331-5
Location: Room331
Model: ZDJ-4A
Manufacture: Shanghai China
Serial No.: 03

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Microcolometric sulfur titration apparatus

Work Instruction: KRC/CL-WI-3-1-35
Instrument No.: CL-M-337-2
Location: Room337
Model: WK-2B
Manufacture: Jianghuan China
Serial No.: 990703

1. Calibration References:

2. Calibration data:
Normal sample
Test Conclusion
Accord percent

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Box resistance furnace

Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-249-2
Location: Room249
Model: SX2-2.5-10
Manufacture: Tianjin China
Serial No.: 01020

1. Calibration References:
Use standard mv meter UJ33a check and set temp.

Remark: at 25,1mv.

Room temp.

26 , Range:80025

2. Calibration data:
In Put M. V.
Display Temp.
Tolerance

32.2mv
805
5

3. Conclusion: Pass
4. Calibration date: 2012.3.15
5. Re Calibration: date: 2013.3.14

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Box resistance furnace

Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-334-1
Location: Room334
Model: SX2-2.5-10
Manufacture: Tianjin China
Serial No.: 021287

1. Calibration References:

2. Calibration data:
In Put M. V.
Display Temp.
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Flame atomic absorption spectrometry apparatus

Work Instruction: KRC/CL-WI-3-1-29
Instrument No.: CL-M-331-1
Location: Room331
Model: AA-55B
Manufacture: VARIAN-USA
Serial No.: S-303

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-127-7
Location: Room127
Model: PB203-E
Manufacture: Mettler shangha China
Serial No.: 1218220021
Temperature: 26

Humidity: 46%

1. Calibration References:
Use standard weight check and calibrate the balance.

2. Calibration data:
standard weight
display

100 g
L. 100.001g

R. 99.999g

F. 100.000g

B. 99.99g

3. Conclusion: Pass
4. Calibration date:

2011.9.14

5. Re Calibration date: 2012.9.13

Calibration By:

C. 100g

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-253-4
Location: Room253
Model: PB3002-S
ManufactureMettler shangha China
Serial No.: 1118261691
Temperature: 25

Humidity: 43%

1. Calibration References:
Use standard weight check and calibrate the balance.

2. Calibration data:
standard weight
display

100 g
L.99.999g

R. 100g

F. 99.999g

B. 99.999g

3. Conclusion: Pass
4. Calibration date:

2011.9.9

5. Re Calibration date: 2012.9.8

Calibration By:

C. 100g

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-243-2
Location: Room243
Model: QC35EDE-S
Manufacture: Germany
Serial No.: 23205424
Temperature: 27

Humidity: 41%

1. Calibration References:
Use standard weight check this electronic balance.

2. Calibration data: d=0.5g

100 g

standard weight
display

L=100g

R.=100g

F.=100g

B.=100g

3. Conclusion: Pass
4. Calibration date:

2011.8.1

5. Re Calibration date: 2012.7.31

Calibration By:

C=100g.

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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

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Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-251-1
Location: Room251
Model: PB203-E
Manufacture: Mettler shangha China
Serial No.: 1218220023
Temperature:

25

Humidity: 43%

1. Calibration References:
Use the standard thermometer check and calibration the balance.
2. Calibration data:
standard weight
display

100 g
L. 100g

R. 99.999g

F. 99.999g

B. 100g

3. Conclusion: Pass
4. Calibration date:

2011.9.7

5. Re Calibration date: 2012.9.6

Calibration By:

C. 100g

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REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-251-1
Location: Room251
Model: AB204-E
Manufacture: Mettler swiss
Serial No.: 1118273429
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

R.

F.

B.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

C.

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REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-251-2
Location: Room251
Model: AB204-E
Manufacture: Mettler swiss
Serial No.: 1118273430
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

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REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-251-4
Location: Room251
Model: PB8001-S
Manufacture: Mettler shanghai China
Serial No.: 1121141414
Temperature:

25

Humidity: 48%

1. Calibration References:
Use the standard thermometer check and calibration the balance.
2. Calibration data:
standard weight
display

100 g
L. 100g

3. Conclusion: Pass
4. Calibration date: 2011.9.7
5. Re Calibration date: 2012.9.6

Calibration By:

R. 100g

F. 100g

B. 99.9g

C. 100g

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REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-335-1
Location: Room335
Model: AB204-E
Manufacture: Mettler swiss
Serial No.: 1118273425
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

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REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-333-3
Location: Room333
Model: CP153
Manufacture: Germany
Serial No.: 15203302
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

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REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-335-3
Location: Room335
Model: AT201
Manufacture: Mettler swiss
Serial No.: 1118261642
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

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REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-334-2
Location: Room334
Model: PB3001-S
Manufacture: Mettler swiss
Serial No.: 8121706
Temperature:

24

Humidity: 35%

1. Calibration References:
Use standard weight check and calibrate this balance.

2. Calibration data:
Standard weight
Display

100 g
L. 100.000g

R. 99.999g

F. 100.000g

B. 100.000g

3. Conclusion: Pass
4. Calibration date:

2011.11.09

5. Re Calibration date: 2012.11.08

Calibration By:

C. 100.000g

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Vacuum distilltion

Work Instruction: KRC/CL-WI-3-1Instrument No.: CL-M-315-1
Location: Room315
Model: HDV632
Manufacture: Herzog
Serial No.: 46320117

1. Calibration References:

2. Calibration data:
pressure
KPa

TEMP. range
mmHg

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

positive cetane

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Carbon/Sulfur analyzer

Work Instruction: KRC/CL-WI-3-1-31
Instrument No.: CL-M-333-2
Location: Room333
Model: EMIA-820V
Manufacture: HORIBA Ltd, Japan
Serial No.: HID4K7NC

1.Calibration References:

1.

Calibration data:
Sample No.

Actual value

Actual value

1
2
3

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Allowable error

Actual error

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Catalytic micro activity index test unit

Work Instruction: KRC/CL-WI-3-1-32&61
Instrument No.: CL-M-333-4
Location: Room333
Model: WFS-1D
Manufacture: Petroleum academe of Beijing China
Serial No.:

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Gas chromtograph instrument

Work Instruction: KRC/CL-WI-3-1-26

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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument No.: CL-M-315-2

Location: Room315
Model: 4890
Manufacture: HP China
Serial No.: CN00005712

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Gas chromtograph instrument

Work Instruction: KRC/CL-WI-3-1-26
Instrument No.: CL-M-124-1

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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Location: Room124
Model: 4890
Manufacture: HP China
Serial No.: CN00005710

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Gas chromtograph instrument

Work Instruction: KRC/CL-WI-3-1-26
Instrument No.: CL-M-124-2
Location: Room124
Model: 4890
Manufacture: HP China

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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Serial No.: CN00005709

1.

Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Gas chromtograph instrument

Work Instruction: KRC/CL-WI-3-1-26
Instrument No.: CL-M-124-3
Location: Room124
Model: 4890
Manufacture: HP China
Serial No.: CN00005711

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Grating spectrophotometer

Work Instruction: KRC/CL-WI-3-1-55
Instrument No.: WL-M-12-2
Location: Room12
Model: 722
Manufacture: Light apparatus factorey shanghai China
Serial No.: 9809J040

1. Calibration References:

Central Laboratory
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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

2. Calibration data:
3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Grating spectrophotometer

Work Instruction: KRC/CL-WI-3-1-55
Instrument No.: CL-M-251-3
Location: Room251
Model: 752N
Manufacture: Shang hai precision & scientific instrument CO., LID
Serial No.: 7610508045

1. Verification References:
Check the 0 and 100%.
2. Verification data:
T0,100%Thats ok.

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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

3. Conclusion: pass
4. Verification date:

2011.7.21

5. Re Verification date: 2012.7.20

Verification By:

Instrument Calibration Record

Instrument Name: Nitrogen content apparatus

Work Instruction: KRC/CL-WI-3-1-34
Instrument No.: CL-M-337-1
Location: Room337
Model: 9000N
Manufacture: ANTEK-USA
Serial No.: 99F-328
1.

Calibration References:

2.

Calibration data:
Sample No.

1
2

Actual
value

Measured value

Allowable error

Actual error

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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Sulfur content apparatus

Work Instruction: KRC/CL-WI-3-1-33
Instrument No.: CL-M-337-3
Location: Room337
Model: 9000S
Manufacture: ANTEK-USA
Serial No.: 99F-331

1. Calibration References:

2. Calibration data:
Sample No.

1
2

Actual
value

Measured value

Allowable error

Actual error

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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Minimum water content detecting apparatus

Work Instruction: KRC/CL-WI-3-1-67
Instrument No.: CL-M-337-11
Location: Room337
Model: WS-3
Manufacture: Zibo Kesen Shandong China
Serial No: 3182

1.Calibration References:

Calibration data:
Standard Sample
Display
Tolerance

3. Conclusion:
4. Calibration date:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Arsenic content detecting apparatus
Work Instruction: KRC/CL-WI-3-1-23
Instrument No.: CL-M-246-1
Location: Room246
Model: AS-1
Manufacture: Jianghuan jiangsu China
Serial No.: 3177
1.

Calibration References:

2.

Calibration data:
Standard Sample
Display
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Calibration By:

Instrument Calibration Record

Instrument Name: Bromine and bromine index content detecting apparatus
Work Instruction: KRC/CL-WI-3-1-22
Instrument No.: CL-M-253-2
Location: Room253
Model: RPA-BR
Manufacture: Jianghuan jiangsu China
Serial No.: 990705
1.

Calibration References:

2.

Calibration data:
Standard Sample
Display
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Calibration By:

Instrument Calibration Record

Instrument Name: Conductivity meter
Work Instruction: KRC/CL-WI-3-1-21
Instrument No.: CL-M-248-4
Location: Room248
Model: MLA900
Manufacture: Maihak
Serial No.: 416110

1. Calibration References:
Use standard auto verification & calibration.
Range:1000cu10cu.
2.Calibration data:
1000cu.
3. Conclusion: Pass
4. Calibration date:

2011.8.4

5. Re Calibration date: 2012.8.3

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Calibration By:

Instrument Calibration Record

Instrument Name: Electrical heated drying oven
Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-N-253-10
Location: Room253
Model: 202-1
Manufacture: Test instrument factory chongqing China
Serial No.: 002

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Lab. manager

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electrical heated drying oven
Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-N-331-3
Location: Room331
Model: DGB20003
Manufacture: Test instrument factory chongqing China
Serial No.: 99061

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:

12.6.2002

5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

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Instrument Calibration Record

Instrument Name: Vapour pressure tester
Work Instruction: KRC/CL-WI-3-1- 4&62
Instrument No.: CL-M-127-6
Location: Room127
Model: 81000-0
Manufacture: Seta-England
Serial No.: W0101

1. Calibration References:
Check and Checks the instruments run program.

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electrical heated water bath
Work Instruction: KRC/CL-WI-3-1-65
Instrument No.: CL-M-253-12
Location: Room253
Model: HW-100T
Manufacture: Dalian Tianyuan petroleum testers CO. LTD. China
Serial No.: 219A008

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electrical-heated drying oven
Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-253-7
Location: Room253
Model: DGB20003
Manufacture: Test instrument factory chongqing China
Serial No.: 99049

1. Calibration References:
Use standard thermometer check and set the bath temp.
Range:1055
2. Calibration data:
Set:105

display: 107

3. Conclusion: Pass
4. Calibration date:

2011.9.8

5. Re Calibration date: 2012.9.7

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electrical heated water bath
Work Instruction: KRC/CL-WI-3-1-65
Instrument No.: CL-N-249-3
Location: Room249
Model: HH-60
Manufacture: Bejing jatric appliance factory
Serial No.: 20389

1. Calibration References:
Use standard thermometer check the bath temp. and set temp.
Range:802

2. Calibration data:

Set Temp.
Bath Temp.
Tolerance

80
79.5
1

3. Conclusion: Pass
4. Calibration date:

2011.9.7

5. Re Calibration date: 2012.9.6

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Density meter
Work Instruction: Instruction Manual
Instrument No.: CL-M-127-12
Location: Room127
Model: DMA4500
Manufacture: Anton paar GmbH
Serial No.: 528375

1.Calibration References:

2. Calibration data:
Standard Sample
Display
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Tester for Sulphur content in dark petroleum

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REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Work Instruction: KRC/CL-WI-3-1-61

Instrument No.: CL-M-254Location: Room254
Model: DSY-032A
Manufacture: Dalian Rigo instrument CO. LTD. China
Serial No.: 99102

1. Calibration References:
2. Calibration data:
Input m.v.
Display Temp.
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Density for LPG apparatus(both)
Work Instruction: KRC/CL-WI-3-1-52
Instrument No.: CL-M-248-1
Location: Room248
Model: TSY-3003

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Manufacture: Tianyuane Dalian instrument CO. LTD. China

Serial No.: 069007

1. Calibration References:
Use standard thermometer check and set the bath temp.
Range:200.1

2.Calibration data:
Standard Thermometer
Display Temp.
Tolerance

20
20
0

3.Conclusion: Pass
4. Calibration date:

2011.9.5

5. Re Calibration date: 2012.9.4

Calibration By:

Instrument Calibration Record

Instrument Name: Twin-column adsorption apparatus
Work Instruction: ASTM D1319
Instrument No.: CL-M-331Location: Room331
Model: 14060
Manufacture: SETA-England
Serial No.: S-255

1. Calibration References:

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Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Density testers for petroleum producs
Work Instruction: KRC/CL-WI-3-1-65
Instrument No.: CL-M-252-15
Location: Room252
Model: TSY-1110
Manufacture: Dalian extra-safety technology CO. LTD. China
Serial No.: 081110026

1. Calibration References:
Use standard thermometer checked & set the bath temp.
2. Calibration data:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Standard Thermometer
Display Temp.
Tolerance

Instrument Calibration Record

Page: 12 of

60
60
0

3. Conclusion: Pass
4. Calibration date:

2011.11.15

5. Re Calibration date: 2012.11.14

Calibration By:

Instrument Calibration Record

Instrument Name: Centrifugal thermostatic crude moisture apparatus
Work Instruction: KRC/CL-WI-3-1Instrument No.: CL-M-249-4
Location: Room249
Model: LDJ-5C
Manufacture: Shanghai anting instrument factory
Serial No.: 1005

1. Calibration References:

2. Calibration data:
Rotate speed
Display Temp.
Tolerance

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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Fluids demulsibilty characteristics apparatus
Work Instruction: KRC/CL-WI-3-1-65
Instrument No.:CL-M-252-8
Location: Room252
Model: TSY-1122
Manufacture: Dalian Tianyuan petroleum testers CO. LTD. China
Serial No.: 021005
Range:540.5

1.Calibration References:

2. Calibration data:
Standard Thermometer
Display Temp.
Tolerance

3. Conclusion:

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Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

4. Calibration date:
5. Re Calibration: date:

Calibration By:

Instrument Calibration Record

Instrument Name: Semi auto RVP. apparatus
Work Instruction: KRC/CL-WI-3-1-62
Instrument No.: CL-MLocation: Room
Model: JS0201
Manufacture: Jinshi petrochemical instrument CO. LTD China
Serial No.: 200304170

1. Calibration References:

2. Calibration data:
Ref. Thermometer
Display
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Ref. Pressure
Display
Tolerance

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Calibration By:

Instrument Calibration Record

Instrument Name: Tester for Sulfur content in tube petroleum product
Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-253-3
Location: Room253
Model: SYP1006-I
Manufacture: Shanghai China
Serial No.:

1. Calibration References:
Use standard mv meter UJ33a check and set temp.

Remark: at 25,1mv.

Room temp.

2. Calibration data:
Input m.v.
Display Temp.
Tolerance

37.4mv
923
3

3. Conclusion: Pass
4. Calibration date:

2012.3.15

5. Re Calibration: date: 2013.3.14

26 , Range:9205

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Calibration By:

Instrument Calibration Record

Instrument Name: Tester for Carbon residue for petroleum products
Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M
Location: Room
Model: DSY-042Z
Manufacture: Shanghai China
Serial No.:

031008003

1. Calibration References:
2. Calibration data:
Input m.v.
Display Temp. (front)
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Input m.v.
Display Temp. (back)
Tolerance

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Calibration By:

Instrument Calibration Record

Instrument Name: Diesel oxidation bath
Work Instruction: KRC/CL-WI-3-1-65
Instrument No.: CL-M-342-4
Location: Room342
Model: 16900-4
Manufacture: Seta-England
Serial No.: R236

1.Calibration References:
2.Calibration data:
Standard Thermometer ()
Display Temp. ()
Tolerance

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Box resistance furnace
Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-249-6
Location: Room249
Model: SX2-2.5-10
Manufacture: Tianjin China
Serial No.: 07043

1. Calibration References:
Use standard UJ-33a check and set the control meter mv value.

Room temp.: 25
2. Calibration data:
In Put M. V.
Display Temp.
Tolerance

33.83mv
843
7

3. Conclusion: Pass
4. Calibration date:

2011.9.19

5. Re Calibration date: 2012.9.18

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Box resistance furnace
Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-334-1
Location: Room334
Model: SX2-4-10
Manufacture: Tianjin China
Serial No.: 041298

1. Calibration References:
Use standard UJ33a MV meter check and set the bath temp. .
Room temp. :25,
Range: 85025

2. Calibration data:
In Put M. V.
Display Temp.
Tolerance

32.98mv
847
3

3. Conclusion: Pass
4. Calibration date:

2011.11.9

5. Re Calibration date: 2012.11.8

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Humidity measuring instrument
Work Instruction:
Instrument No.: CL-M-245-1
Location: Room245
Model: testo 615
Manufacture: Germany
Serial No.:

1. Calibration References:

2. Calibration data:
Room temp.
Standard thermometer. Temp.
Display temp. value

Tolerance

3. Result:
4. Calibration date:
5. Re Calibration: Date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic-heated drying oven

Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-253-8
Location: Room253
Model: DGB20003
Manufacture: Test instrument factory chongqing China
Serial No.: 99060
Range : 1355

1. Calibration References:
Use standard thermometer check and set the oven temp.
2. Calibration data:
standard temp.

135
138

Display temp.

3. Conclusion: Pass
4. Calibration date:

2011.9.25

5. Re Calibration date: 2012.9.24

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: CL-M-333-1
Location: Room333
Model: PB203-E
Manufacture: Mettler shangha China
Serial No.: 1212220022
Temperature: 26

Humidity: 40%

1. Calibration References:
Use standard weight check the balance.
2. Calibration data:
standard weight
display

100 g
L:.100g

R.: 100g

F.: 99.9999g

B.:100g

3. Conclusion: Pass
4. Calibration date:

2011.8.4

5. Re Calibration date: 2012.8.3

Calibration By:

C.:100g

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Flame atomic absorption spectrometry apparatus

Work Instruction: KRC/CL-WI-3-1-29
Instrument No.: CL-M-331-4
Location: Room331
Model: AANalyst200
Manufacture: Singapore
Serial No.: 200S4050301

1. Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Gasoline oxidation stability apparatus

Work Instruction: KRC/CL-WI-3-1-65
Instrument No.: CL-M-246-6
Location: Room246
Model: SETA 15400-2
Manufacture: SETA
Serial No.: 1001978

1. Calibration References:
Use standard thermometer check the bath water temp. , The bath temp. is 98.6.
(Range:1002)

Standard thermometer No.

2. Calibration data:
Standard
thermometer
Display
Tolerance

100
98.6
1.4

3. Conclusion: Pass
4. Calibration date:
2012.2.7
5. Re Calibration: date: 2013.2.6
Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Digital salt-in-crude Analyzer (Titrino plus)

Work Instruction: KRC/CL-IM-370-01
Instrument No.: CL-M-253-1
Location: Room253
Model: 848
Manufacture: Metrohm Herisau switzerland
Serial No.: 1848001010351

1. Verification References:
Use standard sample check and verification this instrument.
Standard sample salt content: 5mg/kg2.3mg/kg.

2. Verification data:
4.77mg/kg

3. Conclusion: pass
4. Verification date: 2011.12.21
5. Re Verification date: 2012.12.20
Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Density hydrometer apparatus
Work Instruction: KRC/CL-WI-3-1-65
Instrument No.: CL-M-127-13
Location: Room127
Model: TSY-1110
Manufacture: Tianyuane Dalian instrument CO. LTD. China
Serial No.: 010011

2. Calibration References:
Use standard thermometer check and set the bath temp.
Range:701
2. Calibration data:
Standard Thermometer
Display Temp.
Tolerance

70
70
0

3. Conclusion: pass
4. Calibration date:

2010.7.22

5. Re Calibration: date: 2011.7.21

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: WL-M-232-2
Location: Room232
Model: PB3002-S
Manufacture: Mettler Swiss
Serial No.: 1121201797
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: WL-M-232-3
Location: Room232
Model: JA5003
Manufacture: Shanghai China
Serial No.: 141
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: WL-M-232-4
Location: Room232
Model: JD500-2
Manufacture: Shenyang China
Serial No.: 1202798
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: WL-M-232-5
Location: Room232
Model: FA2004
Manufacture: Shanghai China
Serial No.: 51426
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: WL-M-232-6
Location: Room232
Model: AY220
Manufacture: Mettler Swiss
Serial No.: D432810947
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Grating spectrophotometer

Work Instruction: KRC/CL-WI-3-1-55
Instrument No.: WL-M-229-4
Location: Room229
Model: 752N
Manufacture: Shang hai precision & scientific instrument CO., LID
Serial No.: 7610508019

2. Verification References:
Check the T: 0 and 100%.
2. Verification data:
The T(0 and 100%) is ok.

3. Conclusion: pass
4. Verification date:

2011.11.22

5. Re Verification date: 2012.11.21

Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Grating spectrophotometer

Work Instruction: KRC/CL-WI-3-1-55
Instrument No.: WL-M-229-5
Location: Room229
Model: 722
Manufacture: Shang hai No.3 analytical instrument factory China
Serial No.: 9809J040

3. Verification References:
Check the T: 0 and 100%.
2. Verification data:
The T(0 and 100%) is ok.

3. Conclusion: Pass
4. Verification date:

2011.11.22

5. Re Verification date: 2012.11.21

Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Grating spectrophotometer

Work Instruction: KRC/CL-WI-3-1-55
Instrument No.: WL-M-232-1
Location: Room232
Model: 752N
Manufacture: Shang hai precision & scientific instrument CO., LID
Serial No.: 7610405036

4. Verification References:
Check the T: 0 and 100%.
2. Verification data:
The T(0 and 100%) is ok.

3. Conclusion: Pass
4. Verification date:

2011.11.22

5. Re Verification date: 2012.11.21

Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Electronic Balance

Work Instruction: KRC/CL-WI-3-1-57
Instrument No.: WL-M-232-5
Location: Room232
Model: FA2004
Manufacture: Shanghai China
Serial No.: 51426
Temperature:

Humidity:

1. Calibration References:

2. Calibration data:
standard weight
display

100 g
L.

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

R.

F.

B.

C.

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Grating spectrophotometer

Work Instruction: KRC/CL-WI-3-1-55
Instrument No.: WL-M-229-7
Location: Room229
Model: 722
Manufacture: Shang hai precision & scientific instrument CO., LID
Serial No.: 9809J043

1.Calibration References:

2. Calibration data:

3. Conclusion:
4. Calibration date:
5. Re Calibration: date:

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: BOD-System oixdirect

Work Instruction: KRC/CL-WI-3-1-58
Instrument No.: WL-M-229-1
Location: Room229
Model: TS606/3-i
Manufacture: GmbH, Germany
Serial No.: 050939

1. Verification References:
Use standard thermometer check and set the bath temp.
Range : 201
2. Verification data:
Ref. Thermometer

20

Display temperature
Tolerance

20
0

3. Conclusion: pass
4. Verification date:

2011.11.20

5. Re Verification date: 2012.11.19

Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: BOD-System oixdirect

Work Instruction: KRC/CL-WI-3-1-58
Instrument No.: WL-M-229-2
Location: Room229
Model: 205-2
Manufacture: HACA,USA
Serial No.: 01046605

1. Verification References:
Use standard thermometer check and set the bath temp.
Range : 201
2. Verification data:
Ref. Thermometer

20

Display temperature
Tolerance

20
0

3. Conclusion: pass
4. Verification date:

2011.11.20

5. Re Verification date: 2012.11.19

Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Biochemical incubator (BOD)

Work Instruction: KRC/CL-WI-3-1-55
Instrument No.: WL-M-229-3
Location: Room229
Model: TF-1A
Manufacture: Jiangyan jiangsu analysis instrument factory China
Serial No.: 010

1. Verification References:
Use standard thermometer check and set the bath temp.
Range : 201
2. Verification data:
Ref. Thermometer

20

Display temperature
Tolerance

20
0

3. Conclusion: pass
4. Verification date:

2011.11.20

5. Re Verification date: 2012.11.19

Verification By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: Automatic flash point apparatus

Work Instruction: Analysis method (flash)
Instrument No.: CL-M-254-18
Location: Room254
Model: HFP 339
Manufacture: Herzog
Serial No.: 093390504

1.Calibration References:
Use standard check and verification this apparatus.
2. Calibration data:

Result
Display result
Tolerance

57.3
57
0.3<1

3. Conclusion: Pass
4. Calibration date:

2009.12.13

5. Re Calibration: date: 2010.12.12

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: SVM 3000 Stabinger Viscometer

Work Instruction: Instruction Manual
Instrument No.: CL-M-252-16
Location: Room252
Model: SVM 3000
Manufacture: Anton paar GmbH Germany
Serial No.: 7972524

1. Calibration References:
Use standard check and calibration this apparatus.
2. Calibration data:

3. Conclusion: Pass
4. Calibration date:

2011.07.25

5. Re Calibration date: 2012.07.24

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: SVM 3000 Stabinger Viscometer

Work Instruction: Instruction Manual
Instrument No.: CL-M-252-14
Location: Room252
Model: SVM 3000
Manufacture: Anton paar GmbH Germany
Serial No.: 80690900

1. Calibration References:
Use standard check and calibration this apparatus.
2. Calibration data:

3. Conclusion: Pass
4. Calibration date:

2011.10.03

5. Re Calibration date: 2012.10.02

Calibration By:

Central Laboratory
REC. No. :KRC/CL-QR-077-2002

Quality Record
Date: 2012. 6.27

Instrument Calibration Record

Page: 12 of

Instrument Calibration Record

Instrument Name: petroleum products carbon residue apparatus

Work Instruction: KRC/CL-WI-3-1-61
Instrument No.: CL-M-249-7
Location: Room249
Model: TSY-1116
Manufacture: Dalian North port petroleum instr. CO. LTD. China
Serial No.: 0912712

1. Calibration References:
Use standard UJ33a MV meter check and set the bath temp. .
Room temp. :25,

Range: 5205
2. Calibration data:
Input mV
Display temp
Tolerance

21.19mv
520
0

3. Conclusion: Pass
4. Calibration date:
2011.11.9
5. Re Calibration date: 2012.11.8

Calibration By: