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Successfully Specify Three-Phase: Separators
Successfully Specify Three-Phase: Separators
Three-Phase
Separators
Hereis a stepwise
procedure
for
designing
liquid/Iiquid/vapor
separutors.
WayneD.Monnery
andWilliam
Y.Svrcek,
University
of Calgary
Selectingthree.phareseparatore
$tokos'lawappliee
As with two-phase designs, threephaseunits can be either vertical or horizontal, althoughthey typically are horizontal (seeFigures l and2). The vertical orientation.Figure 1, is only used if
there is a large amount of vapor to be
separatedfrom a small amount of the
light and heavy liquid (< l0-207o by
weight). Unfortunately, there are no
simple rules for separator selection.
Sometimes,both configurationsshould
be evaluatedto decide which is more
economical. Further, the available plot
space(footprint) may be a factor.
The design of three-phaseseparators
is similar to their two-phase counterparts, except that the liquid section differs. For the vertical type, a baffle commonly keeps the liquid separation
rt -
v T -
1,488g,fi(p,- pr)
18F
(l)
pRoGREss. SEpTEMBER
CHEMTcAL
ENGTNEERTNG
rgga . 29
MULTIPHASE FLOW
i
I
I
t
=
=
!
E
il
_T
J
30 .
1994.
SEpTEMBER
pRocREss
ENGTNEERTNG
CHEMIcAL
l,v
Min.12in.
Min.12in.
Heavy
liquid
outlet
Light
liquid
outlet
* l N , *l L
',l^n.
* * u,n.l
2. InterJacecontrol with boot
NI*-
4. Bucketand weir
Vapor
outlet
Vapor
outlet
Lightliquidholdu/surge
Heavy
liquid
outlet
-t
Heavyliquid
outlet
L,
-t
Light
liquid
outlet
-t
-l
lLzlLslL4l
Note:N= 112d7,1+6in.
drv= Nozzledia'
t - L -
Vertical design.procedur
Refer to Figure 1 for dimensions:
1. Calculate the verlical terminal
vapor velocity:
Pv
U- = ylPt rtt2
Pv
(4)
WV
Qv=
3,600pu
(s)
140-,\"'
D""=l#
|
\nu, )
(6)
0\
(8)
w-"LL
(9)
60pL
-Wrt
n
unr- 60pa
(10)
7. Assume Hr = I ft (minimum)
and calculate the settling time for the
. sEprEMBERrggr
. 31
CHEMTCALENGTNEERTNGpRocREss
MULTIPHASE
(0- .0rl\
o,in{
^ =(t.+aeal\/oo
a,
r,
lI--T-/\----G-/
) Equation13
- 0.6973=2.14ftJs
Ur =0' 313 53.95
I EquationEl
-*
Qv=
=
:
=
-=
415.000lb/h
=165.32ft'ls
3.600s/hx 0.69731Vff
lEquation E2
^
1TVT4STFIs
- r0.13ft
--irISHs
r-\o=
V
lEquation
ou -
E3
16.5000lb/h = 5.10ft'lmin
60 minthx 53.95lbtftt
a EquationE4
"=,{*t#d)
vnr=ffi
l2H,
----------=
(11)
U,,
8. Assume Hn = | ft (minimum)
and calculate the settling time for the
light liquid droplets to rise through
this distance:
t
,LH -
L zH ,
---:
(1 2 )
TI
uLH
32,
= 0.35ft'lmin
lEquation E5
whereD"is inft.
= 3.28084
x 10{ft
Note:1 micron
t
,HL_
l,3o0lb/h
s*=w
(I4a)
- HuAu
A
vHL-
(14b)
H.=+
( 1s )
(eu* eo)r,
Hs=\---TL
Qrt
. CHEMICALENGINEERINGPRoGRESS
sEprEMBERlggd
(16)
10,000
24in.
o_
o
F
c
9,000
-o
G
8,000
r.i
2 . C a l c u l a t et h e r a p o r '\ r r l u r r - t r i "
iili ti-:,r-r' :'1:ri- i1f-;1:
r
_ r _ i l , ) <
r l n t l l l _ i l ) S
flow rate,seeEq. El in the bor.
3. Calculatethe vesselinner diamlL.it'
. . \ : > . r 1 .H
eter,seeEq. E3 in the box.
' t -. = I ) i n . .H r + H n = 2 4
= Hn+ H, + HR+ O^* Ufii
n,
= 10.5fi.
Use
1J
i n . L ' . : r g F r , r L r r-e1 .G = 9 . 8 0 0g p h / f t z .
.a
- jr
4 . C a l c u l a tl h
e c : e t t l i n \ge l o c i l r, r l
{. =
_ c a l i i t ' r r 6m
0 i n i h )( 5 . 1 0
- o.-1-i
the heavyliquid out of the iight liqLrid
r ii' 9..\00gph/iir = 0.25 ft2
..\...ll ti ll
It' a mist eliminatorpad is used,
p h a s e .U s i n g T a b l e l , f t s = 0 . 1 6 3
= J jp..
-,-riionalheightis addedas shownin
Then:
\ \ . , D= - 1 l r 1xl 1 0 . 5=) 0 . 0 3 1 7
: - - l r eI .
Um = 0.163(62.11 53.95)/0.630
= 2 .1 1 i n . / m i n
E x a m p l e1
5. Calculatethe settlingvelocitl of
Sizea verticalseparatorwith a baf'the light liquid out of the heavyliquicl
': :lltc
and wire-meshmist eliminaphase:
: i,.r separatethe mixture given in
U r a = 0 . 1 6 3 ( 6 2 . 1-1 5 3 . 9 5 ) / 0 . 7 6 1
= l.l4 tn.lmin
. -,rleJ. The operatingpressureis 165
'..,:, rrild it is
necessaryto have a
6. Calculatethe light and hearr
Jr'(rcarbon
liquid holduptime of 25
Iiquid volumetric flow rates. see Eq.
:: and a surgetime of only 5 min.
E4 and E5 in the box.
1oa,r=
Ar+A, ft3ls
1. Calculatethe vertical terminal
7 . A s s u m eH r = 1 f t a n d c a l c u l a t e
- .iitr'. Using Table 2, calculateK
the tirne fbr the heavy liquid to sertle
Q , -- vr ,u : . 60
- ' i t h e Y o r k D e m i s t e re q r r r t i o n s . out of the light liquid phase:
Tt:2
,fF;
. . . E q . E 1 i n t h eb o x .
4u,
t n , . =( 1 2 )( 1 . 0 )l 2 . l 1 = 5 . 7m i n
, : n JL ' 1= 0 . 7 5x 2 . 1 4= 2 . 0 5f t l s .
8. AssumeHn = 1 fi and calculate
:.luivalent
expressions,
suchasH',/D
^=#6
. SEPTEMBER
CHEMICAL
ENGINEERING
PROGRESS
1994.
33
MULTIPHASE FLOW
drum
F Fuelgasknock-out
fuelgaslinebetween
NLt andhighlevelshutdown
ZOft.ilug in theincoming
drum
G.FlareKnock-out
20to 30minto Hll
factors(optionall:
Multiply
bythefollowing
Personnel
Factor
Instrumentation
Factor
Experienced
1.0
WellInstrumented
1.0
Trained
1.2
Instrumented
Standard
1.2
Inexperienced
1.5
PoorlvInstrumented
1.5
p,=##
rbtft3
x 53.es
. +ffi x62.It= 54.55
l EquationE6
=r.rrr,
)'''
1994.
SEpTEMBER
Horizontaldesign procedure:
no boot or weir
1. Calculate the vapor volumetric
flow rate, Qu, using Eq. 5.
I EquationE7
34 .
pRocREss
ENGTNEERTNG
CHEMTCAL
(18)
Vs=TsQr
(19)
(20)
A _ TED'
4
(2r)
V, +V,
r _
L _
tr-Au_ (our*,4rr)
(22)
Qrr=
I = H,./L't
Uw= Qr/Av
()L\
Q,,
'=
-"{
trrQ*
tntQ,
e*'(h-Av-o*)
(2s)
(21)
Q3)
1 ?| q r
velocity:
0ur= AorLlQu,
| [.
tro= 12 HHL/ULH
10. Calculate the liquid dropout
-:a:
I\ A ', - A
, -. A 1u , l\ L
'
(28)
(30)
18. CalculateUD.If UD << 1.5,
decreaseD (unlessit is alreadyat its
minimum), and if UD >> 6.0 then
increaseD; repeatfrom Step 5.
19. Calculate the thickness of the
shell and headsaccording to Table 8.
20. Calculate surface area of the
shell and headsaccordingto Table 8.
21.Calculate
t h e a p p r o x i m a tvee s sel weight accordingto Table 8.
22. Increaseor decreasethe vessel
diameter by 6-in. increments and
repeat the calculations :until the UD
ratio ran-eesfrom 1.5-6.0.
23. Using the optimum vesselsize
(minimum wei-eht).calculatethe normal and high liquid levels:
Hau= D - H,
( 31 )
(32)
Horizontaldesign procedure:
heavy liquid boot
1. Calculate the vapor volumetric
flow rate, Q, using Eq. 5.
2. Calcrilate the light and heavy
liquid volumetric flow rates, Q* and
Q n r , p e rE q s . 9 a n d 1 0 .
3. Calculate the vertical terminal
velocity, Ur, using Eq. 4 (the K value
comes from Table 2) and set Uu =
0.15 Ur.
4. Select holdup and surge times
from Table 6 and calculate the holdup
and surge volumes, V, and Vr, from
Eqs. 18 and 19 (unlesssurgeis other-
pRocREss. SEpTEMBER
CHEMTcAL
ENGTNEERTNG
rgs+ . 35
?=
:.::
:-=
:-:
-.
::
MULTIPHASE FLOW
,,,:
wise specified,such as slug volume).
5. Obtain UD from Table 7 and
initially set the diameter according to:
/ l?\
s
I
lt
14
F
F
7
E
F
F
"-
\
:
V.,
+V"o
n
Ar-Au-ArN
1994.
SEpTEMBER
Approximate
'=(t+
(34)
36 .
DishedHeads
ou=
(,q,,-e,)r
eu
(36)
(38)
(39)
(37)
PRocREss
ENGINEERING
cHEMICAL
l2Hu1/Us1
(4r)
A -ndH*
"ut
4en
(42)
(43)
t.
{
ft
I
u
(4s)
the boot
Horizontaldesign prooedure:
weir
(44)
Vn+V,
Ar- Ar.- AuL
(-+6)
Arr=Ar- A,- A*
(4',7)
tru= l2Hrx/Uro
(4e)
( t,,o-, trrQrr\
, A,, I
L1 =maxl:ff
\
(50)
nur
( s 1)
pRoGREss. SEpTEMBER
CHEMTCAL
ENGTNEERTNG
1994. 37
MULTIPHASE FLOW
(o,,e,,+o-,e-,1
-,'.''.]
f
L l -
Hnu=D-H,
(52)
(53)
Obtain Hr'
ANLL|Ar.
Horizontaldesign procedure:
bucket and weir
1. Calculate the vapor volumetric
flow rate, Qu, using Eq. 5.
2. Calculate the light and heavy
liquid volumetric flow rates, Q, and
Qnr,perEqs.9 and 10.
3. Calculate the vertical terminal
vapor velocity, Ur, using Eq. 4 (flnd K
from Table 2) and set Uv= 0.75 Ur.
4. Select residencetimes for light
and heavy liquids, 0r, and 0o.. For
sour water stripper feed drums, 0o. =
g,, =
,=(
+(e,,0,,re,,,O,,(s4)
0J0n(r1r)
235'ooolblh
=343.5'7ft3/s
3.600s/hx 0.190lb/ff
I EquationE8
o,,=
45'ooorblh -=18.52ft'lmin
60min/hx 40.5lb/ft'
I Equation E9
o-, =
7'5oolb/h
=2.y2ft'lmin
60 min/hx62.0lblfr'
tutQrt
A,,
Ur = 0' 175
I Equation811
I EquationE12
- Equation813
s.%ft
I Equation814
rs.02ff
ALL
I Equation E15
ff ls = 4.83ftls
Q u = 343.51
rr
ure=
T
7r.08
te
I Equation816
38 .
1994.
SEPTEMBER
Ar-4,
4=ffi=14.54ft
I Equation810
PROGRESS
ENGINEERING
CHEMICAL
155)
w,D,
tlni
Nomenclbture
proprengli
"'
:, =;il;:::T:1",,-*lllllJli,
==,1'l
l: = :-i;iliill,1l11;1",, "'*ftJil],."',0,'o
'7\
=
0,"0,",,
"'"'.'"
il,,l,l,1l;;
l,'.;l:l
= v o l u m e t r i cf i o w . f l r / s o r l t r / m i n
- vessem
l l l e r i a l s t r e s sv a l u e .p s i
0
S
lne
^-
liquidabor.e
vessel
bor-
:#, ?:light
I i g h ra n d h e a v yl i q u i d r
TC
TH
tut
=
*'
"
iiii,r;
i:i::';i'J'
=;5.,ff::;l
o u t o l l i g h t I i q u i d 'm i n
= ressel
diemeler.
n
"r'llu'
of Western
degreesin
ttu
3' =llJli';,ilr,.ormicrons
1s
t . .f r
D , = r 3 p r l r ' J i s e n g a g e m edni a
=
t
e f f i c i e n c yd. i m e n s i o n -
TH
TS
V,'
:
i
o. r
_\H=H
--\r r l l - X l
Pu l
1 - 1D
. e s i g nt h e l i g h t l i q u i d b u c k e r :
': the top of light liquid u eir'= D
, i l s s u m et h e b o t t o n rr s a t 0 . 1 l 5 D l
. . r t t i e a h o l d u p / s u r g e( t 1 , p r c a l l r .
' . -i min.); assume
HLL is 6 in.
, rrl the weir height andLLL is 6 in.
i e the bottom of the bucket.
. r,c Table 3 with HrrrlD and
D. calculate Au' and Arr.r.
-ulateL,:
lro + r,)9,,
H-
= t e i , s h tl r . . = l i ; . : : i : : : : : = : :
d r o p l e i so L r o
r f l i g h r l i q u i d .i n . t m i n
Un
Up
o u t o f h e a v yl i q u i d ,i n . i m i n
= mixture velocity, tVs
= boot velocitr'.in.lmin
= l c f r n i l r Jilg l 6 . i 1 _ 1
r i.. ' .c r i n . / r r i n
= \ i - L p i \rre l . r c i t r .f L l :
f
L
ii li
: , z z : : .: '
i: -.
H,,;
a,
= ---
.-.-:.:.
:'
H,,H,,,u
- - - :-- - : - - - . . ' - _ - .
= :::::::::-::::,
::-
HP.
= heiSi:t:i,'::r iiir:
Hs
H,..
fle. 11
nv
H,,,
irrroe heiohr
=
ri
::-::
l\:.:::\. !-P
:::.:::.lbr'ft]
:, :: j irLrloui time- s
= h e i g h ld r f l e r e n c eb e l i i e e nl i g h i u n J
(58)
H.
leed nozzle.ft
= disengagementheight. fi
= htrldupheisht. fi
H;,
= s e t t l i n qr e l o c i t vu f h e r v r l i o u i d
u,., = r i s i n g v e l o c i t )o f l i g h r l i q u i d d r o p l e r s
= h e i g h r .f t
H.. = liquid level above baffle, in. or ft
HB,. = liquid height from abor.ebaffle to
fts
(Ar,'r_ Arr,')
l : .
vHL
,.hereD" is in microns.
13. Calculate the differenc- rl
:rsht betweenthe light and he;:,,.,
quid weirs:
= c f a \ i t a r i o n acl o n s t a n tJ, 2 . 1 7 f r , / s r
= baffle liquid toad.gph/fr)
-'
0.00128e'(AsG)Dpr
r-i6,
= \ u r g et r m r .m i n .
= a l l o r l a b l eb o r i z o r r n lv c l o c i t l . f r l s
Y:,
;::]o.oLoint
r p r e l so u l
s r a n t .r i n . / m i n )cr P r i t l b / f r r
= t e r m i n a lr e l o c i t yc o n s L a n fl .r , i s
= vessellengrh.ft
= v a p o r , 4 i q u isde p a r a r i o m
n irrrrnum
K
L
L*,*
;'':liilr,r-Hj
I
(r, + rr)9,,
(5e)
lAorr- Arrr)
17. CalculateL = L, + Lr+ L. + L^.
1 8 . C a l c u l a t eU D . I f U D < < 1 . 5 .
)lr'-:li. l';L
- , ; i
;JL:
L, L;
i:i:i .;;iriti
LLL
: , , . r , r q l i i i e re l
1/
-:.
.\ lI
',:a.tI
I li.','i,l l-. ^l
pRocnEss. sEpTEMBER
cHEMTCAL
ENGTNEERTNG
1994. 39
MULTIPHASE FLOW
w h e r eP: = d e s i g p
n r e s s u raen dD = d r u md i a ,
Example2
Design a three-phasehorizontal
separatorwith a weir to separatethe
mixture in Table 10. The operating
pressure and temperature are 25 psig
and 100, respectively,and it is necessary to have a liquid holdup and surge
time of 15 min.
1. SeeEq. E8, box, p. 38
2. SeeEqs.E9 and E10, box, p. 38
3. K = 0.175 (the Gas Processors
Suppliers'Associationvalue in Table
2 was divided by 2 since there is no
mist eliminator).
S e eE q . E 1 1 ,b o x , p . 3 8
U v = 0 . 7 5 x 2 . 5 5 = 1 . 9 1f t l s
4. Holdup + surgeas specified= 15
min.
Vu+ V, = (15 min) (18.52ft3lmin)
= 211.80 ft3
Assume 10 min holdup, 5 min
surge.
5 . A s s u m eU D = l . l .
SeeEq. El2, box, p. 38
Ar=n/4 (11.0f|'z = 95.03ft2
6. Since the mass rate of vaoor is
1_
"-2xl7M
55xI32
about827oof theloading,setF1yto be
much greaterthan the minimum.
AssumeHv = 0.70D= (0.70)(1
1.0f0
= 7.70 ft. Using Table 3, Av/Ar =
Av= 71.08ft2
0.148,
7 , H r r r =( 0 . 5 ) ( 1 1 .+07) = I 2 . 5 i n . ,
use13in.
Hrr/D = 13/(11.0
x 12)= 0.098
= 0.051
UsingTable3, ALLrj/Ar
(0.051X95.03
Aur=
fP) = 4.95112
8. H, = 11.0- 1.10= 3.30ft
9. SeeEq.El3, box,p. 38
Usel,r = 15.0ft.
= 1.65ft
10.HHL- Hrr= 3.3012
= 0.150
ll. HH//D= 1.65111.0
FromTable3, AH/A, = 0.094
Aur= (0.094X95.03
ft2)= 8.93ft2
- 8.93= 15.02
Au=95.03- 71.08
ftl
12.FromTable1, ks= 0.333
- 40.5)/0.24
=
Uur= (0.333)(62.0
29.83in./min
Use 10in./min(maximum)
- 40.5)10.682
=
Uro= (0.333)(62.0
10.50in./min
Use 10in./min(maximum)
13, tHL = Q2 in./ft)(1.65ft)ilo
in./min= 1.98min, use2.0mins
tr, = tnr = 2.0 min
14. SeeEqs.E14 and E15. box,
p .3 8
Uselr = 3.0ft.
1 5 .L = 3 . 0+ 1 5 . 0= 1 8 . 0f t
'7.10
16.0 =
ftll.gI ftls = 4.03s
17.SeeEq.El6, box.p. 38
*l|rc= 0.307in.
I Equation 817
we11.
t =
ff'ltff#(on.at
rt2
+2x r0r.88
n')= ' 7.s20tb
I EquationE19
40 .
sEpTEMBER
1994.
pRocnEss
CHEMTCAL
ENGTNEERTNG